Automatic sampling device of reaction kettle for cross-linking agent production
By designing an automatic sampling device for corrosion-resistant and high-temperature-resistant materials and high-precision solenoid valves, the problems of low sampling efficiency and poor accuracy of the reactor are solved, and efficient sampling that flexibly adapts to different reactor heights is achieved.
Patent Information
- Application Number
- CN202422293426.2
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-09-20
- Publication Date
- 2025-08-12
- Estimated Expiration
- 2034-09-20
AI Technical Summary
The existing reactors have low efficiency and poor accuracy when sampling, and are inconvenient for adaptive height adjustment according to different reactors, which makes sampling and installation inconvenient.
An automatic sampling device including a control box, sampling tube, sampling pump, fluid conduit, sampling valve and anti-blocking joint is designed. It uses corrosion-resistant and high-temperature resistant materials, combined with high-precision solenoid valve and adjustable threaded joint, equipped with liftable structure and limiting plate to ensure sampling accuracy and stability.
It improves sampling efficiency and accuracy, reduces leakage risk, adapts to different reactor heights, meets multiple sampling needs, and ensures the reliability and stability of the sampling device.
Smart Images

Figure CN223217158U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of cross-linking agent production, in particular to an automatic sampling device for a reaction kettle used in cross-linking agent production. Background Art
[0002] Crosslinkers, also known as bridging agents, curing agents, hardeners, or curing agents, are a crucial component of polyolefin photoresists and a key chemical in the field of polymer materials. They are widely used in a variety of industries, including rubber, plastics, coatings, adhesives, and medical aesthetics. In the rubber industry, crosslinkers (often called vulcanizers) are a key raw material for the preparation of rubber products. In the plastics industry, crosslinkers are used to improve the strength, heat resistance, and wear resistance of plastics. Reactors are a common type of reaction equipment used in production. Through the structural design and parameter configuration of the vessel, they achieve the heating, evaporation, cooling, and low-speed mixing functions required by the process.
[0003] Existing reactors have low sampling efficiency and poor accuracy when sampling, and are not easy to adjust the height according to different reactors, which makes sampling and installation inconvenient.
[0004] Therefore, in view of this, the existing structure and defects are studied and improved, and an automatic sampling device for a reactor used in cross-linking agent production is proposed, in order to achieve a more practical purpose. Utility Model Content
[0005] The purpose of the utility model is to provide an automatic sampling device for a reactor used in cross-linking agent production, so as to solve the problems raised in the above background technology.
[0006] To achieve the above-mentioned purpose, the utility model provides the following technical solutions: an automatic sampling device for a reactor for cross-linking agent production, comprising a control box and a sampling tube, a connecting pad is installed on the top of the control box, and a sampling pump is mounted on the top of the connecting pad, the inlet and outlet ports of the sampling pump are provided with a liquid guide tube, and the liquid outlet end of the liquid guide tube is provided with a discharge guide plate, and the liquid inlet end of the liquid guide tube is provided with a sampling tube, one end of the inner part of the liquid guide tube is connected with a sampling valve, and the bottom of the sampling tube is connected with an anti-blocking joint, a slide rail slider assembly is provided on the inner side of the control box, a limiting plate is installed on the horizontal end of the connecting pad, and an extension arc plate is provided on the other side of the limiting plate, a lifting rod is vertically provided on the bottom of the connecting pad, and a slide plate is installed on the bottom of the lifting rod, and the slide plate and the slide rail slider assembly are detachably fixedly connected, and a sampling barrel is wrapped on the inner side of the limiting plate.
[0007] Furthermore, the upper and lower positions of the discharge ports of the sampling barrel and the discharge guide plate cooperate with each other.
[0008] Furthermore, threaded joints are provided at the upper and lower ends of the sampling tubes, and multiple groups of the sampling tubes can be threadably disassembled and installed.
[0009] Furthermore, the sampling tube, the liquid guiding tube and the anti-blocking joint are fixedly connected by threads.
[0010] Furthermore, the control box forms an up and down lifting structure between the slide rail and slider assembly and the slide, and the lifting rod and the slide form an up and down lifting structure.
[0011] Furthermore, the dimensions of the extended arc plate and the sampling barrel match each other.
[0012] The utility model provides an automatic sampling device for a reactor used in cross-linking agent production, which has the following beneficial effects:
[0013] 1. The sampling tube, the main component of the sampling device, is designed to be adjustable. One end of the sampling tube extends into the reactor and the other end is connected to the sampling valve. The sampling tube is made of corrosion-resistant and high-temperature resistant materials, such as stainless steel or Teflon, to ensure that it will not be affected by chemical corrosion or high temperatures during the crosslinker production process.
[0014] The threaded joint of the sampling tube can adjust the height according to the sampling requirements. On the other hand, when the thread is installed, the connection structure is relatively tight, and it is not easy to be corroded or deformed to cause leakage, thereby reducing the impact on the production of the cross-linking agent.
[0015] 2. In the present invention, the sampling valve is installed on the pipeline between the liquid guide tube and the sampling pump to control the sample flow during the sampling process; the sampling valve adopts a high-precision solenoid valve with the characteristics of fast response, high sealing and long life to ensure the accuracy and reliability of the sampling operation; the sampling pump is controlled by the control system to start and stop and the speed to adjust the sampling flow and speed.
[0016] 3. In this utility model, the liquid outlet is pulled by the discharge guide plate and can flow out from the top nozzle, which is convenient for collection in the sampling bucket at the bottom and for observing the sampling amount through the sampling bucket. In addition, a liftable slide is provided at the bottom of the sampling bucket, which can adapt to sampling buckets of different heights and meet the sampling requirements of different doses.
[0017] A limiting plate is provided on the outside of the connecting pad for support. The limiting plate utilizes the extended arc plate extending from the outside to limit and wrap the sampling barrel, thereby ensuring the overall stability of the sampling barrel. BRIEF DESCRIPTION OF THE DRAWINGS
[0018] The disclosure of the present invention will become more easily understood with reference to the accompanying drawings. Those skilled in the art will readily understand that these drawings are merely used to illustrate the technical solution of the present invention and are not intended to limit the scope of protection of the present invention.
[0019] Figure 1 This is a front view structural schematic diagram of an automatic sampling device for a reactor used in cross-linking agent production according to the present invention;
[0020] Figure 2 This is a schematic diagram of the internal structure of a sampling tube of an automatic sampling device for a reactor for cross-linking agent production according to the present invention;
[0021] Figure 3 The utility model is a schematic diagram of a top view of the limit plate of an automatic sampling device for a reactor for cross-linking agent production.
[0022] In the figure: 1. Control box; 101. Slide rail and slider assembly; 2. Sampling tube; 201. Threaded joint; 3. Sampling valve; 4. Liquid guide tube; 5. Connecting pad; 6. Sampling pump; 7. Discharge guide plate; 8. Lifting rod; 9. Limit plate; 901. Extension arc plate; 10. Slide plate; 11. Sampling barrel; 12. Anti-blocking joint. DETAILED DESCRIPTION
[0023] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the embodiments described are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative efforts are within the scope of protection of the present invention.
[0024] See also Figure 1-3The utility model provides a technical solution: an automatic sampling device for a reactor for cross-linking agent production, comprising a control box 1 and a sampling tube 2, a connecting plate 5 is installed on the top of the control box 1, and a sampling pump 6 is mounted on the top of the connecting plate 5, a liquid guide tube 4 is provided at the inlet and outlet ports of the sampling pump 6, and a discharge guide plate 7 is provided at the liquid outlet end of the liquid guide tube 4, and a sampling tube 2 is provided at the liquid inlet end of the liquid guide tube 4, one end of the inner part of the liquid guide tube 4 is connected to a sampling valve 3, and the bottom of the sampling tube 2 is connected to an anti-blocking joint 12, a slide rail slider assembly 101 is provided on the inner side of the control box 1, a limit plate 9 is installed on the horizontal end of the connecting plate 5, and an extension arc plate 901 is provided on the other side of the limit plate 9, and the connecting plate 5 is provided with a plurality of connecting plates. A lifting rod 8 is vertically provided at the bottom, and a slide 10 is installed at the bottom of the lifting rod 8, and the slide 10 and the slide rail slider assembly 101 are detachably fixedly connected, and the sampling bucket 11 is wrapped on the inner side of the limit plate 9; the upper and lower positions of the sampling bucket 11 and the discharge port of the discharge guide plate 7 cooperate with each other; the upper and lower ends of the sampling tube 2 are provided with threaded joints 201, and multiple groups of sampling tubes 2 can be threadedly detached and installed; the sampling tube 2, the liquid guide tube 4 and the anti-blocking joint 12 are fixedly connected by threads; the control box 1 forms an up and down lifting structure between the slide rail slider assembly 101 and the slide plate 10, and the lifting rod 8 and the slide plate 10 form an up and down lifting structure; the dimensions of the extended arc plate 901 and the sampling barrel 11 cooperate with each other.
[0025] The sampling tube 2, the main component of the sampling device, is adjustable, with one end extending into the reactor and the other connected to the sampling valve. The sampling tube is made of corrosion-resistant and high-temperature-resistant materials, such as stainless steel or Teflon, to ensure it is not affected by chemical corrosion or high temperatures during the crosslinker production process.
[0026] The threaded joint 201 of the sampling tube 2 can adjust the height according to the sampling requirements. On the other hand, when the thread is installed, the connection structure is relatively tight and is not prone to corrosion, deformation and leakage, thereby reducing the impact on the production of the cross-linking agent.
[0027] The sampling valve 3 is installed on the pipeline between the liquid guide tube 4 and the sampling pump 6 to control the flow of samples during the sampling process. The sampling valve 3 adopts a high-precision solenoid valve with the characteristics of fast response, high sealing and long life to ensure the accuracy and reliability of the sampling operation. The sampling pump 6 controls its start and stop and speed through the control system to adjust the sampling flow and speed.
[0028] The liquid is drawn through the discharge guide plate 7 and can flow out from the top nozzle, making it easy for the sampling bucket 11 at the bottom to collect it. It is also convenient to observe the sampling amount through the sampling bucket 11. In addition, a liftable slide 10 is provided at the bottom of the sampling bucket 11, which can adapt to sampling buckets 11 of different heights to meet sampling requirements of different doses.
[0029] A limit plate 9 is provided on the outside of the connecting pad 5 for support. The limit plate 9 uses an extended arc plate 901 extending from the outside to limit and wrap the sampling barrel 11, thereby ensuring the overall stability of the sampling barrel 11.
[0030] The sampling bottle is made of transparent, corrosion-resistant materials, such as glass or polytetrafluoroethylene, to facilitate observation of the sample status and subsequent analysis and testing.
[0031] Working principle: For this type of automatic sampling device for reactors used for cross-linking agent production, first, according to the sampling situation in the reactor, multiple groups of sampling tubes 2 are threadedly installed to adapt to the sampling requirements of the reactor. Then, the sampling tubes 2 and the anti-blocking joint 12 are inserted into the interior of the reactor. At the same time, the sampling barrel 11 is placed at the sampling position of the slide plate 10, and the extended arc plate 901 of the limit plate 9 is used to pre-position the sampling barrel 11. Then, the lifting rod 8 is controlled to drive the sampling barrel 11 to rise, so that the sampling port of the sampling barrel 11 corresponds to the discharge port of the discharge guide plate 7. Then, the sampling valve 3 at the top is controlled to open, so that the liquid collection channel of the liquid guide tube 4 is opened, and the sampling pump 6 of the power source of the sampling device is started. The reagent is sampled and extracted from the anti-blocking joint 12 end at the bottom, so that the reagent passes through the sampling tube 2, the liquid guide tube 4 and the discharge guide plate 7 and enters the sampling barrel 11 for storage.
[0032] The above is only a specific implementation method of the present invention, but the scope of protection of the present invention is not limited to this. Any changes or substitutions that can be thought of by any technician familiar with the field within the technical scope disclosed by the present invention without creative work should be included in the scope of protection of the present invention. Therefore, the scope of protection of the present invention should be based on the scope of protection defined in the claims.
Claims
1. An automatic sampling device for a reactor for crosslinking agent production, comprising a control box (1) and a sampling tube (2), characterized in that: A connecting pad (5) is installed on the top of the control box (1), and a sampling pump (6) is mounted on the top of the connecting pad (5), a liquid guide tube (4) is provided at the inlet and outlet ports of the sampling pump (6), and a discharge guide plate (7) is provided at the liquid outlet end of the liquid guide tube (4), and a sampling tube (2) is provided at the liquid inlet end of the liquid guide tube (4), one end of the interior of the liquid guide tube (4) is connected to a sampling valve (3), and the bottom of the sampling tube (2) is connected to an anti-blocking joint (12), and the control box A slide rail slider assembly (101) is provided on the inner side of (1), a limit plate (9) is installed on the horizontal end of the connecting pad (5), and an extension arc plate (901) is provided on the other side of the limit plate (9), a lifting rod (8) is vertically provided on the bottom of the connecting pad (5), and a slide plate (10) is installed on the bottom of the lifting rod (8), and the slide plate (10) and the slide rail slider assembly (101) are detachably fixedly connected, and a sampling barrel (11) is wrapped on the inner side of the limit plate (9).
2. The automatic sampling device for a reactor for crosslinking agent production according to claim 1, characterized in that: The upper and lower positions of the discharge ports of the sampling barrel (11) and the discharge guide plate (7) cooperate with each other.
3. The automatic sampling device for a reactor for cross-linking agent production according to claim 1, characterized in that: The upper and lower ends of the sampling tube (2) are provided with threaded joints (201), and multiple groups of the sampling tubes (2) can be threadedly disassembled and installed.
4. The automatic sampling device for a reactor for cross-linking agent production according to claim 1, characterized in that: The sampling tube (2), the liquid guiding tube (4) and the anti-blocking joint (12) are fixedly connected by threads.
5. The automatic sampling device for a reactor for cross-linking agent production according to claim 1, characterized in that: The control box (1) forms an up-and-down lifting structure between the slide rail and slider assembly (101) and the slide plate (10), and the lifting rod (8) and the slide plate (10) form an up-and-down lifting structure.
6. The automatic sampling device for a reactor for cross-linking agent production according to claim 1, characterized in that: The dimensions of the extended arc plate (901) and the sampling barrel (11) are matched with each other.