High-efficiency uniform-mixing high-temperature reaction device

Abstract

The utility model belongs to the technical field of experimental equipment, and particularly relates to a high-efficiency uniform-mixing high-temperature reaction device which comprises a muffle furnace, a movable door is arranged on one side of the muffle furnace, a fixed plate is arranged on the other side of the muffle furnace, a rotating motor is mounted on the fixed plate, and the rotating motor is connected with the muffle furnace. An output shaft of the rotating motor penetrates through the side wall of the muffle furnace and is fixedly connected with a sun gear in a planetary gear mechanism, a fixed shaft is fixedly connected to a planetary gear in the planetary gear mechanism, a clamping mechanism is fixedly arranged at the other end of the fixed shaft, and a reaction tank is clamped in the clamping mechanism. The planetary gear mechanism is arranged to drive the reaction tank to revolve and rotate at the same time, uniform heating of reactants is guaranteed, the reaction efficiency is improved, meanwhile, the raising plate is arranged in the reaction tank, sufficient and uniform heating of the reactants can be further guaranteed, and the reaction efficiency is improved. Materials are prevented from sliding and accumulating at the bottom of the reaction tank and the reaction efficiency is further improved.

Description

Technical Field

[0001] This utility model belongs to the field of experimental equipment technology, specifically relating to a high-efficiency mixing high-temperature reaction device. Background Technology

[0002] High-temperature homogeneous reaction is a core process in chemical, metallurgical, and new energy fields for material synthesis, catalyst preparation, and energy conversion. In existing technologies, such reactions typically employ a static heating method: the reaction vessel is sealed and placed directly inside a heating device such as a muffle furnace, where heating is achieved through thermal radiation and natural convection. However, this method has the following technical drawbacks:

[0003] 1. Uneven thermal field distribution

[0004] In static heating mode, a significant axial and radial temperature gradient is formed inside the reaction vessel:

[0005] • The concentrated heat radiation near the heating source caused the local temperature to exceed the threshold, with the highest temperature difference measured in the experiment reaching ±50℃.

[0006] • Cold zones are formed in the reactant accumulation area due to impaired heat conduction, leading to inconsistent reaction kinetics such as abnormal grain growth and deviations in the distribution of active components.

[0007] 2. Low mass transfer efficiency

[0008] When reactants are left to stand, mixing relies solely on natural diffusion or limited convection, which presents the following problems:

[0009] • Particle agglomeration and sedimentation: High-density or large-particle materials tend to accumulate at the bottom of the tank, resulting in a reduction of the effective contact area by more than 50%;

[0010] • Low energy efficiency: Energy waste in local overheated areas accounts for 30%-40% of the total system energy consumption, while cold areas require extended heating time to compensate. Utility Model Content

[0011] This invention provides a highly efficient high-temperature mixing reaction device to address the above-mentioned problems.

[0012] To achieve the above objectives, the present invention adopts the following technical solution:

[0013] A high-efficiency mixing high-temperature reaction device includes a muffle furnace, a movable door on one side of the muffle furnace, a fixed plate on the other side of the muffle furnace, a rotary motor mounted on the fixed plate, the output shaft of the rotary motor passing through the side wall of the muffle furnace and fixedly connected to the sun gear in a planetary gear mechanism, a fixed shaft fixedly connected to the planet gears in the planetary gear mechanism, and a clamping mechanism fixedly mounted at the other end of the fixed shaft, holding a reaction vessel in the clamping mechanism.

[0014] Furthermore, the planetary gear mechanism includes a gear ring, which is fixedly mounted on the inner wall of the muffle furnace. Multiple planetary gears are meshed inside the gear ring, and the multiple planetary gears mesh with a sun gear. A rotating disk is provided on the side of the gear ring away from the rotating motor. The rotating disk is rotatably connected to the gear ring. A fixed shaft passes through the rotating disk and is rotatably connected to the rotating disk.

[0015] Furthermore, a limiting groove is formed on the outer wall of the gear ring, and a limiting ring corresponding to the limiting groove is provided on the rotating disk. The rotational connection between the rotating disk and the gear ring is realized through the cooperation of the limiting groove and the limiting ring.

[0016] Furthermore, the clamping mechanism includes a fixed plate, on which multiple fixed rods are evenly arranged in a circular pattern. A reinforcing ring is connected to the other end of the multiple fixed rods. A locking nut is threaded onto the fixed rod, and the reaction vessel is fixed by the locking nut.

[0017] Furthermore, the reaction vessel includes a vessel body and a cover, which are sealed together. Multiple lifting plates are arranged evenly in a circular pattern inside the vessel body to facilitate the full heating and mixing of the reactants and prevent the reactants from sliding and accumulating at the bottom of the reaction vessel.

[0018] Furthermore, a speed regulator is also provided on the fixed plate, which is electrically connected to the rotating motor to facilitate the adjustment of the rotating motor's speed.

[0019] Compared with the prior art, the present invention has the following advantages:

[0020] This invention uses a planetary gear mechanism to drive the reaction vessel to revolve around the sun while simultaneously rotating on its own axis, ensuring uniform heating of the reactants and improving reaction efficiency. Furthermore, the application includes a lifting plate inside the reaction vessel, which further ensures sufficient and uniform heating of the reactants, preventing materials from sliding and accumulating at the bottom of the vessel, thus further improving reaction efficiency.

[0021] This invention supports simultaneous heating of multiple reaction vessels, which facilitates simultaneous experiments on different reactants and improves experimental efficiency. In addition, the reaction vessels in this invention are detachable, which allows for easy replacement with reaction vessels of suitable materials according to different reactants, thus expanding the application range of this invention. Attached Figure Description

[0022] Figure 1 This is a schematic diagram of the structure of this utility model;

[0023] Figure 2 This is a schematic diagram of the structure of the muffle-free furnace of this utility model;

[0024] Figure 3 This is a schematic diagram of the planetary gear mechanism of this utility model;

[0025] Figure 4 This is a schematic diagram of the clamping mechanism of this utility model;

[0026] Figure 5 This is a schematic diagram of the structure of the reaction vessel of this utility model;

[0027] In the diagram, 1 is a muffle furnace, 2 is a movable door, 3 is a fixed plate, 4 is a rotary motor, 5 is a planetary gear mechanism, 6 is a fixed shaft, 7 is a clamping mechanism, 8 is a reaction vessel, 501 is a gear ring, 502 is a planetary gear, 503 is a sun gear, 504 is a rotating disk, 505 is a limiting groove, 506 is a limiting ring, 701 is a fixed disk, 702 is a fixed rod, 703 is a reinforcing ring, 704 is a locking nut, 801 is a tank body, 802 is a cover, and 803 is a lifting plate. Detailed Implementation

[0028] To further illustrate the technical solution of this utility model, the following embodiments will be used to further explain this utility model.

[0029] like Figures 1 to 5 As shown, a high-efficiency mixing high-temperature reaction device includes a muffle furnace 1, a movable door 2 on one side of the muffle furnace 1, a fixed plate 3 on the other side of the muffle furnace 1, a rotary motor 4 mounted on the fixed plate 3, and a speed regulator electrically connected to the rotary motor 4 to adjust the rotational speed of the rotary motor 4. The output shaft of the rotary motor 4 passes through the side wall of the muffle furnace 1 and is fixedly connected to the sun gear 503 in the planetary gear mechanism 5. A fixed shaft 6 is fixedly connected to the planet gears 502 in the planetary gear mechanism 5, and a clamping mechanism 7 is fixedly mounted at the other end of the fixed shaft 6. A reaction vessel 8 is clamped in the clamping mechanism 7.

[0030] The planetary gear mechanism 5 includes a gear ring 501, which is fixedly mounted on the inner wall of the muffle furnace 1. Multiple planetary gears 502 are meshed inside the gear ring 501, and the multiple planetary gears 502 mesh with a sun gear 503. A rotating disk 504 is provided on the side of the gear ring 501 away from the rotary motor 4. A limiting groove 505 is formed on the outer wall of the gear ring 501. A limiting ring 506 corresponding to the limiting groove 505 is provided on the rotating disk 504. The rotational connection between the rotating disk 504 and the gear ring 501 is realized through the cooperation of the limiting groove 505 and the limiting ring 506. A fixed shaft 6 is provided through the rotating disk 504 and is rotatably connected to the rotating disk 504.

[0031] The clamping mechanism 7 includes a fixed plate 701, on which a plurality of fixed rods 702 are evenly arranged in a circle. A reinforcing ring 703 is connected to the other end of the plurality of fixed rods 702. A locking nut 704 is threaded onto the fixed rod 702, and the reaction vessel 8 is fixed by the locking nut 704.

[0032] The reaction vessel 8 includes a vessel body 801 and a cover body 802, which are sealed together. Multiple lifting plates 803 are arranged evenly in a circular pattern inside the vessel body 801 to facilitate the full heating and mixing of the reactants and prevent the reactants from sliding and accumulating at the bottom of the reaction vessel 8.

[0033] The sealing connection between the tank body 801 and the cover body 802 is a fixed connection through a sealing flange.

[0034] The foregoing has shown and described the main features and advantages of this utility model. It will be apparent to those skilled in the art that this utility model is not limited to the details of the exemplary embodiments described above, and that it can be implemented in other specific forms without departing from the spirit or essential characteristics of this utility model. Therefore, the embodiments should be considered exemplary and non-limiting in all respects. The scope of this utility model is defined by the appended claims rather than the foregoing description, and thus all variations falling within the meaning and scope of equivalents of the claims are intended to be included within this utility model.

[0035] Furthermore, it should be understood that although this specification describes embodiments, not every embodiment contains only one independent technical solution. This narrative style is merely for clarity. Those skilled in the art should consider the specification as a whole, and the technical solutions in each embodiment can also be appropriately combined to form other embodiments that can be understood by those skilled in the art.

Claims

1. A high efficiency mixing and high temperature reaction device, characterized in that: The utility model provides a kind of muffle (1), movable door (2) is provided on one side of the muffle (1), fixed plate (3) is provided on the other side of the muffle (1), rotating motor (4) is installed on the fixed plate (3), the output shaft of the rotating motor (4) is fixedly connected with sun gear (503) in planetary gear mechanism (5) through the side wall of muffle (1), fixed shaft (6) is fixedly connected on planetary gear (502) in the planetary gear mechanism (5), clamping mechanism (7) is fixedly provided on the other end of the fixed shaft (6), reaction tank (8) is clamped in the clamping mechanism (7).

2. The high-efficiency mixing high-temperature reaction device according to claim 1, characterized in that: The planetary gear mechanism (5) includes a ring gear (501) fixedly provided on the inner wall of the muffle (1), a plurality of planetary gears (502) are meshingly connected inside the ring gear (501), a sun gear (503) is commonly meshed with the plurality of planetary gears (502), a rotating disc (504) is provided on the side of the ring gear (501) away from the rotating motor (4), the rotating disc (504) is rotatably connected with the ring gear (501), the fixed shaft (6) penetrates through the rotating disc (504) and is rotatably connected with the rotating disc (504).

3. The high efficiency mixing high temperature reaction device of claim 2, wherein: A limiting groove (505) is formed on the outer wall of the ring gear (501), a limiting ring (506) corresponding to the limiting groove (505) is provided on the rotating disc (504), and the rotating disc (504) and the ring gear (501) are rotatably connected through cooperation of the limiting groove (505) and the limiting ring (506).

4. The high efficiency mixing high temperature reaction device of claim 1, wherein: The clamping mechanism (7) includes a fixed disc (701), a plurality of fixed rods (702) are uniformly arranged on the fixed disc (701) in a circle, a reinforcing ring (703) is commonly connected to the other ends of the plurality of fixed rods (702), a locking nut (704) is threadedly connected to the fixed rod (702), and the reaction tank (8) is fixed through the locking nut (704).

5. The high efficiency mixing high temperature reaction device of claim 1, wherein: The reaction tank (8) includes a tank body (801) and a cover body (802), the tank body (801) and the cover body (802) are sealingly connected, a plurality of paddle blades (803) are uniformly arranged in a circle in the tank body (801), so as to facilitate full heating and mixing of the reactants and prevent the reactants from sliding and accumulating in the lower part of the reaction tank (8).

6. The high efficiency mixing high temperature reaction device of claim 1, wherein: A speed regulator is further provided on the fixed plate (3), and the speed regulator is electrically connected with the rotating motor (4) to adjust the rotating speed of the rotating motor (4).

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