Reaction kettle for processing 9-decenol

Abstract

The utility model relates to the technical field of reaction kettles, and discloses a reaction kettle for processing 9-decenol, which comprises a reaction kettle body, a mixing mechanism is arranged in the reaction kettle body, the mixing mechanism comprises a first connecting shaft, the first connecting shaft is arranged in the reaction kettle body, and a second connecting shaft is arranged in the reaction kettle body. A first stirring frame is fixedly connected to the upper portions of the two sides of the first connecting shaft. According to the stirring device disclosed by the utility model, the first motor, the first connecting shaft, the first stirring frame, the first stirring rod, the second motor, the second connecting shaft, the second stirring frame and the second stirring rod are matched, so that 9-decenol in the reaction kettle can be simultaneously stirred clockwise and anticlockwise, and the mixing efficiency is improved; by virtue of cooperation of a first guide pipe, a first infusion pump, a second guide pipe and a spray head, 9-decenol at the lower part in the reaction kettle can be conveniently pumped and discharged into the upper part in the reaction kettle, so that the 9-decenol can be sufficiently stirred, and the reaction efficiency of the 9-decenol is improved.

Description

Technical Field

[0001] This utility model relates to the field of reaction vessel technology, and more specifically to a reaction vessel for processing 9-decenol. Background Technology

[0002] A reaction vessel is a piece of equipment used to realize chemical reaction processes, widely used in petroleum, chemical, rubber, pesticide, dye, pharmaceutical, and food industries. It is mainly used to complete processes such as vulcanization, nitration, hydrogenation, hydrocarbonation, polymerization, and condensation. 9-Decanol is a colorless to pale yellow liquid chemical substance with floral, aldehyde, rose, and waxy aromas. Its fresh and long-lasting fragrance is mainly used in the formulation of daily chemical fragrances, giving products a fresh and lasting aroma. The processing of 9-decenol requires reaction within a reaction vessel.

[0003] Currently, when 9-decenol is processed inside a reactor, it usually requires mixing and stirring. However, if only the stirring rod inside the reactor is used to stir 9-decenol, the mixing is not thorough enough and the efficiency is low. Furthermore, it is not convenient to take samples to detect the progress and quality of the 9-decenol reaction when it is processed inside the reactor, which needs to be improved. Utility Model Content

[0004] In order to overcome the above-mentioned defects of the prior art, the present invention provides a reaction vessel for processing 9-decenol to solve the problems existing in the background art.

[0005] This utility model provides the following technical solution: a reaction vessel for processing 9-decenol, comprising a reaction vessel body, a mixing mechanism inside the reaction vessel body, the mixing mechanism including a first connecting shaft, the first connecting shaft being disposed inside the reaction vessel body, a first stirring rack fixedly connected to the upper sides of the first connecting shaft, a first stirring rod fixedly connected to the inner wall of the first stirring rack, a first conduit fixedly connected to the lower sides of the reaction vessel body, a first solenoid valve installed on the first conduit, one end of the first conduit extending into the interior of the reaction vessel body, a first liquid pump fixedly connected to the lower sides of the reaction vessel body, the other end of the first conduit fixedly installed at the input end of the first liquid pump, a sampling mechanism provided on the upper side of one side of the reaction vessel body, the sampling mechanism including a fixed cover, a sampling cylinder threadedly sleeved on the lower side of the fixed cover, a fixed frame fixedly connected to the left side of the fixed cover, and one side of the fixed frame fixedly connected to the upper right side of the reaction vessel body.

[0006] Furthermore, a No. 1 motor is fixedly installed at the center of the top of the reactor body. The output end of the No. 1 motor extends into the interior of the reactor body and is fixedly connected to the top of the No. 1 connecting shaft. A limiting plate is fixedly connected to the lower part of the interior of the reactor body. The bottom end of the No. 1 connecting shaft is rotatably mounted on the top of the limiting plate through a bearing.

[0007] Furthermore, a second motor is fixedly installed in the middle of the bottom of the reactor body. The output end of the second motor extends into the interior of the reactor body and is fixedly connected to a second connecting shaft. The top end of the second connecting shaft is rotatably mounted on the bottom of the limiting plate via a bearing. A second stirring rack is fixedly connected to both sides of the second connecting shaft. A second stirring rod is fixedly connected to the inner wall of the second stirring rack. The second stirring rack is located below and outside the first stirring rack.

[0008] Furthermore, the output end of the first pump is fixedly connected to a second conduit, one end of which extends to the upper part of the reactor body and is fixedly connected to a nozzle.

[0009] Furthermore, a liquid extraction pipe is fixedly connected to the right side of the top of the reactor body, and a second solenoid valve is installed on the liquid extraction pipe. The bottom end of the liquid extraction pipe extends to the right side inside the reactor body. A second liquid extraction pump is fixedly installed on the right side of the top of the reactor body. The top end of the liquid extraction pipe is fixedly connected to the input end of the second liquid extraction pump. A drain pipe is fixedly connected to the output end of the second liquid extraction pump, and one end of the drain pipe is fixedly connected to the middle of the top of the fixed cover.

[0010] Furthermore, a feed inlet is provided on the left side of the top of the reactor body, and a discharge pipe is fixedly connected to the bottom of the reactor body. The discharge pipe is located to the left of the No. 2 motor, and a discharge valve is installed on the discharge pipe.

[0011] The technical effects and advantages of this utility model are as follows:

[0012] 1. This utility model utilizes a combination of a No. 1 motor, a No. 1 connecting shaft, a No. 1 stirring frame, a No. 1 stirring rod, a No. 2 motor, a No. 2 connecting shaft, a No. 2 stirring frame, and a No. 2 stirring rod to facilitate simultaneous clockwise and counterclockwise stirring of 9-decenol inside the reactor, thereby improving mixing efficiency. Furthermore, the combination of a No. 1 conduit, a No. 1 liquid pump, a No. 2 conduit, and a nozzle facilitates the extraction of 9-decenol from the lower part of the reactor and its discharge into the upper part of the reactor, ensuring thorough stirring of 9-decenol and improving the reaction efficiency of 9-decenol.

[0013] 2. This utility model, by employing a combination of a suction pipe, a second suction pump, and a discharge pipe, facilitates the extraction of 9-decenol from inside the reaction vessel into a sampling cylinder, and then the sampling cylinder is screwed down, making it convenient to sample 9-decenol from inside the reaction vessel for testing the progress and quality of the 9-decenol reaction. Attached Figure Description

[0014] Figure 1 This is a schematic diagram of the overall structure of this utility model.

[0015] Figure 2 This is a cross-sectional view of the overall structure of this utility model.

[0016] The attached diagram is labeled as follows: 1. Reactor body; 2. Feed inlet; 3. Discharge pipe; 4. Discharge valve; 5. Mixing mechanism; 6. Sampling mechanism; 51. Motor No. 1; 52. Connecting shaft No. 1; 53. Stirring rack No. 1; 54. Stirring rod No. 1; 55. Motor No. 2; 56. Connecting shaft No. 2; 57. Stirring rack No. 2; 58. Stirring rod No. 2; 59. Conduit No. 1; 591. Liquid pump No. 1; 592. Conduit No. 2; 593. Nozzle; 594. Limiting plate; 61. Liquid extraction pipe; 62. Liquid pump No. 2; 63. Discharge pipe; 64. Fixed cover; 65. Sampling cylinder; 66. Fixed frame. Detailed Implementation

[0017] The technical solution of this utility model will be clearly and completely described below with reference to the accompanying drawings. In addition, the forms of the various structures described in the following embodiments are merely illustrative. The 9-decenol processing reactor involved in this utility model is not limited to the structures described in the following embodiments. All other embodiments obtained by those skilled in the art without creative effort are within the scope of protection of this utility model.

[0018] Example 1:

[0019] like Figure 1-2As shown, a reactor for processing 9-decenol includes a reactor body 1. A mixing mechanism 5 is provided inside the reactor body 1. The mixing mechanism 5 includes a first connecting shaft 52, which is disposed inside the reactor body 1. A first stirring frame 53 is fixedly connected to the upper sides of both sides of the first connecting shaft 52. A first stirring rod 54 is fixedly connected to the inner wall of the first stirring frame 53. A first motor 51 is fixedly installed at the middle of the top of the reactor body 1. The output end of the first motor 51 extends into the reactor body 1 and is fixedly connected to the top of the first connecting shaft 52. A limit plate 594 is fixedly connected to the lower part of the interior of the reactor body 1. The bottom end of the first connecting shaft 52 is rotatably mounted on the top of the limit plate 594 via a bearing. A second motor 55 is fixedly installed at the middle of the bottom of the reactor body 1. The output end of the second motor 55 extends into the reactor body 1 and is fixedly connected to a second connecting shaft 56. The top end of the second connecting shaft 56 is rotatably mounted on the top of the limit plate 594 via a bearing. At the bottom of the limiting plate 594, a second stirring frame 57 is fixedly connected to both sides of the second connecting shaft 56. A second stirring rod 58 is fixedly connected to the inner wall of the second stirring frame 57. The second stirring frame 57 is located below the outside of the first stirring frame 53. A first conduit 59 is fixedly connected to the lower sides of both sides of the reactor body 1. A first solenoid valve is installed on the first conduit 59. One end of the first conduit 59 extends into the interior of the reactor body 1. A first liquid pump 591 is fixedly connected to the lower sides of both sides of the reactor body 1. The other end of the first conduit 59 is fixedly installed at the input end of the first liquid pump 591. A second conduit 592 is fixedly connected to the output end of the first liquid pump 591. One end of the second conduit 592 extends into the upper interior of the reactor body 1 and is fixedly connected to a nozzle 593. A feed inlet 2 is provided on the left side of the top of the reactor body 1. A discharge pipe 3 is fixedly connected to the bottom of the reactor body 1. The discharge pipe 3 is located to the left of the second motor 55. A discharge valve 4 is installed on the discharge pipe 3.

[0020] In this embodiment, the output of motor 51 drives the first connecting shaft 52, the first stirring frame 53, and the first stirring rod 54 to rotate clockwise, facilitating clockwise stirring of 9-decenol. The output of motor 55 drives the second connecting shaft 56, the second stirring frame 57, and the second stirring rod 58 to rotate counterclockwise, facilitating counterclockwise stirring of 9-decenol. Simultaneous clockwise and counterclockwise stirring of 9-decenol improves mixing efficiency. The cooperation of conduit 59, pump 591, conduit 592, and nozzle 593 facilitates the extraction of 9-decenol from the lower part of the reactor body 1 and its discharge into the upper part of the reactor body, ensuring thorough stirring of 9-decenol. The inlet 2 facilitates the addition of 9-decenol into the reactor body 1. The discharge pipe 3 and discharge valve 4 facilitate the discharge of 9-decenol after reaction processing.

[0021] Example 2:

[0022] like Figure 1-2 As shown, a sampling mechanism 6 is provided on the upper side of one side of the reactor body 1. The sampling mechanism 6 includes a fixed cover 64, a sampling cylinder 65 is threadedly connected to the lower part of the fixed cover 64, a fixed bracket 66 is fixedly connected to the left side of the fixed cover 64, and one side of the fixed bracket 66 is fixedly connected to the upper right side of the reactor body 1. A liquid extraction pipe 61 is fixedly connected to the right side of the top of the reactor body 1. A second solenoid valve is installed on the liquid extraction pipe 61. The bottom end of the liquid extraction pipe 61 extends to the right side of the interior of the reactor body 1. A second liquid extraction pump 62 is fixedly installed on the right side of the top of the reactor body 1. The top end of the liquid extraction pipe 61 is fixedly connected to the input end of the second liquid extraction pump 62. A drain pipe 63 is fixedly connected to the output end of the second liquid extraction pump 62. One end of the drain pipe 63 is fixedly connected to the middle of the top of the fixed cover 64.

[0023] In this embodiment, the fixing bracket 66 facilitates the fixing of the cover 64 to be fixedly installed on the upper side of one side of the reactor body 1. The 9-decenol inside the reactor is easily drawn into the sampling tube 65 for sampling through the cooperation of the suction pipe 61, the second suction pump 62 and the discharge pipe 63. Since the sampling tube 65 and the fixing cover 64 are connected by threads, the sampling tube 65 is easy to disassemble and assemble. The 9-decenol inside the sampling tube 65 is used to detect the progress and quality of the reaction process. The sampling tube 65 is made of transparent plastic, which makes it convenient for the staff to observe the 9-decenol inside the sampling tube 65 when taking samples.

[0024] In summary, as Figure 1-2 As shown, this is a reaction vessel for processing 9-decenol. When 9-decenol is reacted inside the reaction vessel body 1, the power is turned on, and the output of the first motor 51 is controlled by the switch to drive the first connecting shaft 52, the first stirring rack 53, and the first stirring rod 54 to rotate clockwise, stirring the 9-decenol. The output of the second motor 55 drives the second connecting shaft 56, the second stirring rack 57, and the second stirring rod 58 to rotate counterclockwise, stirring the 9-decenol. Then, the first solenoid valve and the first pump 591 are turned on, and the first conduit 59 and the first pump 591 draw liquid from the lower part of the reaction vessel body 1. 9-Decanol is discharged into the upper part of the reactor body through conduit 592 and nozzle 593, facilitating thorough stirring of 9-decenol. If sampling is required, solenoid valve 2 and pump 62 2 can be opened. 9-decenol from the reactor body 1 is drawn into sampling cylinder 65 through pump 61, pump 62 2, and discharge pipe 63. 9-decenol is collected and sampled using sampling cylinder 65. Then, solenoid valve 2 and pump 62 2 are closed, and the top of sampling cylinder 65 is screwed off from the bottom of fixed cover 64. The progress and quality of the reaction process can then be detected by measuring 9-decenol inside sampling cylinder 65.

[0025] Finally, the following points should be noted: First, in the description of this application, it should be noted that, unless otherwise specified and limited, the terms "installation", "connection", and "linkage" should be interpreted broadly, and can be mechanical or electrical connections, or internal connections between two components, or direct connections. "Up", "down", "left", "right", etc. are only used to indicate relative positional relationships. When the absolute position of the described object changes, the relative positional relationship may change.

[0026] Secondly: The accompanying drawings of the embodiments disclosed in this utility model only involve the structures involved in the embodiments disclosed in this utility model. Other structures can refer to the general design. In the absence of conflict, the same embodiment and different embodiments of this utility model can be combined with each other.

[0027] Finally: The above description is only a preferred embodiment of the present utility model and is not intended to limit the present utility model. Any modifications, equivalent substitutions, improvements, etc., made within the spirit and principles of the present utility model should be included within the protection scope of the present utility model.

Claims

1. A reaction vessel for 9-decenol processing, comprising a reaction vessel body (1), characterized in that, The inside of the reaction kettle body (1) is internally provided with a mixing mechanism (5), the mixing mechanism (5) comprises a first connecting shaft (52), the first connecting shaft (52) is arranged inside the reaction kettle body (1), a first stirring frame (53) is fixedly connected to the upper side of the two sides of the first connecting shaft (52), a first stirring rod (54) is fixedly connected to the inner wall of the first stirring frame (53), a first conduit (59) is fixedly connected to the lower side of the two sides of the reaction kettle body (1), a first electromagnetic valve is installed on the first conduit (59), one end of the first conduit (59) extends to the inside of the reaction kettle body (1), a first liquid pump (591) is fixedly connected to the lower side of the two sides of the reaction kettle body (1), the other end of the first conduit (59) is fixedly installed on the input end of the first liquid pump (591), a sampling mechanism (6) is arranged on the upper side of one side of the reaction kettle body (1), the sampling mechanism (6) comprises a fixed cover (64), a sampling cylinder (65) is threadedly sleeved on the lower side of the fixed cover (64), a fixed frame (66) is fixedly connected to the left side of the fixed cover (64), one side of the fixed frame (66) is fixedly connected to the upper side of the right side of the reaction kettle body (1).

2. The reaction kettle for processing 9-decenol according to claim 1, characterized in that: A first motor (51) is fixedly installed on the middle of the top of the reaction kettle body (1), the output end of the first motor (51) extends to the inside of the reaction kettle body (1) and is fixedly connected to the top end of the first connecting shaft (52), a limiting plate (594) is fixedly connected to the lower side of the inside of the reaction kettle body (1), and the bottom end of the first connecting shaft (52) is rotatably installed on the top of the limiting plate (594) through a bearing.

3. The reaction kettle for processing 9-decenol according to claim 1, characterized in that: A second motor (55) is fixedly installed on the middle of the bottom of the reaction kettle body (1), the output end of the second motor (55) extends to the inside of the reaction kettle body (1) and is fixedly connected to a second connecting shaft (56), the top end of the second connecting shaft (56) is rotatably installed on the bottom of the limiting plate (594) through a bearing, and second stirring frames (57) are fixedly connected to the two sides of the second connecting shaft (56), second stirring rods (58) are fixedly connected to the inner walls of the second stirring frames (57), and the second stirring frames (57) are arranged below the first stirring frame (53) outside.

4. The reaction kettle for processing 9-decenol according to claim 1, characterized in that: A second conduit (592) is fixedly connected to the output end of the first liquid pump (591), one end of the second conduit (592) extends to the upper side of the inside of the reaction kettle body (1) and is fixedly connected to a spray head (593).

5. The reaction kettle for processing 9-decenol according to claim 1, characterized in that: The right side of the top of the reactor body (1) is fixedly connected with a liquid pumping pipe (61), a second electromagnetic valve is installed on the liquid pumping pipe (61), the bottom end of the liquid pumping pipe (61) extends to the right side inside the reactor body (1), a second liquid pumping pump (62) is fixedly installed on the right side of the top of the reactor body (1), the top end of the liquid pumping pipe (61) is fixedly connected with the input end of the second liquid pumping pump (62), the output end of the second liquid pumping pump (62) is fixedly connected with a liquid discharging pipe (63), one end of the liquid discharging pipe (63) is fixedly connected with the middle of the top of a fixed cover (64).

6. The reaction kettle for processing 9-decenol according to claim 1, characterized in that: The left side of the top of the reactor body (1) is provided with a feeding port (2), the bottom of the reactor body (1) is fixedly connected with a discharging pipe (3), the discharging pipe (3) is located on the left side of the second motor (55), a discharging valve (4) is installed on the discharging pipe (3).

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