Easy-to-clean reaction kettle for metal organic framework production

Abstract

The utility model discloses an easy-to-clean reaction kettle for metal organic framework production, which comprises a kettle body, a feeding pipe is fixedly mounted on the left side of the kettle body, a stirring component is arranged at the bottom of the kettle body, a scraper blade is arranged in the kettle body through the stirring component, a conveying component is arranged at the top of the kettle body, and the conveying component is connected with the feeding pipe. The top of the kettle body is provided with a U-shaped pipe through a conveying assembly, the U-shaped pipe is in sliding connection with the kettle body, the bottom of the U-shaped pipe is fixedly provided with an annular pipe, the bottom of the annular pipe is fixedly provided with a spray head, the top of the kettle body is fixedly provided with fixing frames, and the opposite surfaces of the fixing frames are provided with driving assemblies; a moving block is arranged in the fixing frame through a driving assembly. The double functions can effectively remove residues with various properties and different adhesion degrees, it is ensured that the inner wall of the kettle body can be cleaned, the cleaning quality is greatly improved, the spraying head height adjusting function is matched, pollution areas with different heights are comprehensively covered, and the whole cleaning process is efficient and orderly.

Description

TECHNICAL FIELD

[0001] The utility model relates to metal organic framework production technical field especially relates to an easy to clean's reation kettle for metal organic framework production. BACKGROUND

[0002] Metal organic framework is one-dimensional, two-dimensional or three-dimensional framework formed by metal atoms and organic bridging ligand through coordination bond, in the process of processing and producing metal organic framework, we need to put metal organic framework raw materials into the reaction kettle for processing, and the general understanding of the reaction kettle is the container with physical or chemical reaction, through the structure design and parameter configuration of the container, the heating, evaporation, cooling and low speed mixing function of process requirement are realized.

[0003] The existing reaction kettle in the process of using, because metal organic framework raw materials have certain adhesion, metal organic framework raw materials can be adhered to the inner wall of the reaction kettle, the traditional reaction kettle cleaning mode mainly relies on manual cleaning, however, manual cleaning is not only extremely low in efficiency, but also needs to consume a lot of manpower and time cost every time, part of the reaction kettle adopts simple high-pressure water flushing mode, the spray head is usually fixedly installed at a position, cannot be flexibly adjusted according to the pollution degree of different areas in the reaction kettle, so that the cleaning effect is greatly reduced, therefore, the utility model provides an easy-to-clean reaction kettle for metal organic framework production. UTILITY MODEL CONTENT

[0004] In view of the defects of the prior art, the utility model provides an easy-to-clean reaction kettle for metal organic framework production for solving the problems in the background art.

[0005] In order to achieve the above purpose, the utility model adopts the following technical scheme:

[0006] An easy-to-clean reaction kettle for metal organic framework production, including kettle body, the kettle body left side is fixedly installed with feed pipe, the kettle body bottom is provided with stirring assembly, the kettle body is provided with scraper through stirring assembly, the kettle body top is provided with conveying assembly, the kettle body top is provided with U type pipe through conveying assembly, the U type pipe is slidably connected with kettle body, the U type pipe bottom is fixedly installed with ring type pipe, the ring type pipe bottom is fixedly installed with spray head, the kettle body top is fixedly installed with fixed frame, the fixed frame opposite face is provided with drive assembly, the fixed frame is provided with moving block through drive assembly, the moving block is fixedly connected with U type pipe.

[0007] Preferably, the stirring assembly includes a rotary motor arranged at the bottom of the kettle body, the rotary motor output end is fixedly installed with a rotating shaft, the rotating shaft is fixedly connected with the scraper, and the rotating shaft surface is fixedly installed with a stirring rod.

[0008] Preferably, the conveying assembly comprises a storage tank arranged on the top of the kettle body, a conveying pump is fixedly installed on the top of the storage tank, a liquid suction pipe is fixedly installed on the bottom of the conveying pump, the bottom end of the liquid suction pipe extends into the storage tank, a hose is fixedly installed on the top of the conveying pump, and the hose is communicated with the U-shaped pipe.

[0009] Preferably, the driving assembly comprises support plates arranged on the opposite faces of the fixed frame, a double-shaft motor is fixedly installed on the top of the support plate, a first bevel gear is fixedly installed on the output end of the double-shaft motor, a second bevel gear is arranged in mesh with the surface of the first bevel gear, a screw rod is fixedly installed in the second bevel gear, the screw rod is rotatably connected with the fixed frame, and the screw rod is threadedly connected with the moving block.

[0010] Preferably, a discharging pipe is fixedly installed on the bottom of the kettle body, and the discharging pipe is provided with a control valve.

[0011] Preferably, support legs are fixedly installed on the bottom of the kettle body, and the number of the support legs is plural.

[0012] Preferably, the fixed frame is in the structure of a rectangular frame body, and the moving block is slidably connected with the inner wall of the fixed frame.

[0013] Compared with the prior art, the metal organic framework production reaction kettle is easy to clean, when the inner wall of the kettle body needs to be cleaned, the flushing liquid is conveyed into the U-shaped pipe through the conveying assembly, then into the ring-shaped pipe, and finally sprayed out from the spray head, so that the residues adhered to the inner wall of the kettle body are flushed, at the same time, the residues adhered to the inner wall of the kettle body are scraped off through the rotation of the scraper driven by the stirring assembly, and the moving block can move up and down along the fixed frame through the driving assembly, so that the U-shaped pipe, the ring-shaped pipe and the spray head move up and down, the height of the spray head can be adjusted, and the cleaning mode of multiple pipes at the same time can flush the residues through the spray head and scrape off the residues through the rotation of the scraper, the double effects can effectively remove residues of various properties and different adhesion degrees, ensure that the inner wall of the kettle body can be cleaned, greatly improve the cleaning quality, and guarantee that the production environment of the metal organic framework is pure, the height adjustment function of the spray head is matched, different height pollution areas are comprehensively covered, and the whole cleaning process is efficient and orderly. BRIEF DESCRIPTION OF DRAWINGS

[0014] Figure 1 It is a three-dimensional view of the utility model;

[0015] Figure 2 It is a front view of the utility model;

[0016] Figure 3 It is a local structure schematic view of the utility model;

[0017] Figure 4Another partial structure of the utility model is left sectional view.

[0018] In the figure: 1, kettle body;2, feed pipe;3, rotating motor;4, rotating shaft;5, stirring rod;6, scraper;7, storage box;8, suction tube;9, conveying pump;10, hose;11, U-shaped tube;12, ring type tube;13, spray head;14, fixed frame;15, support plate;16, double shaft motor;17, first bevel gear;18, second bevel gear;19, screw;20, moving block;21, blanking pipe;22, support leg. DETAILED DESCRIPTION

[0019] The technical scheme in the embodiments of the utility model will be apparently and completely described below with reference to the drawings in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, rather than all the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by those skilled in the art without creative labor fall within the protection scope of the utility model.

[0020] Refer to Figure 1-4The utility model provides a metal organic framework production easy to clean's reation kettle, including kettle body 1, the left side fixed mounting of kettle body 1 has feed pipe 2, kettle body 1 bottom is provided with stirring subassembly, the inside of kettle body 1 is provided with scraper 6 through stirring subassembly, kettle body 1 top is provided with conveying subassembly, kettle body 1 top is provided with U type pipe 11 through conveying subassembly, conveying subassembly includes the storage tank 7 of setting up in kettle body 1 top, the top fixed mounting of storage tank 7 has conveying pump 9, the bottom fixed mounting of conveying pump 9 has liquid suction tube 8, and liquid suction tube 8 bottom end extends to the inside of storage tank 7, the top fixed mounting of conveying pump 9 has hose 10, and hose 10 is linked with U type pipe 11, and storage tank 7 can prestore enough washing liquid, and conveying pump 9 provides stable power, and draws washing liquid from storage tank 7 through liquid suction tube 8, and the washing liquid is conveyed to U type pipe 11 through hose 10 quickly, ensures that washing liquid supplies continuously during the washing process, guarantees that cleaning work is uninterrupted, improves the cleaning efficiency, U type pipe 11 and kettle body 1 slidingly connect, the bottom fixed mounting of U type pipe 11 has ring type pipe 12, and ring type pipe 12 bottom is fixedly installed with the shower head 13, and kettle body 1 top is fixedly installed with the fixed frame 14, and the opposite surface of fixed frame 14 is provided with drive assembly, and the inside of fixed frame 14 is provided with moving block 20 through drive assembly, and fixed frame 14 is rectangular frame structure, and moving block 20 and fixed frame 14 inner wall slidingly connect, and moving block 20 is fixedly connected with U type pipe 11, and drive assembly includes the support plate 15 of setting up in the opposite surface of fixed frame 14, and the top fixed mounting of support plate 15 has double shaft motor 16, and the output fixed mounting of double shaft motor 16 has first bevel gear 17, and the surface engagement of first bevel gear 17 is provided with second bevel gear 18, and the inside fixed mounting of second bevel gear 18 has screw rod 19, and screw rod 19 and fixed frame 14 rotatably connect, and screw rod 19 and moving block 20 are threadedly connected, through the setting of drive assembly, it is convenient to provide driving force for the up and down of moving block 20, thereby it is convenient to adjust the height of shower head 13 subsequently, and the operator can control the position of shower head 13 accurately according to the actual pollution situation, and the serious area is washed with emphasis to the pollution, improves the cleaning pertinence and effect, and kettle body 1 bottom is fixedly installed with support leg 22, and the number of support leg 22 is multiple, when the utility model provides a metal organic framework production easy to clean's reation kettle, the inside wall of kettle body 1 needs to be cleaned, the washing liquid is conveyed to U type pipe 11 through conveying subassembly, then enters ring type pipe 12, and finally is sprayed from shower head 13, thereby the residual of the adhesion of the inside wall of kettle body 1 is washed, simultaneously, through stirring subassembly, scraper 6 is rotated, and the residual of the adhesion of the inside wall of kettle body 1 is scraped off, and through drive assembly, moving block 20 can move up and down along fixed frame 14, thereby U type pipe 11, ring type pipe 12, shower head 13 move up and down, can adjust the height of shower head 13, and the cleaning mode of many tubes all down, is washed to the residual through shower head 13 sprays the washing liquid, and the residual is scraped off using the rotation of scraper 6, and the dual effect can effectively remove the residual of various properties, different adhesion degree, ensures that the inside wall of kettle body 1 can be cleaned, greatly improves the quality of cleaning,The production environment of the metal organic framework is kept clean, and the height of the spray head 13 is adjusted to fully cover different height pollution areas, and the entire cleaning process is efficient and orderly.

[0021] Specifically, the stirring assembly includes a rotating motor 3 arranged at the bottom of the kettle body 1, a rotating shaft 4 fixedly installed at the output end of the rotating motor 3, a scraper 6 fixedly connected with the rotating shaft 4, and a stirring rod 5 fixedly installed on the surface of the rotating shaft 4. During the material reaction stage, the material in the kettle body 1 can be fully stirred, so that various raw materials required for the production of the metal organic framework are uniformly mixed, and the chemical reaction is promoted to proceed fully.

[0022] Specifically, a discharge pipe 21 is fixedly installed at the bottom of the kettle body 1, and a control valve is arranged on the discharge pipe 21. The control valve can completely close the discharge pipe 21 when no discharge is needed, effectively preventing the material from leaking from the kettle body 1 in an unplanned manner, ensuring the safety and cleanliness of the production environment, and reducing safety accidents, environmental pollution, and material waste that may be caused by material leakage.

[0023] The electrical components in this document are connected to the main controller and 220V mains, and the main controller can be a conventional known device such as a computer.

[0024] In use: raw materials are added to the kettle body 1 from the feed pipe 2, so that the raw materials react in the kettle body 1, and at the same time, the rotating motor 3 is used to rotate the rotating shaft 4, so that the stirring rod 5 rotates and stirs the raw materials. After the reaction is completed, the control valve on the discharge pipe 21 is opened, and the reacted raw materials are discharged from the discharge pipe 21. When the inner wall of the kettle body 1 needs to be cleaned, the flushing liquid in the storage tank 7 is conveyed from the liquid suction pipe 8 to the hose 10 through the conveying pump 9, and then enters the U-shaped pipe 11, and then enters the ring-shaped pipe 12, and finally is sprayed from the spray head 13, thereby flushing the residues adhered to the inner wall of the kettle body 1. At the same time, the rotating motor 3 is used to rotate the rotating shaft 4, so that the scraper 6 rotates, and the residues adhered to the inner wall of the kettle body 1 are scraped off by the scraper 6. The first bevel gear 17 is rotated by the double-shaft motor 16, so that the second bevel gear 18 is rotated, the screw rod 19 is rotated, the moving block 20 is moved up and down along the fixed frame 14, so that the U-shaped pipe 11, the ring-shaped pipe 12, and the spray head 13 are moved up and down, and the height of the spray head 13 can be adjusted.

[0025] It is to be noted that, in the present document, relational terms such as first and second and the like can be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises", "comprising", or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but can include other elements not expressly listed or inherent to such process, method, article, or apparatus.

[0026] While the embodiments of the present application have been illustrated and described, it will be understood by those skilled in the art that various changes, modifications, substitutions, and alterations can be made therein without departing from the spirit and scope of the application, which is defined by the appended claims and their equivalents.

Claims

1. A cleanable reaction vessel for the production of metal-organic frameworks, comprising a vessel body (1), characterized in that, A feed pipe (2) is fixedly installed on the left side of the vessel body (1). A stirring assembly is provided at the bottom of the vessel body (1). A scraper (6) is provided inside the vessel body (1) through the stirring assembly. A conveying assembly is provided at the top of the vessel body (1). A U-shaped tube (11) is provided at the top of the vessel body (1) through the conveying assembly. The U-shaped tube (11) is slidably connected to the vessel body (1). An annular tube (12) is fixedly installed at the bottom of the U-shaped tube (11). A nozzle (13) is fixedly installed at the bottom of the annular tube (12). A fixed frame (14) is fixedly installed at the top of the vessel body (1). A driving assembly is provided on the opposite side of the fixed frame (14). A moving block (20) is provided inside the fixed frame (14) through the driving assembly. The moving block (20) is fixedly connected to the U-shaped tube (11).

2. The easy-to-clean reaction vessel for producing a metal-organic framework according to claim 1, characterized in that, The stirring assembly includes a rotary motor (3) located at the bottom of the vessel body (1), a rotating shaft (4) fixedly installed at the output end of the rotary motor (3), the rotating shaft (4) being fixedly connected to a scraper (6), and a stirring rod (5) fixedly installed on the surface of the rotating shaft (4).

3. The easy-to-clean reaction vessel for producing a metal-organic framework according to claim 1, characterized in that, The conveying assembly includes a storage tank (7) located on the top of the vessel body (1), a conveying pump (9) fixedly installed on the top of the storage tank (7), a suction pipe (8) fixedly installed at the bottom of the conveying pump (9), the bottom end of the suction pipe (8) extending into the storage tank (7), a hose (10) fixedly installed on the top of the conveying pump (9), and the hose (10) connected to a U-shaped pipe (11).

4. The easy-to-clean reaction vessel for producing a metal-organic framework according to claim 1, characterized in that, The drive assembly includes a support plate (15) disposed on the opposing surface of the fixed frame (14). A dual-axis motor (16) is fixedly mounted on the top of the support plate (15). A first bevel gear (17) is fixedly mounted on the output end of the dual-axis motor (16). A second bevel gear (18) is meshed on the surface of the first bevel gear (17). A screw (19) is fixedly mounted inside the second bevel gear (18). The screw (19) is rotatably connected to the fixed frame (14). The screw (19) is threadedly connected to the moving block (20).

5. The easy-to-clean reaction vessel for producing a metal-organic framework according to claim 1, characterized in that, The bottom of the vessel body (1) is fixedly installed with a feeding pipe (21), and a control valve is provided on the feeding pipe (21).

6. The easy-to-clean reaction vessel for producing a metal-organic framework according to claim 1, characterized in that, The bottom of the vessel body (1) is fixedly equipped with support legs (22), and there are multiple support legs (22).

7. The easy-to-clean reaction vessel for producing a metal-organic framework according to claim 1, characterized in that, The fixed frame (14) has a rectangular frame structure, and the movable block (20) is slidably connected to the inner wall of the fixed frame (14).

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