Transesterification grease treatment device

Abstract

The utility model relates to the technical field of deep processing of grease, in particular to a transesterification grease treatment device which comprises a separation device and a vacuum heating device, a funnel is arranged at a top inlet of the separation device and penetrates through the separation device, and the lower end of the funnel is suspended; a first outlet and a second outlet are formed in the side wall of the separation device, and the separation device is connected with a vacuum heating device through the first outlet; a heating structure, a third outlet and a fourth outlet are arranged in the vacuum heating device, and the third outlet and the fourth outlet are arranged on the side wall of the vacuum heating device. According to different conditions of the oil-water separation layer, the flowing-out position of the grease can be accurately adjusted, the oil-water separation accuracy is improved, meanwhile, impurities such as water and methyl alcohol in the grease are effectively removed, and the purity of the grease is remarkably improved.

Description

TECHNICAL FIELD

[0001] The utility model relates to oil and fat deep processing technical field, concretely relates to an ester exchange oil and fat treatment device. BACKGROUND

[0002] In the existing oil and fat ester exchange process, sodium methoxide is widely used as an alkaline catalyst due to its high catalytic efficiency and mild reaction conditions. Traditional processes usually use an acidic aqueous solution as a reaction terminator, such as a 10% citric acid aqueous solution, to neutralize the alkaline catalyst and terminate the reaction. In the subsequent purification stage, multiple water washing operations are required, including adding excess pure water for mixing and shaking to dissolve residual catalyst and by-products, followed by static separation and filtration of the aqueous phase.

[0003] However, this process has the following technical defects: (1) the large interfacial tension between oil and water results in low separation efficiency, requiring extended static time or increased centrifugal assistance, significantly reducing production efficiency; (2) multiple water washing processes can form stable emulsions, increasing product loss; (3) it is difficult to completely remove dissolved monoglycerides, diglycerides, and other by-products in the aqueous phase, and trace amounts of sodium ions and citrate may cause oil oxidation deterioration; (4) a large amount of organic wastewater is generated during the treatment process, increasing the cost of subsequent water treatment. These problems collectively result in technical bottlenecks such as insufficient purity (usually less than 98.5%), dark color, and poor storage stability of the final product, making it difficult to meet the quality requirements of ester exchange oil and fat in high-end food and cosmetic fields. SUMMARY

[0004] To overcome the shortcomings of the prior art, the present application provides an ester exchange oil and fat treatment device, aiming to simplify the ester exchange oil and fat treatment steps and improve the purity of ester exchange oil and fat.

[0005] The technical means adopted by the utility model to solve its technical problems is: an ester exchange oil and fat treatment device, which is improved in that it comprises a separation device and a vacuum heating device; a hopper is provided at the top inlet of the separation device, the hopper is throughly arranged in the separation device and the lower end is suspended; a first outlet and a second outlet are provided on the side wall of the separation device, the separation device is connected with the vacuum heating device through the first outlet; a heating structure is arranged in the vacuum heating device, and a third outlet and a fourth outlet are provided on the side wall of the vacuum heating device.

[0006] In the above technical solution, the lower end of the hopper is provided with a spiral flow guide structure, the flow guide structure comprises a tapered propeller flow guide surface with an outer diameter gradually tapering from top to bottom, the taper angle is 15-30 degrees, and the flow guide surface is provided with staggered protruding flow guide teeth.

[0007] The first outlet is located at the upper part of the separation device, and the second outlet is located at the lower part of the separation device; the first adjustable baffle is arranged at the first outlet, and is used for adjusting the position of the flow of the coarsely separated ester-exchanged oil.

[0008] The third outlet is located at the upper part of the vacuum heating device, and the fourth outlet is located at the lower part of the vacuum heating device; the second adjustable baffle is arranged in the vacuum heating device, and is arranged at the top end of the heating structure, and is used for isolating the coarsely separated ester-exchanged oil from the heating structure.

[0009] The separation device further comprises a detachable filter screen assembly, which is arranged between the suspended section at the lower end of the funnel and the inner wall of the separation device.

[0010] The second adjustable baffle is a porous structure, and the porous structure is used for uniformly passing the coarsely separated ester-exchanged oil through the baffle and the heating structure for heat exchange.

[0011] The heating structure is in a wave shape.

[0012] The second outlet, the third outlet and the fourth outlet are all provided with plugs.

[0013] The beneficial effects of the present application are as follows:

[0014] Flexible oil-water separation: the first outlet of the separation device is provided with an adjustable baffle, which can accurately adjust the position of the flow of oil according to different conditions of the oil-water separation layer, not only improves the accuracy of oil-water separation, but also enhances the adaptability of the device, so that it can cope with various oil processing needs;

[0015] Efficient purification means: the wave-shaped heating device in the vacuum heating device is combined with the second adjustable baffle to form an efficient oil purification system. By opening the second adjustable baffle, the coarsely separated ester-exchanged oil can flow down along the wave-shaped lines, and the third outlet is used for vacuum heating to make water and methanol gasify and discharge. Not only the water and methanol impurities in the oil are effectively removed, but also the purity of the oil is significantly improved. BRIEF DESCRIPTION OF DRAWINGS

[0016] Figure 1 The structure of the ester-exchanged oil processing device is shown in the embodiment of the present application.

[0017] Figure 2 The propeller guide surface is shown in the embodiment of the present application. DETAILED DESCRIPTION

[0018] The utility model is further illustrated below in combination with the drawings and embodiments.

[0019] The utility model discloses the conception, specific structure and the technical effect produced will be clearly and completely described below in combination with the embodiments and drawings, to fully understand the purpose, features and effects of the utility model. Obviously, the described embodiment is only a part of the embodiment of the utility model, and not all embodiments, based on the embodiment of the utility model, the other embodiments obtained by the skilled in the art without paying creative labor all belong to the protection scope of the utility model. In addition, all the connection / connection relations involved in the patent do not mean that the components directly connect, but can form a better connection structure by adding or reducing the connection auxiliary parts according to the specific implementation situation. The various technical features in the utility model creation can be interactively combined under the premise of not mutually contradictory conflict.

[0020] As Figure 1 The utility model provides an ester exchange oil and fat treatment device, including separation device 1 and vacuum heating device 2, the separation device 1 top entrance is provided with a hopper 11, the hopper 11 is through being provided in separation device 1 and the lower end is suspended, the side wall of separation device 1 is provided with first outlet 12 and second outlet 13, and the separation device 1 is connected with vacuum heating device 2 through first outlet 11, and the vacuum heating device 2 is provided with heating structure 21, and the third outlet 22 and fourth outlet 23 are provided in the side wall of vacuum heating device 2.

[0021] In a possible implementation manner, as Figure 2 The lower end of the hopper 11 is provided with a spiral flow guide structure 14, the flow guide structure 14 includes a tapered propeller flow guide surface 15 formed by gradually tapering from top to bottom, the taper angle is 15-30 degrees, and the flow guide surface 15 is provided with staggered distribution protruding flow guide teeth.

[0022] Hot water is injected from the hopper 11 to drive the spiral flow guide structure 14 to rotate, and the hot water is stirred into the oil and fat mixture after ester exchange is completed, so that it is fully mixed and cleaned, and the specific angle tapered flow guide + flow guide tooth innovative design enhances the material distribution effect.

[0023] In a possible implementation manner, the first outlet 12 is located at the upper part of the separation device 1, and the second outlet 13 is located at the lower part of the separation device 1; the first adjustable baffle 16 is arranged at the first outlet 12 for adjusting the position of the rough separation ester exchange oil and fat outflow.

[0024] By the continuous increase of hot water, water can be discharged through the second outlet 12, the water solution can be diluted, and the grease can flow out of the first outlet 12 to the vacuum heating device 2 to realize oil-water separation; the first adjustable baffle 16 is used to cope with different oil-water separation layers, the position of the grease outflow is adjusted, and the effects of separating water and grease are achieved.

[0025] In a possible implementation, the third outlet 22 is located at the upper part of the vacuum heating device 2, and the fourth outlet 23 is located at the lower part of the vacuum heating device 2; the second adjustable baffle 24 is arranged in the vacuum heating device 2 and is arranged at the top end of the heating structure and used for isolating the coarsely separated interesterified grease from the heating structure.

[0026] The second adjustable baffle 24 is opened to allow the coarsely separated interesterified grease to flow down along the heating structure 21, and the interesterified grease carrying water and methanol and other substances is extracted through the third outlet by vacuum heating, so that the water and methanol substances are discharged by gasification, thereby achieving the purpose of purifying the grease.

[0027] Optionally, the heating structure is in a wave shape. The wave-shaped heating structure can significantly increase the contact area with the grease. This means that under the same heating power, the wave-shaped heating structure can quickly transfer heat to the grease, thereby improving the heat exchange efficiency.

[0028] In a possible implementation, the separation device 1 further comprises a detachable filter screen assembly arranged between the suspended section at the lower end of the funnel and the inner wall of the separation device and used for preliminarily filtering large-particle impurities in the interesterified grease entering the separation device 1, thereby improving the efficiency and effect of subsequent processing.

[0029] In a possible implementation, the second adjustable baffle 24 is in a porous structure, and the porous structure is used for uniformly passing the coarsely separated interesterified grease through the baffle to exchange heat with the heating structure.

[0030] In a possible implementation, the second outlet 13, the third outlet 22, and the fourth outlet 23 are each provided with a plug 25.

[0031] The rotation of the plug 25 controls the alignment or misalignment of the opening and the fluid passage to control the flow of the fluid, which can effectively prevent fluid leakage and ensure the safety and stability of the system; meanwhile, the flow of the fluid can be controlled, and the working efficiency is greatly improved.

[0032] The above is a specific description of the preferred implementation of the present application, but the present application is not limited to the embodiments described above. Those skilled in the art can make various equivalent modifications or replacements without departing from the spirit of the present application. These equivalent modifications or replacements are all included in the scope defined by the claims of the present application.

Claims

1. A transesterified oil and fat treatment device, characterized by comprising: The device comprises a separating device and a vacuum heating device; a hopper is arranged on the top inlet of the separating device, the hopper is arranged through the separating device and the lower end is suspended; a first outlet and a second outlet are arranged on the sidewall of the separating device, the separating device is connected with the vacuum heating device through the first outlet; a heating structure is arranged in the vacuum heating device, and a third outlet and a fourth outlet are arranged on the sidewall of the vacuum heating device.

2. The transesterification fat treating apparatus according to claim 1, wherein The suspended section of the lower end of the hopper is provided with a spiral flow guide structure, the flow guide structure comprises a tapered propeller flow guide surface with a gradually reduced outer diameter from top to bottom, the taper angle is 15-30 degrees, and the flow guide surface is provided with staggered distribution of convex flow guide teeth.

3. The transesterification oil treatment apparatus according to claim 1, wherein The first outlet is located on the upper part of the separating device, and the second outlet is located on the lower part of the separating device; a first adjustable baffle is arranged at the first outlet, which is used for adjusting the position of the rough separation of the ester exchange oil and fat.

4. The transesterification fat treating apparatus according to claim 3, wherein The third outlet is located on the upper part of the vacuum heating device, and the fourth outlet is located on the lower part of the vacuum heating device; a second adjustable baffle is arranged in the vacuum heating device, the second adjustable baffle is arranged on the top end of the heating structure, which is used for isolating the rough separation of the ester exchange oil and fat from the heating structure.

5. The transesterification fat treating apparatus according to claim 1, wherein The separating device further comprises a detachable filter screen assembly, which is arranged between the suspended section of the lower end of the hopper and the inner wall of the separating device.

6. The transesterification fat treating apparatus according to claim 4, wherein The second adjustable baffle is a porous structure, which is used for making the rough separation of the ester exchange oil and fat uniformly pass through the baffle and the heating structure for heat exchange.

7. The transesterification fat treating apparatus according to claim 1, wherein The heating structure is in a wave shape.

8. The transesterification fat treating apparatus according to claim 1, wherein A plug is arranged at the second outlet, the third outlet and the fourth outlet.

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