The application discloses a method for recovering
propylene glycol methyl
ether and
propylene glycol methyl
ether acetate from waste
diluent, belongs to the field of
diluent recovery, and aims at the technical problems that the
recovery purity,
recovery rate and long-period operation stability of PM and PGMEA in waste
diluent need to be further improved, and specifically comprises the following steps: after pretreatment, the waste diluent is transported to a fixed complex separation
bed filled with non-
halogen hydrogen bond
acceptor complex materials, so that
propylene glycol methyl
ether and water are complexed with the non-
halogen hydrogen bond
acceptor complex materials and are retained, the non-
halogen hydrogen bond
acceptor complex materials are constructed,
propylene glycol methyl ether acetate is preferentially flowed out, and three-stage vacuum
pyrolysis complexing is performed to realize segmented release and material regeneration, so that the high-purity recovery of
propylene glycol methyl ether or
propylene glycol methyl ether acetate is ensured, and the high recovery rate and long-period operation stability are maintained.