Temperature control reaction furnace for producing mercaptopropyltriethoxysilane

By introducing a cleaning scraper and stirring device into the temperature-controlled reactor, the problem of cumbersome cleaning of existing equipment has been solved, achieving efficient cleaning and temperature control, and improving production efficiency and energy saving.

CN223505270UActive Publication Date: 2025-11-04HUBEI KANGHEYUAN NEW MATERIALS CO LTD
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Patent Information

Application Number
CN202422997266.X
Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2024-12-05
Publication Date
2025-11-04
Estimated Expiration
2034-12-05

AI Technical Summary

Technical Problem

Existing mercaptopropyltriethoxysilane production facilities require disassembly or machine cleaning during the cleaning process, which is cumbersome and energy-intensive.

Method used

A temperature-controlled reactor was designed, equipped with a cleaning scraper and a stirring device. The cleaning scraper slides along the inner wall to remove residual raw materials, reducing the tedious steps of disassembly and machine cleaning, and saving energy.

Benefits of technology

It improves the ease of use and efficiency of the device, reduces energy consumption during the cleaning process, and allows for easy control of the reaction temperature, thus minimizing the impact on the raw materials.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model provides a temperature control reaction furnace for producing mercaptopropyltriethoxysilane, which comprises a device base body, a heating device is mounted and connected on the inner wall of the side end of a water inlet pipeline, a stirring rod is mounted and connected on the inner wall of the side end of a driving rod, a rotating rod is mounted and connected on the inner wall of the top of the middle of a mounting plate, and the rotating rod is mounted and connected on the inner wall of the top of the middle of the mounting plate. A cleaning scraping plate is slidably connected to the inner wall of the side end of the sliding groove, a fixing rod is mounted and connected to the inner wall of the top of the cleaning scraping plate, a rotary mounting frame is mounted and connected to the inner walls of the side ends of the fixing rod and the rotary rod, and a sealing cover plate is mounted and connected to the inner wall of the top of the mounting plate. According to the temperature control reaction furnace for producing mercaptopropyltriethoxysilane, the cleaning scrapers are arranged at the two ends of the temperature control reaction furnace, a structural workpiece can be directly subjected to sliding cleaning treatment along the inner wall of the temperature control reaction furnace, the tedious work in the using and cleaning process is reduced, the working efficiency of the temperature control reaction furnace is improved, and meanwhile in the cleaning process, the temperature control reaction furnace is convenient to clean. And the energy loss can be reduced.
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Description

Technical Field

[0001] This utility model relates to the field of chemical equipment technology, and in particular to a temperature-controlled reaction furnace for the production of mercaptopropyltriethoxysilane. Background Technology

[0002] Mercaptopropyltriethoxysilane is an important organosilicon compound with wide applications in rubber, plastics, coatings and other fields. It plays an important role in the production of this product, providing precise temperature control and improving production efficiency and product quality.

[0003] After use, existing equipment usually requires cleaning to reduce the adverse effects of residual materials. However, the cleaning process usually involves workers disassembling the equipment or using machinery, which is quite cumbersome.

[0004] Therefore, it is necessary to provide a temperature-controlled reactor for the production of mercaptopropyltriethoxysilane to solve the above-mentioned technical problems. Utility Model Content

[0005] This invention provides a temperature-controlled reactor for the production of mercaptopropyltriethoxysilane, which solves the problem that existing equipment requires manual disassembly or mechanical cleaning, making it cumbersome to use.

[0006] To solve the above-mentioned technical problems, this utility model provides a temperature-controlled reactor for the production of mercaptopropyltriethoxysilane, comprising: a device base; an inlet pipe installed and connected to the inner wall of the top left end of the device base; an outlet pipe installed and connected to the inner wall of the bottom right end of the device base; a water inlet pipe installed and connected to the inner wall of ... A stirring rod is installed on the inner wall. A mounting plate is installed on the top inner wall of the device base. Sliding grooves are fixedly connected to the inner walls at both ends of the mounting plate. A rotating rod is installed on the top inner wall of the middle of the mounting plate. A rotating disk is installed on the top inner wall of the rotating rod. A rotating handle is installed on the top inner wall of the rotating disk. A cleaning scraper is slidably connected to the inner wall of the side end of the sliding groove. A fixing rod is installed on the top inner wall of the cleaning scraper. A rotating mounting frame is installed on the inner wall of the side end of the fixing rod and the rotating rod. A rotating connecting rod is installed between the inner walls of the side end of the rotating mounting frame. A sealing cover is installed on the top inner wall of the mounting plate.

[0007] Preferably, a control base is installed and connected to the inner wall of the side end of the liquid inlet pipe and the liquid outlet pipe, and a control valve is installed and connected to the inner wall of the top of the control base.

[0008] Preferably, a fixed base is installed and connected to the inner wall of the bottom of the device base, a load-bearing base plate is installed and connected to the inner wall of the bottom of the fixed base, and limit plates are installed and connected to the inner walls at both ends of the fixed base.

[0009] Preferably, a fixed side plate is installed and connected to the inner wall of the base of the device, and a controller is installed and connected to the inner wall of the fixed side plate.

[0010] Preferably, a fastening base plate is installed and connected to the inner wall of the side end of the mounting plate, a fastening rod is installed and connected to the inner wall of the top of the fastening base plate, and a fastening plate is installed and connected to the inner wall of the side end of the sealing cover.

[0011] Preferably, a fixed handle is installed on the inner wall of both ends of the sealing cover, and a motor support is installed on the inner wall of the side end of the drive motor.

[0012] Compared with related technologies, the temperature-controlled reactor for the production of mercaptopropyltriethoxysilane provided by this utility model has the following beneficial effects:

[0013] This invention provides a temperature-controlled reactor for the production of mercaptopropyltriethoxysilane. During the reaction process, after the reaction is complete, the residual material on the inner wall of the reactor needs to be cleaned. To improve ease of use, cleaning scrapers at both ends of the reactor allow for direct sliding cleaning of the structural components along the inner wall, reducing the tedious cleaning process and improving the reactor's efficiency. Simultaneously, energy consumption is saved during cleaning, and the internal temperature can be easily controlled during the reaction, minimizing the impact of temperature on the raw materials. Attached Figure Description

[0014] Figure 1 A schematic diagram of a preferred embodiment of a temperature-controlled reactor for the production of mercaptopropyltriethoxysilane provided by this utility model;

[0015] Figure 2 for Figure 1 The diagram shows the structure of the sealing cover.

[0016] Figure 3 for Figure 1 The diagram shows a front view of a temperature-controlled reactor for the production of mercaptopropyltriethoxysilane.

[0017] Figure 4 for Figure 1 The diagram shows the structure of the drive motor.

[0018] Figure 5 for Figure 1 The diagram shows the structure of the heating device.

[0019] Figure 6 for Figure 1 The diagram shows the structure of the cleaning scraper.

[0020] Numbered in the diagram: 1. Device base, 2. Inlet pipe, 3. Outlet pipe, 4. Control base, 5. Control valve, 6. Fixed side plate, 7. Controller, 8. Water inlet pipe, 9. Connecting pipe, 10. Water outlet pipe, 11. Heating device, 12. Fixed base, 13. Load-bearing base plate, 14. Limiting plate, 15. Drive motor, 16. Drive rod, 17. Stirring rod, 18. Motor support, 19. Mounting plate, 20. Sliding groove, 21. Fastening base plate, 22. Fastening rod, 23. Rotating rod, 24. Rotating disc, 25. Rotating handle, 26. Cleaning scraper, 27. Fixed rod, 28. Rotating mounting frame, 29. Rotating connecting rod, 30. Sealing cover plate, 31. Fixed handle, 32. Fastening plate. Detailed Implementation

[0021] The present invention will be further described below with reference to the accompanying drawings and embodiments.

[0022] Please refer to the following: Figure 1 , Figure 2 , Figure 3 , Figure 4 and Figure 5 , Figure 6 ,in, Figure 1 A schematic diagram of a preferred embodiment of a temperature-controlled reactor for the production of mercaptopropyltriethoxysilane provided by this utility model; Figure 2 for Figure 1 The diagram shows the structure of the sealing cover. Figure 3 for Figure 1 The diagram shows a front view of a temperature-controlled reactor for the production of mercaptopropyltriethoxysilane. Figure 4 for Figure 1 The diagram shows the structure of the drive motor. Figure 5 for Figure 1 The diagram shows the structure of the heating device. Figure 6 for Figure 1The diagram shows a structural schematic of a cleaning scraper. A temperature-controlled reactor for the production of mercaptopropyltriethoxysilane includes: a device base 1; a liquid inlet pipe 2 is installed and connected to the inner wall of the top left end of the device base 1; a liquid outlet pipe 3 is installed and connected to the inner wall of the bottom right end of the device base 1; a water inlet pipe 8 is installed and connected to the inner wall of the right end of the device base 1; a connecting pipe 9 is installed and connected to the inner wall of one end of the water inlet pipe 8; a water outlet pipe 10 is installed and connected to the inner wall of one end of the connecting pipe 9; a heating device 11 is installed and connected to the inner wall of the side end of the water inlet pipe 8; a drive motor 15 is installed and connected to the inner wall of the bottom of the device base 1; a drive rod 16 is installed and connected to the output end of the drive motor 15; and a stirring rod 17 is installed and connected to the inner wall of the side end of the drive rod 16. A mounting plate 19 is installed on the inner wall of the top of the body 1. Sliding grooves 20 are fixedly connected to the inner walls of both ends of the mounting plate 19. A rotating rod 23 is installed on the inner wall of the top of the middle of the mounting plate 19. A rotating disk 24 is installed on the inner wall of the top of the rotating rod 23. A rotating handle 25 is installed on the inner wall of the top of the rotating disk 24. A cleaning scraper 26 is slidably connected to the inner wall of the side end of the sliding groove 20. A fixing rod 27 is installed on the inner wall of the top of the cleaning scraper 26. A rotating mounting frame 28 is installed on the inner wall of the side end of the fixing rod 27 and the rotating rod 23. A rotating connecting rod 29 is installed between the inner walls of the side end of the rotating mounting frame 28. A sealing cover plate 30 is installed on the inner wall of the top of the mounting plate 19.

[0023] A control base 4 is installed and connected to the inner wall of the side end of the liquid inlet pipe 2 and the liquid outlet pipe 3. A control valve 5 is installed and connected to the inner wall of the top of the control base 4. When the raw material is discharged into the device, the staff can easily control the feeding speed of the raw material to avoid the reaction being unstable due to being too fast or too slow.

[0024] A fixed base 12 is installed and connected to the bottom inner wall of the device base 1. A load-bearing base plate 13 is installed and connected to the bottom inner wall of the fixed base 12. Limiting plates 14 are installed and connected to the inner walls at both ends of the fixed base 12 to improve the stability support of the device and reduce the phenomenon of position loosening during use.

[0025] A fixed side plate 6 is installed and connected to the inner wall of the side end of the device base 1, and a controller 7 is installed and connected to the inner wall of the side end of the fixed side plate 6. During use, the device can be easily controlled and operated by the staff.

[0026] A fastening base plate 21 is installed and connected to the inner wall of the side end of the mounting plate 19. A fastening rod 22 is installed and connected to the inner wall of the top of the fastening base plate 21. A fastening plate 32 is installed and connected to the inner wall of the side end of the sealing cover plate 30, thereby improving the sealing performance of the device and reducing leakage.

[0027] Fixed handles 31 are installed and connected to the inner walls at both ends of the sealing cover plate 30, and motor support 18 is installed and connected to the inner wall at the side end of the drive motor 15 to prevent the motor from deviating in position during operation.

[0028] The working principle of the temperature-controlled reactor for the production of mercaptopropyltriethoxysilane provided by this utility model is as follows:

[0029] During the reaction process, the raw materials are first added into the device body 1. Then, the drive motor 15 at the bottom of the device body 1 stirs the raw materials inside to prevent uneven heating. At the same time, water is circulated inside the device through heating. After the reaction is completed, when cleaning is required, the rotating disk 24 at the top can be rotated directly. After the rotating disk 24 rotates, the rotating connecting rods 29 at both ends can drive the cleaning scrapers 26 at the side to slide. At this time, the cleaning scrapers 26 at both ends will clean the raw materials remaining on the inner wall of the device through the sliding grooves 20, so as to reduce the cumbersome process during use.

[0030] Compared with related technologies, the temperature-controlled reactor for the production of mercaptopropyltriethoxysilane provided by this utility model has the following beneficial effects:

[0031] During the reaction process of the raw materials, it is usually necessary to clean the residual raw materials on the inner wall of the device after the reaction is completed. In order to improve the ease of use of the device, the cleaning scrapers 26 set at both ends of the device can directly slide and clean the structural workpiece along the inner wall of the device, reducing the tedious work during use and cleaning, improving the working efficiency of the device. At the same time, energy consumption can be saved during the cleaning process, and the internal temperature of the device can be easily controlled during the reaction, reducing the impact of temperature on the raw materials.

[0032] The above description is merely an embodiment of this utility model and does not limit the patent scope of this utility model. Any equivalent structural or procedural transformations made based on the content of this utility model specification and drawings, or direct or indirect applications in other related technical fields, are similarly included within the patent protection scope of this utility model.

Claims

1. A temperature-controlled reactor for the production of mercaptopropyltriethoxysilane, characterized in that, include: The device base has an inlet pipe installed on the inner wall of the top left end, an outlet pipe installed on the inner wall of the bottom right end, a water inlet pipe installed on the inner wall of the right end, a connecting pipe installed on the inner wall of one end of the water inlet pipe, a water outlet pipe installed on the inner wall of the connecting pipe, a heating device installed on the inner wall of the side end of the water inlet pipe, a drive motor installed on the inner wall of the bottom of the device base, a drive rod installed on the output end of the drive motor, and a stirring rod installed on the inner wall of the side end of the drive rod. The top of the device base... An installation plate is installed on the inner wall. Sliding grooves are fixedly connected to the inner walls at both ends of the installation plate. A rotating rod is installed on the top inner wall of the middle of the installation plate. A rotating disk is installed on the top inner wall of the rotating rod. A rotating handle is installed on the top inner wall of the rotating disk. A cleaning scraper is slidably connected to the inner wall of the side end of the sliding groove. A fixing rod is installed on the top inner wall of the cleaning scraper. A rotating installation frame is installed on the inner wall of the side end of the fixing rod and the rotating rod. A rotating connecting rod is installed between the inner walls of the side end of the rotating installation frame. A sealing cover is installed on the top inner wall of the installation plate.

2. The temperature-controlled reactor for the production of mercaptopropyltriethoxysilane according to claim 1, characterized in that, A control base is installed and connected to the inner wall of the side end of the liquid inlet pipe and the liquid outlet pipe, and a control valve is installed and connected to the inner wall of the top of the control base.

3. The temperature-controlled reactor for the production of mercaptopropyltriethoxysilane according to claim 1, characterized in that, A fixed base is installed on the inner wall of the bottom of the device base, a load-bearing base plate is installed on the inner wall of the bottom of the fixed base, and limit plates are installed on the inner walls of both ends of the fixed base.

4. The temperature-controlled reactor for the production of mercaptopropyltriethoxysilane according to claim 1, characterized in that, A fixed side plate is installed and connected to the inner wall of the base of the device, and a controller is installed and connected to the inner wall of the fixed side plate.

5. The temperature-controlled reactor for the production of mercaptopropyltriethoxysilane according to claim 1, characterized in that, A fastening base plate is installed and connected to the inner wall of the side end of the mounting plate, a fastening rod is installed and connected to the inner wall of the top of the fastening base plate, and a fastening plate is installed and connected to the inner wall of the side end of the sealing cover.

6. The temperature-controlled reactor for the production of mercaptopropyltriethoxysilane according to claim 1, characterized in that, Fixed handles are installed on the inner walls of both ends of the sealing cover, and motor support components are installed on the inner wall of the side end of the drive motor.