Automatic acid adding device for chemical sample

By designing an automatic acid addition device for chemical samples including reagent barrels, liquid adding pipes, controllable flow solenoid valves and liquid adding pumps, the problem of high labor intensity and high health risks in the process of acid addition is solved, and the quantitative automatic acid addition of geochemical samples is achieved, which improves the efficiency and consistency of acid addition.

CN223006168UActive Publication Date: 2025-06-20INST OF GEOPHYSICAL & GEOCHEMICAL EXPLORATION CHINESE ACAD OF GEOLOGICAL SCI
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Patent Information

Application Number
CN202421137721.2
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-05-23
Publication Date
2025-06-20
Estimated Expiration
2034-05-23

AI Technical Summary

Technical Problem

In the geochemical sample analysis laboratory, when the experimenter uses reagents such as volatile, strong acids and alkalis to dissolve the sample, he needs to do a lot of repetitive work, which leads to physical fatigue and is prone to inhaling a large amount of volatile reagents, causing health risks. In addition, the acid addition process is cumbersome and can easily lead to uneven acid addition.

Method used

An automatic acid addition device for chemical samples is designed, including a reagent barrel, liquid adding pipe, a controlled flow solenoid valve, a solenoid valve bracket and a liquid adding pump. Through the cooperation of a controlled flow solenoid valve and a liquid adding pump, the quantitative automatic acid addition of geochemical samples is achieved.

Benefits of technology

The quantitative automatic addition of acid to geochemical samples is achieved, which reduces the labor intensity of the experimenters, protects the physical health of the experimenters, and improves the efficiency and consistency of the acid addition process.

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Abstract

The utility model relates to the field of chemical sample treatment, in particular to an automatic acid adding device for a chemical sample. The utility model provides an automatic acid adding device for a chemical sample, which can be used for quantitatively and automatically adding acid into a geochemical sample, reducing the labor intensity of experimenters and protecting the physical health of the experimenters. An automatic chemical sample acid adding device comprises a reagent barrel, a liquid adding pipe, a liquid adding pump and the like, the liquid adding pump is placed on the left side of the reagent barrel, and the liquid adding pipe is connected between the liquid adding pump and the reagent barrel. By adjusting the position of the liquid adding gun to be above the beaker at the leftmost end, starting the liquid adding pump, opening the flow-controllable electromagnetic valve and adjusting the liquid adding amount, the liquid adding gun can complete liquid adding of the five beakers at the same time, quantitative and automatic acid adding of geochemical samples can be achieved, the labor intensity of experimenters is relieved, and the working efficiency is improved. And the body health of experimenters is protected.
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Description

Technical Field

[0001] The utility model relates to the field of chemical sample processing, in particular to an automatic acid adding device for chemical samples. Background Art

[0002] Geochemical samples refer to various geological and environmental samples collected in geochemical research, such as rocks, minerals, soils, sediments, water bodies, etc. These samples contain information on geochemical elements and their isotopes. By analyzing these samples, the composition, structure, evolutionary history of the earth's materials and the geochemical cycle process, etc. can be understood, which is of great significance for studying the internal structure of the earth, geological processes, environmental evolution, etc.

[0003] In geochemical sample analysis laboratories, reagents such as volatile strong acids and alkalis are often used to dissolve samples. Most dissolution processes need to be heated on a hot plate, which accelerates the volatilization of reagents such as strong acids and alkalis. Experimental personnel need to dissolve hundreds of samples every day. During the process of adding acid one by one with an acid adding spoon, a large amount of repetitive labor easily leads to physical fatigue, and it is easy to inhale a large amount of volatilized reagents during the reagent adding process, causing harm to the body. In addition, the workload of quantitative acid adding one by one is cumbersome and huge, and it is also easy to cause uneven acid adding.

[0004] Therefore, an automatic acid adding device for chemical samples is now developed, which can achieve quantitative automatic acid adding to geochemical samples, reduce the labor intensity of experimental personnel, and protect the physical health of experimental personnel. Summary of the Utility Model

[0005] In order to overcome the shortcomings that a large amount of repetitive labor in the existing acid adding to geochemical samples easily leads to physical fatigue, and it is easy to inhale a large amount of volatilized reagents during the acid adding process, causing harm to the body, the utility model provides an automatic acid adding device for chemical samples, which can achieve quantitative automatic acid adding to geochemical samples, reduce the labor intensity of experimental personnel, and protect the physical health of experimental personnel.

[0006] The technical solution is: an automatic acid adding device for chemical samples, including a reagent barrel, a liquid adding pipe, a controllable flow type solenoid valve, a solenoid valve bracket and a liquid adding pump. The liquid adding pump is placed on the left side of the reagent barrel. A liquid adding pipe is connected between the liquid adding pump and the reagent barrel. The solenoid valve bracket is placed on the left side of the liquid adding pump. A controllable flow type solenoid valve is connected to the solenoid valve bracket. A liquid adding pipe is liquid-connected between the controllable flow type solenoid valve and the liquid adding pump.

[0007] Furthermore, both the reagent barrel and the liquid adding pipe are made of materials with strong acid resistance.

[0008] Furthermore, it also includes a longitudinal sliding rail, a liquid filling gun, a transverse sliding rail, an installation bracket, a vertical sliding rail, an installation base and a five-piece pipe. There are two left and right installation bases, both of which are located on the left side of the solenoid valve bracket. A plurality of fixing screw holes are opened on the installation base. The upper sides of the front and rear parts of the installation base are connected to the vertical sliding rails, and the installation bracket is slidably connected between the vertical sliding rails. The left and right parts of the installation bracket are connected to the longitudinal sliding rails, and a plurality of transverse sliding rails are connected between the longitudinal sliding rails. The transverse sliding rails are slidably connected to the liquid filling guns, and the liquid filling guns are connected to the controllable flow type solenoid valve through the five-piece pipe.

[0009] Furthermore, it also includes a wire drawing wheel, and the right part of the device bracket is rotatably connected to two upper and lower wire drawing wheels.

[0010] Furthermore, it also includes a beaker, a hydraulic cylinder and an electric heating plate. The upper middle part of the device base is connected to two front and rear hydraulic cylinders, and an electric heating plate is connected between the telescopic ends of the hydraulic cylinders. A plurality of beakers are placed on the electric heating plate.

[0011] Furthermore, it also includes a heat preservation wire and a constant temperature wire. The heat preservation wire is connected inside the reagent barrel, and the constant temperature wire is connected to the controllable flow type solenoid valve.

[0012] The beneficial effect is that the utility model adjusts the position of the liquid adding gun to the top of the leftmost beaker, starts the liquid adding pump, opens the controllable flow type solenoid valve and adjusts the liquid adding amount, so that the liquid adding gun can complete the liquid adding of five beakers at the same time, thereby achieving the effect of quantitative automatic acid addition for geochemical samples, reducing the labor intensity of experimenters and protecting the health of experimenters. BRIEF DESCRIPTION OF THE DRAWINGS

[0013] Figure 1 It is a three-dimensional structural schematic diagram of the utility model.

[0014] Figure 2 It is a schematic cross-sectional view of the three-dimensional structure of the storage assembly of the utility model.

[0015] Figure 3 It is a three-dimensional structural schematic diagram of the adapter assembly of the utility model.

[0016] Figure 4 It is a three-dimensional structural schematic diagram of the liquid adding component of the utility model.

[0017] In the accompanying drawings: 1-reagent barrel, 2-liquid adding tube, 20-quintuple tube, 3-longitudinal sliding rail, 4-liquid adding gun, 5-lateral sliding rail, 6-device bracket, 60-wire wheel, 7-beaker, 70-hydraulic cylinder, 71-electric heating plate, 8-vertical sliding rail, 9-device base, 10-fixing screw hole, 11-controllable flow type solenoid valve, 110-constant temperature wire, 12-solenoid valve bracket, 13-liquid adding pump, 99-insulation wire. Detailed implementation mode

[0018] The embodiments of the present utility model will be described in detail below with reference to the accompanying drawings.

[0019] An automatic acid adding device for chemical samples, as Figures 1-3 shown, includes a reagent barrel 1, a liquid adding pipe 2, a controllable flow type solenoid valve 11, a solenoid valve bracket 12 and a liquid adding pump 13. The liquid adding pump 13 is placed on the left side of the reagent barrel 1. A liquid adding pipe 2 is connected between the liquid adding pump 13 and the reagent barrel 1. The solenoid valve bracket 12 is placed on the left side of the liquid adding pump 13. The controllable flow type solenoid valve 11 is connected to the solenoid valve bracket 12. A liquid adding pipe 2 is liquid-connected between the controllable flow type solenoid valve 11 and the liquid adding pump 13. The reagent barrel 1 and the liquid adding pipe 2 are both made of materials with strong acid resistance to avoid corrosion.

[0020] As Figure 1 and Figure 4 shown, it further includes a longitudinal sliding rail 3, a liquid adding gun 4, a transverse sliding rail 5, a device bracket 6, a vertical sliding rail 8, a device base 9 and a five-way tube 20. There are two device bases 9 on the left and right. The device bases 9 are both located on the left side of the solenoid valve bracket 12. Nine fixing screw holes 10 are opened on the device bases 9. The front and rear upper sides of the device bases 9 are both connected with vertical sliding rails 8. The device bracket 6 is slidably connected between the vertical sliding rails 8. The left and right parts of the device bracket 6 are both connected with longitudinal sliding rails 3. Five transverse sliding rails 5 are connected between the longitudinal sliding rails 3. The liquid adding guns 4 are slidably connected to the transverse sliding rails 5. The liquid adding guns 4 are all connected to the controllable flow type solenoid valve 11 through the five-way tube 20.

[0021] As Figures 1-4 shown, it further includes a wire arranging wheel 60, a beaker 7, a hydraulic cylinder 70 and a hot plate 71, a heat preservation wire 99 and a constant temperature wire 110. The right part of the device bracket 6 is rotatably connected with two upper and lower wire arranging wheels 60. The front and rear upper sides of the middle part of the device base 9 are both connected with two hydraulic cylinders 70. A hot plate 71 is connected between the telescopic ends of the hydraulic cylinders 70. Fifty beakers 7 are placed on the hot plate 71. A heat preservation wire 99 is connected inside the reagent barrel 1. A constant temperature wire 110 is connected to the controllable flow type solenoid valve 11.

[0022] When using the present utility model, first place the reagent barrel 1 in the chemical sample acid addition area, install the device base 9 on the left side of the reagent barrel 1 through bolts and fixed screw holes 10, then connect the reagent barrel 1 to the liquid addition pump 13 through the liquid addition pipe 2, connect the liquid addition pump 13 to the controllable flow type solenoid valve 11 through the liquid addition pipe 2, then connect the controllable flow type solenoid valve 11 to the liquid addition gun 4 through the five-way pipe 20, then start the hydraulic cylinder 70 to make the electric heating plate 71 move downward, and then place 10*5 beakers 7 containing chemical samples on the electric heating plate 71 respectively. Due to the variety of geochemical samples, the sizes and spacings of the beakers 7 may not be consistent. Then start the hydraulic cylinder 70 to make the electric heating plate 71 rise to a certain height to prevent the chemical samples from tipping over due to accidental contact by personnel. When it is necessary to add acid to the chemical samples, start the horizontal sliding rail 5, the vertical sliding rail 3 and the vertical sliding rail 8, adjust the position of the liquid addition gun 4 above the leftmost beaker 7, then start the liquid addition pump 13, then open the controllable flow type solenoid valve 11 and adjust the liquid addition amount, so that the reagent in the reagent barrel 1 flows through the controllable flow type solenoid valve 11 through the liquid addition pipe 2 and then flows from the five-way pipe 20 to the liquid addition gun 4, so that the liquid addition gun 4 can complete the liquid addition of five beakers 7 at the same time, and then repeat the work from left to right in turn to complete the acid addition of all chemical samples, so as to realize the quantitative automatic acid addition to geochemical samples, reduce the labor intensity of experimental personnel and protect the physical health of experimental personnel. When adding acid to the chemical, start the heat preservation wire 99 and the constant temperature wire 110 to keep the reagent in the reagent barrel 1 and the five-way pipe 20 warm. When connecting the controllable flow type solenoid valve 11 to the liquid addition gun 4 through the five-way pipe 20, make the five-way pipe 20 pass through between the wire arranging wheels 60 to prevent the five-way pipe 20 from knotting during the movement of the liquid addition gun 4.

[0023] The above embodiments are only the preferred embodiments of the present utility model, and are not used to limit the scope of implementation of the present utility model. Therefore, all equivalent changes made according to the content described in the claims of the present utility model should be included within the scope of the claims of the present utility model.

Claims

1. A chemical sample automatic acid addition device, characterized in that it includes The invention comprises a reagent barrel (1), a liquid adding pipe (2), a controllable flow type electromagnetic valve (11), a electromagnetic valve bracket (12) and a liquid adding pump (13); the liquid adding pump (13) is placed on the left side of the reagent barrel (1); the liquid adding pipe (2) is connected between the liquid adding pump (13) and the reagent barrel (1); the electromagnetic valve bracket (12) is placed on the left side of the liquid adding pump (13); the controllable flow type electromagnetic valve (11) is connected to the electromagnetic valve bracket (12); the controllable flow type electromagnetic valve (11) and the liquid adding pump (13) are liquid-connected with the liquid adding pipe (2); and the invention also comprises a heat preservation wire (99) and a constant temperature wire (110); the heat preservation wire (99) is connected inside the reagent barrel (1), and the controllable flow type electromagnetic valve (11) is connected to the constant temperature wire (110).

2. The automatic acid adding device for chemical samples as claimed in claim 1, characterized in that: The reagent barrel (1) and the liquid adding pipe (2) are both made of materials with strong acid resistance.

3. The automatic acid adding device for chemical samples as claimed in claim 1, characterized in that: The invention also comprises a longitudinal sliding rail (3), a liquid adding gun (4), a transverse sliding rail (5), a device bracket (6), a vertical sliding rail (8), a device base (9) and a five-joint pipe (20). The device base (9) has two left and right sides, and both device bases (9) are located on the left side of the electromagnetic valve bracket (12). The device base (9) is provided with a plurality of fixing screw holes (10). The upper sides of the front and rear parts of the device base (9) are connected to the vertical sliding rail (8). The device bracket (6) is slidably connected between the vertical sliding rails (8). The left and right parts of the device bracket (6) are connected to the longitudinal sliding rail (3). A plurality of transverse sliding rails (5) are connected between the longitudinal sliding rails (3). The transverse sliding rails (5) are slidably connected to the liquid adding gun (4). The liquid adding gun (4) is connected to the controllable flow electromagnetic valve (11) through the five-joint pipe (20).

4. A chemical sample automatic acid addition device as claimed in claim 3, characterized in that: It also includes a wire drawing wheel (60), and the right part of the device bracket (6) is rotatably connected to the upper and lower wire drawing wheels (60).

5. The automatic acid adding device for chemical samples as claimed in claim 3, characterized in that: The device also comprises a beaker (7), a hydraulic cylinder (70) and an electric heating plate (71); the upper middle part of the device base (9) is connected to two front and rear hydraulic cylinders (70); the electric heating plate (71) is connected between the telescopic ends of the hydraulic cylinders (70); and a plurality of beakers (7) are placed on the electric heating plate (71).