A plasticizer esterification reaction apparatus

By designing a plasticizer esterification reaction device and utilizing a stirring blade and air pump system to treat harmful gases, the problem of gas emissions during the plasticizer esterification reaction was solved, achieving both high-efficiency reaction and environmental protection.

CN224422887UActive Publication Date: 2026-06-30SHANDONG TONGYUAN ENVIRONMENTAL MATERIAL CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
SHANDONG TONGYUAN ENVIRONMENTAL MATERIAL CO LTD
Filing Date
2025-08-21
Publication Date
2026-06-30

AI Technical Summary

Technical Problem

The harmful gases produced during the esterification process of existing plasticizers are released directly into the atmosphere without treatment, endangering the environment and human health.

Method used

A plasticizer esterification reaction device was designed, comprising a tank, a filter box, a servo motor, a heating chamber, a stirring blade, a suction pump, and a filter plate. The stirring blade is driven by the servo motor to stir, and the heating chamber is heated by heat transfer oil. The suction pump draws in harmful gases and filters them through the filter plate and activated carbon filter plate to reduce emissions.

Benefits of technology

It improved reaction efficiency, reduced the emission of harmful gases, and protected the environment and the health of workers.

✦ Generated by Eureka AI based on patent content.

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Abstract

This utility model discloses a plasticizer esterification reaction device, including a tank and a filter box. A mounting cover is provided on the upper surface of the tank, and a feed inlet is opened on the upper surface of the mounting cover. A servo motor is mounted on the upper surface of the mounting cover, and a connecting air pipe is connected to the upper surface of the mounting cover. The filter box contains a filter plate and an activated carbon filter plate arranged from top to bottom. An air pump is connected to one side of the filter box, and an air suction pipe is connected to the upper surface of the filter box. A rotating rod is provided at the output end of the servo motor. This utility model uses the servo motor to drive the rotating rod at the output end to rotate. The rotating rod drives several stirring blades evenly spaced on the circumferential side to stir the liquid in the tank. Simultaneously, the heating base is activated to heat the heating tubes and heat the heat transfer oil in the heating chamber. The simultaneous operation of heating and stirring of the liquid in the tank further improves the reaction effect of the liquid in the tank.
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Description

Technical Field

[0001] This utility model belongs to the field of plasticizer esterification reaction technology, and in particular relates to a plasticizer esterification reaction apparatus. Background Technology

[0002] As is well known, plasticizers are substances added during the molding of polymers such as rubber, plastics, and coatings to increase their plasticity, flowability, and make the finished product flexible. They are essential additives in the plastics industry. However, studies have shown that phthalic plasticizers have potential carcinogenicity, and the production volume of green plasticizers such as epoxy resins and citrate esters is difficult to meet the huge market demand in the short term. Therefore, phthalic plasticizers will remain the main products on the market in the future.

[0003] Existing plasticizers react inside a reactor, but harmful gases are generated during the reaction. These gases are released directly into the atmosphere without treatment, which will have a certain impact on the environment. At the same time, long-term inhalation of harmful gases by workers will cause certain damage to their health. Therefore, a plasticizer esterification reaction device is proposed. Summary of the Invention

[0004] The purpose of this invention is to provide a plasticizer esterification reaction apparatus to solve existing problems.

[0005] To solve the above-mentioned technical problems, this utility model is achieved through the following technical solution:

[0006] This utility model relates to a plasticizer esterification reaction device, comprising a tank and a filter box. The tank has a mounting cover on its upper surface, an inlet on its upper surface, a servo motor on its upper surface, and a connecting air pipe. The filter box contains a filter plate and an activated carbon filter plate arranged from top to bottom. An air pump is connected to one side of the filter box, and an air suction pipe is connected to its upper surface. A rotating rod is located at the output end of the servo motor. A heating chamber is formed inside the tank, containing a heating tube. An inlet pipe and a outlet pipe are respectively formed on the circumferential side of the tank, and a heating base is provided on the circumferential side of the tank.

[0007] Furthermore, the tank body is fitted with a heat insulation plate on its periphery, and the bottom surface of the tank body is symmetrically provided with liquid outlet pipes. The liquid outlet pipes and the feed inlet are both connected to a solenoid valve on their periphery. The liquid inlet pipe and the liquid outlet pipe are respectively connected to the heating chamber. The heating base is electrically connected to the heating tube. The heating chamber is provided with heat-conducting oil, and the heating tube has a spiral plate structure.

[0008] Furthermore, the rotating rod is provided with several stirring blades on its circumferential side, and the stirring blades are disposed inside the tank. The free end of the connecting air pipe is fixedly connected to the top of the suction pipe through a connecting flange. The upper surface of the filter box is connected to the suction pipe. Several support legs are provided at equal intervals on the bottom surface of the tank.

[0009] This utility model has the following beneficial effects:

[0010] This invention utilizes a servo motor to drive a rotating rod at the output end. The rotating rod, in turn, drives several equally spaced stirring blades on the circumferential side to stir the liquid inside the tank. Simultaneously, a heating element is activated to heat the heat transfer oil within the heating chamber. This simultaneous heating and stirring of the liquid inside the tank further enhances the reaction efficiency. Furthermore, a heat insulation plate, a polyurethane-aerogel composite board, is used to insulate the tank's circumference. This board combines the low cost of polyurethane with the high performance of aerogel, exhibiting a thermal conductivity of approximately 0.018–0.022 W / (m·K). During the reaction of the liquid inside the tank, some harmful gases may be generated. In this case, an air pump is activated. The air pump extracts the generated gases through an air intake pipe and connecting pipe. The gases are then filtered through a filter plate and an activated carbon filter plate (a high-efficiency filter plate made of glass fiber or synthetic fiber) before being discharged by the air pump, minimizing harm to workers.

[0011] Of course, any product implementing this utility model does not necessarily need to achieve all of the advantages described above at the same time. Attached Figure Description

[0012] To more clearly illustrate the technical solutions of the embodiments of this utility model, the accompanying drawings used in the description of the embodiments will be briefly introduced below. Obviously, the drawings described below are only some embodiments of this utility model. For those skilled in the art, other drawings can be obtained based on these drawings without creative effort.

[0013] Figure 1 This is a schematic diagram of the overall structure of a plasticizer esterification reaction device;

[0014] Figure 2 This is a right view of a plasticizer esterification reaction apparatus;

[0015] Figure 3 for Figure 2 Cross-sectional view of section AA.

[0016] The components represented by each number in the attached diagram are listed below: 1. Tank body; 10. Heating chamber; 100. Liquid inlet pipe; 101. Liquid outlet pipe; 102. Heating pipe; 103. Heating base; 104. Liquid outlet pipe; 105. Solenoid valve; 11. Heat insulation plate; 12. Mounting cover; 121. Feed inlet; 120. Servo motor; 1201. Rotating rod; 1202. Stirring blade; 122. Connecting air pipe; 2. Filter box; 201. Suction pipe; 202. Filter plate; 203. Activated carbon filter plate; 204. Suction pump. Detailed Implementation

[0017] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0018] In the description of this utility model, it should be understood that the terms "upper", "middle", "outer", "inner", etc., which indicate orientation or positional relationship, are only for the convenience of describing this utility model and simplifying the description, and do not indicate or imply that the components or elements referred to must have a specific orientation, or be constructed and operated in a specific orientation, and therefore should not be construed as a limitation of this utility model.

[0019] In the description of this utility model, it should be noted that, unless otherwise explicitly specified and limited, the terms "installed," "equipped with," "connected," etc., should be interpreted broadly. For example, "connection" can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediate medium; it can be a connection within two components. Those skilled in the art can understand the specific meaning of the above terms in this utility model based on the specific circumstances.

[0020] Please see Figures 1-3 As shown, this utility model is a plasticizer esterification reaction device, including a tank 1 and a filter box 2. The upper surface of the tank 1 is provided with a mounting cover 12, and the upper surface of the mounting cover 12 is provided with a feed port 121. The upper surface of the mounting cover 12 is provided with a servo motor 120. The upper surface of the mounting cover 12 is connected to a connecting air pipe 122. The filter box 2 is provided with a filter plate 202 and an activated carbon filter plate 203 arranged from top to bottom. One side of the filter box 2 is connected to a suction pump 204. The upper surface of the filter box 2 is connected to a suction pipe 201. The output end of the servo motor 120 is provided with a rotating rod 1201.

[0021] Furthermore, a heating chamber 10 is provided inside the tank body 1, and a heating pipe 102 is installed inside the heating chamber 10. An inlet pipe 100 and a drain pipe 101 are respectively provided on the sides of the tank body 1. A heating seat 103 is provided on the sides of the tank body 1. A heat insulation plate 11 is fitted on the sides of the tank body 1. A liquid outlet pipe 104 is symmetrically provided on the bottom surface of the tank body 1. A solenoid valve 105 is provided on both the sides of the liquid outlet pipe 104 and the inlet 121.

[0022] Furthermore, the inlet pipe 100 and the outlet pipe 101 are respectively connected to the heating chamber 10, the heating seat 103 is electrically connected to the heating tube 102, the heating chamber 10 is filled with heat-conducting oil, and the heating tube 102 has a spiral plate structure.

[0023] Furthermore, a number of stirring blades 1202 are provided on the circumferential side of the rotating rod 1201, and the stirring blades 1202 are provided on the circumferential side of the rotating rod 1201 and are located inside the tank body 1. The free end of the connecting air pipe 122 is fixedly connected to the top of the suction pipe 201 through a connecting flange. The upper surface of the filter box 2 is connected to the suction pipe 201. A number of support legs are provided at equal intervals on the bottom surface of the tank body 1.

[0024] It should be noted that this utility model uses a servo motor 120 to drive the rotating rod 1201 at the output end to rotate. The rotating rod 1201 drives several stirring blades 1202 evenly spaced on the circumferential side to stir the liquid in the tank 1. At the same time, the heating seat 103 is activated to heat the heating tube 102, which in turn heats the heat transfer oil in the heating chamber 10. By simultaneously operating the heating and stirring of the liquid in the tank 1 by the stirring blades 1202, the reaction effect of the liquid in the tank 1 is further improved. Additionally, a heat insulation plate 11 is used to insulate the circumferential side of the tank 1. The heat insulation plate 11 is a polyurethane-aerogel composite plate, characterized by combining the low cost of polyurethane with the high performance of aerogel, and a thermal conductivity of approximately (0.018). ~0.022W / (m·K); At the same time, some harmful gases may be generated during the reaction of the liquid in tank 1. At this time, the suction pump 204 is started. The suction pump 204 extracts the gas generated in tank 1 through suction pipe 201 and connecting pipe 122. The gas passes through suction pipe 201 and connecting pipe 122 and passes through filter plate 202 and activated carbon filter plate 203 for filtration. Filter plate 202 is a high-efficiency filter plate made of glass fiber or synthetic fiber. The gas is then discharged through suction pump 204 to reduce harm to workers. The air outlet of suction pump 204 is equipped with an air inspection device to check the quality of the filtered gas. If the gas quality does not meet the standard, it will be purified in the next process.

[0025] In the description of this specification, references to terms such as "an embodiment," "example," and "specific example" indicate that a specific feature, structure, material, or characteristic described in connection with that embodiment or example is included in at least one embodiment or example of the present invention. In this specification, illustrative expressions of the above terms do not necessarily refer to the same embodiment or example. Furthermore, the specific features, structures, materials, or characteristics described may be combined in any suitable manner in one or more embodiments or examples.

[0026] The preferred embodiments of this utility model disclosed above are merely illustrative of the present utility model. These preferred embodiments do not exhaustively describe all details, nor do they limit the invention to the specific implementations described. Clearly, many modifications and variations can be made based on the content of this specification. This specification selects and specifically describes these embodiments to better explain the principles and practical applications of this utility model, thereby enabling those skilled in the art to better understand and utilize it. This utility model is limited only by the claims and their full scope and equivalents.

Claims

1. A plasticizer esterification reaction apparatus comprising a tank body (1) and a filter box (2), characterized by: The upper surface of the tank (1) is provided with a mounting cover (12), the upper surface of the mounting cover (12) is provided with a feed inlet (121), the upper surface of the mounting cover (12) is provided with a servo motor (120), the upper surface of the mounting cover (12) is connected to a connecting air pipe (122), the filter box (2) is provided with a filter plate (202) and an activated carbon filter plate (203) respectively arranged from top to bottom, one side of the filter box (2) is connected to a suction pump (204), the upper surface of the filter box (2) is connected to a suction pipe (201), and the output end of the servo motor (120) is provided with a rotating rod (1201).

2. The plasticizer esterification reaction apparatus according to claim 1, wherein A heating chamber (10) is provided inside the tank (1), and a heating pipe (102) is provided inside the heating chamber (10). An inlet pipe (100) and a drain pipe (101) are respectively provided on the periphery of the tank (1), and a heating seat (103) is provided on the periphery of the tank (1).

3. The plasticizer esterification reaction apparatus according to claim 2, wherein The tank body (1) is fitted with a heat insulation plate (11) on its periphery. The bottom surface of the tank body (1) is symmetrically provided with liquid outlet pipes (104). The liquid outlet pipes (104) and the feed inlet (121) are both connected to a solenoid valve (105).

4. The plasticizer esterification reaction apparatus according to claim 2, wherein The inlet pipe (100) and outlet pipe (101) are respectively connected to the heating chamber (10), the heating seat (103) is electrically connected to the heating tube (102), the heating chamber (10) is filled with heat-conducting oil, and the heating tube (102) has a spiral plate structure.

5. The plasticizer esterification reaction apparatus according to claim 1, wherein The rotating rod (1201) is provided with a plurality of stirring blades (1202) on its circumferential side, and the plurality of stirring blades (1202) on its circumferential side are provided inside the tank body (1).

6. The plasticizer esterification reaction apparatus according to claim 1, wherein The free end of the connecting air pipe (122) is fixedly connected to the top end of the suction pipe (201) through a connecting flange. The upper surface of the filter box (2) is connected to the suction pipe (201). Several support legs are equidistantly arranged on the bottom surface of the tank (1).