Separation system and method for polysilicon cold hydrogenation product

By setting the difference in the number of trays between the gas phase balance port and the side sampling port to 0-2 in the polycrystalline silicon cold hydrogenation process, and using the gas phase balance pipe to achieve pressure balance, the problem of pressure stability in the silicon tetrachloride buffer tank was solved, the consumption and emission of hydrogen and silicon tetrachloride were reduced, and the separation efficiency and energy efficiency were improved.

WO2026011624A1PCT designated stage Publication Date: 2026-01-15HUALU ENG & TECH
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Patent Information

Application Number
PCT/CN2024/130660
Authority / Receiving Office
WO · WO
Patent Type
Applications
Current Assignee / Owner
Priority Date
2024-07-08
Filing Date
2024-11-07
Publication Date
2026-01-15

AI Technical Summary

Technical Problem

In the existing polysilicon cold hydrogenation process, the pressure of the silicon tetrachloride buffer tank needs to be stabilized by adding hydrogen, resulting in high consumption and emissions of hydrogen and silicon tetrachloride.

Method used

By setting the difference in the number of trays between the gas phase balance port and the side sampling port in the coarse separator to 0-2, the pressure balance between the silicon tetrachloride buffer tank and the coarse separator is achieved using the gas phase balance pipe, thereby reducing the dependence on hydrogen.

Benefits of technology

This reduces waste gas emissions during the inlet of the silicon tetrachloride buffer tank, decreases the consumption and emissions of hydrogen and silicon tetrachloride, improves separation efficiency, and reduces energy consumption.

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Abstract

The present application provides a separation system and method for a polysilicon cold hydrogenation product. The separation system for a polysilicon cold hydrogenation product comprises a coarse separation tower, a silicon tetrachloride buffer tank, and a gas-phase equalizing pipe. The coarse separation tower comprises a side draw port and a gas-phase equilibrium port; the number of trays between the gas-phase equilibrium port and the side draw port differs by 0 to 2; the side draw port is communicated with the silicon tetrachloride buffer tank; and the gas-phase equilibrium port is communicated with the silicon tetrachloride buffer tank by means of the gas-phase equalizing pipe. The separation system can reduce the consumption and emissions of hydrogen and silicon tetrachloride, achieving excellent economic benefits.
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Citation Information

Patent Citations

  • Polycrystalline silicon production process and system

    CN117623314A

  • Polycrystalline silicon cold hydrogenation product separation system and method

    CN118993083A

  • Polycrystalline silicon cold hydrogenation product separation system and method

    CN118993085A

  • Method for the hydrogenation of poly-si

    US8580661B1