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Method for preparing gamma'-Fe4N soft magnetic material by utilizing liquid nitrogen via high-speed ball milling

The invention discloses a method for preparing a gamma'-Fe4N soft magnetic material by utilizing liquid nitrogen via high-speed ball milling, and belongs to the field of soft magnetic materials. According to the method, high-energy low-temperature grinding in the liquid nitrogen is utilized to obtain a nano material FexN with a nitrogen atom supersaturation degree; and at low temperature, the material is crispy and the surface volume ratio is very high, so that 22% of nitrogen atoms are adsorbed on the surface of a sample; after the temperature is up to 300 DEG C, annealing is carried out to ensure that alpha-Fe directly undergoes phase change to be converted to gamma'-Fe4N, so as to prepare a nanocrystal gamma'-Fe4N soft magnetic material. The method is simple to convenient to operate, low in cost and suitable for large-scale industrial production, and is a novel replacement method for preparing high-level soft magnetic materials with ideal magnetism. The gamma'-Fe4N soft magnetic material prepared by the method has the advantages of being high in Ms, low in coercive force and high surface resistivity, and can be applied to transformer and inductors operated in high-frequency semi-conductor switches.
Owner:无锡市临碳电子科技有限公司
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