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1918 results about "Fluorhydric Acid" patented technology

Hydrofluoric Acid: HF. Also known as: hydrogen fluoride, hydrofluoride, hydrogen monofluoride, fluorhydric acid. Although it is highly corrosive, hydrofluoric acid is considered a weak acid because it doesn't usually dissociate completely. The acid will eat glass and metals, so HF is stored in plastic containers.

Electrothermal film and manufacturing method thereof

The invention relates to an electrothermal film and a manufacturing method thereof, belonging to the technical field of semiconductor heating. The electrothermal film is mainly prepared by adopting stannic chloride, titanium tetrachloride, stannic chloride, titanium trichloride, ferric chloride, antimony trichloride, calcium chloride, potassium chloride, cadmium chloride, stannic dioxide, stannictetroxide, hydrofluoric acid, boric acid, ethanol, isopropyl alcohol and inorganic water. By adopting the above formula, the mixture is mixed, stirred and heated to prepare into electrothermal film treating fluid, a semi-finished product of the electrothermal film is obtained by spraying the electrothermal film treating fluid at negative pressure on the electrothermal film carrier, and then silveroxide slurry is coated on the semi-finished product of the electrothermal film for baking to form a finished product of the electrothermal film. The electrothermal film has reasonable proportion andsimple manufacturing process, can be manufactured into various electrothermal film heating devices, has a working temperature capable of being up to 500 DEG C, and has wider application range. The electrothermal film of the invention also has the function of far infrared radiation, can play a role of physical therapy and health care to human body, and can help improve the quality and output of agricultural products.
Owner:GUANGDONG HALLSMART INTELLIGENCE TECH CORP LTD

Method for producing fluorine series compounds and white carbon black

The invention relates to a method utilizing waste gas containing fluoride in fertilizer production or fluorine-containing gas or sodium fluorosilicate in fluorine chemical production as raw materials to product series compounds of fluorine and white carbon black. The ammonium fluoride and/or ammonia are/is introduced into an absorption system to get a (NH4) 2SiF6 solution with the absorbing solution concentration of 25 to 37 percent or the ammonium fluoride and the sodium fluorosilicate react to get a reaction product of sodium fluoride crystallization, fluosilicic acid solution and septenary-fluorine compound NH4F.(NH4)2SiF6 crystallization. The absorption liquid or the reaction product is aminated to get precipitated silica (white carbon black) with the specific surface of 100-180m<2>/g, and the latter can get a sodium fluoride product and an NH4F solution with the concentration of 30 to 45 percent. The solution used as a starting point can nearly prepare all inorganic fluoride chemical products, and ammonium fluoride, sodium fluoride, potassium fluoride, ammonium bifluoride, cryolite, aluminum fluoride, sodium hydrogen diffluoride and hydrofluoric acid production, etc. are main. The method has simplicity, effectiveness and higher economic benefit, and simultaneously, fluorine and silicon in the waste gas containing fluoride of phosphate fertilizer for the pollution of environment can be basically eliminated, and basically no waste water, waste gas and waste residue are discharged.
Owner:夏克立

Preparation method and application of iron-nitrogen co-doped porous carbon sphere material

The invention discloses a preparation method for an iron-nitrogen co-doped porous carbon sphere material. The preparation method comprises the following steps: by taking 2-aminopyridine as a monomer and taking ammonium persulfate and ferric chloride as oxidants, performing in-situ polymerization reaction in a duct of a porous silicon dioxide template to obtain a precursor; performing high-temperature carbonization treatment on the precursor in a tubular furnace and an inert gas nitrogen-gas environment; and removing the silicon dioxide template by hydrofluoric acid to obtain the iron-nitrogen co-doped porous carbon sphere material which is taken as an electric catalyst to achieve good catalytic effect in oxygen gas reduction reaction. The preparation method has the advantages that the process is simple and easy to perform and the raw materials are cheap. The prepared carbon material contains a three-dimensional communicated pore structure, has a high specific surface area and a large pore volume, can effectively improve the electric catalytic activity through the heteroatom nitrogen-iron doping, has relatively high electric catalytic efficiency while being applied as a low-price electric catalyst, and has an important value and significance in the fields of doped type porous carbon material preparation and proton membrane fuel battery electric catalysis.
Owner:NANKAI UNIV

Fluoropolymer organic lining anticorrosive material for chimney, flue and other pipelines and containers and construction method thereof

The invention provides an anticorrosive material for a chimney, a flue and other containers and pipelines and an anticorrosive construction process. The construction method of the anticorrosive material comprises the following steps: using crude rubber with higher fluorine content as a raw material, then adding curing agent, stabilizer, special stuffing and other components, and mixing to form precuring gross rubber; dissolving the rubber by using low-molecular weight esters and ketones as the solvent to form a putty type rubber paste; and finally, adding special additives, uniformly mixing, coating to the inner walls of a chimney, a flue and a chemical container, and curing into the polymerized fluororubber organic lining under the room-temperature condition. The material can be independently used as the anticorrosive material, and can also be used for protecting common foam glass bricks (ceramic bricks) and adhesive for anticorrosive purpose in the domestic chimney (flue) at present. The invention well solves the technical problems of fluororubber room-temperature curing and difficult anticorrosive construction, can be used in a high-temperature environment of more than 230 DEG C, and can endure high-concentration sulfuric acid, nitric acid, hydrochloric acid, phosphoric acid, hydrofluoric acid, corresponding salts and a mixture thereof. The anticorrosive lining material is economically affordable, has extremely high comprehensive anticorrosive properties such as temperature resistance, acid resistance and the like, and is applicable to the anticorrosive treatment of a cured chimney.
Owner:重庆大众防腐股份有限公司

Titanium dioxide nano tube electrode and its preparation process and application

The invention relates to a titanium dioxide nanometer tube electrode in the technology field of fathering the environmental pollution and its preparation method as well as its application. Its features lie in: choose the pure titanium or titanium alloy as the substrate, carry out the electrochemical oxidation in the condition of hydrofluoric acid with its density between 0.01wt% and 0.5wt%, form a titanium dioxide nanometer tube with its diameter between 40nm and 100nm and its length between 20nm and 50nm on the substrate vertically and get the integrative titanium dioxide nanometer tube electrode. The preparation features lie in: choose the substrate as the anode after grinding, etching and drying and the platinum sheet as the cathode, control the distance between the two electrodes between 10mm and 50mm, put them into the reactor, power on the stabilized voltage power supply with it voltage between 15V and 25V, after 1-to-30-minute reaction calcine them at the temperature of 400deg.C to 600deg.C for 40nin to 80min, cool it in natural condition and get the titanium dioxide nanometer tube electrode. The titanium dioxide nanometer tube electrode can be applied to the photocatalysed degradation and photoelectroncatalysed degradation to the organic pollutants. It has larger surface area and simple preparation method.
Owner:DALIAN UNIV OF TECH

Preparation of silicon nanowire array

The invention relates to a method for preparing silicon nanowires, belonging to the nanophase material preparation technical field. The method comprises the following steps that: a silicon chip is washed and shaken by acetone and alcohol and is processed by an acid cleaning liquid and a No.1 standard cleaning solution; a silicon dioxide spheres solution with a weight percentage density between 0.02 and 2.0 percent is added on the silicon chip surface which is washed off in the step one drop by drop by a micro pipette, the processed silicon chip is placed in air to air naturally; the silicon chip with silicon dioxide sphere arrays is annealed for one to three hours at a temperature of between 900 and 1000 DEG C; afterwards, the silicon chip is put into a diluent hydrofluoric acid solution to be eroded for 2 to 20 minutes so that the diameters of the spheres become small; an Ag film with a thickness between 20 and 80nm is deposited on the silicon chip surface by the plating technique or the vacuum evaporating technique; and a sample deposited with the Ag film is dipped into the hydrofluoric acid and hydrogen peroxide etching solution (or ferric nitrate) to be eroded for 4 to 100 minutes. The preparation method can rapidly prepare a large area of silicon nanowire arrays, thereby being suitable for the large-scale industrial production.
Owner:BEIJING NORMAL UNIVERSITY

Branch controllable titanium dioxide nanotube array thin film and preparation method thereof

The invention discloses a branch controllable titanium dioxide nanotube array thin film and a preparation method thereof. The thin film consists of an array of a titanium dioxide nanotube formed by connecting a main tube and a branch tube in series; the thickness of the thin film is 1-100mum, and the porosity factor is 40-60 percent. The preparation method comprises the following steps: preparinga main tube electrolyte according to the proportion that the mole ratio of ammonium fluoride to glycol to water is 0.05-0.15:17.7:0.015-0.025, and preparing a branch tube electrolyte according to theproportion that the mole ratio of hydrofluoric acid to glycol is 0.15-0.25:17.7; then firstly, putting one surface of a titanium sheet in the main tube electrolyte to serve as the anode; carrying outanode oxidization under the conditions that the DC voltage is 55-65V and the temperature is 0-35 DEG C for 0.5-6h; then using the glycol to clean the anode; subsequently, putting the surface which isanodized in the branch tube electrolyte to serve as the anode, and carrying out anode oxidization under the conditions that the DC voltage is 30-120V and the temperature is 0-35 DEG C for more than 30min, thereby preparing the thin film. The thin film can be widely used for fields of dye-sensitized solar cells, gas sensors, photolytic water hydrogen production and photonic crystal.
Owner:HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI

Preparation and application of nitrogen, sulphur or chlorine-doped three-dimensional porous graphene catalyst

The invention provides a preparation and an application of a nitrogen, sulphur or chlorine-doped three-dimensional porous graphene catalyst. The preparation comprises the following steps: dissolving graphene oxide, an alkyl compound, a transition metal salt containing nitrogen, sulphur or chlorine and hydrochloric acid into a solvent, and carrying out ultrasonic treatment and drying to obtain a precursor; heating the precursor to 600-1,000 DEG C under inert gas protection and carrying out roasting reduction treatment for 1-3 hours to obtain primary carbide; carrying out pickling treatment on the obtained primary carbide with a mixed solution of hydrofluoric acid and hydrochloric acid at a room temperature for 12-24 hours, centrifuging the primary carbide, cleaning the primary carbide with deionized water and then drying the primary carbide to obtain the three-dimensional porous graphene material containing nitrogen, sulphur or chlorine; and heating the three-dimensional porous graphene material to 600-1,000 DEG C under inert gas protection, and carrying out roasting reduction treatment for 1-3 hours to obtain the nitrogen, sulphur or chlorine-doped three-dimensional porous graphene catalyst. The nitrogen, sulphur or chlorine-doped three-dimensional porous graphene catalyst has the characteristics of being high in stability, not easy to poison and the like, and has a good application prospect in the fields of wastewater treatment of a fuel cell, a metal-air cell, a super capacitor, an energy storage battery and a microbial fuel cell and the like.
Owner:DONGHUA UNIV

Method for preparing high-adhesion micro-nano array structure film through wet etching and reverse transfer printing

The invention discloses a method for preparing a high-adhesion micro-nano array structure film through wet etching and reverse transfer printing. The method comprises the following steps: with a silver nitrate/hydrofluoric acid solution as a silver deposition solution, depositing a layer of porous silver film on a silicon chip so as to obtain an etching catalytic metal and etching a desired micro-nano array structure in a hydrofluoric acid/hydrogen peroxide solution or potassium hydroxide/isopropanol solution; carrying out soaking with concentrated nitric acid so as to remove the silver film, carrying out air drying and using the treated silicon chip as a template silicon chip; uniformly coating the template silicon chip with organic matter colloid and standing the template silicon chip for a period of time; and placing the template silicon chip on a heating plate after precipitation and uniform distribution of bubbles, heating the template silicon chip at a certain temperature for a period of time, stripping off a colloid film when the colloid completely solidifies and printing a reversed structure of the prepared micro-nano array structure on the colloid film through transfer printing so as to realize preparation of the high-adhesion micro-nano array structure film. The method is simple to operate, has low cost, is not restricted by a preparation area and can be extensively applied to the field of bionic adhesion.
Owner:HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI

Method for simultaneously determining contents of various elements in soil or deposits

The invention relates to detection technology for element contents, and provides a method for simultaneously determining contents of arsenic, cadmium, lead, vanadium, zinc, manganese and phosphor in soil or deposits. The method mainly comprises the following steps: (1) 0.1g of a grinded drying soil sample is accurately weighed and placed in a TFM microwave digestion pot, a certain proportion of aqua regia and hydrofluoric acid are added, and a solution is allowed to stand; (2) an appropriate microwave digestion program is set, and microwave digestion is carried out for the solution in the step (1); (3) after the microwave digestion program ends, an acid-driving device is used for heating and evaporating the digestion solution in the step (2) to a dry state, and total transfer, volumetric flask preparation, and filtering are carried out; (4) ICP-OES is used for determining contents of arsenic, cadmium, lead, vanadium, zinc, manganese and phosphor in the clear liquor in the step (3); (5) ICP-MS is used for determining contents of elements in the clear liquor in the step (3) which do not reach detection limits in the step (4) once more. The method has the advantages of simple steps, simplified operation, saved soil samples, reduced personal error, minimized environment interference, and improved working environments.
Owner:RES CENT FOR ECO ENVIRONMENTAL SCI THE CHINESE ACAD OF SCI

Method for analyzing and detecting free carbon in chromium carbide

ActiveCN101329242ASolve the intractableTechnical Difficulty Ensuring InsolubilityWeighing by removing componentPreparing sample for investigationFiltrationHigh pressure
The invention provides an analysis detection method for free carbons in chromium carbide, comprising the steps as follows: a chromium carbide sample is arranged in a polytetrafluoroethylene crucible; after the crucible wall is washed by deionized water, hydrofluoric acid and nitric acid are sequentially added into the crucible and mixed uniformly; the crucible containing the hydrofluoric acid and the nitric acid are arranged inside a high-pressure kettle and subsequently heated in a graphite oven; samples are decomposed according to the given melting temperature, time and high pressure. After the decomposing and cooling, the chromium carbide sample solution and free carbons are transferred and washed cleanly to be arranged in a platinum extraction-filtration crucible which is padded by acid cleaning asbestoses; after the filtration and dryly pumping, the acid-cleaning asbestos pad and the free carbons are completely transferred into a porcelain boat; subsequently, the porcelain boat is arranged in baking box for drying; the dried porcelain boat is tested on a carbon content tester and the analysis result of the free carbon is calculated. The method of the invention adopts a mixed acid high-pressure decomposition method to solve the difficult problem that the chromium carbide is difficult to decompose, ensures that the free carbons are not dissolved, and has the testing range of 0.050 to 1.00 percent, good accuracy and precision.
Owner:ZHUZHOU HARD ALLOY GRP CO LTD
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