Alkyl xanthate synthesis reaction neutralization device

Abstract

The utility model discloses a neutralization device for alkyl xanthate synthesis reaction. The neutralization device comprises a neutralization tank, the neutralization tank is used for supporting the whole mechanism element, and the neutralization tank is provided with a trace liquid inlet hopper, a large-flow liquid inlet hopper, a driving box, a driver, a stirring frame, a drip irrigation head and a movable PH value detection assembly. Therefore, the PH value of the solution at each position in the tank body from top to bottom can be detected, the mixing uniformity of the solution can be obtained through the obtained numerical value difference, and the accurate numerical value of the pH value of the solution can be obtained when the PH values at each position are consistent, so that the accuracy of the components of the final finished product is improved.

Description

TECHNICAL FIELD

[0001] The utility model relates to alkyl xanthate synthesis technical field, concretely is a kind of alkyl xanthate synthesis reaction neutralizing device. BACKGROUND

[0002] When alkyl xanthate synthesis is carried out, the PH value in the mixing tank needs to be detected at any time, but the general detection method can only detect at a certain position of the tank body, and once the solution composition cannot be mixed uniformly, the PH value reading will be inaccurate, thereby affecting the composition ratio of the final product. UTILITARY MODEL

[0003] To achieve the above object, the utility model is realized by the following technical scheme: a kind of alkyl xanthate synthesis reaction neutralizing device, including neutralizing tank;The neutralizing tank is used to support the whole mechanism element, the neutralizing tank is equipped with: trace liquid inlet hopper, large flow liquid inlet hopper, drive box, driver, stirring frame, drip irrigation head and mobile PH value detection component;

[0004] The trace liquid inlet hopper and the large flow liquid inlet hopper are installed at the top of the neutralizing tank, the drive box is installed at the top center position of the neutralizing tank, the driver is installed in the drive box, the stirring frame is installed in the neutralizing tank and is connected to the output end of the driver, and the drip irrigation head is connected to the bottom of the trace liquid inlet hopper.

[0005] Among them, the mobile PH value detection component includes: motor box, rotary motor, threaded rod, threaded hole, slide, lifting block, mounting groove, PH value detector and detection head.

[0006] The motor box is installed at the top of the neutralizing tank, the rotary motor is installed in the motor box, the threaded rod is installed in the neutralizing tank and is connected to the output end of the rotary motor, the slide is installed on the side wall of the neutralizing tank, the lifting block is installed on the slide, the mounting groove is installed on the lifting block, the PH value detector is embedded in the mounting groove, and the detection head is installed at the detection end of the PH value detector and extends out of the mounting groove. Through the component, the PH of the solution at each height inside the tank body can be detected.

[0007] Preferably, a sealing ring is provided between the mounting groove opening and the detection head.

[0008] Preferably, the threaded rod, slide and lifting block are made of glass steel material.

[0009] Preferably, the drip irrigation head is provided with an electronic valve.

[0010] Preferably, the trace liquid inlet hopper and the large flow liquid inlet hopper are provided with dust covers.

[0011] ADVANTAGEOUS EFFECTS

[0012] The alkyl xanthate synthesis reaction neutralization device has the following beneficial effects:

[0013] The mobile PH value detection assembly can detect the PH values of the solution at various positions from top to bottom in the tank body, and the uniformity of the solution can be known according to the obtained numerical difference, and the accurate value of the acid-base degree of the solution can be obtained when the PH values at various positions are consistent, thereby improving the accuracy of the final product composition. BRIEF DESCRIPTION OF DRAWINGS

[0014] Fig. 1 It is a front view structural schematic diagram of the alkyl xanthate synthesis reaction neutralization device.

[0015] Fig. 2 It is a front view structural schematic diagram of the alkyl xanthate synthesis reaction neutralization device.

[0016] Fig. 3 It is a partial enlarged structural schematic diagram of the mobile PH value detection assembly of the alkyl xanthate synthesis reaction neutralization device.

[0017] In the figure: 1, neutralization tank; 2, trace liquid inlet hopper; 3, large flow liquid inlet hopper; 4, drive box; 5, driver; 6, stirring frame; 7, drip irrigation head; 8, motor box; 9, rotary motor; 10, threaded rod; 11, threaded hole; 12, slide; 13, lifting block; 14, mounting groove; 15, PH value detector; 16, detection head; DETAILED DESCRIPTION

[0018] Based on the embodiments in the utility model, all other embodiments obtained by the ordinary skilled in the art without creative labor belong to the protection range of the utility model.

[0019] Please refer to Figs. 1-3 The utility model provides a technical scheme.

[0020] An alkyl xanthate synthesis reaction neutralization device, comprising a neutralization tank 1; the neutralization tank 1 is used to support the whole mechanism element, and is provided with a trace liquid inlet hopper 2, a large flow liquid inlet hopper 3, a drive box 4, a driver 5, a stirring frame 6, a drip irrigation head 7 and a mobile PH value detection assembly on the neutralization tank 1;

[0021] The trace liquid inlet hopper 2 and the large flow liquid inlet hopper 3 are installed at the top of the neutralization tank 1, the drive box 4 is installed at the top center position of the neutralization tank 1, the driver 5 is installed in the drive box 4, the stirring frame 6 is installed in the neutralization tank 1 and is connected to the output end of the driver 5, and the drip irrigation head 7 is connected to the bottom of the trace liquid inlet hopper 2.

[0022] The mobile PH value detection assembly comprises a motor box 8, a rotating motor 9, a threaded rod 10, a threaded hole 11, a slide 12, a lifting block 13, a mounting groove 14, a PH value detector 15 and a detection head 16.

[0023] The motor box 8 is installed on the top of the neutralization tank 1, the rotating motor 9 is installed in the motor box 8, the threaded rod 10 is installed in the neutralization tank 1 and connected to the output end of the rotating motor 9, the slide 12 is installed on the sidewall of the neutralization tank 1, the lifting block 13 is installed on the slide 12, the mounting groove 14 is started on the lifting block 13, the PH value detector 15 is embedded in the mounting groove 14, and the detection head 16 is installed on the detection end of the PH value detector 15 and extends out of the mounting groove 14.

[0024] It should be noted that during the reaction of the preparation of the alkyl xanthate, the mixing of the solution can be realized by rotating the stirring frame 6 driven by the driver 5, and the solution can be directly poured into the tank through the large-flow liquid inlet 3. When it is necessary to add a small amount of solvent, the solvent needs to be poured into the micro-liquid inlet 2 and added by the drip head 7, so as to stably control the addition flow and improve the mixing precision of the solvent. During the mixing of the solution, the lifting block 13 performs lifting movement on the slide 12 by rotating the threaded rod 10 in the threaded hole 11 driven by the rotating motor 9, and the PH value detector 15 can detect the PH value of the solution at each position of the tank body during the mixing process through the data detection of the detection head 16, so as to know whether the mixing of the solution is completely uniform. When the PH value of the solution at each height is consistent, the accurate PH value can be obtained, and then the solvent can be continuously added according to the needs.

[0025] As preferred, further, a sealing ring is arranged between the opening of the mounting groove 14 and the detection head 16.

[0026] It should be noted that the sealing ring is used to place the PH value detector 15 in case of water failure.

[0027] As preferred, further, the threaded rod 10, the slide 12 and the lifting block 13 are made of glass steel material.

[0028] It should be noted that the glass steel is a corrosion-resistant material, which can realize the environment of acid-base mixing.

[0029] As preferred, further, an electronic valve is arranged on the drip head 7.

[0030] It should be noted that the electronic valve is used to control the opening and closing of the drip head 7.

[0031] As preferred, further, dust covers are arranged on the micro-liquid inlet 2 and the large-flow liquid inlet 3.

[0032] It should be noted that the dust cover is used to prevent dust from falling on the trace liquid inlet hopper 2 and the large flow liquid inlet hopper 3 in the air during work.

[0033] Although the embodiments of the present application have been shown and described, it should be understood by those ordinary skilled in the art that various changes, modifications, replacements and variations can be made to these embodiments without departing from the principles and spirits of the present application, and the scope of the present application is defined by the appended claims and their equivalents.

Claims

1. An alkyl xanthate synthesis reaction neutralization apparatus comprising a neutralization tank; the neutralization tank is used to support the entire mechanism components, characterized in that, The neutralization tank is provided with trace liquid inlet hopper, large flow liquid inlet hopper, driving box, driver, stirring frame, drip irrigation head and mobile PH value detection assembly. The trace liquid inlet hopper and the large flow liquid inlet hopper are installed on the top of the neutralization tank, the driving box is installed on the center of the top of the neutralization tank, the driver is installed in the driving box, the stirring frame is installed in the neutralization tank and connected to the output end of the driver, and the drip irrigation head is connected to the bottom of the trace liquid inlet hopper. The mobile PH value detection assembly comprises motor box, rotary motor, threaded rod, threaded hole, slide, lifting block, installation slot, PH value detector and detection head. The motor box is installed on the top of the neutralization tank, the rotary motor is installed in the motor box, the threaded rod is installed in the neutralization tank and connected to the output end of the rotary motor, the slide is installed on the side wall of the neutralization tank, the lifting block is installed on the slide, the installation slot is installed on the lifting block, the PH value detector is embedded in the installation slot, and the detection head is installed on the detection end of the PH value detector and extends out of the installation slot.

2. An alkyl xanthate synthesis neutralization apparatus according to claim 1, wherein A sealing ring is arranged between the opening of the installation slot and the detection head.

3. An alkyl xanthate synthesis neutralization apparatus according to claim 1, wherein The threaded rod, the slide and the lifting block are made of glass fiber reinforced plastic.

4. The alkyl xanthate synthesis neutralization apparatus of claim 1, wherein, The drip irrigation head is provided with an electronic valve.

5. The alkyl xanthate synthesis neutralization apparatus of claim 1, wherein, The trace liquid inlet hopper and the large flow liquid inlet hopper are provided with dustproof covers.

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