Methyl methacrylate polymerization inhibitor adding structure
By combining the material storage assembly with the metering pump, equipped with a filter shell and a jacketed heat exchanger, the problems of inaccurate inhibitor addition and insufficient temperature control in the polymerization reaction of methyl methacrylate are solved, high-precision addition and temperature regulation are achieved, and the consistency of the reaction and product quality are improved.
Patent Information
- Application Number
- CN202422166607.9
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-09-04
- Publication Date
- 2025-08-05
- Estimated Expiration
- 2034-09-04
AI Technical Summary
In the prior art, in the polymerization reaction of methyl methacrylate, the precise addition of polymerization inhibitors is difficult to control, the temperature control of the traditional feeding method is insufficient, and impurities affect the reaction purity and efficiency.
The material storage assembly is combined with a metering pump, equipped with a filter shell and a jacketed heat exchanger, which achieves precise addition and temperature regulation, removes impurities, and ensures that the inhibitor is pure and the temperature is appropriate.
It improves the consistency and stability of the reaction, enhances product quality and reaction efficiency, reduces side reactions, and ensures product purity and yield.
Smart Images

Figure CN223184525U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of feeding devices, in particular to a methyl methacrylate polymerization inhibitor adding structure. Background Art
[0002] In the chemical industry, particularly in processes involving the polymerization of methyl methacrylate (MMA), the precise addition and handling of polymerization inhibitors is crucial. Previously, the addition of MMA polymerization inhibitors to a mixing reactor often encountered numerous challenges. For example, the lack of precise metering equipment made it difficult to accurately control the dosage, resulting in unstable reaction results and varying product quality. Furthermore, traditional addition methods lacked temperature control, preventing the inhibitor from reaching the appropriate temperature before addition, impacting reaction efficiency and effectiveness. Furthermore, the presence of impurities can negatively impact the reaction, but previous addition systems lacked effective filtration mechanisms, making it difficult to ensure inhibitor purity. Utility Model Content
[0003] The purpose of the utility model is to provide a methyl methacrylate polymerization inhibitor addition structure to solve the problems raised in the background technology.
[0004] To achieve the above-mentioned purpose, the present invention provides the following technical solution, which includes a material storage component, a metering pump is provided on the side of the material storage component, the feed port of the metering pump is connected to the material storage component through a conduit 1, and the discharge port of the metering pump is connected to the discharge component through a conduit 2.
[0005] As a preferred embodiment of the present invention, the material storage assembly includes an inner barrel, a loading tube is provided on the top of the inner barrel, a sealing cover is provided on the loading tube, a discharge valve tube is provided at the bottom of the inner barrel, the discharge valve tube is connected to a conduit, an outer barrel is provided on the outside of the inner barrel, and a vacuum chamber is formed between the inner barrel and the outer barrel.
[0006] As a preferred embodiment of the present invention, the unloading assembly includes a buffer shell, a first feed port is provided on one side of the buffer shell, the other end of the conduit 2 is arranged on the first feed port, a temperature conducting pipe is provided at the bottom of the buffer shell, a spiral unloading trough is provided in the temperature conducting pipe, a jacketed heat exchanger is provided at the bottom of the buffer shell, the jacketed heat exchanger is sleeved on the outside of the temperature conducting pipe, and limiting slots are provided on several inner walls of the buffer shell.
[0007] As a preferred embodiment of the present invention, a detachable filter shell is provided in the buffer shell, a plurality of plug blocks are provided on the outer wall of the filter shell, the plug blocks are inserted in the limiting slots, a second feed port is provided at the position of the first feed port on the side wall of the filter shell, a guide plate is provided on the inner wall of one side of the filter shell, and the guide plate is located below the second feed port.
[0008] As a preferred embodiment of the present invention, a plurality of magnetic blocks are provided on the top of the buffer shell, the top of the buffer shell is magnetically connected to the iron plate cover, and the top of the iron plate cover is provided with a handle.
[0009] As a preferred embodiment of the present invention, a mounting plate is provided on one side of the outer barrel, a water level sensor is provided on the mounting plate, a probe of the water level sensor is located on the inner wall of the inner barrel, a sealing sleeve is provided on the probe, the sealing sleeve is located in the wall of the inner barrel, a sealing ring is provided on the connecting line of the water level sensor, and the sealing ring is provided in the wall of the outer barrel.
[0010] Compared with the prior art, the above technical solution of the present invention has the following beneficial technical effects:
[0011] 1. The utility model effectively removes impurities in the inhibitor by setting a filter shell, so that the pure inhibitor participates in the reaction, which can reduce the interference and adverse effects of impurities on the reaction, improve the selectivity and efficiency of the reaction, and ensure the quality and performance of the product.
[0012] 2. The utility model can extract a set amount of methyl methacrylate polymerization inhibitor with high precision through the use of a metering pump, which ensures that the amount of inhibitor added is accurate during each feeding process, greatly improving the consistency and stability of the reaction. Whether it is a small-scale experiment or large-scale production, the accuracy of the reaction conditions can be guaranteed, thereby effectively improving product quality and the repeatability of the reaction effect.
[0013] 3. The utility model can provide precise temperature regulation for the inhibitor through the combination of the jacketed heat exchanger and the temperature conducting tube, so that the inhibitor reaches the appropriate temperature before being added to the mixed reaction equipment, which helps to promote the reaction, increase the reaction rate and conversion rate, reduce the occurrence of side reactions, and thus improve the purity and yield of the product.
[0014] 3. The storage assembly of the present invention greatly weakens the heat exchange between the inner barrel and the external environment through the vacuum chamber design between the inner barrel and the outer barrel, which can prevent the external temperature changes from affecting the temperature of the inhibitor too quickly, ensure its stable performance, and extend its effective storage time. BRIEF DESCRIPTION OF THE DRAWINGS
[0015] Figure 1 It is a schematic diagram of the overall structure of the utility model;
[0016] Figure 2 This is a schematic diagram of the structure of the material storage component of the utility model;
[0017] Figure 3 This is a side sectional view of the material storage component of the present invention;
[0018] Figure 4 This is a schematic structural diagram of the water level sensor of the utility model;
[0019] Figure 5 This is a schematic diagram of the structure of the metering pump of the utility model;
[0020] Figure 6 This is a schematic diagram of the blanking component structure of the present utility model;
[0021] Figure 7 This is an exploded view of the blanking component of the present invention;
[0022] Figure 8 for Figure 7 Enlarged view of point A in the middle;
[0023] Figure 9 This is a side sectional view showing the jacketed heat exchanger after the blanking assembly of the utility model is removed.
[0024] Figure numerals: material storage assembly 1, inner barrel 10, loading pipe 11, discharge valve pipe 12, sealing cover 13, support frame 14, mounting plate 15, outer barrel 16, vacuum chamber 17, water level sensor 2, sealing ring 20, sealing sleeve 21, metering pump 3, conduit one 30, conduit two 31, discharge assembly 4, buffer shell 40, first feed port 41, temperature guide tube 42, spiral discharge chute 43, limit slot 44, jacketed heat exchanger 45, filter shell 46, insert block 47, second feed port 48, guide plate 49, magnetic block 410, iron plate cover 411, handle 412. DETAILED DESCRIPTION
[0025] To make the objectives, technical solutions, and advantages of the present invention more clearly understood, the present invention is further described below in conjunction with specific embodiments and with reference to the accompanying drawings. It should be understood that these descriptions are merely illustrative and are not intended to limit the scope of the present invention. Furthermore, descriptions of known structures and technologies are omitted in the following description to avoid unnecessary confusion regarding the concepts of the present invention.
[0026] like Figures 1-9 As shown, the utility model provides a methyl methacrylate polymerization inhibitor adding structure, which includes a material storage component 1, a metering pump 3 and a material discharge component 4.
[0027] A metering pump 3 is installed on the side of the storage assembly 1. The feed port of metering pump 3 is connected to the storage assembly 1 via a conduit 1 30. The storage assembly 1 includes an inner barrel 10. A charging pipe 11 is installed on the top of the inner barrel 10. The charging pipe 11 is equipped with a sealing cap 13 to ensure sealing during the feeding process. A discharge valve pipe 12 is installed at the bottom of the inner barrel 10, which is connected to the conduit 1 30. It is worth mentioning that an outer barrel 16 is also installed on the outside of the inner barrel 10. A vacuum chamber 17 is formed between the inner barrel 10 and the outer barrel 16. This design helps to maintain the temperature of the material in the inner barrel 10.
[0028] The discharge port of the metering pump 3 is connected to the discharge component 4 through the second conduit 31. The discharge component 4 includes a buffer shell 40. A first feed port 41 is provided on one side of the buffer shell 40. The other end of the second conduit 31 is accurately set on the first feed port 41. A temperature guide tube 42 is provided at the bottom of the buffer shell 40. A spiral discharge trough 43 is provided in the temperature guide tube 42. In order to better control the temperature, a jacketed heat exchanger 45 is provided at the bottom of the buffer shell 40, and the jacketed heat exchanger 45 is sleeved on the outside of the temperature guide tube 42. Limiting slots 44 are provided on several inner walls of the buffer shell 40 for installing a detachable filter shell 46. Several plug blocks 47 are provided on the outer wall of the filter shell 46. The plug blocks 47 are inserted in the limiting slots 44 to achieve stable installation of the filter shell 46. A second feed inlet 48 is provided on the side wall of the filter housing 46 at a position corresponding to the first feed inlet 41. A guide plate 49 is provided on one inner wall of the filter housing 46. The guide plate 49 is located below the second feed inlet 48 to help guide the flow of materials.
[0029] The top of the buffer shell 40 is provided with several magnetic blocks 410. The top of the buffer shell 40 is connected to the iron plate cover 411 through magnetism. The top of the iron plate cover 411 is provided with a handle 412 for easy operation.
[0030] A mounting plate 15 is provided on one side of the outer tub 16, on which the water level sensor 2 is mounted. The probe of the water level sensor 2 is located on the inner wall of the inner tub 10. To ensure a tight seal, the probe is covered with a sealing sleeve 21, which is located within the wall of the inner tub 10. A sealing ring 20 is installed on the connecting line of the water level sensor 2, which is located within the wall of the outer tub 16, thus ensuring the tightness and stability of the entire device.
[0031] Before use, the feed port of the mixing reaction device is accurately placed below the temperature conducting pipe 42. Next, the methyl methacrylate polymerization inhibitor is loaded into the inner barrel 10 through the charging pipe 11. Then, the jacketed heat exchanger 45 is started to heat according to the preset temperature.
[0032] When adding material, the discharge valve 12 is first opened. The metering pump 3 is then adjusted to pump out a set amount of methyl methacrylate polymerization inhibitor. The inhibitor then flows into the buffer housing 40 via the second conduit 31. As the inhibitor flows into the buffer housing 40, it passes through the filter housing 46, where impurities are filtered out. The inhibitor then flows into the spiral discharge chute 43 of the thermal conduit 42. During its flow within the spiral discharge chute 43, due to its increased travel distance, it is fully affected by the temperature of the thermal conduit 42, allowing the inhibitor to reach a suitable temperature before being added to the mixing reaction equipment for mixing.
[0033] When the filter housing 46 needs to be cleaned, the handle 412 is simply pulled, and the iron plate cover 411 is pulled out of the filter housing 46 under the action of the magnetic block 410 for cleaning.
[0034] It should be understood that the above-described specific embodiments of the present invention are merely illustrative of or explanation of the principles of the present invention and do not constitute limitations of the present invention. Therefore, any modifications, equivalent substitutions, improvements, etc. made without departing from the spirit and scope of the present invention shall be included within the scope of protection of the present invention. In addition, the appended claims of the present invention are intended to cover all changes and modifications that fall within the scope and metes and bounds of the appended claims, or equivalents of such scope and metes and bounds.
Claims
1. A methyl methacrylate polymerization inhibitor adding structure, comprising a metering pump (3), characterized in that: The feed port of the metering pump (3) is connected to the material storage component (1) through the first conduit (30), and the discharge port of the metering pump (3) is connected to the material discharge component (4) through the second conduit (31).
2. The methyl methacrylate polymerization inhibitor addition structure according to claim 1, characterized in that: The material storage assembly (1) includes an inner barrel (10), a loading tube (11) is provided on the top of the inner barrel (10), a sealing cover (13) is provided on the loading tube (11), a discharge valve tube (12) is provided at the bottom of the inner barrel (10), the discharge valve tube (12) is connected to the conduit 1 (30), an outer barrel (16) is provided on the outside of the inner barrel (10), and a vacuum chamber (17) is provided between the inner barrel (10) and the outer barrel (16).
3. The methyl methacrylate polymerization inhibitor addition structure according to claim 2, characterized in that: The material discharge assembly (4) includes a buffer shell (40), a first feed port (41) is provided on one side of the buffer shell (40), the other end of the second conduit (31) is arranged on the first feed port (41), a temperature conducting pipe (42) is provided at the bottom of the buffer shell (40), a spiral material discharge trough (43) is provided in the temperature conducting pipe (42), a jacketed heat exchanger (45) is provided at the bottom of the buffer shell (40), the jacketed heat exchanger (45) is sleeved on the outside of the temperature conducting pipe (42), and several inner walls of the buffer shell (40) are provided with limiting slots (44).
4. The methyl methacrylate polymerization inhibitor addition structure according to claim 3, characterized in that: A detachable filter shell (46) is provided in the buffer shell (40), and a plurality of plug blocks (47) are provided on the outer wall of the filter shell (46), and the plug blocks (47) are inserted into the limiting slots (44). A second feed inlet (48) is provided on the side wall of the filter shell (46) at a position corresponding to the first feed inlet (41), and a guide plate (49) is provided on the inner wall of one side of the filter shell (46), and the guide plate (49) is located below the second feed inlet (48).
5. The methyl methacrylate polymerization inhibitor addition structure according to claim 4, characterized in that: A plurality of magnetic blocks (410) are provided on the top of the buffer shell (40), the top of the buffer shell (40) is magnetically connected to an iron plate cover (411), and a handle (412) is provided on the top of the iron plate cover (411).
6. The methyl methacrylate polymerization inhibitor addition structure according to claim 5, characterized in that: A mounting plate (15) is provided on one side of the outer barrel (16), and a water level sensor (2) is provided on the mounting plate (15). A probe of the water level sensor (2) is located on the inner wall of the inner barrel (10), and a sealing sleeve (21) is provided on the probe. The sealing sleeve (21) is located in the wall of the inner barrel (10). A sealing ring (20) is provided on the connecting line of the water level sensor (2), and the sealing ring (20) is provided in the wall of the outer barrel (16).