Centrifugal separation device for dye intermediate

Abstract

The utility model discloses a centrifugal separation device for dye intermediates, which belongs to the field of dye purification and comprises a centrifugal separation tank, a centrifugal purification tank is arranged in the centrifugal separation tank, a rotating motor is arranged below the centrifugal purification tank, and the centrifugal separation tank is of a single-opening structure. Compared with the prior art, the device has the advantages that in the machining process, air is sprayed to the inner wall of the centrifugal separation tank body in real time through the air pressure shunting pipeline in the sealing cover, so that water vapor on the inner wall of the centrifugal separation tank body is accelerated to form water drops, and the water drops flow to the secondary filter screen on the bottom surface of the centrifugal separation tank body; the dyeing intermediates are condensed again through the secondary filter screen, so that the yield of the dyeing intermediates is increased, and the situation that the inner wall of the centrifugal separation tank is adhered to the interlayer of the dyeing intermediates is avoided.

Description

TECHNICAL FIELD

[0001] The utility model relates to the field of dye purification, specifically refers to a centrifugal separation device for dye intermediate. BACKGROUND

[0002] Dye intermediate refers to various aromatic hydrocarbon derivatives for producing dyes and organic pigments, which are intermediate products for manufacturing dyes, pesticides, medicines, resins, auxiliaries, plasticizers and other products. Dye intermediate is initially used for manufacturing dyes, so it is also called dye intermediate. The synthesis process of dye intermediate includes raw material selection, intermediate generation, intermediate conversion and intermediate purification. The purification of intermediate mainly relies on a centrifugal separation device for dye intermediate.

[0003] The existing centrifugal separation device for dye intermediate mainly drives the centrifugal purification tank to rotate at high speed in the centrifugal separation tank body through a rotating motor. Under the action of the same centrifugal force, impurities, waste liquid and intermediate penetrate the side separation hole of the centrifugal purification tank at different speeds. The impurities inside the dye intermediate are thrown out of the centrifugal purification tank, so as to purify the dye intermediate.

[0004] This device can quickly purify the dye intermediate in a short time through centrifugal force. However, during the swinging of the centrifugal purification tank, some dye intermediate will be carried out of the centrifugal purification tank by water vapor and then thrown onto the inner wall of the centrifugal separation tank body. After the water vapor condenses into water droplets, it slides downward and flows into the water outlet of the centrifugal separation tank body. However, after the centrifugal purification tank stops rotating, water mist will remain on the inner wall of the centrifugal separation tank body. Because the volume of the water mist is too small, the dye intermediate components in the water mist adhere to the inner wall of the centrifugal separation tank body. After a long time of normal temperature evaporation, the dye intermediate will condense into a powder layer and stick to the inner wall of the centrifugal separation tank body. UTILITY MODEL CONTENTS

[0005] The technical problem to be solved by the utility model is that the water vapor and dye intermediate gas components on the inner wall of the centrifugal separation tank body cannot be discharged in time during the finishing stage of the existing centrifugal separation device for dye intermediate.

[0006] To solve the above technical problems, the technical scheme provided by the utility model is as follows: a centrifugal separation device for dye intermediate, comprising a centrifugal separation tank body, a centrifugal purification tank is arranged in the centrifugal separation tank body, a rotating motor is arranged below the centrifugal purification tank, the centrifugal separation tank body is a single open structure, a sealing cover is arranged on one side of the open end of the centrifugal separation tank body, a gas pressure shunt pipeline is arranged in the sealing cover, and a secondary filter screen is arranged at the bottom end of the centrifugal separation tank body.

[0007] As improved, the bottom end of the centrifugal purification tank is provided with a detachable fixing plate, one side of the detachable fixing plate is provided with a polygonal fixing column, and the polygonal fixing column penetrates the bottom end of the centrifugal purification tank.

[0008] As improved, the output shaft of the rotary motor penetrates the bottom end of the centrifugal separation tank body and the bottom end of the detachable fixing plate, the output shaft of the rotary motor is connected with the through hole at the bottom end of the detachable fixing plate through a connecting key, the rotary motor is connected with the bottom of the centrifugal separation tank body through a bolt structure, and the detachable fixing plate and the bottom of the centrifugal purification tank and the centrifugal separation tank body and the sealing cover are all connected through buckling.

[0009] As improved, the centrifugal purification tank is of a single open structure, and the open end of the centrifugal purification tank is provided with a T-shaped cover, and the thin column end of the T-shaped cover penetrates the bottom of the sealing cover.

[0010] As improved, the side of the centrifugal separation tank body is provided with a cleaning door above the secondary filter screen, and the inside of the centrifugal separation tank body is provided with a bevel water control port below the secondary filter screen.

[0011] As improved, the secondary filter screen is connected with the inner wall of the centrifugal separation tank body through a bolt structure.

[0012] Compared with the prior art, the device has the advantages that: in the process of machining, the inner wall of the centrifugal separation tank body is sprayed with air in real time through the air pressure shunt pipeline in the sealing cover, so that the water vapor on the inner wall of the centrifugal separation tank body forms water droplets quickly, and then flows to the secondary filter screen on the bottom surface of the centrifugal separation tank body, and the dye intermediate is re-aggregated through the secondary filter screen, so that the yield of the dye intermediate is improved, and the phenomenon that the dye intermediate is adhered to the inner wall of the centrifugal separation tank body is avoided. BRIEF DESCRIPTION OF DRAWINGS

[0013] Figure 1 is a total structure view of the centrifugal separation device for dye intermediates.

[0014] Figure 2 is a total structure sectional view of the centrifugal separation device for dye intermediates.

[0015] Figure 3 is an explosion view of the total structure of the centrifugal separation device for dye intermediates.

[0016] Figure 4 is a centrifugal separation tank body structure view of the centrifugal separation device for dye intermediates.

[0017] As shown in the figure: 1, centrifugal separation tank body; 11, sealing cover; 111, air pressure shunt pipeline; 12, secondary filter screen; 13, cleaning door; 14, inclined water control port; 2, centrifugal purification tank; 21, detachable fixed plate; 211, polygonal fixed column; 22, T-shaped cover; 3, rotating motor. DETAILED DESCRIPTION

[0018] The utility model makes further detailed description in combination with the drawings.

[0019] As shown in the description accompanying drawings Figure 1 , 2 , 3, 4, including centrifugal separation tank body 1, the bottom surface end of centrifugal separation tank body 1 is equipped with secondary filter screen 12, the side of centrifugal separation tank body 1 is equipped with cleaning door 13 located above secondary filter screen 12, the inside of centrifugal separation tank body 1 is equipped with inclined water control port 14 located below secondary filter screen 12, and secondary filter screen 12 is connected with the inner wall of centrifugal separation tank body 1 by bolt structure;Secondary filter screen 12 is placed above the inclined groove of inclined water control port 14 on the bottom surface of centrifugal separation tank body 1, and the two are fixed by using screw, so that the secondary recovery of water and dye intermediate is facilitated, and cleaning door 13 is fixed by using hinge device.

[0020] The inside of centrifugal separation tank body 1 is equipped with centrifugal purification tank 2, the lower portion of centrifugal purification tank 2 is equipped with rotating motor 3, the bottom surface end of centrifugal purification tank 2 is equipped with detachable fixed plate 21, one side of detachable fixed plate 21 is equipped with polygonal fixed column 211, polygonal fixed column 211 penetrates the bottom surface end of centrifugal purification tank 2, the output shaft of rotating motor 3 penetrates the bottom surface end of centrifugal separation tank body 1 and the bottom surface end of detachable fixed plate 21, the output shaft of rotating motor 3 is connected with the through hole of the bottom surface end of detachable fixed plate 21 by connecting key, rotating motor 3 is connected with the bottom surface of centrifugal separation tank body 1 by bolt structure, the bottom surface of detachable fixed plate 21 and the bottom surface of centrifugal purification tank 2 and the sealing cover 11 of centrifugal separation tank body 1 are all connected by buckle, the output shaft of rotating motor 3 penetrates the through hole in the center of centrifugal separation tank body 1, rotating motor 3 is fixed to the bottom surface of centrifugal separation tank body 1 by using screw, connecting key is installed in the bottom surface through hole of detachable fixed plate 21 and is sleeved on the output shaft of rotating motor 3, in order to the fixity of the two, screw can be used for reinforcing, the polygonal recess of the bottom surface of centrifugal purification tank 2 is sleeved on polygonal fixed column 211 to be position-fixed, buckle on detachable fixed plate 21 is clamped on the clamping groove on the bottom surface of centrifugal purification tank 2 to be fixed by opening cleaning door 13.

[0021] The centrifugal separation tank body 1 is single open structure, one side of the open end of the centrifugal separation tank body 1 is equipped with a sealing cover 11, the inside of the sealing cover 11 is equipped with a gas pressure shunt pipeline 111, the centrifugal purification tank 2 is single open structure, the open end of the centrifugal purification tank 2 is equipped with a T-shaped cover 22, the thin column end of the T-shaped cover 22 passes through the bottom surface of the sealing cover 11, the thick column surface of the T-shaped cover 22 is covered on the open end of the centrifugal purification tank 2, and the T-shaped cover 22 is fixed by using a screw, the bearing corresponding to the thin column end of the T-shaped cover 22 is inserted into the center through hole of the sealing cover 11, the sealing cover 11 is covered on the open end of the centrifugal separation tank body 1, and the buckle on the sealing cover 11 is sealed, the gas pressurizing pump is connected to the gas inlet of the gas pressure shunt pipeline 111, and finally the pressurizing pump and the rotating motor 3 are powered.

[0022] In the specific implementation, the dye intermediate semi-finished product is put into the centrifugal purification tank 2, the T-shaped cover 22 is closed, the screw is used for sealing connection, the T-shaped cover 22 thin column end through hole in the center of the sealing cover 11 is sleeved on the T-shaped cover 22 thin column, the buckle on the outer wall of the sealing cover 11 is fixed, the rotating motor 3 and the gas pressure shunt pipeline 111 connected gas pressure pump are started, the centrifugal purification of the dye intermediate is carried out, the centrifugal separation tank body 1 inner wall is ensured to be residual-free, after the purification is finished, the rotating motor 3 and the gas pressure pump are closed, the cleaning door 13 is opened, the dye intermediate on the secondary filter screen 12 is scraped off by using a brush, the buckle of the sealing cover 11 is opened, the sealing cover 11 is removed, the buckle between the detachable fixing plate 21 and the centrifugal purification tank 2 is removed through the cleaning door 13, the centrifugal purification tank 2 is taken out, is placed in a pouring position, the T-shaped cover 22 is opened, the dye intermediate is taken out, the centrifugal purification tank 2 is cleaned, the centrifugal purification tank 2 is placed back to the original position, and the buckle is clamped.

[0023] The above describes the utility model and its implementation mode, and the description is not limited, and the embodiment shown in the drawings is only one of the utility model, and the actual structure is not limited thereto. In summary, if a person skilled in the art is inspired, without departing from the creative purpose of the utility model, similar structure modes and embodiments are not creatively designed, which should belong to the protection scope of the utility model.

Claims

1. A centrifugal separation device for dye intermediates, comprising a centrifugal separation tank (1), wherein a centrifugal purification tank (2) is disposed inside the centrifugal separation tank (1), and a rotary motor (3) is disposed below the centrifugal purification tank (2), characterized in that: The centrifugal separation tank (1) has a single open structure. A sealing cover (11) is provided on one side of the open end of the centrifugal separation tank (1). A gas pressure diversion pipe (111) is provided inside the sealing cover (11). A secondary filter screen (12) is provided on the bottom end of the centrifugal separation tank (1).

2. The centrifugal separation device for dye intermediates according to claim 1, characterized in that: The bottom end of the centrifugal purification tank (2) is provided with a detachable fixing plate (21), and a polygonal fixing column (211) is provided on one side of the detachable fixing plate (21), and the polygonal fixing column (211) passes through the bottom end of the centrifugal purification tank (2).

3. A centrifugal separation device for dye intermediates according to claim 2, characterized in that: The output shaft of the rotary motor (3) passes through the bottom end of the centrifugal separation tank (1) and the bottom end of the detachable fixing plate (21). The output shaft of the rotary motor (3) is connected to the through hole at the bottom end of the detachable fixing plate (21) by a connecting key. The rotary motor (3) is connected to the bottom of the centrifugal separation tank (1) by a bolt structure. The detachable fixing plate (21) is connected to the bottom of the centrifugal purification tank (2), and the centrifugal separation tank (1) is connected to the sealing cover (11) by a snap fastener.

4. A centrifugal separation device for dye intermediates according to claim 1, characterized in that: The centrifugal purification tank (2) has a single open structure. The open end of the centrifugal purification tank (2) is provided with a T-shaped cover (22). The thin column end of the T-shaped cover (22) passes through the bottom surface of the sealing cover (11).

5. A centrifugal separation device for dye intermediates according to claim 1, characterized in that: The centrifugal separation tank (1) has a cleaning door (13) on its side above the secondary filter screen (12), and the centrifugal separation tank (1) has a sloping water control port (14) below the secondary filter screen (12) inside.

6. A centrifugal separation device for dye intermediates according to claim 1, characterized in that: The secondary filter (12) is connected to the inner wall of the centrifugal separation tank (1) by bolts.

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