An intelligent oxygen absorption detection system for deoxidizers

By designing an intelligent deoxidant oxygen absorption detection system and using an electronic control system to automatically monitor and calculate the oxygen absorption, problems such as cumbersome manual operations and no automation in the existing technology have been solved, and efficient and accurate detection results and improved work efficiency are achieved.

CN119290657BActive Publication Date: 2025-03-14HUAIAN VITALITY ANTISTALING CO LTD
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Patent Information

Application Number
CN202411832873.9
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2024-12-13
Publication Date
2025-03-14
Estimated Expiration
2044-12-13

AI Technical Summary

Technical Problem

The existing methods for detecting oxygen absorption of deoxidant have problems such as cumbersome manual operation, no automation, errors in artificial reading, errors in exposure to air, inability to record data in real time, low oxygen absorption due to water seal, difficult oil bath to clean, and tool placement of deep detection bottles is required.

Method used

An intelligent deoxidant oxygen absorption detection system is designed, including supporting table, computer body, constant temperature frame, detection bottle, digital pressure sensor and temperature and humidity sensor. The oxygen absorption is automatically monitored and calculated through an electronic control system. The data is recorded in the computer system in real time without the need to place the deoxidant with the help of tools.

Benefits of technology

It realizes automated detection, reduces manual operations, improves reading accuracy, avoids errors caused by air exposure by deoxidants, monitors data in real time, solves the problems caused by water seals and oil baths, and improves work efficiency, and can detect multiple samples at the same time.

✦ Generated by Eureka AI based on patent content.

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Abstract

The present invention relates to the technical field of deoxidizer detection, specifically to an intelligent deoxidizer oxygen absorption detection system, comprising a support table, the surface of the support table is provided with a computer body, the top surface of the support table is fixedly connected with a mounting frame, the back of the support table is fixedly connected with a bottom plate, the top surface of the bottom plate is provided with a PLC control cabinet, the front surface of the support table is provided with a connector, the back of the connector is provided with a constant temperature frame, and a constant temperature tank is provided inside the constant temperature frame; an air intake pipe, the air intake pipe is installed on the left side surface of the detection bottle. The present invention calculates the oxygen absorption by using an electronic control system to monitor the changes in air pressure and oxygen concentration in a closed detection bottle in real time, which completely avoids the inaccurate readings and the inability to monitor in real time when reading manually, and also avoids the problem that the measured value in the water seal is slightly smaller than that in the oil seal. At the same time, the device also solves the problem of low experimental work efficiency.
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Description

Technical Field

[0001] The invention relates to the technical field of deoxidizer detection, in particular to an intelligent deoxidizer oxygen absorption detection system. Background Art

[0002] The detection principle of the oxygen absorption of the deoxidizer is to place the deoxidizer in a liquid-sealed closed container under normal pressure and temperature conditions. After the deoxidizer reacts chemically with the oxygen in the air, a pressure difference is formed inside and outside the container, causing the liquid level of the closed container to rise. The volume of the rising liquid level is the oxygen absorption volume of the oxygen absorption. The oxygen absorption of the measured deoxidizer is obtained by calculating the liquid level difference before and after the closed container.

[0003] The current method for detecting the oxygen absorption of deoxidizer is as follows: fix the deoxidizer on the bracket, and form a beaker, a measuring cylinder, a bracket, an ear cleaning bulb and a silicone tube as shown in the figure. Fig.13 The test system shown. Use the ear-washing bulb to adjust the page in the measuring cylinder to the reading scale of the measuring cylinder, then pull out the rubber tube from the measuring cylinder, and observe the initial position of the page and the change in the liquid level position under constant temperature and pressure conditions;

[0004] Every 24 hours, replace the measuring cylinder filled with fresh air and repeat the above steps until the liquid level no longer rises significantly within 24 hours.

[0005] The first change in the position of the measuring cylinder page is represented as ∆V1; the second change in the position of the measuring cylinder page is represented as ∆V2; and so on, the nth change in the position of the measuring cylinder page is represented as ∆Vn.

[0006] Taking into account the effect of ambient temperature on the air pressure in the measuring cylinder, a blank control experiment was set up under the same experimental conditions to calibrate the scale change value.

[0007] The oxygen absorption of the sample is calculated as follows: V = ∆V1 + ∆V2 + ... + ∆Vn

[0008] Where: V is oxygen uptake, in milliliters (mL);

[0009] ∆V1-∆Vn is the change in page position from the first to the nth time, in milliliters (mL).

[0010] The above detection methods have certain problems: (1) Manual operation is cumbersome; (2) There is no automation and traceability; (3) Manual readings result in errors; (4) The deoxidizer is directly exposed to the air due to the repeated ventilation, resulting in errors; (5) Data cannot be recorded in real time; (6) The use of water seals will cause the oxygen absorption of the deoxidizer to be slightly less than the actual measured value, but the use of oil baths is not easy to clean. At the same time, when placing the deoxidizer for testing, most of them are placed manually. At the same time, when the depth of the test bottle is deep, it is necessary to use tools to place it. Therefore, there are certain limitations when placing the deoxidizer for testing. Therefore, it is urgent to improve and perfect the above problems. Summary of the invention

[0011] The purpose of the present invention is to provide an intelligent deoxidizer oxygen absorption detection system to solve certain problems existing in the detection method proposed in the above background technology: cumbersome manual operation; no automation and no traceability; manual reading, resulting in errors; the back and forth replacement of ventilation causes the deoxidizer to be directly exposed to the air, resulting in errors; it is impossible to record data in real time; the use of water seal will cause the oxygen absorption of the deoxidizer to be slightly less than the actual measured value, but the use of oil bath is not easy to clean, and at the same time, when the depth of the detection bottle is deep, it needs to be placed with the help of tools, so there are certain limitations when placing the deoxidizer for detection.

[0012] To achieve the above-mentioned purpose, the present invention provides the following technical solutions: an intelligent deoxidizer oxygen absorption detection system, comprising a support table, a computer body is arranged on the surface of the support table, a mounting frame is fixedly connected to the top surface of the support table, a bottom plate is fixedly connected to the back of the support table, a PLC control cabinet is arranged on the top surface of the bottom plate, a connecting piece is arranged on the front surface of the support table, a constant temperature frame is arranged on the back of the connecting piece, a constant temperature tank is arranged inside the constant temperature frame, a detection bottle is arranged inside the constant temperature tank, and five groups of the constant temperature frame are arranged;

[0013] An air inlet pipe is installed on the left side surface of the detection bottle, an air outlet pipe and a humidity regulating port are sequentially provided on the right side surface of the detection bottle from top to bottom, a pneumatic valve body is provided on the outer surface of the air inlet pipe, a digital pressure sensor body and a temperature and humidity sensor body are sequentially installed on the top surface of the detection bottle from left to right, the temperature and humidity sensor body is inserted and installed inside the detection bottle, a take-and-place groove is provided on the right side surface of the detection bottle, a rotating shaft is inserted and installed inside the detection bottle, and twenty groups of detection bottles are provided.

[0014] Preferably, a sealing plate is provided on the outer surface of the rotating shaft, and sealing gaskets are provided on the upper and lower ends of the sealing plate, and the sealing plate and the placing and taking groove are adapted to each other.

[0015] Preferably, a pull column is provided on the right side surface of the sealing plate, and an elastic band body is installed on the left side surface of the sealing plate.

[0016] Preferably, a support rod is provided on the inner bottom wall of the detection bottle, and a magnet is installed on the top surface of the support rod.

[0017] Preferably, an iron block is magnetically connected to the inner wall of the magnet stone, and a sample disk is fixedly connected to the top surface of the iron block.

[0018] Preferably, a connecting plate is fixedly connected to the right surface of the iron block, spring shafts are inserted and installed at the upper and lower ends of the connecting plate, a top block is fixedly connected to the top surface of the spring shaft, a connecting frame is provided at the lower end of the top block, and an auxiliary roller is provided inside the connecting frame.

[0019] Preferably, a connecting tube is fixedly connected to the back of the connecting plate, a mounting plate is installed on the back of the connecting tube, a fixing piece is fixedly connected to the right side surface of the mounting plate, and the fixing piece is fixedly connected to the elastic band body.

[0020] Preferably, the back side of the top block is fixedly connected to a side plate, the lower surface of the side plate is fixedly connected to a limiting roller, the outer surface of the limiting roller is provided with a limiting ring, and the right side surface of the limiting ring is fixedly connected to a limiting frame.

[0021] Preferably, a movable shaft is provided on the inner side wall of the sealing plate, and a conveying block is provided on the left side surface of the movable shaft.

[0022] Preferably, the connection frame is mounted on the inner wall of the detection bottle, the left end of the elastic belt body is mounted on the surface of the fixing member, and the outer surface of the elastic belt body is in contact with the outer surfaces of the limiting roller and the auxiliary roller.

[0023] Compared with the prior art, the present invention has the following beneficial effects:

[0024] 1. The intelligent deoxidizer oxygen absorption detection system is designed by placing twenty groups of detection bottles inside five groups of constant temperature frames and constant temperature tanks, and the sizes of the detection bottles can be different. Compared with the above-mentioned manually constructed instruments, this design has the advantages of easy use, accurate readings, no need to change media, and automatic calibration; the deoxidizer oxygen absorption detection system has a high degree of automation, can set relevant parameters according to user needs, and automatically measure and calculate the total oxygen absorption of the sample, with the advantage of unattended operation; according to user needs, multiple deoxidizer samples can be tested simultaneously within a unit time, greatly improving work efficiency, and innovatively using electronic control systems to monitor the changes in air pressure and oxygen concentration in the closed detection bottle in real time to calculate the oxygen absorption, The data is recorded in the computer system in the form of electronic data, which completely avoids the inaccurate readings that exist during manual readings, the inability to monitor inadequately in real time, and the problem that the measured value in the water seal is slightly smaller than that in the oil seal. At the same time, the device also solves the problem of low experimental work efficiency. Since the oxygen absorption test of the deoxidizer is time-consuming, depending on the type of sample, some samples may even take up to 240 hours. If the number of experimental samples is increased at the same time, the efficiency of the experiment per unit time can be improved. Therefore, the deoxidizer oxygen absorption detection system proposed by the present invention can be appropriately expanded as needed, the number of detection bottles can be increased, and the oxygen absorption test of multiple deoxidizers can be carried out simultaneously per unit time. A set of detection system can perform at least one hundred groups of samples at the same time.

[0025] 2. The intelligent deoxidizer oxygen absorption detection system solves the problem that the cover needs to be screwed out before feeding. This design does not require the use of tools for placement, and the speed of placing the deoxidizer is fast. This design can facilitate the removal and placement of the deoxidizer, and the overall operation efficiency is high. At the same time, after the deoxidizer is taken out and placed, the sealing plate can automatically return to its original position for detection through the elasticity of the elastic belt body and the spring shaft. The overall linkage effect is better, which reflects the functionality of the design. BRIEF DESCRIPTION OF THE DRAWINGS

[0026] Figure 1 It is a three-dimensional schematic diagram of the structure of the present invention;

[0027] Figure 2 It is a three-dimensional schematic diagram of the constant temperature frame structure of the present invention;

[0028] Figure 3 It is a three-dimensional schematic diagram of the detection bottle structure of the present invention;

[0029] Figure 4 It is a schematic diagram of the disassembly of the detection bottle and the digital pressure sensor body structure of the present invention;

[0030] Figure 5 This is a schematic diagram of the disassembly of the detection bottle structure of the present invention;

[0031] Figure 6It is a three-dimensional schematic diagram of the sample tray and top block structure of the present invention;

[0032] Figure 7 It is a three-dimensional schematic diagram of the support rod and magnet stone structure of the present invention;

[0033] Figure 8 It is a three-dimensional schematic diagram of the iron block and the elastic belt main body structure of the present invention;

[0034] Fig. 9 It is a three-dimensional schematic diagram of the connecting tube and the fixing member structure of the present invention;

[0035] Fig.10 It is a schematic diagram of the side plate and limiting roller structure of the present invention;

[0036] Fig.11 It is a schematic diagram of the disassembly of the sealing plate and the elastic belt body structure of the present invention;

[0037] Fig.12 It is a schematic diagram of the movable shaft and conveying block structure of the present invention;

[0038] Fig.13 Schematic diagram of a prior art test system.

[0039] In the figure: 1. Support table; 2. Computer body; 3. Installation frame; 4. Bottom plate; 5. PLC control cabinet; 6. Connectors; 7. Constant temperature frame; 8. Constant temperature tank; 9. Detection bottle; 10. Air inlet pipe; 11. Air outlet pipe; 12. Humidity adjustment port; 13. Pneumatic valve body; 14. Digital pressure sensor body; 15. Rotating shaft; 16. Sealing plate; 17. Sealing pad; 18. Pull column; 19. Elastic belt body; 2 0. Support rod; 21. Magnet; 22. Iron block; 23. Sample plate; 24. Connecting plate; 25. Spring shaft; 26. Connecting frame; 27. Connecting cylinder; 28. Mounting plate; 29. ​​Fixing piece; 30. Side plate; 31. Limit roller; 32. Limit ring; 33. Limit frame; 34. Auxiliary roller; 35. Top block; 37. Movable shaft; 38. Conveying block; 39. Pick-up and drop slot; 40. Temperature and humidity sensor body. DETAILED DESCRIPTION

[0040] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0041] See also Figure 1-13 , an embodiment provided by the present invention:

[0042] A smart deoxidizer oxygen absorption detection system, the computer body 2, PLC control cabinet 5, constant temperature frame 7, constant temperature bath 8, detection bottle 9, pneumatic valve body 13, digital display pressure sensor body 14, magnet 21, temperature and humidity sensor body 40 and iron block 22 used in this application are all products that can be directly purchased on the market, and their principles and connection methods are all existing technologies well known to those skilled in the art, so they are not repeated here, including a support table 1, the surface of the support table 1 is provided with a computer body 2, the top surface of the support table 1 is fixedly connected with a mounting frame 3, the back of the support table 1 is fixedly connected with a bottom plate 4, the top surface of the bottom plate 4 is provided with a PLC control cabinet 5, the front surface of the support table 1 is provided with a connector 6, the back of the connector 6 is provided with a constant temperature frame 7, the interior of the constant temperature frame 7 is provided with a constant temperature bath 8, the interior of the constant temperature bath 8 is provided with a detection bottle 9, and the constant temperature frame 7 is provided with five groups;

[0043] An air inlet pipe 10 is installed on the left side surface of the detection bottle 9. An air outlet pipe 11 and a humidity regulating port 12 are arranged on the right side surface of the detection bottle 9 from top to bottom. A pneumatic valve body 13 is arranged on the outer surface of the air inlet pipe 10. A digital pressure sensor body 14 and a temperature and humidity sensor body 40 are arranged on the top surface of the detection bottle 9 from left to right. The temperature and humidity sensor body 40 is inserted and installed inside the detection bottle 9. A pick-up and drop groove 39 is provided on the right side surface of the detection bottle 9. A rotating shaft 15 is inserted and installed inside the detection bottle 9. Twenty groups of detection bottles 9 are arranged. A sealing plate 16 is arranged on the outer surface of the rotating shaft 15. A sealing gasket 17 is arranged on the upper and lower ends of the sealing plate 16. The sealing plate 16 and the pick-up and drop groove 39 are adapted to each other. The sealing plate A pull column 18 is provided on the right surface of 16, an elastic band body 19 is installed on the left surface of the sealing plate 16, a support rod 20 is provided on the inner bottom wall of the detection bottle 9, a magnet stone 21 is installed on the top surface of the support rod 20, an iron block 22 is magnetically connected to the inner wall of the magnet stone 21, a sample disk 23 is fixedly connected to the top surface of the iron block 22, a connecting plate 24 is fixedly connected to the right surface of the iron block 22, a spring shaft 25 is inserted and installed at the upper and lower ends of the connecting plate 24, a top block 35 is fixedly connected to the top surface of the spring shaft 25, a connecting frame 26 is provided at the lower end of the top block 35, an auxiliary roller 34 is provided inside the connecting frame 26, a connecting cylinder 27 is fixedly connected to the back of the connecting plate 24, a mounting plate 28 is installed on the back of the connecting cylinder 27, and the right side of the mounting plate 28 The side surface is fixedly connected with a fixing piece 29, and the fixing piece 29 is fixedly connected to the elastic band body 19. The back of the top block 35 is fixedly connected with a side plate 30. The lower surface of the side plate 30 is fixedly connected with a limiting roller 31. The outer surface of the limiting roller 31 is provided with a limiting ring 32. The right side surface of the limiting ring 32 is fixedly connected with a limiting frame 33. The inner side wall of the sealing plate 16 is provided with a movable shaft 37. The left side surface of the movable shaft 37 is provided with a conveying block 38. The connecting frame 26 is installed on the inner wall of the detection bottle 9. The left end of the elastic band body 19 is installed on the surface of the fixing piece 29. The outer surface of the elastic band body 19 is in contact with the outer surfaces of the limiting roller 31 and the auxiliary roller 34. First, the computer body 2, the bottom plate 4 and the digital pressure sensor body 14 on the top surface of the detection bottle 9 The temperature and humidity sensor bodies 40 are all electrically connected, and the digital pressure sensor body 14 and the temperature and humidity sensor body 40 can transmit the collected data to the computer body 2 and the PLC control cabinet 5. The overall data collection effect is relatively accurate. This design places twenty groups of test bottles 9 inside the five groups of constant temperature frames 7 and the constant temperature bath 8, and the sizes of the test bottles 9 can be different. When testing, first place the deoxidizer to be tested on the surface of the sample tray 23, and then cover the sealing plate 16. The sealing between the sealing plate 16 and the test bottle 9 is good, and then the computer body 2 can record the data collected by the digital pressure sensor body 14 and the temperature and humidity sensor body 40, so that the temperature, humidity, pressure, and residual oxygen content can be measured in real time.At the same time, the outer surface of the air inlet pipe 10 is provided with a pneumatic valve body 13 for controlling the inlet and outlet of gas, which can quantitatively fill the required gas into the detection bottle 9 to meet different experimental requirements. Compared with the above-mentioned manually constructed instruments, this design has the advantages of easy use, accurate readings, no need to change the medium, and automatic calibration; the deoxidizer oxygen absorption detection system has a high degree of automation, can set relevant parameters according to user needs, and automatically measure and calculate the total oxygen absorption of the sample, and has the advantage of unattended operation; according to user needs, multiple deoxidizer samples can be tested simultaneously within a unit time, greatly improving work efficiency, and innovatively using an electronic control system to monitor the changes in air pressure and oxygen concentration in the closed detection bottle 9 in real time to calculate the oxygen absorption, and the data is in the form of electronic data The mode of the data is recorded in the computer system, which completely avoids the inaccurate readings that exist during manual readings, the inability to monitor in real time, and the problem that the measured value in the water seal is slightly smaller than that in the oil seal. At the same time, the device also solves the problem of low experimental work efficiency. Since the oxygen absorption test of the deoxidizer is time-consuming, depending on the type of sample, some samples may even take up to 240 hours. If the number of experimental samples is increased at the same time, the efficiency of the experiment per unit time can be improved. Therefore, the oxygen absorption detection system of the deoxidizer proposed in the present invention can be appropriately expanded as needed, and the number of detection bottles 9 can be increased. The oxygen absorption test of multiple deoxidizers can be carried out simultaneously per unit time. A set of detection system can do at least one hundred groups of samples at the same time. When conducting actual detection, first First, hold the pulling column 18, and by pulling the pulling column 18, the sealing plate 16 will rotate through the rotating shaft 15, and then the sealing plate 16 will rotate with the rotating shaft 15 as the center, so that the sealing plate 16 will pull the elastic belt body 19 to move. At this time, the outer surface of the elastic belt body 19 will fit on the back of the auxiliary roller 34 and the limiting roller 31. The position of the elastic belt body 19 can be limited by the design of the auxiliary roller 34 and the limiting roller 31. Then, since the elastic belt body 19 is pulled, and the left end of the elastic belt body 19 is installed on the surface of the fixing member 29, the fixing member 29 and the mounting plate 28 can be pulled. At this time, after the mounting plate 28 rotates, it will also drive the connecting plate 24 to rotate. Since the upper and lower ends of the connecting plate 24 are both installed There is a spring shaft 25, so that the connecting plate 24 will drive the iron block 22 and the sample tray 23 to rotate, so that the sample tray 23 can rotate with the connecting plate 24. When the connecting plate 24 rotates to a suitable angle, the connecting plate 24 will move to the vicinity of the pick-up and placement groove 39, and then place the deoxidizer on the surface of the sample tray 23, so that rapid placement can be completed. This feeding method solves the problem of needing to screw out the cover body before feeding. At the same time, when the bottle body is deep, the placement of the deoxidizer requires the aid of tools. This design does not require the aid of tools for placement. The speed of placing the deoxidizer is fast, and then the pull column 18 is slowly released. Since the elastic belt body 19 is elastic, no tension is applied to the elastic belt body 19.At this time, the elastic band body 19 will slowly shrink, and then the mounting plate 28 and the fixing member 29 will slowly return to their original positions, and finally the connecting plate 24 and the iron block 22 will return to their original positions, so that the sample tray 23 will also return to its original position. At this time, the deoxidizer on the surface of the sample tray 23 can be stably placed, and at the same time, the elastic band body 19 has elasticity, so that the elastic band body 19 will also stably pull the sealing plate 16, and at this time, the sealing effect between the sealing plate 16 and the placement groove 39 is good, and at the same time, the elastic design of the spring shaft 25 can also well restore the sample tray 23 with the deoxidizer placed thereon to its original position, and at the same time, when returning to its original position, the outer surface of the iron block 22 will contact the inner wall of the magnet stone 21, so that the iron block 22 and the magnet stone 21 are magnetically attracted to each other, and the overall magnetic attraction effect is good, so that the iron block 22 is overall stable on the surface of the magnet stone 21, which enhances the stability of the sample tray 23 during detection, and the design can facilitate the placement of the deoxidizer, and the overall operation efficiency is high. At the same time, after the deoxidizer is placed, the sealing plate 16 is moved by the elastic band body 19 and The elasticity of the spring shaft 25 can automatically restore to its original position for detection, and the overall linkage effect is relatively good. Subsequently, after the sealing plate 16 is rotated, the movable shaft 37 can be rotated on the inner surface of the sealing plate 16, so that the conveying block 38 can be overlapped on the surface of the sample tray 23, and then the deoxidizer can be directly placed on the surface of the movable shaft 37, so that the deoxidizer will slide from the surface of the movable shaft 37 to the surface of the sample tray 23, so that the overall placement of the deoxidizer is simpler, and the position of the elastic belt body 19 can be limited by the cooperation of the limiting roller 31 and the limiting frame 33. Through the design of the spring shaft 25, when the sealing plate 16 does not apply tension, the spring shaft 25 can drive the connecting tube 27 and the fixing member 29 to rotate, so that the sealing plate 16 is pulled by the elastic belt body 19, so that the sealing plate 16 body can be attached to the outer surface of the detection bottle 9. At this time, the detection bottle 9 is in a sealed state, and the sealing plate 16 is always attached to the detection bottle 9 by the tension of the elastic belt body 19 to seal the detection bottle 9;

[0044] Testing steps:

[0045] ① After placing the deoxidizer on the sample tray 23, the sealing plate 16 will automatically cover it to ensure its sealing.

[0046] ② Click the start button on the desktop of the computer body 2 to record the temperature, humidity, pressure and residual oxygen content in real time.

[0047] ③When the temperature and volume are constant, according to the ideal gas state equation PV=nRT

[0048] Assume that initially: P1V1=n1RT1....①

[0049] At any time: P2V2=n2RT2....②

[0050] Because V1=V2; T1=T2, so P1 / P2=n1 / n2

[0051] And because the oxygen absorption V = (1- (n2 / n1)) * V1, so V = (1- (p2 / p1)) * V1

[0052] P1-The initial gas pressure in the reactor, i.e. atmospheric pressure, unit (Pa).

[0053] P2-Real-time gas pressure in the reactor, unit (Pa).

[0054] v1-Real-time gas volume inside the reactor, i.e. reactor volume, unit (m3).

[0055] V2-The volume of gas inside the reactor at the end of the reaction, that is, the volume of the reactor, unit (m3).

[0056] T1-initial temperature inside the reactor, unit (K).

[0057] T2-Real-time temperature inside the reactor, unit (K).

[0058] n1-the amount of initial gas substance inside the reactor, unit (mol).

[0059] n2-The real-time amount of gaseous substances inside the reactor, unit (mol).

[0060] Ideal gas constant, unit (J / (mol·K)). V-oxygen absorption

[0061] ④ Oxygen absorption is also equal to: volume * (20.9-residual oxygen content) * %

[0062] It can meet the needs of various types of deoxidizers for oxygen absorption analysis and real-time monitoring.

[0063] Working principle: When the staff uses this device, first connect the device to an external power supply to provide power support for the device. First, the computer body 2, the bottom plate 4 and the digital pressure sensor body 14 and the temperature and humidity sensor body 40 on the top of the detection bottle 9 are electrically connected. The digital pressure sensor body 14 and the temperature and humidity sensor body 40 can transmit the collected data to the computer body 2 and the PLC control cabinet 5. The overall data collection effect is relatively accurate. This design places twenty groups of detection bottles 9 inside the five groups of constant temperature frames 7 and the constant temperature bath 8, and the detection bottles 9 are The size can be different. When testing, first place the deoxidizer to be tested on the surface of the sample tray 23, then cover the sealing plate 16, the sealing plate 16 and the test bottle 9 have good sealing performance, and then the computer body 2 can record the data collected by the digital pressure sensor body 14 and the temperature and humidity sensor body 40, so that the temperature, humidity, pressure, and residual oxygen content can be measured in real time. At the same time, the outer surface of the air inlet pipe 10 is provided with a pneumatic valve body 13 for controlling the inlet and outlet of the gas, and the required gas can be quantitatively filled into the test bottle 9 to meet different experimental requirements;

[0064] During the actual test, first hold the pulling column 18, and by pulling the pulling column 18, the sealing plate 16 will rotate through the rotating shaft 15, and then the sealing plate 16 will rotate around the rotating shaft 15 as the center, so that the sealing plate 16 will pull the elastic belt body 19 to move. At this time, the outer surface of the elastic belt body 19 will fit on the back of the auxiliary roller 34 and the limiting roller 31. The position of the elastic belt body 19 can be limited by the design of the auxiliary roller 34 and the limiting roller 31. Then, due to the pulling of the elastic belt body 19, the left end of the elastic belt body 19 is installed on the surface of the fixing member 29. Thereby, the fixing member 29 and the mounting plate 28 can be pulled. At this time, after the mounting plate 28 rotates, the connecting plate 24 will also be driven to rotate. Since the upper and lower ends of the connecting plate 24 are both equipped with spring shafts 25, the connecting plate 24 will drive the iron block 22 and the sample tray 23 to rotate, so that the sample tray 23 can rotate with the connecting plate 24. When the connecting plate 24 rotates to a suitable angle, the connecting plate 24 will move to the vicinity of the pick-up and placement groove 39, and then place the deoxidizer on the surface of the sample tray 23, so that rapid placement can be completed, and then the pulling column 18 is slowly released. The elastic belt body 19 is elastic, so that after no tension is applied to the elastic belt body 19, the elastic belt body 19 will slowly shrink, and then the mounting plate 28 and the fixing member 29 will slowly return to their original positions, and finally the connecting plate 24 and the iron block 22 will return to their original positions, so that the sample tray 23 will also return to their original positions. At this time, the deoxidizer on the surface of the sample tray 23 can be stably placed. At the same time, the elastic belt body 19 is elastic, so that the elastic belt body 19 will also stably pull the sealing plate 16. At this time, the sealing effect between the sealing plate 16 and the pick-up and placement groove 39 is better, and at the same time, the elasticity of the spring shaft 25 The design can also well restore the sample tray 23 with the deoxidizer placed in it to its original position. At the same time, when restoring to its original position, the outer surface of the iron block 22 will contact the inner wall of the magnet stone 21, so that the iron block 22 and the magnet stone 21 are magnetically attracted to each other, and the overall magnetic attraction effect is good, so that the iron block 22 is overall stable on the surface of the magnet stone 21, and the stability of the sample tray 23 during detection is enhanced. This design can facilitate the removal and placement of the deoxidizer. At the same time, after the deoxidizer is removed and placed, the sealing plate 16 can automatically restore to its original position for detection through the elasticity of the elastic band body 19 and the spring shaft 25. The above is all the working principles of the present invention.

[0065] The above description is only a preferred embodiment of the present invention and does not limit the present invention in any form. Any ordinary technician in the industry can smoothly implement the present invention as shown in the drawings and described above. However, any equivalent changes, modifications and evolutions made by technicians familiar with the profession without departing from the scope of the technical solution of the present invention using the technical content disclosed above are all equivalent embodiments of the present invention. At the same time, any equivalent changes, modifications and evolutions made to the above embodiments based on the essential technology of the present invention are still within the protection scope of the technical solution of the present invention.

Claims

1. An intelligent deoxidizer oxygen absorption detection system, comprising a support table (1), a computer body (2) is arranged on the surface of the support table (1), a mounting frame (3) is fixedly connected to the top surface of the support table (1), a bottom plate (4) is fixedly connected to the back surface of the support table (1), and a PLC control cabinet (5) is arranged on the top surface of the bottom plate (4), characterized in that: The front surface of the support table (1) is provided with a connecting piece (6), the back surface of the connecting piece (6) is provided with a constant temperature frame (7), a constant temperature tank (8) is provided inside the constant temperature frame (7), a detection bottle (9) is provided inside the constant temperature tank (8), and the constant temperature frame (7) is provided with five groups; An air intake pipe (10), the air intake pipe (10) being mounted on the left side surface of the detection bottle (9), the right side surface of the detection bottle (9) being provided with an air outlet pipe (11) and a humidity adjustment port (12) in sequence from top to bottom, the outer surface of the air intake pipe (10) being provided with a pneumatic valve body (13), the top surface of the detection bottle (9) being provided with a digital pressure sensor body (14) and a temperature and humidity sensor body (40) in sequence from left to right, the temperature and humidity sensor body (40) being inserted and mounted inside the detection bottle (9), the detection bottle ( A pick-up and release groove (39) is provided on the right side surface of the detection bottle (9), a rotating shaft (15) is inserted and installed inside the detection bottle (9), and the detection bottle (9) is provided with twenty groups. A sealing plate (16) is provided on the outer surface of the rotating shaft (15), and sealing gaskets (17) are provided at the upper and lower ends of the sealing plate (16). The sealing plate (16) and the pick-up and release groove (39) are adapted to each other, a pulling column (18) is provided on the right side surface of the sealing plate (16), and an elastic band body (19) is installed on the left side surface of the sealing plate (16).

2. According to claim 1, an intelligent deoxidizer oxygen absorption detection system is characterized in that: The inner bottom wall of the detection bottle (9) is provided with a support rod (20), and a magnet (21) is installed on the top surface of the support rod (20).

3. The intelligent deoxidizer oxygen absorption detection system according to claim 2 is characterized in that: The inner wall of the magnet (21) is magnetically connected to an iron block (22), and the top surface of the iron block (22) is fixedly connected to a sample plate (23).

4. The intelligent deoxidizer oxygen absorption detection system according to claim 3 is characterized in that: A connecting plate (24) is fixedly connected to the right side surface of the iron block (22), a spring shaft (25) is inserted and installed at the upper and lower ends of the connecting plate (24), a top block (35) is fixedly connected to the top surface of the spring shaft (25), a connecting frame (26) is provided at the lower end of the top block (35), and an auxiliary roller (34) is provided inside the connecting frame (26).

5. The intelligent deoxidizer oxygen absorption detection system according to claim 4 is characterized in that: The back of the connecting plate (24) is fixedly connected to a connecting tube (27), the back of the connecting tube (27) is mounted with a mounting plate (28), the right side surface of the mounting plate (28) is fixedly connected to a fixing member (29), and the fixing member (29) is fixedly connected to the elastic band body (19).

6. The intelligent deoxidizer oxygen absorption detection system according to claim 4 is characterized in that: The back surface of the top block (35) is fixedly connected to a side plate (30), the lower surface of the side plate (30) is fixedly connected to a limiting roller (31), the outer surface of the limiting roller (31) is provided with a limiting ring (32), and the right side surface of the limiting ring (32) is fixedly connected to a limiting frame (33).

7. The intelligent deoxidizer oxygen absorption detection system according to claim 1 is characterized in that: A movable shaft (37) is provided on the inner side wall of the sealing plate (16), and a conveying block (38) is provided on the left side surface of the movable shaft (37).

8. The intelligent deoxidizer oxygen absorption detection system according to claim 4 is characterized in that: The connection frame (26) is mounted on the inner wall of the detection bottle (9), the left end of the elastic belt body (19) is mounted on the surface of the fixing member (29), and the outer surface of the elastic belt body (19) is in contact with the outer surfaces of the limiting roller (31) and the auxiliary roller (34).

Citation Information

Patent Citations

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    CN104990833A

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    CN204718917U