Wet-process multi-stage internal circulation purification equipment

By designing a wet multi-stage internal circulation purification device, the problems of inconvenient electrolyte purification and loading/unloading in nickel alloy electrolysis equipment were solved, realizing multi-stage purification and efficient production of electrolyte.

CN223974235UActive Publication Date: 2026-03-06TONGCHUAN HUAYAODA TECHNOLOGY CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2025-03-13
Publication Date
2026-03-06

AI Technical Summary

Technical Problem

Existing nickel alloy electrolysis equipment cannot effectively purify electrolytes that have been used multiple times, leading to the accumulation of impurities that affect the electroplating effect. Furthermore, the inconvenience of loading and unloading materials reduces production efficiency.

Method used

A wet multi-stage internal circulation purification device was designed, comprising a U-shaped support, a purification tank, an electrolysis tank, a lifting plate, and a lifting mechanism. Multi-stage purification and circulation of the electrolyte are achieved through overflow, a filter pump, and an ion exchanger. Combined with anode plates and cathode rods, the electrolyte is purified efficiently, thereby improving production efficiency.

Benefits of technology

This technology enables multi-stage purification of the electrolyte, improves the quality of nickel-based alloy products, simplifies loading and unloading operations, and increases production efficiency.

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Abstract

The utility model discloses wet-process multi-stage internal circulation purification equipment which comprises a [-shaped bracket, a purification box is fixedly connected to the [-shaped bracket, an electrolysis box is fixedly connected to the top of the [-shaped bracket, three lifting plates are arranged above the electrolysis box, placing frames are arranged at the bottoms of the three lifting plates, and the left side and the right side of the electrolysis box are respectively provided with a water inlet and a water outlet. Three lifting mechanisms are arranged on the [-shaped bracket; the lifting mechanism comprises a mounting box fixedly connected to the n-shaped support, and two symmetrically-distributed fixing cylinders are connected to the top of the mounting box in a penetrating mode. According to the wet-process multi-stage internal circulation purification equipment, multiple purification can be conveniently conducted on electrolyte in the electrolysis box through the purification box arranged below the electrolysis box, meanwhile, the placement frame can be conveniently lifted out of the electrolysis box through the arranged lifting mechanism, feeding and discharging are convenient, and therefore the overall production efficiency is improved.
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Description

Technical Field

[0001] This utility model relates to the field of nickel-based alloy production technology, specifically a wet multi-stage internal circulation purification device. Background Technology

[0002] Nickel alloys are alloys composed of nickel as the base and other elements. Nickel has good mechanical, physical and chemical properties. Adding appropriate elements can improve its oxidation resistance, corrosion resistance, high temperature strength and some physical properties. Nickel alloys can be used as materials for electron tubes, precision alloys (magnetic alloys, precision resistance alloys, electrothermal alloys, etc.), nickel-based high-temperature alloys, nickel-based corrosion-resistant alloys and shape memory alloys, etc. Nickel-based alloys need to be electrolyzed during production.

[0003] Publication No. CN 220450344 U discloses an electrolytic cell for zinc-nickel alloy rack plating, including a fixed base. An electrolytic cell is fixedly installed in the middle of the fixed base. Hydraulic rods are installed on both sides of the top of the fixed base. A movable base is fixedly connected to the top of the two hydraulic rods. A connecting base is fixedly connected to the bottom of the movable base. The connecting base matches the size of the electrolytic cell. Multiple rack plating rods are fixedly installed at the bottom of the connecting base. A purification mechanism for purifying harmful gases generated by the electrolytic cell is installed on the top of the movable base. The top of the electrolytic cell is sealed by a sealing ring inside the sealing groove, so that the gas will not overflow during electrolysis. It can also prevent electrolyte solution from splashing when the workpiece is placed into the electrolytic cell, reducing safety hazards. The gas generated during electrolysis is introduced into a storage tank by an air pump. After being purified by a filter plate, an activated carbon layer and the corresponding liquid in the storage tank, the harmful gases are purified, reducing air pollution during electrolysis and reducing the harm of harmful gases to workers.

[0004] However, this electrolysis device has the following shortcomings: while it can electroplate nickel alloys, it often cannot purify the electrolyte after repeated use, resulting in a large number of impurities that affect the electroplating effect on nickel alloys. In addition, it is inconvenient to load and unload nickel-based alloys during use, which affects the overall production efficiency.

[0005] Therefore, this utility model provides a wet multi-stage internal circulation purification device to solve the above problems. Utility Model Content

[0006] To address the shortcomings of existing technologies, this invention provides a wet multi-stage internal circulation purification device, which solves the aforementioned problems.

[0007] To achieve the above objectives, this utility model is implemented through the following technical solution: a wet multi-stage internal circulation purification device, including a C-shaped support, a purification box fixedly connected to the C-shaped support, an electrolysis box fixedly connected to the top of the C-shaped support, three lifting plates arranged above the electrolysis box, a placement rack arranged at the bottom of each of the three lifting plates, and three lifting mechanisms arranged on the C-shaped support;

[0008] The lifting mechanism includes a mounting box fixedly connected to a U-shaped bracket. Two symmetrically distributed fixed cylinders are connected through the top of the mounting box. A threaded rod is rotatably connected through the bottom inner wall of each fixed cylinder. A telescopic sleeve is threaded onto each of the two threaded rods. The top of the telescopic sleeve slides out of the fixed cylinder and is connected to a corresponding lifting plate. A driven bevel gear is fixedly connected to the bottom end of the threaded rod. A drive motor is fixedly connected to one outer wall of the mounting box. A transmission shaft is fixedly connected to the output shaft of the drive motor. One end of the transmission shaft rotatably extends into the mounting box. A driving bevel gear is fixedly fitted onto the transmission shaft. The two driving bevel gears mesh with their corresponding driven bevel gears.

[0009] Preferably, multiple partitions are fixedly connected inside the electrolytic tank, and multiple permeation holes are opened on the partitions. A polymer membrane cloth is provided on the partitions, and multiple titanium baskets are provided inside the electrolytic tank. The multiple titanium baskets and multiple partitions are alternately distributed. By using the partitions, permeation holes, polymer membrane cloth and titanium baskets in combination, nickel-based products can be easily electroplated.

[0010] Preferably, six anode plates are fixedly connected inside the U-shaped bracket, and multiple communication ports are opened on the three corresponding anode plates. Multiple cathode rods are fixedly connected inside the purification box. The combination of the anode plates, communication ports and cathode rods can facilitate the purification of the electrolysis box.

[0011] Preferably, an overflow bend is connected to the outside of one side of the electrolysis tank, and multiple infusion pipes are connected to the overflow bend. A switch valve is fixedly connected to each infusion pipe. The overflow bend, infusion pipes and switch valve are used in combination to facilitate the overflow of electrolyte in the electrolysis tank into the purification tank.

[0012] Preferably, a filter pump is fixedly connected to the C-shaped bracket, and a return pipe is fixedly connected to the inlet end of the filter pump. One end of the return pipe extends into the purification tank. The combination of the filter pump and the return pipe facilitates the delivery of electrolyte.

[0013] Preferably, an ion exchanger is fixedly connected to the U-shaped support. The inlet of the ion exchanger is connected to the outlet of the filter pump. A circulation pipe is fixedly connected to the outlet of the ion exchanger. One end of the circulation pipe extends into the electrolysis tank. A flow valve is fixedly connected to the circulation pipe. By using the ion exchanger, circulation pipe and flow valve together, the purified electrolyte can be easily returned to the electrolysis tank.

[0014] Preferably, the outer wall of the fixed cylinder has a limiting port, and the outer wall of the telescopic sleeve is fixedly connected with a stop bar. One end of the stop bar slides through the corresponding limiting port. By using the limiting port and the stop bar together, the telescopic sleeve can be limited, making its movement smoother.

[0015] Beneficial effects

[0016] This invention provides a wet multi-stage internal circulation purification device. Compared with the prior art, it has the following advantages:

[0017] (1) The wet multi-stage internal circulation purification equipment can easily perform multiple purifications of the electrolyte in the electrolysis tank through the purification tank set below the electrolysis tank. At the same time, the lifting mechanism can easily lift the placement rack out of the electrolysis tank, which is convenient for loading and unloading, thereby improving the overall production efficiency.

[0018] (2) The wet multi-stage internal circulation purification equipment can facilitate the overflow of electrolyte in the electrolysis tank to the purification tank for purification and impurity removal through the overflow pipe, and then return it to the electrolysis tank through the filter pump to achieve the effect of circulation purification and effectively improve the product quality of nickel-based alloys. Attached Figure Description

[0019] Figure 1 This is a perspective view of the external structure of this utility model;

[0020] Figure 2 This is a partial cross-sectional view of the lifting mechanism in this utility model;

[0021] Figure 3 This is a top view of the purification box in this utility model.

[0022] Figure 4 This is a side view of the structure of this utility model.

[0023] In the diagram: 1. C-shaped support; 2. Purification box; 3. Electrolysis box; 4. Lifting plate; 5. Placement rack; 6. Mounting box; 7. Fixing cylinder; 8. Threaded rod; 9. Telescopic sleeve; 10. Driven bevel gear; 11. Drive motor; 12. Transmission shaft; 13. Driving bevel gear; 14. Partition plate; 15. Permeation hole; 16. Polymer diaphragm cloth; 17. Titanium basket; 18. Anode plate; 19. Connecting port; 20. Cathode rod; 21. Overflow bend; 22. Infusion pipe; 23. Switch valve; 24. Filter pump; 25. Return pipe; 26. Ion exchanger; 27. Circulation pipe; 28. Flow valve; 29. ​​Limiting port; 30. Stop bar. Detailed Implementation

[0024] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0025] Example 1:

[0026] Please see Figure 1 and Figure 2 A wet multi-stage internal circulation purification device includes an inverted bracket 1, a purification box 2 fixedly connected to the inverted bracket 1, and an electrolysis box 3 fixedly connected to the top of the inverted bracket 1. Both the purification box 2 and the electrolysis box 3 are made of acid and alkali resistant polymer materials. Three lifting plates 4 are provided above the electrolysis box 3, and a placement rack 5 is provided at the bottom of each of the three lifting plates 4. The placement rack 5 can be connected to the lifting plates 4 by hoisting or other detachable connection methods. Three lifting mechanisms are provided on the inverted bracket 1.

[0027] The lifting mechanism includes a mounting box 6 fixedly connected to a U-shaped bracket 1. Two symmetrically distributed fixed cylinders 7 are connected through the top of the mounting box 6. Threaded rods 8 are rotatably connected through the inner bottom wall of the fixed cylinders 7. Telescopic sleeves 9 are threadedly fitted on both threaded rods 8. The top of the telescopic sleeves 9 slides out of the fixed cylinders 7 and is connected to the corresponding lifting plate 4. A driven bevel gear 10 is fixedly connected to the bottom end of the threaded rods 8. A drive motor 11 is fixedly connected to one outer wall of the mounting box 6. A transmission shaft 12 is fixedly connected to the output shaft of the drive motor 11. One end of the transmission shaft 12 rotatably extends into the mounting box 6. An active bevel gear 13 is fixedly fitted on the transmission shaft 12. The two active bevel gears 13 mesh with the corresponding driven bevel gears 10.

[0028] Example 2:

[0029] Please see Figures 1 to 4 This embodiment provides a technical solution based on Embodiment 1: Multiple partitions 14 are fixedly connected inside the electrolysis tank 3. Multiple seepage holes 15 are opened on the partitions 14, and a polymer membrane cloth 16 is provided on the partitions 14. Multiple titanium baskets 17 are arranged inside the electrolysis tank 3, with the titanium baskets 17 and partitions 14 alternating. Six anode plates 18 are fixedly connected inside the U-shaped support 1. There is a height difference between each pair of adjacent anode plates 18, and multiple connecting ports 19 are opened on each of the three corresponding anode plates 18. Multiple cathode rods 20 are fixedly connected inside the purification tank 2. An overflow bend 21 is connected through one side of the electrolysis tank 3, and multiple infusion pipes 22 are connected through the overflow bend 21. A switch valve 23 is fixedly connected to the infusion tube 22; a filter pump 24 is fixedly connected to the C-shaped support 1, and a return pipe 25 is fixedly connected to the inlet end of the filter pump 24, with one end of the return pipe 25 extending into the purification tank 2; an ion exchanger 26 is fixedly connected to the C-shaped support 1, with the inlet end of the ion exchanger 26 connected to the outlet end of the filter pump 24, and a circulation pipe 27 is fixedly connected to the outlet end of the ion exchanger 26, with one end of the circulation pipe 27 extending into the electrolysis tank 3, and a flow valve 28 is fixedly connected to the circulation pipe 27; a limit port 29 is opened on the outer wall of the fixed cylinder 7, and a stop bar 30 is fixedly connected to the outer wall of the telescopic sleeve 9, with one end of the stop bar 30 sliding through the corresponding limit port 29.

[0030] Furthermore, any content not described in detail in this specification is existing technology known to those skilled in the art.

[0031] Working principle: During use, the operator places the nickel-based alloy product to be electroplated in the placement rack 5, then hoists it to the bottom of the lifting plate 4. The drive motor 11 is then started, which drives two active bevel gears 13 to rotate via the transmission shaft 12. The active bevel gears 13 drive the driven bevel gears 10 meshing with them to rotate, which in turn drives the connected threaded rod 8 to rotate. The threaded rod 8 drives the threaded telescopic sleeve 9, which is connected to it, to descend, causing the lifting plate 4 to descend until the nickel-based alloy in the placement rack 5 is immersed in the electrolyte. After the electroplating process is complete, the process is reversed to remove the product. Simultaneously, when purification of the electrolyte in the electrolysis tank 3 is required, the electrolyte in the electrolysis tank 3... The electrolyte overflows into the purification tank 2 through the overflow bend 21. At this time, the appropriate switch valve 23 is opened according to the corresponding purification requirements, so that the electrolyte in the overflow bend 21 enters the purification tank 2. The electrolyte enters the purification tank 2 through the infusion pipes 22 at different positions, and its flow path is different, so that it undergoes different degrees of purification. The electrolyte flows through the anode plates 18 at different heights and the connecting port 19 in the purification tank 2. At the same time, the anode plates 18 and the cathode rods 20 can purify it. Then, the filter pump 24 is started. The filter pump 24 delivers the purified electrolyte to the ion exchanger 26 through the return pipe 25, and then flows back to the electrolysis tank 3 through the circulation pipe 27 to complete the circulation.

[0032] It should be noted that, in this document, relational terms such as "first" and "second" are used only to distinguish one entity or operation from another, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Furthermore, the terms "comprising," "including," or any other variations thereof are intended to cover non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements includes not only those elements but also other elements not expressly listed, or elements inherent to such process, method, article, or apparatus.

[0033] In this description, it should also be noted that, unless otherwise explicitly specified and limited, the terms "set up," "install," "connect," and "link" should be interpreted broadly. For example, they can refer to fixed connections, detachable connections, or integral connections; they can refer to mechanical connections or electrical connections; they can refer to direct connections or connections through an intermediate medium; and they can refer to the internal communication between two components. Those skilled in the art can understand the specific meaning of the above terms in this utility model according to the specific circumstances.

[0034] Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made to these embodiments without departing from the principles and spirit of the present invention, the scope of which is defined by the appended claims and their equivalents.

Claims

1. A wet multistage internal circulation purification apparatus comprising a box-type support (1), characterized in that: The -type bracket (1) is fixedly connected with a purification box (2), the top of the -type bracket (1) is fixedly connected with an electrolytic tank (3), the top of the electrolytic tank (3) is provided with three lifting plates (4), the bottom of the three lifting plates (4) is provided with a placing rack (5), and the -type bracket (1) is provided with three lifting mechanisms; The lifting mechanism comprises a mounting box (6) fixedly connected with the -type bracket (1), the top of the mounting box (6) is penetratingly connected with two symmetrical fixed cylinders (7), the bottom inner wall of the fixed cylinder (7) is rotatingly penetratingly connected with a threaded rod (8), the threaded rod (8) is threadedly sleeved with a telescopic sleeve (9), the top end of the telescopic sleeve (9) extends to the outside of the fixed cylinder (7), the top end of the telescopic sleeve (9) is connected with the corresponding lifting plate (4), the bottom end of the threaded rod (8) is fixedly connected with a driven bevel gear (10), one side outer wall of the mounting box (6) is fixedly connected with a driving motor (11), the output shaft of the driving motor (11) is fixedly connected with a transmission shaft (12), one end of the transmission shaft (12) extends into the mounting box (6), the transmission shaft (12) is fixedly sleeved with a driving bevel gear (13), and the two driving bevel gears (13) are meshed with the corresponding driven bevel gears (10).

2. A wet multi-stage internal circulation purification apparatus according to claim 1, characterized by: A plurality of partition plates (14) are fixedly connected in the electrolytic tank (3), a plurality of seepage holes (15) are formed in the partition plates (14), a high-molecular diaphragm cloth (16) is arranged on the partition plates (14), and a plurality of titanium baskets (17) are arranged in the electrolytic tank (3).

3. A wet multi-stage internal circulation purification apparatus according to claim 1, characterized by: Six anode plates (18) are fixedly connected in the -type bracket (1), a plurality of communication openings (19) are formed in the corresponding three anode plates (18), and a plurality of cathode rods (20) are fixedly connected in the purification box (2).

4. A wet multi-stage internal circulation purification apparatus according to claim 1, characterized by: A overflow elbow (21) is penetratingly connected to one side of the electrolytic tank (3), a plurality of infusion tubes (22) are penetratingly connected to the overflow elbow (21), and a switch valve (23) is fixedly connected to the infusion tube (22).

5. A wet multi-stage internal circulation purification apparatus according to claim 1, characterized by: A filter pump (24) is fixedly connected to the -type bracket (1), a backflow pipe (25) is fixedly connected to the water inlet end of the filter pump (24), and one end of the backflow pipe (25) extends into the purification box (2).

6. A wet multi-stage internal circulation purification apparatus according to claim 1, characterized by: An ion exchanger (26) is fixedly connected to the -type bracket (1), the water inlet end of the ion exchanger (26) is connected with the water outlet end of the filter pump (24), a circulating pipe (27) is fixedly connected to the water outlet end of the ion exchanger (26), one end of the circulating pipe (27) extends into the electrolytic tank (3), and a flow valve (28) is fixedly connected to the circulating pipe (27).

7. A wet multi-stage internal circulation purification apparatus according to claim 1, characterized by: Limiting openings (29) are formed in the outer wall of the fixed cylinder (7), and a stop rod (30) is fixedly connected to the outer wall of the telescopic sleeve (9).

Citation Information

Patent Citations

  • Zinc-nickel alloy rack plating wire electrolytic bath

    CN220450344U