A nano-dispersion stirring device for imidacloprid and acetamiprid emulsifiable concentrate

CN224628827UActive Publication Date: 2026-08-14吴忠领航生物药业科技有限公司
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
Filing Date
2025-08-07
Publication Date
2026-08-14

AI Technical Summary

Technical Problem

[0003]目前,在乳油制备时,常面临分散不均匀、粒径过大且分布较宽等问题,这会影响乳油的溶解性、渗透性和生物活性,进而降低药效、缩短持效期,同时,传统的搅拌装置在处理过程中,难以实现对温度、搅拌速度等参数的精细化控制,导致乳油剂型的均一性和稳定性不佳,还可能增加农药的流失和浪费,加大环境风险,此外,现有装置在结合高效载体与助剂筛选技术以及精细化剂型制备技术方面存在不足,无法很好地满足提升乳油性能的需求

Benefits of technology

[0016]通过搅拌罐体、搅拌组件、温控组件、进料组件、监测组件和控制器的配合使用,本装置能够提高乳油制备时原料的分散效果,进而能够提高乳油的溶解性、渗透性和生物活性,同时能够提高乳油剂型的均一性和稳定性,减少农药的流失和浪费。

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Abstract

This utility model belongs to the technical field of imidacloprid and acetamiprid emulsifiable concentrate processing, and discloses a nano-dispersion and stirring device for imidacloprid and acetamiprid emulsifiable concentrate. It includes a base, a stirring tank, a stirring assembly, a temperature control assembly, a feeding assembly, a monitoring assembly, and a controller. The temperature control assembly includes a heating and cooling unit and a temperature-controlled circulating pump. The temperature-controlled circulating pump is connected to the outlet of the heating and cooling unit via a metal pipe. The stirring tank is mounted on the upper surface of the base. The stirring tank has a double-layered jacket structure; the inner layer of the double-layered jacket is a reaction chamber, and the outer layer is a temperature-controlled chamber. The temperature-controlled circulating pump is connected to the upper side of one side of the temperature-controlled chamber via a metal pipe. The inlet of the heating and cooling unit is connected to the lower side of one side of the temperature-controlled chamber via a metal pipe. A sealing cap is bolted to the top of the stirring tank, and the stirring assembly is mounted on the sealing cap. This device has a simple and reasonable structure, a novel design, and is easy to operate. It has high practicality and is easy to widely promote and use.
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Description

Technical Field

[0001] This utility model belongs to the field of imidacloprid acetamiprid emulsifiable concentrate processing technology, and more specifically, it relates to an imidacloprid acetamiprid emulsifiable concentrate nano-dispersion stirring device. Background Technology

[0002] In the production of imidacloprid and acetamiprid emulsifiable concentrates, the stability, efficacy, and duration of effect of the emulsifiable concentrate formulation are crucial.

[0003] Currently, the preparation of emulsifiable concentrates (ECs) often faces problems such as uneven dispersion, excessively large particle size, and wide distribution. These issues affect the solubility, permeability, and bioactivity of the ECs, thereby reducing efficacy and shortening the duration of action. Furthermore, traditional stirring devices struggle to achieve precise control over parameters such as temperature and stirring speed during processing, resulting in poor homogeneity and stability of the EC formulation. This can also increase pesticide loss and waste, and amplify environmental risks. In addition, existing equipment falls short in combining efficient carrier and adjuvant screening technologies with refined formulation preparation techniques, failing to adequately meet the demands for improved EC performance.

[0004] Therefore, in view of this, we have studied and improved the existing structure and its shortcomings, and provided a nano-dispersion and stirring device for imidacloprid acetamiprid emulsifiable concentrate, in order to achieve a more practical purpose. Utility Model Content

[0005] To solve the above-mentioned technical problems, this utility model provides a nano-dispersion stirring device for imidacloprid and acetamiprid emulsifiable concentrate, which is achieved by the following specific technical means:

[0006] A nano-dispersion and stirring device for imidacloprid and acetamiprid emulsifiable concentrate includes a base, a stirring tank, a stirring assembly, a temperature control assembly, a feeding assembly, a monitoring assembly, and a controller. The temperature control assembly includes a heating and cooling unit and a temperature-controlled circulating pump. The temperature-controlled circulating pump is connected to the outlet of the heating and cooling unit via a metal pipe. The stirring tank is mounted on the upper surface of the base. The stirring tank includes a double-layered jacket structure. The inner layer of the double-layered jacket structure is a reaction chamber, and the outer layer is a temperature-controlled chamber. The temperature-controlled circulating pump is connected to the upper end of one side of the temperature-controlled chamber via a metal pipe. The inlet of the heating and cooling unit is connected to the lower end of one side of the temperature-controlled chamber via a metal pipe. A sealing cap is bolted to the top of the stirring tank, and the stirring assembly is mounted on the sealing cap. An outlet is provided at the bottom of the stirring tank. The feeding assembly consists of several feeding pipes, one end of which penetrates one side of the stirring tank and extends into the reaction chamber.

[0007] Furthermore, the stirring assembly includes a drive motor, a stirring shaft, stirring paddles, and a dispersing disc. The drive motor is mounted on the upper surface of the sealing cover. The top of the sealing cover is rotatably connected to the stirring shaft. The top end of the stirring shaft passes through the upper surface of the sealing cover and is connected to the output end of the drive motor. The bottom end of the stirring shaft extends into the temperature control chamber. A dispersing disc is installed at the bottom end of the stirring shaft. Several stirring paddles are installed above the dispersing disc around the periphery of the stirring shaft.

[0008] Furthermore, the integrated heating and cooling unit is installed on the upper surface of the base near the mixing tank.

[0009] Furthermore, the temperature-controlled circulating pump is installed on the upper surface of the base between the mixing tank and the integrated heating and cooling unit.

[0010] Furthermore, the controller is mounted on the upper surface of the base on the side away from the integrated heating and cooling unit.

[0011] Furthermore, a guide plate is installed on one side of the inner wall of the mixing tank below several feed pipes.

[0012] Furthermore, the monitoring components include a particle size sensor, a temperature sensor, and a pressure sensor. The particle size sensor is installed on the inner wall of one side of the mixing tank, and the temperature sensor and pressure sensor are installed on the top of the sealing cover.

[0013] Furthermore, a valve is installed on the feed pipe, and a metering pump is connected to one end of the feed pipe.

[0014] Furthermore, the controller is electrically connected to the drive motor, temperature control component, feeding component, and monitoring component.

[0015] Compared with the prior art, the present invention has the following beneficial effects:

[0016] By using the mixing tank, mixing components, temperature control components, feeding components, monitoring components, and controller in combination, this device can improve the dispersion effect of raw materials during emulsifiable concentrate preparation, thereby improving the solubility, permeability, and biological activity of the emulsifiable concentrate. At the same time, it can improve the uniformity and stability of the emulsifiable concentrate formulation and reduce pesticide loss and waste. Attached Figure Description

[0017] Figure 1 This is a front-view stereoscopic diagram of the present invention.

[0018] Figure 2 This is a rear-view stereoscopic diagram of the present invention.

[0019] Figure 3 This is a three-dimensional cross-sectional view of the present invention.

[0020] Figure 4This is a three-dimensional cross-sectional view of the present invention.

[0021] In the diagram, the correspondence between component names and drawing numbers is as follows:

[0022] 1. Base; 2. Mixing tank; 201. Reaction chamber; 202. Temperature control chamber; 203. Discharge port; 204. Baffle plate; 3. Mixing assembly; 301. Drive motor; 302. Mixing shaft; 303. Mixing paddle; 304. Dispersion disc; 4. Temperature control assembly; 401. Integrated heating and cooling unit; 402. Temperature control circulating pump; 5. Feeding assembly; 501. Feeding pipe; 502. Valve; 503. Metering pump; 6. Monitoring assembly; 601. Particle size sensor; 602. Temperature sensor; 603. Pressure sensor; 7. Controller; 8. Sealing cover. Detailed Implementation

[0023] The embodiments of this utility model will be described in further detail below with reference to the accompanying drawings and examples. The following examples are for illustrative purposes only and should not be construed as limiting the scope of this utility model.

[0024] In the description of this utility model, unless otherwise stated, "a plurality of" means two or more; the terms "upper," "lower," "left," "right," "inner," "outer," "front end," "rear end," "head," "tail," etc., indicate the orientation or positional relationship based on the orientation or positional relationship shown in the accompanying drawings, and are only for the convenience of describing this utility model and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation, and therefore should not be construed as a limitation of this utility model. In addition, the terms "first," "second," "third," etc., are used for descriptive purposes only and should not be construed as indicating or implying relative importance.

[0025] In the description of this utility model, it should be noted that, unless otherwise explicitly specified and limited, the terms "connected" and "linked" should be interpreted broadly. For example, they can refer to a fixed connection, a detachable connection, or an integral connection; they can refer to a mechanical connection or an electrical connection; they can refer to a direct connection or an indirect connection through an intermediate medium. Those skilled in the art can understand the specific meaning of the above terms in this utility model based on the specific circumstances.

[0026] Example:

[0027] As attached Figure 1 To be continued Figure 4 As shown:

[0028] This invention provides a nano-dispersion stirring device for imidacloprid acetamiprid emulsifiable concentrate, comprising a base 1, a stirring tank 2, a stirring assembly 3, a temperature control assembly 4, a feeding assembly 5, a monitoring assembly 6, and a controller 7. The temperature control assembly 4 includes a heating and cooling unit 401 and a temperature-controlled circulating pump 402. The temperature-controlled circulating pump 402 is connected to the outlet of the heating and cooling unit 401 via a metal pipe. The temperature-controlled circulating pump 402 is used to drive the temperature-controlled medium to circulate within the temperature-controlled chamber 202, thereby achieving precise control of the material temperature within the reaction chamber 201. The stirring tank 2 is mounted on the upper surface of the base 1. The stirring tank 2 includes a double-layer jacket structure, with the inner layer of the double-layer jacket structure serving as the reaction chamber. The outer layer of the double-layer jacketed structure is the temperature control chamber 202. The temperature control circulation pump 402 is connected to the upper side of the temperature control chamber 202 through a metal pipe. The water inlet of the integrated heating and cooling machine 401 is connected to the lower side of the temperature control chamber 202 through a metal pipe. The top of the mixing tank 2 is bolted with a sealing cover 8, and a stirring assembly 3 is installed on the sealing cover 8. The bottom of the mixing tank 2 is provided with a discharge port 203. It should be noted that a control valve is provided at the discharge port 203 to control the discharge of materials. The feeding assembly 5 is composed of several feeding pipes 501. One end of the feeding pipes 501 passes through one side of the mixing tank 2 and extends into the reaction chamber 201.

[0029] The stirring assembly 3 includes a drive motor 301, a stirring shaft 302, stirring paddles 303, and a dispersing disc 304. The drive motor 301 is mounted on the upper surface of the sealing cover 8. The top of the sealing cover 8 is rotatably connected to the stirring shaft 302. The top end of the stirring shaft 302 passes through the upper surface of the sealing cover 8 and is connected to the output end of the drive motor 301. The bottom end of the stirring shaft 302 extends into the temperature control chamber 202. The dispersing disc 304 is installed at the bottom end of the stirring shaft 302. Several stirring paddles 303 are installed on the periphery of the stirring shaft 302 above the dispersing disc 304. The dispersing disc 304 has multiple small dispersing holes, which can refine and disperse the material. The multi-layer stirring paddles 303 adopt a blade design with different angles, which can enhance the mixing effect of the material.

[0030] The integrated heating and cooling unit 401 is installed on the upper surface of the base 1 near the mixing tank 2.

[0031] The temperature-controlled circulating pump 402 is installed on the upper surface of the base 1 between the mixing tank 2 and the integrated heating and cooling unit 401. When the temperature inside the mixing tank 2 is too high, the integrated heating and cooling unit 401 heats the temperature-controlled medium and delivers the medium to the temperature-controlled chamber 202 through the temperature-controlled circulating pump 402 to raise the temperature of the mixing tank 2. When the temperature inside the mixing tank 2 is too low, the integrated heating and cooling unit 401 cools the temperature-controlled medium and delivers the temperature-controlled medium to the temperature-controlled chamber 202 through the temperature-controlled circulating pump 402 to cool the mixing tank 2.

[0032] The controller 7 is installed on the upper surface of the base 1 on the side away from the integrated cooling and heating unit 401.

[0033] Among them, a guide plate 204 is installed on one side of the inner wall of the mixing tank 2 below several feed pipes 501. The raw materials enter evenly under the action of the guide plate 204 to avoid excessive local concentration.

[0034] The monitoring component 6 includes a particle size sensor 601, a temperature sensor 602, and a pressure sensor 603. The particle size sensor 601 is installed on the inner wall of one side of the mixing tank 2 and is used to monitor the particle size distribution of the material in real time. The top of the sealing cover 8 is equipped with a temperature sensor 602 and a pressure sensor 603. The temperature sensor 602 is used to monitor the temperature inside the mixing tank 2 in real time, and the pressure sensor 603 is used to monitor the pressure inside the mixing tank 2 in real time.

[0035] The feed pipe 501 is equipped with a valve 502, and one end of the feed pipe 501 is connected to a metering pump 503. Each feed pipe 501 corresponds to the feeding of raw materials such as imidacloprid, acetamiprid, emulsifier, stabilizer, and additives. Each feed pipe 501 is equipped with a metering pump 503 and a valve 502, which can accurately control the feeding amount of each raw material.

[0036] The controller 7 is electrically connected to the drive motor 301, the temperature control component 4, the feeding component 5, and the monitoring component 6. The controller 7 has a control program that can automatically adjust parameters such as stirring speed, reaction temperature, and feed amount of each raw material according to the data transmitted from the monitoring component 6, so as to realize the automated control of the entire stirring and dispersion process.

[0037] It should be noted that the device structure and accompanying drawings of this utility model mainly describe the principle of this utility model. In terms of the technical aspects of this design principle, the setting of the power mechanism, power supply system and controller 7 of the device is not fully described. However, under the premise that those skilled in the art understand the principle of the above utility model, the specific details of its power mechanism, power supply system and controller 7 can be clearly understood. The control method in the application document is automatic control through controller 7. The control circuit of controller 7 can be implemented by those skilled in the art through simple programming.

[0038] The working principle of this embodiment:

[0039] 1. Preparation stage: Check whether each part of the device is operating normally, ensure that the reaction chamber 201 of the stirring tank 2 is clean and free of impurities, and set the parameters such as the feed rate of each raw material, stirring speed, and reaction temperature through the controller 7 according to the preset emulsion formula.

[0040] 2. Feeding process: Start the feeding assembly 5, and through the metering pump 503 and valve 502 on each feeding pipe 501, the raw materials such as imidacloprid, acetamiprid, emulsifier, stabilizer, and additives are sequentially transported into the reaction chamber 201 of the mixing tank 2 according to the set amount. The raw materials enter evenly under the action of the guide plate 204 to avoid excessive local concentration.

[0041] 3. Stirring and Dispersion Process: The drive motor 301 of the stirring assembly 3 is started, and stirring begins at the set stirring speed. In the initial stage, the multi-layer stirring paddle 303 performs preliminary mixing of the materials. As stirring progresses, the nano-dispersion disk 304 begins to function, dispersing the materials at the nanoscale. Simultaneously, the temperature control assembly 4 starts working, maintaining the temperature within the reaction chamber 201 within the set range through heating or cooling. The monitoring assembly 6 monitors the particle size distribution, temperature, and pressure of the materials in real time and transmits the data to the controller 7. Based on the monitoring data, the controller 7 automatically adjusts the stirring speed and temperature to ensure uniform material dispersion.

[0042] 4. Adjustment and Optimization Process: During the stirring and dispersion process, if the particle size distribution of the material is found to be unsatisfactory, the controller 7 will automatically increase the stirring speed or extend the stirring time; if the temperature deviates from the set value, the temperature control component 4 will adjust it in a timely manner. Through such dynamic adjustments, the uniformity and stability of the emulsifiable concentrate formulation are ensured.

[0043] 5. Completion Stage: When the monitoring component 6 displays that the particle size distribution, temperature, and other parameters of the material reach the preset standards, the controller 7 sends a signal to stop the operation of the stirring component 3, the temperature control component 4, and the feeding component 5. The control valve of the discharge port 203 at the bottom of the stirring tank 2 is opened to discharge the prepared imidacloprid acetamiprid emulsifiable concentrate for collection and later use.

[0044] 6. Cleaning stage: After the material has been completely discharged, the reaction chamber 201 of the mixing tank 2 is cleaned to prepare for the next production.

[0045] The embodiments of this utility model are given for illustrative and descriptive purposes only, and are not intended to be exhaustive or to limit the utility model to the forms disclosed. Many modifications and variations will be apparent to those skilled in the art. The embodiments were chosen and described in order to better illustrate the principles and practical applications of this utility model, and to enable those skilled in the art to understand this utility model and design various embodiments with various modifications suitable for a particular purpose.

Claims

1. A nano-dispersion stirring device for imidacloprid acetamiprid emulsifiable concentrate, comprising a base (1), a stirring tank (2), a stirring assembly (3), a temperature control assembly (4), a feeding assembly (5), a monitoring assembly (6), and a controller (7), wherein the temperature control assembly (4) comprises a heating and cooling unit (401) and a temperature-controlled circulating pump (402), and the temperature-controlled circulating pump (402) is connected to the outlet of the heating and cooling unit (401) via a metal pipe, characterized in that: A stirring tank (2) is installed on the upper surface of the base (1). The stirring tank (2) includes a double-layer jacket structure. The inner layer of the double-layer jacket structure is a reaction chamber (201), and the outer layer of the double-layer jacket structure is a temperature control chamber (202). The temperature control circulation pump (402) is connected to the upper side of the temperature control chamber (202) through a metal pipe. The water inlet of the integrated heating and cooling machine (401) is connected to the lower side of the temperature control chamber (202) through a metal pipe. A sealing cover (8) is bolted to the top of the stirring tank (2). A stirring assembly (3) is installed on the sealing cover (8). A discharge port (203) is provided at the bottom of the stirring tank (2). The feeding assembly (5) is composed of several feeding pipes (501). One end of several feeding pipes (501) passes through one side of the stirring tank (2) and extends into the reaction chamber (201).

2. The nano-dispersion stirring device for imidacloprid and acetamiprid emulsifiable concentrate as described in claim 1, characterized in that: The stirring assembly (3) includes a drive motor (301), a stirring shaft (302), a stirring paddle (303), and a dispersing disc (304). The drive motor (301) is mounted on the upper surface of the sealing cover (8). The top of the sealing cover (8) is rotatably connected to the stirring shaft (302). The top end of the stirring shaft (302) passes through the upper surface of the sealing cover (8) and is connected to the output end of the drive motor (301). The bottom end of the stirring shaft (302) extends into the temperature control chamber (202). The bottom end of the stirring shaft (302) is equipped with a dispersing disc (304). Several stirring paddles (303) are installed on the periphery of the stirring shaft (302) above the dispersing disc (304).

3. The nano-dispersion stirring device for imidacloprid and acetamiprid emulsifiable concentrate as described in claim 1, characterized in that: The integrated heating and cooling unit (401) is installed on the upper surface of the base (1) near the mixing tank (2).

4. The nano-dispersion stirring device for imidacloprid and acetamiprid emulsifiable concentrate as described in claim 1, characterized in that: The temperature-controlled circulating pump (402) is installed on the upper end face of the base (1) between the mixing tank (2) and the integrated heating and cooling unit (401).

5. The nano-dispersion stirring device for imidacloprid and acetamiprid emulsifiable concentrate as described in claim 1, characterized in that: The controller (7) is installed on the upper surface of the base (1) away from the heat and cold integrated unit (401).

6. The nano-dispersion stirring device for imidacloprid and acetamiprid emulsifiable concentrate as described in claim 1, characterized in that: A guide plate (204) is installed on one side of the inner wall of the mixing tank (2), below several feed pipes (501).

7. The nano-dispersion stirring device for imidacloprid and acetamiprid emulsifiable concentrate as described in claim 1, characterized in that: The monitoring component (6) includes a particle size sensor (601), a temperature sensor (602) and a pressure sensor (603). The particle size sensor (601) is installed on the inner wall of one side of the mixing tank (2), and the temperature sensor (602) and the pressure sensor (603) are installed on the top of the sealing cover (8).

8. The nano-dispersion stirring device for imidacloprid and acetamiprid emulsifiable concentrate as described in claim 1, characterized in that: A valve (502) is installed on the feed pipe (501), and a metering pump (503) is connected to one end of the feed pipe (501).

9. The nano-dispersion stirring device for imidacloprid and acetamiprid emulsifiable concentrate as described in claim 2, characterized in that: The controller (7) is electrically connected to the drive motor (301), the temperature control component (4), the feeding component (5), and the monitoring component (6).