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2417 results about "Sodium fluoride" patented technology

This medication is used to prevent cavities. It makes teeth stronger and more resistant to decay caused by acid and bacteria.

Method for recovering polysilicon ingots, carborundum powder and polyethylene glycol from cutting waste mortar

The invention discloses a method for recovering polysilicon ingots, carborundum powder and polyethylene glycol from cutting waste mortar. The recovering method comprises the following steps shown as an attached diagram, wherein the high temperature purification comprises the following steps of: mixing the prepared silicon micro powder with a fluxing agent according to the weight ratio of 1: 0.5-5 into lumps, carrying out high temperature treatment in a high temperature vacuum furnace with the treatment temperature range of 1450-1800 DEG C and the treatment time range of 1-10h; and then carrying out directional solidification on melting-state high purity silicon subjected to the high temperature treatment to obtain the polysilicon ingots; wherein the fluxing agent is selected from one or any mixture of silica, alumina, calcium oxide, magnesium oxide, potassium oxide, sodium oxide, calcium fluoride, magnesium fluoride, sodium fluoride, sodium chloride, potassium chloride and calcium chloride. The invention has the advantages that: the yields of carborundum and polyethylene glycol are high and can reach more than 70-80 percent; and the recovered polysilicon ingots reach the purity of 6-7N and completely satisfy of the requirement for preparing silicon slices of silicon solar cell.
Owner:唐康宁

Method for preparing fluorescent nano material converted on NaYF4

The invention relates to a method for preparing fluorescent nano material converted on NaYF4, comprising the steps: yttrium nitrate, ytterbium nitrate and erbium nitrate or yttrium chloride, ytterbium chloride, erbium chloride and thulium chloride are dissolved in de-ionized water according to the mixture radio that the mol ratio of rare earth ions which are yttrium ion, ytterbium ion and erbium ion is equal to (70-95): (1-25): (0.5-10), so that the mixed solution is prepared; water soluble polymer having the ligand radical with the rare earth ions is added into the mixed solution for stirring reaction to form complex compound; the pH value of the mixed solution is adjusted to be 2-6; sodium fluoride, ammonium fluoride or hydrofluoric acid can be added into the mixed solution and stirred until colloid solution that is approximately transparent is obtained; then, the colloid solution is put into a high pressure closed reactor and heated at the temperature of 140-200 DEG C; after that the obtained product is cooled to be the room temperature, centrifugated, separated, washed and dried, finally, the fluorescent nano material converted on NaYF4 is obtained. The method can be used for preparing the converted material at lower temperature, the particle size and the appearance can be controlled, and the water-solubility is good.
Owner:CHANGCHUN INST OF OPTICS FINE MECHANICS & PHYSICS CHINESE ACAD OF SCI

Method for recovering valuable metal from electroplating sludge

The invention relates to a method for recovering valuable metals from electroplating sludge. Electroplating sludge is used as a raw material; advanced theories and scientific means of leaching principle, redox principle, extraction principle, iron filing displacement principle and evaporation crystallization principle in a wet method metallurgy are integrally utilized; and a technology of ''acid decomposition of electroplating sludge-leachate purification to remove ferrochrome-P204 impurity removal-P507 enrichment-condensation crystallization'' is employed. Meanwhile, calcium and magnesium are removed by an extraction method, which substitutes a traditional sodium fluoride method for removing calcium and magnesium. A recovery rate of nickel reaches 95%, and copper content of recovered copper sponge is larger than 80%. Besides, acid dissolved slag and purifying slag can be solidified to reach requirements of environmental protection and will not cause secondary pollution; waste water can be recycled and has a strong technological versatility. The method is suitable for treating various routine electroplating sludge, has easily controllable technical conditions and low operating cost and is easy for realizing large scale production; therefore, the method is a practical novel technology for treating electroplating sludge in a way of quantitative reduction, harmlessness and resource.
Owner:朱小红

Method for preparing environment-friendly micro-arc oxidation black ceramic film on aluminum alloy surface

The invention discloses a method for preparing an environment-friendly micro-arc oxidation black ceramic film on an aluminum alloy surface, and the method comprises the following steps: firstly, pouring deionized water into an oxidation tank, weighing 1-10g / L of sodium hexametaphosphate, 1-3g / L of sodium silicate, 0.5-2g / L of potassium hydroxide, 0.2-2g / L of sodium fluoride and 0.5-20g / L of ferric ammonium oxalate in terms of the volume of the added deionized water, and uniformly stirring and mixing the sodium hexametaphosphate, the sodium silicate, the potassium hydroxide and the sodium fluoride to obtain a micro-arc oxidation base electrolyte; adding the weighed ferric ammonium oxalate into the base electrolyte, and stirring and mixing uniformly to obtain an aluminum alloy micro-arc oxidant solution; and then, sequentially carrying out surface deoiling and cleaning, water washing, aluminum alloy micro-arc oxidation, sealing and drying on the aluminum alloy to prepare the environment-friendly micro-arc oxidation black ceramic film on the aluminum alloy surface. By means of the preparation method disclosed by the invention, the problems of single color, limited application range, and environment pollution caused by a vanadate electrolyte, of the existing aluminum alloy ceramic film layer, are solved.
Owner:CSIC NO 12 RES INST

Treating fluid and method for preparing vanadium-zirconium composite conversion coatings with self-repairing performance on aluminum alloy surfaces through same

The invention belongs to the technical field of chemical materials, and relates to a treating fluid and a method for preparing vanadium-zirconium composite conversion coatings with self-repairing performance on aluminum alloy surfaces through the same. The method includes the steps of firstly preparing the treating fluid containing fluorozirconate, metavanadate, sodium fluoride, nitrate, an accelerate and an additive; then putting an aluminum alloy after surface pretreatment into a working fluid made of the diluted treating fluid for 2min-10min; and finally subjecting the aluminum alloy to washing, drying and cooling to obtain the vanadium-zirconium composite conversion coatings. The preparation process is simple, heavy metals such as hexavalent chromium and nickel are not contained, the environment is friendly, the conversion coatings of the aluminum alloy after a conversion coating treatment are dense and high in binding force, metal ions in the conversion coatings can bond with base metal under a corrosion environment and provided with a certain self-repairing performance, and the treating technology of vanadium-zirconium conversion coatings can effectively replace chromate treatment on aluminum alloy surfaces.
Owner:湖南松井先进表面处理与功能涂层研究院有限公司

460MPa-level flux-cored wire for ocean engineering and application thereof

The invention provides a 460MPa-level flux-cored wire for ocean engineering. The 460MPa-level flux-cored wire comprises a carbon steel sheath and a flux core, wherein the carbon steel sheath accounts for 84-87% of the total mass of the flux core; the flux core accounts for 13-16% of the total mass of the flux-cored wire; the flux-cored wire consists of the following components in percentage by mass: 30-42% of rutile, 1-2% of sodium fluoride, 3-6% of feldspar, 3-5% of ferrotitanium, 1-3% of silicon iron, 0.5-1% of rear earth, 3-5% of magnesium powder, 5-10% of electrolytic manganese, 1-2% of aluminum powder, 7-9% of nickel powder, 4-7% of ferroboron, 0.2-0.5% of graphite, 3-6% of silicon-manganese alloy, 0.5-1% of zircon sand and the balance of Fe and inevitable impurities. By virtue of control in aspects of chemical components, diffusible hydrogen, low-temperature stability and the like, the 460MPa-level flux-cored wire meets the requirements of crack resistance and low-temperature impact resistance, is good in all-position welding process, attractive in welding seam and excellent in mechanical property, has seawater corrosion resistance; and content of diffusible hydrogen of deposited metal reaches ultralow hydrogen level.
Owner:WUHAN TEMO WELDING CONSUMABLES CO LTD

Rare-earth modified Ti-Zr chemical passivation solution for surface treatment of aluminium profiles and using method of rare-earth modified Ti-Zr chemical passivation solution

The invention discloses a rare-earth modified Ti-Zr chemical passivation solution for surface treatment of aluminium profiles and a using method of the rare-earth modified Ti-Zr chemical passivation solution. The rare-earth modified Ti-Zr chemical passivation solution is characterized in that the passivation solution is a main salt for auxiliary film-formation, which takes rare-earth compounds as a Ti-Zr passivation treatment solution, and a passivation film is light yellow in appearance and has field judgement property on the quality of a formed film. A formula of the rare-earth modified Ti-Zr chemical passivation solution is as follows: each litre of solution contains 0.5g.L<-1>-10g.L<-1> of potassium fluotitanate (hexafluorotitanic acid), 0.5g.L<-1>-10g.L<-1> of potassium fluozirconate (fluozirconic acid), 0.5g.L<-1>-5g.L<-1> of cerium nitrate (ceric sulfate and ammonium ceric nitrate), 2g.L<-1>-10g.L<-1> of potassium nitrate, 0.5g.L<-1>-3g.L<-1> of sodium fluoride (potassium fluoride), 0.5g.L<-1>-1g.L<-1> of sodium dodecyl benzene sulfonate or OP-10, 0.2mL-5mL.L<-1> of nitric acid and 1g.L<-1>-5g.L<-1> of boric acid. The using method of the rare-earth modified Ti-Zr chemical passivation solution comprises the following steps of: (1) clearing dirt, such as dirt attached to an aluminium alloy; (2) pretreating the surface of the aluminium alloy; (3) carrying out passivating treatment on the surface of the aluminium alloy by using the rare-earth modified Ti-Zr chemical passivation solution; and (4) washing the aluminium alloy by using water and drying the aluminium alloy. The rare-earth modified Ti-Zr chemical passivation solution disclosed by the invention has the advantages of light yellow appearance, high film formation speed, simple process, uniformity in film layer, strong corrosion resistance, low environment pollution and the like.
Owner:GUANGDONG XINGFA ALUMINUM

Slag-free flux-cored wire

The invention provides a novel process for a formula of a slag-free flux-cored wire, and relates to a welding material. The manufacturing method adds the combination of molybdenum powder, nickel powder and rare earth silicon to a formula of raw materials, eliminates mineral powder in a common formula, and optimizes the proportion of various types of metal powder in the formula. According to the formula, the welding material comprises the following components: 4 to 8 parts of micro carbon ferrochromium, 12 to 18 parts of low carbon ferromanganese, 56 to 67 parts of iron powder, 2 to 6 parts of molybdenum powder, 0.1 to 0.4 part of ferroboron, 2 to 5 parts of rare earth silicon, 1 to 3 parts of ferrosilicon, 2 to 3 parts of ferrotitanium, 2 to 3 parts of sodium fluoride, 3 to 7 parts of ferroaluminum, 1 to 3 parts of aluminum to magnesium powder and 4 to 8 parts of nickel powder. The invention improves the toughness, strength and anti-fatigue performance of welding seams and thins welding-seam grains by adding the combination of molybdenum powder, nickel powder and rare earth silicon into the raw materials of the formula, eliminating the mineral powder in the common formula, and optimizing the proportion of various types of metal powder in the formula. Meanwhile, slagging on the surfaces of the welding seams is avoided, and welding efficiency is raised by 20 percent compared with slag-type processes.
Owner:山东聚力焊接材料有限公司

Preparation method of vanadium sodium fluophosphate cathode material of hybrid ion battery

The invention provides a preparation method of a vanadium sodium fluophosphate cathode material of a hybrid ion battery. The method comprises the following steps: 1) grinding of a mixed material: taking trivalent or pentavalent vanadium oxide (V), ammonium dihydrogen phosphate (P), sodium fluoride (F) and a reducing agent carbon source (C) as raw materials, wherein the molar ratio of V to P to F is 2:(1.9-2.3):3, the molar ratio of V to C in the reducing agent carbon source is 1:(1-2), then weighing carbon source accounting for 3-5% of the total weight of the raw materials to serve as a conductive agent, and carrying out mixed grinding to obtain a precursor mixture; 2) precalcination: precalcinating the precursor mixture for 6-10 hours at the temperature of 300-400 DEG C at the warming speed of 3-5 DEG C per minute under the protection of inert gas, cooling the mixture to room temperature and taking out the mixture for secondary grinding; and 3) secondary calcination: carrying out the secondary calcination on the mixture ground in the step 2) for 6-10 hours at the temperature of 550-750 DEG C at the warming speed of 3-5 DEG C per minute under the protection of the inert gas, and naturally cooling to room temperature to obtain the vanadium sodium fluophosphate cathode material. The vanadium sodium fluophosphate cathode material has good electrochemical performance which is obviously improved.
Owner:CENT SOUTH UNIV
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