The invention discloses a
polyimide-
zinc organic framework loaded
graphene oxide hybrid membrane. A preparation process comprises the following steps: preparing
graphene oxide by adopting a Hummer method, preparing dispersing liquid with a
mass ratio of
methanol to water of (1 to 4) to 1, and performing
ultrasonic dispersion; adding the
graphene oxide and the dispersing liquid into a
mixed solution of
zinc nitrate hexahydrate and 2-methylimidazole, and performing a stirring reaction at
room temperature, thus preparing a
zinc organic framework loaded graphene oxide compound
nanosheet; and blending the zinc organic framework loaded graphene oxide compound
nanosheet and a
polyimide solution to prepare a membrane
casting solution, and preparing the
hybrid membrane through a
tape casting method. The
polyimide-zinc organic framework loaded graphene oxide
hybrid membrane disclosed by the invention has the advantages that the raw materials of the hybrid membrane are easy to obtain, and the preparation process is simple and controllable; and the prepared compound membrane is used for
gas separation, and has excellent separation performance. Particularly, under a humidification condition, the permeability of CO2 pure gas is 238
barrer, and the CO2 / N2 selectivity is 65.