Novel high-precision mercury generating device

Through the combination of gas supply, permeation and concentration detection mechanisms, the problems of high difficulty in controlling and low safety of mercury vapor generators are solved, and the generation and safe output of high-precision mercury vapor are achieved.

CN223259371UActive Publication Date: 2025-08-22杭州晟境科技有限公司
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Patent Information

Application Number
CN202422458005.0
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-10-11
Publication Date
2025-08-22
Estimated Expiration
2034-10-11

AI Technical Summary

Technical Problem

The existing mercury vapor generation device is difficult to control, the mercury vapor generated has a low concentration accuracy, and its safety factor is low, which can easily cause damage to the physical health of the operator.

Method used

The combination of gas supply mechanism, mercury permeation mechanism, mercury vapor output mechanism and concentration detection mechanism is adopted to achieve precise control of mercury vapor concentration through dilution gas flow regulation and concentration detection, and the standardization of the detection environment is ensured with the temperature regulation mechanism, and a purification mechanism is equipped to balance the system pressure.

Benefits of technology

Accurate output and rapid adjustment of mercury vapor concentration is achieved, control accuracy and safety are improved, and health risks to operators are reduced.

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Abstract

The utility model relates to the technical field of sheet processing, in particular to a novel high-precision mercury generation device, which comprises a gas supply mechanism for controlling the introduction of diluent gas, a mercury permeation mechanism for generating pure mercury vapor, and a mercury vapor output mechanism for diluting the pure mercury vapor to output mercury vapor with set concentration, and the concentration detection mechanism is used for detecting and transmitting mercury vapor concentration information so as to adjust the mercury vapor concentration. According to the utility model, mercury vapor with set concentration can be accurately output, pure mercury vapor is diluted by adopting the high-range output end of the gas supply mechanism in a mode of adjusting the flow of diluent gas, and the concentration of the output mercury vapor can be conveniently controlled; meanwhile, the concentration detection mechanism is adopted to detect the diluted mercury vapor and transmit mercury vapor concentration information to the gas supply mechanism, compensation and correction of the mercury vapor concentration are facilitated, the control precision is high, and the adjusting speed is high.
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Description

Technical Field

[0001] The utility model relates to the technical field of sheet material processing, in particular to a novel high-precision mercury generating device. Background Art

[0002] Mercury pollution has become a global issue. Mercury is a toxic heavy metal that exists in the environment in three valence states (Hg0, Hg1+, and Hg2+). It is persistent, has long-range mobility, and is bioaccumulative. Emissions primarily come from coal-fired power plants, industrial boilers, waste combustion, and some industrial processes. Due to its toxicity, persistence, and bioaccumulation, Hg pollution among heavy metals is receiving increasing attention. Analyzers in existing monitoring systems, which continuously monitor mercury levels in real-time from pollutant emissions such as coal-fired boilers and waste incinerator flue gases, are calibrated using standard mercury vapor to ensure accuracy.

[0003] Existing standard mercury vapor generators generally obtain mercury vapor of different concentrations by controlling the temperature of a mercury permeation tube. For example, a generator for producing elemental mercury standard gas disclosed in a Chinese patent (Announcement No.: CN105300760B) obtains elemental mercury standard gas of a certain concentration by controlling the carrier gas flow rate and the temperature of a water bath. In actual implementation, due to the lag in operating air pressure changes and temperature regulation, the output mercury vapor concentration is difficult to control, which is not conducive to subsequent calibration work. At the same time, it has no exhaust gas treatment device, which makes it easy for operators to come into contact with mercury vapor, which can easily cause damage to the operator's health. At the same time, the air pressure in the system loop is difficult to control, resulting in a low safety factor. Utility Model Content

[0004] The technical problem to be solved by the utility model is that the existing mercury vapor generating device is difficult to control, the concentration accuracy of the generated mercury vapor is low, and the safety factor is low, which is easy to cause damage to the health of the operator.

[0005] To solve the above technical problems, the present invention adopts the following technical solution: a new type of high-precision mercury generating device, comprising an air supply mechanism for controlling the introduction of dilution gas, a mercury penetration mechanism for generating pure mercury vapor, a mercury vapor output mechanism for diluting pure mercury vapor to output mercury vapor of a set concentration, and a concentration detection mechanism for detecting and transmitting mercury vapor concentration information to adjust the mercury vapor concentration. The air supply mechanism is provided with a low-range output end and a high-range output end for adjusting the mercury vapor concentration through flow regulation. The low-range output end of the air supply mechanism is connected to the input end of the mercury penetration mechanism, the input end of the mercury vapor output mechanism is connected to the high-range output end of the air supply mechanism and the output end of the mercury penetration mechanism through an air path component, the output end of the mercury vapor output mechanism is respectively connected to the input end of the corresponding analysis equipment and the concentration detection mechanism, and the signal output end of the concentration detection mechanism is connected to the signal input end of the air supply mechanism.

[0006] When the utility model is working, it can accurately output mercury vapor of a set concentration, and the high-range output end of the gas supply mechanism is used to dilute the pure mercury vapor by adjusting the dilution gas flow rate, so as to facilitate the control of the concentration of the output mercury vapor. At the same time, the concentration detection mechanism is used to detect the diluted mercury vapor and transmit the mercury vapor concentration information to the gas supply mechanism, so as to facilitate the compensation correction of the mercury vapor concentration, with high control accuracy and fast adjustment speed.

[0007] Preferably, the concentration detection mechanism includes a gas power device, a detection gas chamber, a light source assembly, a detection assembly and a photometer control module. The mercury vapor output mechanism is provided with a detection output end for outputting part of the mercury vapor for detection by the concentration detection mechanism to achieve concentration adjustment of the mercury vapor. The air inlet end of the detection gas chamber is connected to the detection output end of the mercury vapor output mechanism, and the air outlet end of the detection gas chamber is connected to the corresponding gas collection device through the gas power device. A chamber for mercury vapor to pass through is provided in the detection gas chamber. The light source assembly and the detection assembly are spaced apart at both ends of the cavity of the detection gas chamber, and the light source assembly and the detection assembly are both connected to the photometer control module.

[0008] Preferably, the concentration detection mechanism also includes a photometer mounting bracket, a light source emitting part, a light source receiving part and a first temperature adjustment mechanism for adjusting the mercury vapor temperature in the concentration detection mechanism to a preset standard temperature. The light source emitting part and the light source receiving part are both installed on the photometer mounting bracket, the air inlet end of the detection gas chamber is connected to the detection output end of the mercury vapor output mechanism through the light source emitting part, the air outlet end of the detection gas chamber is connected to the gas power device through the light source receiving part, the light emitting part of the light source assembly is arranged inside the light source emitting part and is connected to the chamber of the detection gas chamber, the detection part of the detection assembly is arranged inside the light source receiving part and is connected to the chamber, and the temperature adjustment end of the first temperature adjustment mechanism is arranged inside the light source emitting part.

[0009] When the utility model is working, it can realize the detection of mercury vapor concentration. At the same time, the first temperature adjustment mechanism is used to adjust the temperature of the mercury vapor in the concentration detection mechanism to a preset standard temperature, so that the detection environment of the concentration detection mechanism can be maintained in the standard detection environment for a long time, which can further improve the accuracy of concentration detection.

[0010] Preferably, the concentration detection mechanism is further provided with a standard gas inlet end for introducing standard gas for calibration.

[0011] Preferably, the mercury infiltration mechanism includes a mercury infiltration furnace, a infiltration furnace control module, a mercury infiltration tube and a second temperature regulating mechanism for regulating the temperature of the mercury infiltration furnace to a preset standard temperature. The interior of the mercury infiltration furnace is provided with a mercury infiltration chamber for installing the mercury infiltration tube, and the mercury infiltration tube is arranged in the mercury infiltration chamber of the mercury infiltration furnace. The temperature regulating end and the temperature detection end of the temperature regulating mechanism are both installed on the mercury infiltration furnace. The control end of the infiltration furnace control module is connected to the second temperature regulating mechanism, the signal input end of the infiltration furnace control module is connected to the signal output end of the concentration detection mechanism, the air inlet end of the mercury infiltration chamber of the mercury infiltration furnace is connected to the low-range output end of the air supply mechanism, and the air outlet end of the mercury infiltration chamber of the mercury infiltration furnace is connected to the input end of the mercury vapor output mechanism.

[0012] Preferably, a meandering preheating pipe is provided in the mercury permeation furnace, the temperature regulating end of the second temperature regulating mechanism is connected to the preheating pipe, and the air inlet end of the mercury permeation chamber of the mercury permeation furnace is connected to the low-range output end of the air supply mechanism through the preheating pipe.

[0013] When the utility model is working, it can realize the penetration generation of pure mercury vapor with a fast generation rate and a good generation effect. At the same time, a second temperature adjustment mechanism is used to adjust the temperature of the mercury penetration furnace to a preset standard temperature, so that the penetration rate during mercury penetration is within a better range. At the same time, it is also convenient to trace the concentration of mercury penetration, which can further improve the control accuracy of mercury vapor concentration.

[0014] Preferably, the mercury vapor output mechanism is provided with a purification mechanism for balancing the pressure in the system, the purification mechanism is filled with a filler for purifying mercury vapor, and part of the mercury vapor in the mercury vapor output mechanism is output to the outside after being purified by the purification mechanism.

[0015] The beneficial technical effects of the utility model include:

[0016] 1. The utility model can accurately output mercury vapor of a set concentration. The high-range output end of the gas supply mechanism is used to dilute the pure mercury vapor by adjusting the dilution gas flow rate, which facilitates the control of the concentration of the output mercury vapor. At the same time, a concentration detection mechanism is used to detect the diluted mercury vapor and transmit the mercury vapor concentration information to the gas supply mechanism, which facilitates the compensation correction of the mercury vapor concentration, with high control accuracy and fast adjustment speed.

[0017] 2. The present invention can detect the concentration of mercury vapor, and at the same time, adopts a first temperature adjustment mechanism to adjust the temperature of the mercury vapor in the concentration detection mechanism to a preset standard temperature, so that the detection environment of the concentration detection mechanism can be maintained in a standard detection environment for a long time, which can further improve the accuracy of concentration detection.

[0018] 3. The utility model can realize the infiltration generation of pure mercury vapor with a fast generation rate and good generation effect. At the same time, a second temperature adjustment mechanism is used to adjust the temperature of the mercury infiltration furnace to a preset standard temperature, so that the infiltration rate during mercury infiltration is within a better range. At the same time, it is also convenient to trace the concentration of mercury infiltration, which can further improve the control accuracy of mercury vapor concentration.

[0019] Other features and advantages of the present invention will be disclosed in detail in the following specific embodiments and drawings. BRIEF DESCRIPTION OF THE DRAWINGS

[0020] The present invention will be further described below with reference to the accompanying drawings:

[0021] Attachment Figure 1 This is a schematic diagram of the structure of a new type of high-precision mercury generating device;

[0022] Attachment Figure 2 This is an exploded view of the concentration detection mechanism;

[0023] Attachment Figure 3 is a cross-sectional view of the concentration detection mechanism;

[0024] Attachment Figure 4 This is an exploded view of the mercury penetration mechanism;

[0025] Attachment Figure 5 is a cross-sectional view of the mercury penetration mechanism;

[0026] Attachment Figure 6 This is the working flow chart of a new type of high-precision mercury generation device. DETAILED DESCRIPTION

[0027] The following is an explanation and description of the technical solutions of the embodiments of the present invention in conjunction with the drawings of the embodiments of the present invention, but the following embodiments are only preferred embodiments of the present invention and are not exhaustive. Based on the embodiments in the embodiments, other embodiments obtained by those skilled in the art without creative work are all within the scope of protection of the present invention.

[0028] In the following description, terms such as "inside", "outside", "up", "down", "left", "right", etc. that indicate directions or positional relationships are only used to facilitate the description of the embodiments and simplify the description, and do not indicate or imply that the device or element referred to must have a specific direction, be constructed and operate in a specific direction. Therefore, they should not be understood as limiting the present invention.

[0029] Example 1:

[0030] Please see the attached Figure 1 This embodiment discloses a novel high-precision mercury generating device, including an air supply mechanism 1 for controlling the introduction of dilution gas, a mercury permeation mechanism 2 for generating pure mercury vapor, a mercury vapor output mechanism 3 for diluting the pure mercury vapor to output mercury vapor of a set concentration, and a concentration detection mechanism 4 for detecting and transmitting mercury vapor concentration information to adjust the mercury vapor concentration. Detailed description will be given below with reference to the accompanying drawings.

[0031] Please see the attached Figure 2 To the attached Figure 6 In this embodiment, the gas supply mechanism 1 is provided with a low-range output end 11 and a high-range output end 12 for adjusting the mercury vapor concentration through flow regulation. In specific implementation, an electronic pressure photometer control module 45 and a sonic orifice can be used to perform low-range output of the dilution gas, which facilitates control and provides stable flow output. The low-range output end 11 of the gas supply mechanism 1 is connected to the input end of the mercury permeation mechanism 2, and the input end of the mercury vapor output mechanism 3 is connected to the high-range output end 12 of the gas supply mechanism 1 and the output end of the mercury permeation mechanism 2 through an air path assembly. In specific implementation, the air path assembly can be configured to consist of a solenoid valve and an inerting tube. Each component is connected through the inerting tube, and the opening and closing control of the gas path between each component is controlled by the solenoid valve. This has a good sealing effect, a long service life, and can also reduce the difficulty of control. The output end of the mercury vapor output mechanism 3 is respectively connected to the corresponding analysis equipment and the input end of the concentration detection mechanism 4, and the signal output end of the concentration detection mechanism 4 is connected to the signal input end of the gas supply mechanism 1.

[0032] When this embodiment is working, it can accurately output mercury vapor of a set concentration. The high-range output end 12 of the gas supply mechanism 1 is used to dilute the pure mercury vapor by adjusting the dilution gas flow rate, which facilitates the control of the concentration of the output mercury vapor. At the same time, the concentration detection mechanism 4 is used to detect the diluted mercury vapor and transmit the mercury vapor concentration information to the gas supply mechanism 1, which facilitates the compensation correction of the mercury vapor concentration, with high control accuracy and fast adjustment speed.

[0033] Preferably, the mercury infiltration mechanism 2 includes a mercury infiltration furnace 21, a infiltration furnace control module 22, a mercury infiltration tube 23 and a second temperature regulating mechanism 24 for regulating the temperature of the mercury infiltration furnace 21 to a preset standard temperature. The interior of the mercury infiltration furnace 21 is provided with a mercury infiltration cavity for installing the mercury infiltration tube 23. The mercury infiltration tube 23 is arranged in the mercury infiltration cavity of the mercury infiltration furnace 21. The temperature regulating end and the temperature detection end of the temperature regulating mechanism are both installed on the mercury infiltration furnace 21. The control end of the infiltration furnace control module 22 is connected to the second temperature regulating mechanism 24. The signal input end of the infiltration furnace control module 22 is connected to the signal output end of the concentration detection mechanism 4. The air inlet end of the mercury infiltration cavity of the mercury infiltration furnace 21 is connected to the low-range output end 11 of the air supply mechanism 1. The air outlet end of the mercury infiltration cavity of the mercury infiltration furnace 21 is connected to the input end of the mercury vapor output mechanism 3.

[0034] As a further improvement of this embodiment, a preheating pipe 211 arranged in a winding manner is provided in the mercury permeation furnace 21, and the temperature regulating end of the second temperature regulating mechanism 24 is connected to the preheating pipe 211. The air inlet end of the mercury permeation chamber of the mercury permeation furnace 21 is connected to the low-range output end 11 of the gas supply mechanism 1 through the preheating pipe 211, which can achieve sufficient preheating of the dilution gas, thereby improving the efficiency of mercury permeation and the generation effect of pure mercury vapor. In specific implementation, the dilution gas can be any suitable gas such as nitrogen.

[0035] When this embodiment is working, it can realize the infiltration generation of pure mercury vapor with a fast generation rate and good generation effect. At the same time, the second temperature adjustment mechanism 24 is used to adjust the temperature of the mercury infiltration furnace 21 to a preset standard temperature, so that the infiltration rate during mercury infiltration is within a better range. At the same time, it is also convenient to trace the concentration of mercury infiltration, which can further improve the control accuracy of mercury vapor concentration.

[0036] Preferably, the mercury vapor output mechanism 3 is provided with a purification mechanism 31 for balancing the pressure in the system. The purification mechanism 31 is filled with a filler for purifying mercury vapor. Part of the mercury vapor in the mercury vapor output mechanism 3 is output to the outside after being purified by the purification mechanism 31, which can balance the pressure in the system and prevent gas backflow.

[0037] Example 2:

[0038] Please see the attached Figure 1This embodiment provides a new type of high-precision mercury generating device. The same points as those in the first embodiment will not be described in detail. The differences will be described in detail below with reference to the accompanying drawings.

[0039] Please see the attached Figure 2 To the attached Figure 6 In this embodiment, the concentration detection mechanism 4 includes a gas power device 41, a detection gas chamber 42, a light source assembly 43, a detection assembly 44 and a photometer control module 45. The mercury vapor output mechanism 3 is provided with a detection output end for outputting part of the mercury vapor for detection by the concentration detection mechanism 4 to achieve concentration adjustment of the mercury vapor. The air inlet end of the detection gas chamber 42 is connected to the detection output end of the mercury vapor output mechanism 3, and the air outlet end of the detection gas chamber 42 is connected to the corresponding gas collection device through the gas power device 41. A chamber for mercury vapor to pass through is provided in the detection gas chamber 42. The light source assembly 43 and the detection assembly 44 are arranged at intervals at both ends of the chamber of the detection gas chamber 42. The light source assembly 43 and the detection assembly 44 are both connected to the photometer control module 45.

[0040] In a specific implementation, the detection gas chamber 42 can be set to be made of quartz, and quartz window glass slides can be conveniently arranged at both ends thereof, which can improve the sealing effect and prevent mercury vapor leakage. Preferably, a flow stabilizing valve can be added between the detection gas chamber 42 and the gas power device 41 to improve the detection accuracy. In this embodiment, the light source component 43 can be set to a mercury lamp, which generates a characteristic spectrum containing 254nm. After irradiating the mercury vapor, the detection component 44 receives the signal and generates mercury vapor concentration information, thereby realizing real-time detection of mercury vapor. Of course, any other existing mercury vapor concentration detection device can also be used.

[0041] Preferably, the concentration detection mechanism 4 also includes a photometer mounting bracket 46, a light source emitting part 47, a light source receiving part 48 and a first temperature adjustment mechanism 49 for adjusting the temperature of the mercury vapor in the concentration detection mechanism 4 to a preset standard temperature. The light source emitting part 47 and the light source receiving part 48 are both mounted on the photometer mounting bracket 46. The air inlet end of the detection gas chamber 42 is connected to the detection output end of the mercury vapor output mechanism 3 through the light source emitting part 47, and the air outlet end of the detection gas chamber 42 is connected to the gas power device 41 through the light source receiving part 48. The light emitting part of the light source assembly 43 is arranged inside the light source emitting part 47 and is connected to the cavity of the detection gas chamber 42. The detection part of the detection assembly 44 is arranged inside the light source receiving part 48 and is connected to the cavity. The temperature adjustment end of the first temperature adjustment mechanism 49 is arranged inside the light source emitting part 47. By adjusting the temperature of the mercury vapor in the concentration detection mechanism 4 to a preset standard temperature, such as the calibration temperature set when calibrating the concentration detection mechanism 4, the detection error is further reduced and the accuracy of the output mercury vapor concentration is improved.

[0042] When this embodiment is working, it is possible to detect the concentration of mercury vapor. At the same time, the first temperature adjustment mechanism 49 is used to adjust the temperature of the mercury vapor in the concentration detection mechanism 4 to a preset standard temperature, so that the detection environment of the concentration detection mechanism 4 can be maintained in a standard detection environment for a long time, which can further improve the accuracy of concentration detection.

[0043] As a further improvement of this embodiment, the concentration detection mechanism 4 is also provided with a standard gas inlet end for introducing standard gas for calibration, which facilitates the calibration of the concentration detection mechanism 4. During the use of the high-precision mercury generating device, the standard gas inlet end of the concentration detection mechanism 4 can be connected to the output end of the concentration detection mechanism 4 through an air path component, which facilitates the emptying of the concentration detection mechanism 4, avoids mercury vapor residue, and improves the safety factor.

[0044] Example 3:

[0045] Please see the attached Figure 6 This embodiment provides a control method for a high-precision mercury generating device, which uses a new type of high-precision mercury generating device as described in the above embodiment, including the following steps:

[0046] S1: Initialize the high-precision mercury generator by introducing dilution gas;

[0047] S2: Setting the required mercury vapor concentration, starting the low-range output terminal 11 of the gas supply mechanism 1 to pass the dilution gas into the mercury penetration mechanism 2 to perform mercury penetration to generate pure mercury vapor;

[0048] S3: The pure mercury vapor generated by the mercury permeation mechanism 2 and the dilution gas outputted from the high-range output terminal 12 of the gas supply mechanism 1 are introduced into the mercury vapor output mechanism 3 for dilution. The pure mercury vapor is diluted by adjusting the output power of the high-range output terminal 12 of the gas supply mechanism 1.

[0049] S4: The diluted mercury vapor is passed into the concentration detection mechanism 4 for concentration detection, and the concentration information is fed back to the gas supply mechanism 1 to control the output power of the high-range output terminal 12 of the gas supply mechanism 1. When the concentration of the diluted mercury vapor reaches the set concentration, the mercury vapor is output by the mercury vapor output mechanism 3.

[0050] Preferably, the method further includes the following steps: in step S2, adjusting the working temperature of the mercury infiltration mechanism 2 during the mercury infiltration operation to a preset standard temperature;

[0051] In step S4, the following steps are also included: adjusting the working temperature of the concentration detection mechanism 4 during concentration detection to a preset standard temperature.

[0052] In a specific implementation, step S2 further includes the following steps: balancing the internal pressure of the high-precision mercury generating device by purifying the pure mercury vapor generated by the diversion part and then discharging it.

[0053] When this embodiment is in operation, it can achieve a series of operations including generation of pure mercury vapor, mixing and dilution, concentration detection and compensation correction of mercury vapor, and output of mercury vapor of a set concentration. The mercury vapor generation rate is fast and stable, the generation effect is good, and high-precision mercury vapor can be output. At the same time, the mercury vapor is purified and discharged, and the air pressure can be balanced while preventing the operator from being exposed to the mercury vapor, thereby improving the safety factor and protecting the personal safety of the operator.

[0054] The beneficial technical effects of this embodiment include: being able to accurately output mercury vapor of a set concentration, using the high-range output end of the gas supply mechanism to dilute the pure mercury vapor by adjusting the dilution gas flow rate, thereby facilitating control of the concentration of the output mercury vapor, and simultaneously using a concentration detection mechanism to detect the diluted mercury vapor and transmit the mercury vapor concentration information to the gas supply mechanism, thereby facilitating compensation and correction of the mercury vapor concentration, with high control accuracy and fast adjustment speed.

[0055] The above description is merely a specific embodiment of the present invention, but the scope of protection of the present invention is not limited thereto. Those skilled in the art will understand that the present invention includes, but is not limited to, the contents described in the drawings and the above specific embodiments. Any modifications that do not deviate from the functional and structural principles of the present invention are intended to be included within the scope of the claims.

Claims

1. A new type of high-precision mercury generator, characterized by: The invention comprises an air supply mechanism (1) for controlling the introduction of dilution gas, a mercury permeation mechanism (2) for generating pure mercury vapor, a mercury vapor output mechanism (3) for diluting pure mercury vapor to output mercury vapor of a set concentration, and a concentration detection mechanism (4) for detecting and transmitting mercury vapor concentration information to adjust the mercury vapor concentration. The air supply mechanism (1) is provided with a low-range output end (11) and a high-range output end (12) for adjusting the mercury vapor concentration by flow regulation. The low-range output end (11) of the air supply mechanism (1) is connected to the input end of the mercury permeation mechanism (2). The input end of the mercury vapor output mechanism (3) is connected to the high-range output end (12) of the air supply mechanism (1) and the output end of the mercury permeation mechanism (2) through an air path component. The output end of the mercury vapor output mechanism (3) is respectively connected to the input end of a corresponding analysis device and the concentration detection mechanism (4). The signal output end of the concentration detection mechanism (4) is connected to the signal input end of the air supply mechanism (1).

2. A novel high-precision mercury generating device according to claim 1, characterized in that: The concentration detection mechanism (4) comprises a gas power device (41), a detection gas chamber (42), a light source assembly (43), a detection assembly (44) and a photometer control module (45); the mercury vapor output mechanism (3) is provided with a detection output end for outputting a portion of mercury vapor for detection by the concentration detection mechanism (4) to achieve concentration adjustment of the mercury vapor; the air inlet end of the detection gas chamber (42) is connected to the detection output end of the mercury vapor output mechanism (3); the air outlet end of the detection gas chamber (42) is connected to a corresponding gas collection device through the gas power device (41); a chamber for mercury vapor to pass through is provided in the detection gas chamber (42); the light source assembly (43) and the detection assembly (44) are arranged at intervals at both ends of the chamber of the detection gas chamber (42); and the light source assembly (43) and the detection assembly (44) are both connected to the photometer control module (45).

3. A novel high-precision mercury generating device according to claim 2, characterized in that: The concentration detection mechanism (4) further comprises a photometer mounting bracket (46), a light source emitting portion (47), a light source receiving portion (48), and a first temperature regulating mechanism (49) for regulating the temperature of the mercury vapor in the concentration detection mechanism (4) to a preset standard temperature. The light source emitting portion (47) and the light source receiving portion (48) are both mounted on the photometer mounting bracket (46). The air inlet end of the detection gas chamber (42) is connected to the detection output end of the mercury vapor output mechanism (3) through the light source emitting portion (47). The air outlet end of the detection gas chamber (42) is connected to the gas power device (41) through the light source receiving portion (48). The light emitting portion of the light source assembly (43) is arranged inside the light source emitting portion (47) and is connected to the chamber of the detection gas chamber (42). The detection portion of the detection assembly (44) is arranged inside the light source receiving portion (48) and is connected to the chamber. The temperature regulating end of the first temperature regulating mechanism (49) is arranged inside the light source emitting portion (47).

4. A novel high-precision mercury generating device according to claim 1, characterized in that: The concentration detection mechanism (4) is also provided with a standard gas inlet end for introducing standard gas for calibration.

5. A novel high-precision mercury generating device according to claim 4, characterized in that: The mercury infiltration mechanism (2) comprises a mercury infiltration furnace (21), a infiltration furnace control module (22), a mercury infiltration tube (23), and a second temperature regulating mechanism (24) for regulating the temperature of the mercury infiltration furnace (21) to a preset standard temperature. A mercury infiltration chamber for installing the mercury infiltration tube (23) is provided inside the mercury infiltration furnace (21). The mercury infiltration tube (23) is arranged in the mercury infiltration chamber of the mercury infiltration furnace (21). The temperature regulating end and the temperature detecting end of the temperature regulating mechanism are both installed on the mercury infiltration furnace (21). The control end of the infiltration furnace control module (22) is connected to the second temperature regulating mechanism (24). The signal input end of the infiltration furnace control module (22) is connected to the signal output end of the concentration detecting mechanism (4). The air inlet end of the mercury infiltration chamber of the mercury infiltration furnace (21) is connected to the low-range output end (11) of the air supply mechanism (1). The air outlet end of the mercury infiltration chamber of the mercury infiltration furnace (21) is connected to the input end of the mercury vapor output mechanism (3).

6. A novel high-precision mercury generating device according to claim 1, characterized in that: A preheating pipe (211) arranged in a zigzag pattern is provided in the mercury permeation furnace (21); a temperature regulating end of a second temperature regulating mechanism (24) is connected to the preheating pipe (211); and an air inlet end of a mercury permeation chamber of the mercury permeation furnace (21) is connected to a low-range output end (11) of the air supply mechanism (1) via the preheating pipe (211).

7. A novel high-precision mercury generating device according to claim 6, characterized in that: The mercury vapor output mechanism (3) is provided with a purification mechanism (31) for balancing the pressure in the system. The purification mechanism (31) is filled with a filler for purifying mercury vapor. Part of the mercury vapor in the mercury vapor output mechanism (3) is purified by the purification mechanism (31) and then output to the outside.

Citation Information

Patent Citations

  • A generator for producing a standard gas of elemental mercury

    CN105300760B