Electronic-grade hydrofluoric acid 200L barrel sampler
By designing a sampling component and utilizing the negative pressure principle, the problem of bubble generation during the sampling process of a 200L barrel of electronic-grade hydrofluoric acid was solved, ensuring sample representativeness, achieving bubble-free sampling, and obtaining high-quality samples.
Patent Information
- Application Number
- CN202422567965.0
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-10-24
- Publication Date
- 2025-09-23
- Estimated Expiration
- 2034-10-24
AI Technical Summary
In the prior art, when sampling electronic-grade hydrofluoric acid using a 200L barrel and a pneumatic pump, direct sampling generates a large amount of bubbles, resulting in a high particle content in the sample and insufficient sample representativeness.
The sampling assembly includes a sampler, a long hose, a short hose, a first-hand valve and a second-hand valve. Sampling is performed through the negative pressure principle to avoid bubble generation and ensure sample representativeness.
Bubble-free sampling is achieved, the sample is highly representative, and can truly reflect the quality of the product in the 200L barrel.
Smart Images

Figure CN223376997U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to a sampler, in particular to a 200L barrel sampler for electronic-grade hydrofluoric acid. Background Art
[0002] Hydrofluoric acid is highly corrosive and toxic, causing deep skin burns. Fluoride ions, upon entering the body, combine with calcium ions, leading to hypocalcemia, tetany, irregular heartbeats, and even cardiac arrest. Currently, sampling of 200L drums of electronic-grade hydrofluoric acid primarily involves using a pneumatic pump to obtain a sample directly from a sampling bottle below the sampling port. This process generates numerous bubbles, resulting in a high particle content and a lack of representativeness. Utility Model Content
[0003] In view of the above situation, in order to overcome the defects of the existing technology, the utility model provides an electronic-grade hydrofluoric acid 200L barrel sampler, which effectively solves the problem that the current sampling method of electronic-grade hydrofluoric acid 200L barrel is mainly to use a pneumatic pump to directly use a sampling bottle to obtain the sample below the sampling port. A large number of bubbles will be generated during the sampling process, resulting in a high particle content in the sample and a lack of representativeness of the sample.
[0004] To achieve the above-mentioned object, the present invention provides the following technical solution: the present invention includes a chemical reagent storage barrel for storing hydrofluoric acid, a liquid extraction port provided on one side of the top of the chemical reagent storage barrel, and an air inlet and outlet provided on the other side of the top of the chemical reagent storage barrel, and also includes a sampling assembly, wherein the sampling assembly is connected to the chemical reagent storage barrel;
[0005] The sampling assembly includes a sampler, an end cover, a long hose, a short hose, a first hand valve and a second hand valve. The top of the sampler is provided with an end cover, a long hose is inserted and welded on the end cover, a short hose is inserted and welded on one side of the long hose, the long hose is installed with a first hand valve, and the short hose is installed with a second hand valve.
[0006] Preferably, the long hose and the short hose are both made of PFA material.
[0007] Preferably, the first hand valve and the second hand valve are PFA needle-type hand valves.
[0008] Preferably, the sampler is made of PFA material and has a cylindrical bottle-shaped structure.
[0009] Preferably, the long hose is located at the bottom of the sampler, and the short hose is located at the top of the sampler.
[0010] Preferably, the chemical reagent storage barrel is a 200L chemical reagent storage barrel.
[0011] Beneficial effect: When the present invention is used, one end of the long hose is inserted below the liquid level of the chemical reagent storage barrel to complete the installation of the device. When sampling, the first hand valve on the long hose is closed and the second hand valve on the short hose is opened. At this time, the sampler is squeezed hard to deform, and the gas in the sampler is discharged through the short hose, so that the sampler is in a negative pressure state. At this time, the second hand valve is closed and the first hand valve is opened, so that the sampler is deformed and reset, thereby sucking the electronic-grade hydrofluoric acid in the chemical reagent storage barrel into the sampler through the long hose, and the sampling operation is completed. The present invention has a novel structure and an ingenious conception, which ensures the rationality of the sampling process of a 200L barrel of electronic-grade hydrofluoric acid; ensures that no bubbles are generated during the sampling process, and the sample is quite representative, so that the extracted sample can truly reflect the quality of the product in the 200L barrel. BRIEF DESCRIPTION OF THE DRAWINGS
[0012] The accompanying drawings are used to provide a further understanding of the present invention and constitute a part of the specification. Together with the embodiments of the present invention, they are used to explain the present invention and do not constitute a limitation of the present invention. In the accompanying drawings:
[0013] Figure 1 It is a schematic diagram of the overall structure of the utility model;
[0014] Numbers in the figure: 1. Chemical reagent storage barrel; 2. Liquid collection port; 3. Inlet and outlet ports; 4. Sampling assembly; 5. Sampler; 6. End cover; 7. Long hose; 8. Short hose; 9. First-hand valve; 10. Second-hand. DETAILED DESCRIPTION
[0015] The following is combined with Figure 1 The specific implementation methods of the present utility model are further described in detail.
[0016] Embodiment 1, by Figure 1 The utility model provides a 200L barrel sampler for electronic-grade hydrofluoric acid, comprising a chemical reagent storage barrel 1 for storing hydrofluoric acid, a liquid extraction port 2 provided on one side of the top of the chemical reagent storage barrel 1, and an air inlet and outlet 3 provided on the other side of the top of the chemical reagent storage barrel 1, and further comprising a sampling assembly 4, a sampler 5, an end cover 6, a long hose 7, a short hose 8, a first hand valve 9, and a second hand valve 10. The sampling assembly 4 is connected to the chemical reagent storage barrel 1;
[0017] The sampling assembly 4 includes a sampler 5, an end cover 6, a long hose 7, a short hose 8, a first hand valve 9 and a second hand valve 10. The top of the sampler 5 is provided with an end cover 6, the long hose 7 is welded through the end cover 6, and the short hose 8 is welded through one side of the long hose 7. The first hand valve 9 is installed on the long hose 7, and the second hand valve 10 is installed on the short hose 8.
[0018] The long hose 7 and the short hose 8 are both made of PFA material, which facilitates the plugging and bending of the long hose 7 .
[0019] The first hand valve 9 and the second hand valve 10 are PFA needle-type hand valves, which are convenient for controlling the long hose 7 and the short hose 8 .
[0020] The sampler 5 is made of PFA material and has a cylindrical bottle-like structure, which facilitates the deformation and recovery of the sampler 5 .
[0021] The long hose 7 is located at the bottom of the sampler 5 , and the short hose 8 is located at the top of the sampler 5 , which is convenient for the long hose 7 to suck liquid and the short hose 8 to exhaust.
[0022] The chemical reagent storage barrel 1 adopts a 200L chemical reagent storage barrel, which is convenient for storing chemical reagents.
[0023] Working principle: When the present invention is used, one end of the long hose 7 is inserted below the liquid level of the chemical reagent storage barrel 1 to complete the installation of the device. When sampling, close the first hand valve 9 on the long hose 7 and open the second hand valve 10 on the short hose 8. At this time, squeeze the sampler 5 hard to deform the sampler 5, and the gas in the sampler 5 is discharged through the short hose 8, so that the sampler 5 is in a negative pressure state. At this time, close the second hand valve 10 and open the first hand valve 9, so that the sampler 5 is deformed and reset, thereby sucking the electronic grade hydrofluoric acid in the chemical reagent storage barrel 1 into the sampler 5 through the long hose 7, and the sampling operation can be completed.
[0024] Beneficial effects: The utility model has a novel structure and ingenious conception, which ensures the rationality of the sampling process of a 200L barrel of electronic-grade hydrofluoric acid; ensures that no bubbles are generated during the sampling process, and the samples are quite representative, so that the extracted samples can truly reflect the quality of the product in the 200L barrel.
[0025] Through the use of wires by those skilled in the art, all electrical components in this case are connected to their corresponding power supplies, and appropriate controllers and encoders should be selected according to actual conditions to meet control requirements. The specific connection and control sequence should refer to the following working principle, in which the electrical components are electrically connected in sequence. The detailed connection means are well-known technologies in this field. The following mainly introduces the working principle and process, and no longer explains the electrical control.
[0026] Finally, it should be noted that the above description is merely a preferred embodiment of the present invention and is not intended to limit the present invention. Although the present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art will be able to modify the technical solutions described in the aforementioned embodiments or replace some of the technical features therein with equivalents. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principles of the present invention shall be included within the scope of protection of the present invention.
Claims
1. A 200L barrel sampler for electronic-grade hydrofluoric acid, comprising a chemical reagent storage barrel (1) for storing hydrofluoric acid, a liquid extraction port (2) provided on one side of the top of the chemical reagent storage barrel (1), and an air inlet and outlet (3) provided on the other side of the top of the chemical reagent storage barrel (1), characterized in that: It also includes a sampling assembly (4), a sampler (5), an end cover (6), a long hose (7), a short hose (8), a first hand valve (9) and a second hand valve (10), and the chemical reagent storage barrel (1) is connected to the sampling assembly (4); The sampling assembly (4) comprises a sampler (5), an end cover (6), a long hose (7), a short hose (8), a first hand valve (9) and a second hand valve (10). The top end of the sampler (5) is provided with an end cover (6), a long hose (7) is welded through the end cover (6), a short hose (8) is welded through one side of the long hose (7), the first hand valve (9) is installed on the long hose (7), and the second hand valve (10) is installed on the short hose (8).
2. The electronic-grade hydrofluoric acid 200L barrel sampler according to claim 1, characterized in that: The long hose (7) and the short hose (8) are both made of PFA material.
3. The electronic-grade hydrofluoric acid 200L barrel sampler according to claim 1, characterized in that: The first hand valve (9) and the second hand valve (10) are PFA needle-type hand valves.
4. The electronic-grade hydrofluoric acid 200L barrel sampler according to claim 1, characterized in that: The sampler (5) is made of PFA material and has a cylindrical bottle-shaped structure.
5. The electronic grade hydrofluoric acid 200L barrel sampler according to claim 1, characterized in that: The long hose (7) is located at the bottom of the sampler (5), and the short hose (8) is located at the top of the sampler (5).
6. The electronic-grade hydrofluoric acid 200L barrel sampler according to claim 1, characterized in that: The chemical reagent storage barrel (1) is a 200L chemical reagent storage barrel.