Continuous carbonization, graphitization and purification equipment and method and readable storage medium
Through the integration of carbonization, graphitization and purification equipment, and the continuous production method of multi-processing bins and steering mechanisms is adopted, the problems of low production efficiency and high cost of hard carbon felt are solved, and efficient and low-cost continuous production is achieved.
Patent Information
- Application Number
- CN202510815231.6
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-06-18
- Publication Date
- 2025-07-18
- Estimated Expiration
- 2045-06-18
AI Technical Summary
The carbonization, graphitization and purification processes of hard carbon felt have problems such as low working efficiency and high production costs. The existing equipment covers a large area and has high energy consumption.
A continuous carbonization, graphitization and purification equipment is designed to integrate carbonization, graphitization and purification equipment, and multiple processing tanks and transition tanks are used to achieve continuous production of materials through steering mechanisms and propulsion components, and the temperature is controlled using a vacuum pump and heating system.
The continuous production of hard carbon felt is achieved, which reduces production costs, reduces floor area, improves production efficiency, and prevents the failure of moving parts at high temperatures through dynamic sealing and propulsion components.
Smart Images

Figure CN120333155A_ABST
Abstract
Description
Technical Field
[0001] The present invention provides a continuous carbonization, graphitization, purification equipment, method and readable storage medium, belonging to the technical field of carbon felt processing. Background Art
[0002] Hard carbon felt is widely used as a heat insulation material in vacuum thermal equipment such as high-temperature purification furnaces, silicon carbide coating furnaces, silicon carbide crystal growth furnaces and tantalum carbide coating furnaces. The main manufacturing processes of hard carbon felt include forming, curing, carbonization, graphitization and purification. At present, the carbonization of hard carbon felt requires putting the hard carbon felt into an intermittent carbonization furnace, heating up, keeping warm and cooling down, and then taking it out of the intermittent carbonization furnace, and then entering an intermittent graphitization furnace, which also requires heating up, keeping warm and cooling down and then taking it out of the graphitization furnace. If high-quality hard carbon felt is required, the hard carbon felt also needs to be put into an intermittent purification furnace for further purification. This results in long production time, high production cost, high production energy consumption, and high product price of hard carbon felt, seriously restricting the development of the industry.
[0003] Based on this, the Chinese utility model patent (CN203699918U) proposes a carbonization graphitization continuous high-temperature furnace, which includes a feeding chamber, a graphite partition door, a boat pushing mechanism, a carbonization cavity, a transition chamber, a graphitization cavity and a discharging chamber. The carbonization cavity and the graphitization cavity are connected together through the transition chamber, so that the graphite raw material after carbonization directly enters the graphitization high-temperature furnace through the transition chamber, thus realizing continuous production of carbonization and graphitization. However, its carbonization cavity and graphitization cavity are separately arranged, resulting in large equipment floor area and high manufacturing cost. Summary of the Invention
[0004] In order to solve the technical problems of low working efficiency and high manufacturing cost in the carbonization, graphitization and purification of hard carbon felt, the present invention proposes a continuous carbonization, graphitization, purification equipment, method and readable storage medium, integrating the carbonization equipment, graphitization equipment and purification equipment into one, and realizing continuous production of carbonization, graphitization and purification of hard carbon felt.
[0005] In order to solve the above technical problems, the technical solution adopted by the present invention is: a continuous carbonization, graphitization, purification equipment, including a first vacuum pump, a plurality of processing chambers and a plurality of transition chambers, the two processing chambers are connected through the transition chambers, at least one first steering mechanism is arranged on each of the processing chambers, at least one second steering mechanism is arranged on each of the transition chambers, and the first steering mechanism and the second steering mechanism cooperate with each other; The multiple processing chambers are respectively a carbonization graphitization chamber, a purification chamber and a cooling chamber, the carbonization graphitization chamber, the purification chamber and the cooling chamber are connected in sequence, the carbonization graphitization chamber is further connected with a feeding chamber, and the cooling chamber is further connected with a discharging chamber; The feeding bin, the transition bin, and multiple processing bins are respectively movably connected with at least one propulsion component, and the propulsion component acts on the tray. The carbonization and graphitization bin includes a carbonization area and a graphitization area, which are partitioned. The carbonization area is provided with a number of first transmission components, and the graphitization area is provided with a number of second transmission components, and the first transmission components and the second transmission components cooperate with each other; the first transmission components, the second transmission components cooperate with the first steering mechanism. The third transmission component arranged in the purification bin cooperates with the first steering mechanism and the second steering mechanism. The fourth transmission component arranged in the cooling bin cooperates with the first steering mechanism and the second steering mechanism. The feeding bin and the carbonization area are connected to the first vacuum pump through a cyclone filter device arranged in the air extraction pipeline.
[0006] Further, the multiple transition bins are respectively a first transition bin and a second transition bin. The first transition bin is arranged between the carbonization and graphitization bin and the purification bin, and the second transition bin is arranged between the purification bin and the cooling bin.
[0007] Further, a first plug valve is arranged between the feeding bin and the carbonization and graphitization bin and between the cooling bin and the discharging bin, and a second plug valve is arranged between the processing bin and the transition bin.
[0008] Further, a first transmission device is arranged on the first steering mechanism, and a second transmission device is arranged on the second steering mechanism, and the first transmission device and the second transmission device cooperate with each other.
[0009] Further, the first steering mechanism includes a lifting mechanism and a commutation mechanism. The lifting mechanism includes a first rotating shaft and a lifting shaft, the first rotating shaft and the lifting shaft are connected to each other, the first rotating shaft is connected to the output end of the lifting motor, the lifting shaft is rotatably connected to the second rotating shaft of the commutation mechanism, the second rotating shaft is connected to the processing bin through a first magnetic fluid sealing assembly, the second rotating shaft is also connected with a pulley and a bottom plate, the pulley is connected to the output end of the rotating motor through a belt, a tray is placed on the bottom plate, the structure of the second steering mechanism is the same as the structure of the first steering mechanism, and the second rotating shaft of the second steering mechanism is connected to the transition bin through a second magnetic fluid sealing assembly.
[0010] Further, a third plug valve is movably connected to both the carbonization and graphitization bin and the purification bin, and the third plug valve cooperates with the propulsion component.
[0011] Further, the first transition bin and the purification bin are connected to the second vacuum pump through a first filter tank arranged in the first vacuum pipeline, and the first vacuum pipeline is connected between the first transition bin, the purification bin and the second vacuum pump; The second transition bin and the cooling bin are connected to the output end of the strong cooling fan through a second filter tank arranged in the second vacuum pipeline, and the second vacuum pipeline is connected between the second transition bin, the cooling bin and the output end of the strong cooling fan.
[0012] Furthermore, a first heating system and a first temperature measuring system are installed in the carbonization area. The first heating system and the first temperature measuring system are electrically connected to form a feedback loop to control the temperature in the carbonization area to meet the carbonization requirements; a second heating system and a second temperature measuring system are installed in the graphitization area. The second heating system and the second temperature measuring system are electrically connected to form a feedback loop to control the temperature in the graphitization area to meet the graphitization requirements; a third heating system and a third temperature measuring system are installed in the purification bin. The third heating system and the third temperature measuring system are electrically connected to form a feedback loop to control the temperature in the purification bin to meet the purification requirements; a fourth temperature measuring system and a strong cooling fan are installed in the cooling bin. The fourth temperature measuring system and the strong cooling fan are electrically connected to form a feedback loop to ensure that the material placed in the cooling bin meets the discharge temperature requirements before being transported to the discharge bin.
[0013] A continuous carbonization, graphitization, and purification method uses the above-mentioned continuous carbonization, graphitization, and purification equipment, including the following steps: Step S1: Place the first material to be carbonized, graphitized, and purified into the feeding bin, and perform vacuum pumping on the feeding bin through the first vacuum pump. Step S2: Open the first plug valve between the feeding bin and the carbonization and graphitization bin, send the first material into the carbonization area of the carbonization and graphitization bin for carbonization treatment to obtain the second material, and then the first transmission part and the second transmission part cooperate with each other to send the second material into the graphitization area of the carbonization and graphitization bin for graphitization treatment to obtain the third material. Step S3: Open the second plug valve arranged between the carbonization and graphitization bin and the first transition bin and the second plug valve arranged between the first transition bin and the purification bin, and send the third material into the purification bin for purification treatment to obtain the fourth material. Step S4: Open the second plug valve arranged between the purification bin and the second transition bin and the second plug valve arranged between the second transition bin and the cooling bin, and send the fourth material into the cooling bin for cooling treatment. Step S5: Open the first plug valve arranged between the cooling bin and the discharge bin, and send the cooled fourth material into the discharge bin and then take it out. Step S6: Repeat the above steps S1 to S5 to realize the continuous production of carbonization, graphitization, and purification of the first material.
[0014] A readable storage medium stores a computer program thereon, and when the computer program is executed by a processor, the above-mentioned method steps are realized.
[0015] The beneficial effects of the present invention compared with the prior art are: 1. The present invention integrates traditional intermittent carbonization equipment, graphitization equipment, purification equipment, and cooling equipment into one, with multiple processing chambers provided, and adjacent processing chambers are connected through transition chambers to achieve continuous production of carbonization, graphitization, and purification of materials. Among them, the carbonization equipment and graphitization equipment are integrated into a carbonization and graphitization chamber, which greatly reduces the production costs of carbonization, graphitization, and purification, reduces the floor area occupied by the carbonization, graphitization, and purification production processes, and improves production efficiency. 2. The setting of the propulsion component in the present invention, compared with general moving components, can effectively prevent the situation where the moving components fail at high temperatures and thus affect the operation efficiency. 3. The propulsion component of the present invention cooperates with the steering mechanism. When the propulsion component needs to push multiple trays, the thrust of the propulsion component can be reduced, thereby improving production efficiency. 4. The present invention connects the steering mechanism to the processing chamber through the first magneto - fluid sealing assembly, which can achieve dynamic sealing and ensure that the inside of the processing chamber is in a vacuum state. BRIEF DESCRIPTION OF THE DRAWINGS
[0016] The following further describes the present invention with reference to the drawings: Figure 1 is a schematic structural diagram of the present invention; Figure 2 is a schematic structural diagram of the first steering mechanism of the present invention; Figure 3 is a schematic structural diagram of the cooperation between the first steering mechanism and the bottom plate of the present invention; Figure 4 is a schematic structural diagram of the first steering mechanism of the present invention before rotating the tray; Figure 5 is a schematic structural diagram of the first steering mechanism of the present invention after rotating the tray; Figure 6 is a schematic structural diagram of the cooperation between the first steering mechanism and the first transmission member of the present invention; In the figure: 1 is the first vacuum pump, 2 is the material tray, 3 is the feeding bin, 4 is the carbonization and graphitization bin, 5 is the purification bin, 6 is the cooling bin, 7 is the discharging bin, 8 is the first transition bin, 9 is the second transition bin, 10 is the first plug valve, 11 is the second plug valve, 12 is the third plug valve, 13 is the fourth plug valve, 14 is the propulsion component, 15 is the material, 16 is the cyclone filter device, 17 is the first working part, 18 is the second working part, 19 is the third working part, 20 is the fourth working part, 21 is the first push rod, 22 is the second push rod, 23 is the second vacuum pump, 24 is the first filter tank, 25 is the strong cooling fan, 26 is the first vacuum pipeline, 27 is the graphite roller, 28 is the first steering mechanism 1, 29 is the first steering mechanism 2, 30 is the second steering mechanism 1, 31 is the first steering mechanism 3, 32 is the second steering mechanism 2, 33 is the first steering mechanism 4, 34 is the first temperature measurement system, 35 is the second temperature measurement system, 36 is the third temperature measurement system, 37 is the fourth temperature measurement system, 38 is the first steering mechanism, 39 is the third push rod, 40 is the control system, 41 is the second vacuum pipeline, 42 is the second filter tank, 201 is the lifting motor, 202 is the connecting key, 203 is the first rotating shaft, 204 is the lifting nut, 205 is the lifting shaft, 206 is the pulley, 207 is the belt, 208 is the rotating motor, 209 is the first magneto-fluid sealing component, 210 is the second rotating shaft, 211 is the bottom plate. Detailed implementation mode
[0017] In the description of the present invention, it should be understood that the terms "center", "longitudinal", "transverse", "up", "down", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", etc. indicate relative orientation or position relationships, and are only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and thus cannot be understood as a limitation of the present invention. In addition, the terms "first", "second", etc. are only used for descriptive purposes and cannot be understood as indicating or implying relative importance or implicitly indicating the quantity of the indicated technical features. Thus, features defined with "first", "second", etc. may explicitly or implicitly include one or more of such features. In the description of the present invention, unless otherwise specified, the meaning of "a plurality" is two or more.
[0018] In the description of the present invention, it should be noted that unless otherwise clearly specified and defined, the terms "installation", "connection", and "coupling" should be understood in a broad sense. For example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediate medium, and it can be the communication inside two components. For those of ordinary skill in the art, the specific meanings of the above terms in the present invention can be understood according to specific circumstances.
[0019] As Figures 1 to 6 shown, the present invention provides a continuous carbonization, graphitization, and purification equipment, including a first vacuum pump 1, a plurality of processing chambers, and a plurality of transition chambers. The processing chambers are connected through the transition chambers in pairs. At least one first steering mechanism 38 is movably connected to each processing chamber, and at least one second steering mechanism is movably connected to each transition chamber. The first steering mechanism 38 and the second steering mechanism cooperate with each other.
[0020] The plurality of processing chambers are respectively a carbonization and graphitization chamber 4, a purification chamber 5, and a cooling chamber 6. The carbonization and graphitization chamber 4, the purification chamber 5, and the cooling chamber 6 are connected in sequence. The carbonization and graphitization chamber 4 is further connected to a feeding chamber 3, and the cooling chamber 6 is further connected to a discharging chamber 7. At least one pushing member 14 is movably connected to the feeding chamber 3, the transition chamber, and the plurality of processing chambers respectively. The pushing member 14 acts on a material tray 2, and the material tray 2 contains materials 15. The pushing member 14 includes a plurality of first push rods 21, a plurality of second push rods 22, and a plurality of third push rods 39.
[0021] In this embodiment, three first push rods 21 are provided, two of which are movably connected to the carbonization and graphitization chamber 4, respectively located in the carbonization area and the graphitization area, and the other is movably connected to the purification chamber 5.
[0022] In this embodiment, two second push rods 22 are provided, and the two second push rods 22 are respectively movably connected to the first transition chamber 8 and the second transition chamber 9.
[0023] In this embodiment, two third push rods 39 are provided, and the two third push rods 39 are respectively movably connected to the feeding chamber 3 and the cooling chamber 6. The two third push rods 39 respectively correspond to the valves on the feeding chamber 3 and the valves on the cooling chamber 6.
[0024] A first plug valve 10 is movably connected between the feeding chamber 3 and the carbonization and graphitization chamber 4, and between the cooling chamber 6 and the discharging chamber 7. The first plug valve 10 corresponds to and cooperates with the third push rod 39 one by one; a second plug valve 11 is movably connected between the processing chamber and the transition chamber. The second plug valve 11 corresponds to and cooperates with the second push rod 22 one by one; a third plug valve 12 is movably connected to both the carbonization and graphitization chamber 4 and the purification chamber 5. The third plug valve 12 corresponds to and cooperates with the first push rod 21 one by one.
[0025] The plurality of transition bins are respectively a first transition bin 8 and a second transition bin 9. The first transition bin 8 is arranged between the carbonization and graphitization bin 4 and the purification bin 5, and the second transition bin 9 is arranged between the purification bin 5 and the cooling bin 6.
[0026] In this embodiment, four first steering mechanisms 38 are provided, namely the first steering mechanism one 28, the first steering mechanism two 29, the first steering mechanism three 31, and the first steering mechanism four 33. A first transmission device is rotatably connected to the first steering mechanism 38; two second steering mechanisms are provided, namely the second steering mechanism one 30 and the second steering mechanism two 32, and a second transmission device is rotatably connected to the second steering mechanism. The first transmission device and the second transmission device cooperate with each other. The first steering mechanism one 28 is movably connected to the carbonization area of the carbonization and graphitization bin 4, the first steering mechanism two 29 is movably connected to the graphitization area of the carbonization and graphitization bin 4, the second steering mechanism one 30 is movably connected to the first transition bin 8, the first steering mechanism three 31 is movably connected to the purification bin 5, the second steering mechanism two 32 is movably connected to the second transition bin 9, and the first steering mechanism four 33 is movably connected to the cooling bin 6.
[0027] Specifically, a first through hole is provided through the bottom of the processing bin. The first steering mechanism 38 accesses the inside of the processing bin through the first through hole, and the first steering mechanism 38 is movably connected to the processing bin through the first through hole. More specifically, the first steering mechanism 38 includes a lifting mechanism and a commutation mechanism. The lifting mechanism includes a first rotating shaft 203 and a lifting shaft 205. The first rotating shaft 203 and the lifting shaft 205 are connected to each other. The first rotating shaft 203 is connected to the output end of the lifting motor 201 through a connection key 202. A lifting nut 204 is movably arranged on the first rotating shaft 203. The lifting nut 204 is fixedly connected to the lifting shaft 205. A second rotating shaft 210 is sleeved outside the lifting shaft 205. The lifting shaft 205 and the second rotating shaft 210 are rotatably connected, that is, the second rotating shaft 210 can rotate around the central axis of the second rotating shaft 210. The second rotating shaft 210 is also connected with a pulley 206 and a bottom plate 211. The pulley 206 is connected to the pulley 206 rotatably connected to the output end of the rotating motor 208 through a belt 207. A material 15 is placed on the bottom plate 211, and the material 15 is located inside the processing bin. The second rotating shaft 210 is connected to the processing bin through a first magnetic fluid sealing assembly 209. The first magnetic fluid sealing assembly 209 is closely matched with the first through hole to achieve the purpose of sealing. The structure of the second steering mechanism is the same as that of the first steering mechanism 38. The second rotating shaft 210 of the second steering mechanism is connected to the transition bin through a second magnetic fluid sealing assembly of the second steering mechanism. The second magnetic fluid sealing assembly is closely matched with a second through hole provided through the bottom of the transition bin to achieve the purpose of sealing. The second steering mechanism can access the inside of the transition bin through the second through hole. The structure of the second magnetic fluid sealing assembly is the same as that of the first magnetic fluid sealing assembly 209.
[0028] The carbonization and graphitization chamber 4 includes a carbonization zone and a graphitization zone, which are partitioned. Integrating the carbonization zone and the graphitization zone into the carbonization and graphitization chamber 4 can save manufacturing costs and reduce the floor area. Taking PAN-based rigid carbon felt as an example, since non-carbon elements in PAN-based fibers are discharged in the form of gases, such as ammonia, nitrogen, and hydrogen, during high-temperature carbonization of PAN-based rigid carbon felt, and there are also some resin glue substances in PAN-based fibers that produce a large amount of tar and gas at high temperatures, forming liquid tar in the vacuum pipeline. The main function of the PAN-based rigid carbon felt during high-temperature graphitization in the graphitization zone is to improve its structure and enhance its performance, that is, to transform the structure of the PAN-based carbon material from a disordered carbonaceous structure into an ordered graphite structure, and only a small amount of gas is discharged during the graphitization process. Therefore, the feeding bin 3 and the carbonization zone of the carbonization and graphitization chamber 4 are connected to the first vacuum pump 1 through the cyclone filtration device 16 installed in the extraction pipeline, which is used to quickly condense the tar generated during the carbonization process into a liquid and store it in the liquid accumulation tank of the cyclone filtration device 16, preventing the tar from entering the interior of the first vacuum pump 1 and avoiding the impurities discharged during carbonization from contaminating the material 15 in the graphitization zone.
[0029] The carbonization zone is equipped with a first heating system and a first temperature measurement system 34. When its output power reaches the set value, the temperature of the carbonization zone can reach 1100°C. The first temperature measurement system 34 is electrically connected to the first heating system to form a feedback loop, and the first heating system regulates the temperature of the carbonization zone to control the temperature of the carbonization zone to meet the carbonization requirements. The graphitization zone is equipped with a second heating system and a second temperature measurement system 35. When its output power reaches the set value, the temperature of the carbonization zone can reach 2000°C. The second temperature measurement system 35 is electrically connected to the second heating system to form a feedback loop, and the second heating system regulates the temperature of the graphitization zone to control the temperature of the carbonization zone to meet the graphitization requirements.
[0030] The carbonization zone is also equipped with a first vacancy detection device and several first transmission members. Two first transmission members cooperate with each other. In this embodiment, two first transmission members are provided, and the two first transmission members and the first transmission device on the first steering mechanism 28 form three first working parts 17. The first steering mechanism 28 is installed at one end of the carbonization zone close to the feeding bin 3, that is, the first steering mechanism 28 is installed at the first working part 17 at the leftmost end of the carbonization zone. The first steering mechanism 28 cooperates with the third push rod 39 to transfer the material 15 from the feeding bin 3 to the first transmission device of the first steering mechanism 28, that is, the material 15 can be transferred from the feeding bin 3 to the first working part 17 at the leftmost end of the carbonization zone. The first steering mechanism 28 cooperates with the first push rod 21 to transfer the material 15 from the first transmission device of the first steering mechanism 28 to the next first working part 17 in the carbonization zone.
[0031] The graphitization area is equipped with a second vacancy detection device and several second transfer components. In this embodiment, two second transfer components are provided. The two second transfer components and the first transfer device on the second steering mechanism 29 form three second working parts 18. The second steering mechanism 29 is installed at one end of the graphitization area far from the feeding bin 3, that is, the second steering mechanism 29 is installed at the second working part 18 at the rightmost end of the graphitization area, and the two second transfer components cooperate with each other. The upper surfaces of the second transfer component and the first transfer component are in the same plane. The first transfer component, the second transfer component, the first steering mechanism 1 28, the second steering mechanism 29 and the first push rod 21 connected to the carbonization area cooperate with each other to convey the material 15 from the carbonization area to the graphitization area. The second steering mechanism 29, the first steering mechanism 1 30 and the first push rod 21 connected to the graphitization area cooperate with each other to convey the material 15 from the graphitization area to the second transfer device on the first steering mechanism 1 30 in the first transition bin 8, specifically to the second transfer device on the first steering mechanism 1 30.
[0032] Both the first vacancy detection device and the second vacancy detection device are electrically connected to the control system 40. The first vacancy detection device is used to detect whether there is a material 15 stored on the leftmost first working part 17 in the carbonization area, and the second vacancy detection device is used to detect whether there is a material 15 placed on the rightmost second working part 18 in the graphitization area.
[0033] The second transfer device on the first steering mechanism 1 30 interacts with the second push rod 22 connected to the first transition bin 8 to convey the material 15 from the first transition bin 8 to the purification bin 5. Five third transfer components are installed in the purification bin 5, and the two third transfer components cooperate with each other. The five third transfer components and the first transfer device on the third steering mechanism 31 form six third working parts 19. The third steering mechanism 31 is installed at one end of the purification bin 5 far from the first transition bin 8, that is, the third steering mechanism 31 is installed on the rightmost third working part 19 in the purification bin 5. The second transfer device on the first steering mechanism 1 30, the third transfer component and the second push rod 22 connected to the first transition bin 8 interact with each other to convey the material 15 from the leftmost third working part 19 in the purification bin 5 to the rightmost third working part 19.
[0034] A third heating system and a third temperature measurement system 36 are also installed in the purification bin 5. When its output power reaches the set value, the temperature in the purification bin 5 can reach 2400 °C. The third temperature measurement system 36 is electrically connected to the third heating system to form a feedback loop, and the third heating system regulates the temperature in the purification bin 5 to control the temperature in the purification bin 5 to meet the purification requirements.
[0035] A third vacant position detection device is installed in the first transfer bin 8. The third vacant position detection device is electrically connected to the control system 40. The third vacant position detection device is used to detect whether there is any material 15 placed on the second transfer device of the second steering mechanism 30 in the first transfer bin 8. A fourth vacant position detection device is installed in the purification bin 5. The fourth vacant position detection device is electrically connected to the control system 40. The fourth vacant position detection device is used to detect whether there is any material 15 placed on the third working part 19 at the rightmost end in the purification bin 5, that is, the fourth vacant position detection device is used to detect whether there is any material 15 placed on the first transfer device of the third steering mechanism 31.
[0036] The first transfer device on the third steering mechanism 31, the second transfer device on the second steering mechanism 32 and the first push rod 21 connected to the purification bin 5 cooperate with each other to transfer the material 15 from the purification bin 5 to the second transfer bin 9, specifically to the second transfer device on the second steering mechanism 32. The second transfer device on the second steering mechanism 32 and the second push rod 22 connected to the second transfer bin 9 cooperate with each other to convey the material 15 from the second transfer bin 9 to the cooling bin 6.
[0037] The cooling bin 6 is equipped with five fourth transfer members. Two fourth transfer members cooperate with each other. The five fourth transfer members and the first transfer device on the fourth steering mechanism 33 form six fourth working parts 20. The fourth steering mechanism 33 is installed at one end of the cooling bin 6 far from the second transfer bin 9, that is, the fourth steering mechanism 33 is installed on the rightmost fourth working part 20 in the cooling bin 6. The second transfer device on the second steering mechanism 32, the fourth transfer members and the second push rod 22 connected to the second transfer bin 9 interact to convey the material 15 from the leftmost fourth working part 20 in the cooling bin 6 to the rightmost fourth working part 20. The first transfer device on the fourth steering mechanism 33 and the third push rod 39 connected to the cooling bin 6 cooperate with each other to transfer the material 15 from the cooling bin 6 to the discharge bin 7.
[0038] A fourth temperature measurement system 37 is also installed in the cooling bin 6. The fourth temperature measurement system 37 is electrically connected to the strong cooling fan 25 to form a feedback loop. The rotation speed of the strong cooling fan 25 is adjusted according to the quantity of the material 15 to be cooled and the transmission speed of the fourth transfer members to ensure that the material 15 meets the discharge temperature requirement before being transferred to the discharge bin 7.
[0039] A fifth vacant position detection device is installed in the second transfer bin 9. The fifth vacant position detection device is electrically connected to the control system 40. The fifth vacant position detection device is used to detect whether there is any material 15 placed on the second transfer device of the second steering mechanism 32 in the second transfer bin 9.
[0040] A sixth vacant position detection device is installed in the cooling bin 6. The sixth vacant position detection device is electrically connected to the control system 40 and is used to detect whether there is a material 15 placed on the fourth working part 20 at the rightmost end in the cooling bin 6. More specifically, the first conveyor, the second conveyor, the third conveyor, the fourth conveyor, the first conveying device, and the second conveying device are all composed of a plurality of parallel graphite rollers 27. Driving the rotation of the graphite rollers 27 can drive the material tray 2 placed thereon to move, thereby realizing the conveying operation of the material 15.
[0041] The graphite roller 27 can rotate around its central axis, and the driving method of the graphite roller 27 can be manual operation or electric operation.
[0042] A plurality of third plug valves 12 are also movably connected to the carbonization and graphitization bin 4 and the purification bin 5 to prevent the high temperature in the carbonization and graphitization bin 4 and the purification bin 5 from affecting the performance of the propulsion component 14. Specifically, the third plug valves 12 correspond to the first push rods 21 one by one. When it is necessary to extend the first push rod 21 into the carbonization and graphitization bin 4 or the purification bin 5 to push the material 15, the third plug valve 12 is opened. When the first push rod 21 is used to push the material 15 to the designated position, after the first push rod 21 is withdrawn from the carbonization and graphitization bin 4 or the purification bin 5, the third plug valve 12 is closed. In this embodiment, three third plug valves 12 are provided, two of which are movably connected to the carbonization and graphitization bin 4. The two third plug valves 12 are both placed between the carbonization and graphitization bin 4 and the corresponding first push rod 21. More specifically, the two third plug valves 12 correspond to the carbonization area and the graphitization area respectively; the other third plug valve 12 is movably connected to the purification bin 5, and this third plug valve 12 is placed between the purification bin 5 and the first push rod 21 corresponding to the purification bin 5.
[0043] A fourth plug valve 13 is also movably connected to the transition bin. The fourth plug valve 13 corresponds to the second push rod 22 one by one. When it is necessary to extend the second push rod 22 into the transition bin to push the material 15, the fourth plug valve 13 is opened. When the second push rod 22 is used to push the material 15 to the designated position, after the second push rod 22 is withdrawn from the transition bin, the fourth plug valve 13 is closed.
[0044] The first transition bin 8 and the purification bin 5 are connected to the second vacuum pump 23 through a first filter tank 24 installed in the first vacuum pipeline 26. The first vacuum pipeline 26 is connected between the first transition bin 8, the purification bin 5 and the second vacuum pump 23, that is, the first transition bin 8, the purification bin 5 and the second vacuum pump 23 are interconnected through the first vacuum pipeline 26. The second transition bin 9 and the cooling bin 6 are connected to the output end of the strong cooling fan 25 through a second filter tank 42 installed in the second vacuum pipeline 41. The vacuum pipeline 26 is connected between the second transition bin 9, the cooling bin 6 and the output end of the strong cooling fan 25, that is, the second transition bin 9, the cooling bin 6 and the output end of the strong cooling fan 25 are interconnected through the second vacuum pipeline 41.
[0045] In this embodiment, the material 15 uses PAN-based hard carbon felt.
[0046] A continuous carbonization, graphitization, and purification method provided by the present invention uses the above-mentioned continuous carbonization, graphitization, and purification equipment, including the following steps: Step S1: Place the first material to be carbonized, graphitized, and purified into the feeding bin 3, and perform vacuum pumping on the feeding bin 3 through the first vacuum pump 1; Specifically, place the tray 2 filled with the first material to be carbonized, graphitized, and purified into the feeding bin 3. After closing the feeding bin 3, start the first vacuum pump 1 to perform vacuum pumping on the feeding bin 3.
[0047] Step S2: Open the first plug valve 10 between the feeding bin 3 and the carbonization and graphitization bin 4, send the first material into the carbonization zone of the carbonization and graphitization bin 4 for carbonization treatment to obtain the second material, and then the first transmission member and the second transmission member cooperate with each other to send the second material into the graphitization zone of the carbonization and graphitization bin 4 for graphitization treatment to obtain the third material. Specifically, it includes the following steps: Step S21: Open the first plug valve 10 movably connected between the feeding bin 3 and the carbonization and graphitization bin 4 and the valve of the feeding bin 3, drive the third push rod 39 corresponding to the valve of the feeding bin 3. The third push rod 39 is movably connected to the feeding bin 3 and acts on the tray 2 to push the tray 2 into the leftmost first working part 17 in the carbonization zone. At this time, the transmission direction of the leftmost first working part 17 in the carbonization zone is the same as the movement direction of the tray 2. Then, drive the third push rod 39 corresponding to the valve of the feeding bin 3 to withdraw from the carbonization and graphitization bin 4 and move to the initial position, and close the first plug valve 10 and the valve of the feeding bin 3.
[0048] Before pushing the tray 2 into the leftmost first working part 17 in the carbonization zone, the first vacancy detection device transmits the signal of whether there is a tray 2 placed on the first working part 17 collected to the control system 40, and the control system 40 controls the action of the third push rod 39 corresponding to the valve of the feeding bin 3. Specifically, when the first vacancy detection device detects that there is a tray 2 placed on the leftmost first working part 17 in the carbonization zone, the control system 40 receives this signal and controls the third push rod 39 corresponding to the valve of the feeding bin 3 not to act. When the first vacancy detection device detects that there is no tray 2 placed on the leftmost first working part 17 in the carbonization zone, the control system 40 receives this signal and controls the third push rod 39 corresponding to the valve of the feeding bin 3 to enter the feeding bin 3 and push the tray 2 onto the leftmost first working part 17 in the carbonization zone.
[0049] Step S22: Start the first steering mechanism 28. The bottom plate 211 of the first steering mechanism 28 acts on the first transmission device of the first steering mechanism 28 on the first working part 17. The lifting mechanism of the first steering mechanism 28 lifts the material tray 2 placed on the first transmission device of the first steering mechanism 28 and then starts the reversing mechanism to change the transmission direction of the first transmission device of the first steering mechanism 28, so that the transmission direction of the first transmission device of the first steering mechanism 28 is consistent with the transmission direction of the first transmission member, that is, the rotation directions of the multiple graphite rollers 27 on the first transmission device of the first steering mechanism 28 are consistent with the rotation directions of the multiple graphite rollers 27 on the first transmission member installed in the carbonization area. After adjusting the transmission direction of the first transmission device on the first steering mechanism 28, start the lifting mechanism to return the lifted material tray 2 to its original position, that is, make the first transmission device on the first steering mechanism 28 and the first transmission member in the same plane.
[0050] Step S23: Open the third plug valve 12 movably connected to the left side of the carbonization area of the carbonization and graphitization chamber 4, drive the first push rod 21 corresponding to the third plug valve 12 and act it on the material tray 2, push the material tray 2 to move to the next first working part 17, then the first push rod 21 is withdrawn from the carbonization and graphitization chamber 4 and moves to the initial position, and close the third plug valve 12.
[0051] Step S24: Repeat steps S21 to S23. When the second material tray 2 is pushed to the first working part 17 where the previous material tray 2 is located, the first material tray 2 is pushed to the next first working part 17. In this way, multiple material trays 2 filled with the first materials to be carbonized, graphitized, and purified can be moved to the carbonization area for carbonization operation.
[0052] Since the carbonization area and the graphitization area are integrated in the carbonization and graphitization chamber 4, the structures of the corresponding first transmission member and the second transmission member are the same, and the upper surfaces of the first transmission member and the second transmission member are in the same plane. Repeating steps S21 to S24 can push the carbonized first material to the graphitization area for graphitization operation, thereby obtaining the third material.
[0053] Before pushing the tray 2 to the next first working part 17, the second vacancy detection device transmits the signal of whether there is a tray 2 placed on the second working part 18 at the rightmost end of the graphitization area to the control system 40, and the control system 40 controls the action of the first push rod 21 corresponding to the third sluice valve 12 in the carbonization area. Specifically, when the second vacancy detection device detects that there is a tray 2 placed on the second working part 18 at the rightmost end of the graphitization area, the control system 40 receives this signal and controls the first push rod 21 not to act. When the second vacancy detection device detects that there is no tray 2 on the second working part 18 at the rightmost end of the graphitization area, the control system 40 receives this signal and controls the first push rod 21 corresponding to the third sluice valve 12 in the carbonization area to enter the carbonization area to push the tray 2 to be transmitted to the next first working part 17.
[0054] Step S3: Open the second sluice valve 11 provided between the carbonization and graphitization bin 4 and the first transition bin 8 and the second sluice valve 11 provided between the first transition bin 8 and the purification bin 5, and send the third material into the purification bin 5 for purification treatment to obtain the fourth material. Specifically, it includes the following steps: Step S31: Start the second steering mechanism 29. The bottom plate 211 of the second steering mechanism 29 acts on the first transmission device of the second steering mechanism 29 on the second working part 18 at the rightmost end of the graphitization area to adjust its transmission direction to be consistent with the transmission direction of the second transmission device of the first steering mechanism 30 located in the first transition bin 8.
[0055] Step S32: After opening the second sluice valve 11 movably connected between the carbonization and graphitization bin 4 and the first transition bin 8 and the third sluice valve 12 movably connected to the graphitization area end of the carbonization and graphitization bin 4, drive the first push rod 21 corresponding to the third sluice valve 12 to push the tray 2 located at the second working part 18 at the rightmost end of the graphitization area onto the second transmission device of the first steering mechanism 30. At this time, the transmission direction of the second transmission device of the first steering mechanism 30 is consistent with the moving direction of the tray 2. Then drive the first push rod 21 to withdraw from the carbonization and graphitization bin 4 and close the corresponding third sluice valve 12 and the second sluice valve 11 movably connected between the carbonization and graphitization bin 4 and the first transition bin 8.
[0056] A third vacant position detecting device is installed in the first transition bin 8. Before the material tray 2 is pushed to the second transmission device of the first second steering mechanism 30, the third vacant position detecting device transmits the signal of whether the material tray 2 is placed on the second transmission device of the first second steering mechanism 30 to the control system 40, and the control system 40 controls the action of the first push rod 21 corresponding to the third shutter valve 12 in the graphitization area. Specifically, when the third vacant position detecting device detects that the material tray 2 is placed on the second transmission device of the first second steering mechanism 30, the control system 40 controls the first push rod 21 corresponding to the third shutter valve 12 in the graphitization area not to act after receiving the signal. When the third vacant position detecting device detects that there is no material tray 2 on the second transmission device of the first second steering mechanism 30, the control system 40 controls the first push rod 21 corresponding to the third shutter valve 12 in the graphitization area to enter the graphitization area to push the material tray 2 placed at the second working part 18 at the rightmost end of the graphitization area to be transmitted to the second transmission device of the first second steering mechanism 30 in the first transition bin 8.
[0057] Step S33: Start the second vacuum pump 23 to pump out the gas entering the first transition bin 8 from the carbonization and graphitization bin 4 to prevent the gas from entering the purification bin 5.
[0058] Step S34: Make the bottom plate 211 of the first second steering mechanism 30 act on the second transmission device of the first second steering mechanism 30 in the first transition bin 8. Start the lifting mechanism of the first second steering mechanism 30, lift the material tray 2 placed on the second transmission device of the first second steering mechanism 30, and then start its reversing mechanism to change the transmission direction of the second transmission device of the first second steering mechanism 30, that is, to make the transmission direction of the second transmission device of the first second steering mechanism 30 consistent with the transmission direction of the third transmission part of the third working part 19 in the purification bin 5. After adjusting the transmission direction of the second transmission device of the first second steering mechanism 30, start the lifting mechanism to lower the lifted material tray 2 back to the original position, that is, make the upper surface of the second transmission device of the first second steering mechanism 30 and the upper surface of the third transmission part be in the same plane.
[0059] Step S35: Open the fourth shutter valve 13 movably connected to the first transition bin 8 and the second shutter valve 11 movably connected between the first transition bin 8 and the purification bin 5. Drive the second push rod 22 corresponding to the fourth shutter valve 13 and act on the material tray 2 to push the material tray 2 to move to the third working part 19 at the leftmost end in the purification bin 5. Then, the second push rod 22 is withdrawn from the first transition bin 8 and moved to the initial position. Finally, close the fourth shutter valve 13 and the second shutter valve 11.
[0060] A fourth vacant position detection device is installed in the purification bin 5. Before the tray 2 is pushed into the purification bin 5, the fourth vacant position detection device transmits the signal of whether there is a tray 2 placed on the third working part 19 at the rightmost end in the purification bin 5 to the control system 40, and the control system 40 controls the action of the second push rod 22 corresponding to the fourth plug valve 13 of the first transition bin 8. Specifically, when the fourth vacant position detection device detects that there is a tray 2 placed on the first transmission device of the first steering mechanism three 31 in the purification bin 5, after the control system 40 receives this signal, it controls the second push rod 22 corresponding to the fourth plug valve 13 of the first transition bin 8 not to act. When the fourth vacant position detection device detects that there is no tray 2 on the third working part 19 at the rightmost end in the purification bin 5, after the control system 40 receives this signal, it controls the second push rod 22 corresponding to the fourth plug valve 13 of the first transition bin 8 to enter the first transition bin 8 to push the tray 2 placed in the first transition bin 8 to be transmitted to the third working part 19 at the leftmost end in the purification bin 5.
[0061] Step S36: Repeat steps S31 to S35, and multiple third materials to be purified can be pushed into the purification bin 5 for purification operations.
[0062] Among them, when performing step S33 and step S34, the order of the two can be interchanged.
[0063] Step S4: Open the second plug valve 11 provided between the purification bin 5 and the second transition bin 9 and the second plug valve 11 provided between the second transition bin 9 and the cooling bin 6, and send the fourth material into the cooling bin 6 for cooling treatment. The specific steps include: Step S41: Start the first steering mechanism three 31, and the bottom plate 211 of the first steering mechanism three 31 acts on the first transmission device of the first steering mechanism three 31 in the purification bin 5 to adjust the transmission direction of the first transmission device so that it is consistent with the transmission direction of the second transmission device of the second steering mechanism two 32 located in the second transition bin 9.
[0064] Step S42: After opening the second plug valve 11 movably connected between the purification bin 5 and the second transition bin 9 and the third plug valve 12 movably connected to the purification bin 5, drive the first push rod 21 corresponding to the third plug valve 12 to push the tray 2 at the third working part 19 at the rightmost end of the purification bin 5 to the second transmission device of the second steering mechanism two 32 in the second transition bin 9. At this time, the transmission direction of the second transmission device of the second steering mechanism two 32 is consistent with the moving direction of the tray 2. Then drive the first push rod 21 to withdraw from the purification bin 5 and close the third plug valve 12 corresponding to it and the second plug valve 11 movably connected between the purification bin 5 and the second transition bin 9.
[0065] A fifth vacancy detection device is installed in the second transition bin 9. Before the tray 2 is pushed to the second transmission device of the second steering mechanism 32, the fifth vacancy detection device transmits the signal collected on whether there is a tray 2 placed on the second transmission device of the second steering mechanism 32 to the control system 40, and the control system 40 controls the action of the first push rod 21 corresponding to the third plug valve 12 of the purification bin 5. Specifically, when the fifth vacancy detection device detects that there is a tray 2 placed on the second transmission device of the second steering mechanism 32, the control system 40 receives this signal and controls the first push rod 21 corresponding to the third plug valve 12 of the purification bin 5 not to act. When the fifth vacancy detection device detects that there is no tray 2 on the second transmission device of the second steering mechanism 32, the control system 40 receives this signal and controls the first push rod 21 corresponding to the third plug valve 12 of the purification bin 5 to enter the purification bin 5 to push the tray 2 placed at the rightmost end of the purification bin 5 to the second transmission device of the second steering mechanism 32 in the second transition bin 9.
[0066] Step S43: Start the strong cooling fan 25. The strong cooling fan 25 performs staged forced cooling according to the cooling characteristics of different materials 15 to ensure that the material 15 meets the furnace-out conditions when it moves to the rightmost end of the cooling bin 6.
[0067] Step S44: Make the bottom plate 211 of the second steering mechanism 32 act on the second transmission device of the second steering mechanism 32. Start the lifting mechanism of the second steering mechanism 32, lift the tray 2 placed on the second transmission device of the second steering mechanism 32, and then start the reversing mechanism to change the transmission direction of the second transmission device of the second steering mechanism 32, that is, to make the transmission direction of the second transmission device of the second steering mechanism 32 consistent with the transmission direction of the fourth transmission member of the fourth working part 20 in the cooling bin 6. After adjusting the transmission direction of the second transmission device of the second steering mechanism 32, start the lifting mechanism to lower the lifted tray 2 and restore it to the original position, that is, make the upper surface of the second transmission device of the second steering mechanism 32 and the upper surface of the fourth transmission member be in the same plane.
[0068] Step S45: Then open the fourth plug valve 13 movably connected to the second transition bin 9 and the second plug valve 11 movably connected between the second transition bin 9 and the cooling bin 6. Drive the second push rod 22 corresponding to the fourth plug valve 13 and act on the tray 2, push the tray 2 to move to the fourth working part 20 at the leftmost end in the cooling bin 6, then the second push rod 22 is withdrawn from the second transition bin 9 and moves to the initial position, and finally close the fourth plug valve 13 and the second plug valve 11.
[0069] A sixth vacant position detection device is installed in the temperature reduction bin 6. Before the tray 2 is pushed into the temperature reduction bin 6, the sixth vacant position detection device transmits the signal of whether there is a tray 2 placed on the fourth working part 20 at the rightmost end in the temperature reduction bin 6 to the control system 40, and the control system 40 controls the second push rod 22 corresponding to the fourth plug valve 13 of the second transition bin 9 to act. Specifically, when the sixth vacant position detection device detects that there is a tray 2 placed on the fourth working part 20 at the rightmost end in the temperature reduction bin 6, the control system 40 controls the second push rod 22 corresponding to the fourth plug valve 13 of the second transition bin 9 not to act after receiving this signal. When the sixth vacant position detection device detects that there is no tray 2 on the fourth working part 20 at the rightmost end in the temperature reduction bin 6, the control system 40 controls the second push rod 22 corresponding to the fourth plug valve 13 of the second transition bin 9 to enter the second transition bin 9 to push the tray 2 placed in the second transition bin 9 to be transmitted to the fourth working part 20 at the leftmost end in the temperature reduction bin 6. Step S46: Repeat the above steps S41 to S45, and multiple fourth materials to be cooled can be pushed into the temperature reduction bin 6 for cooling operation.
[0070] Among them, when performing step S43 and step S44, the order of the two can be interchanged.
[0071] Step S5: Open the first plug valve 10 provided between the temperature reduction bin 6 and the discharge bin 7, send the cooled fourth material into the discharge bin 7 and then take it out, which specifically includes the following steps: Step S51: Start the fourth first steering mechanism 33. The bottom plate 211 of the fourth first steering mechanism 33 acts on the first transmission device of the fourth first steering mechanism 33 to adjust the transmission direction of the first transmission device so that the transmission direction of the first transmission device is consistent with the moving direction of the tray 2 towards the discharge bin 7. Step S52: Open the first plug valve 10 movably connected between the temperature reduction bin 6 and the discharge bin 7 and the valve on the temperature reduction bin 6, start the third push rod 39 corresponding to the valve on the temperature reduction bin 6 to push the tray 2 on the first transmission device of the fourth first steering mechanism 33 at the rightmost end of the temperature reduction bin 6, push the tray 2 into the discharge bin 7, and then drive the third push rod 39 to withdraw from the temperature reduction bin 6 and then close the first plug valve 10 movably connected between the temperature reduction bin 6 and the discharge bin 7 and the valve of the temperature reduction bin 6.
[0072] A seventh vacancy detection device is installed in the discharge bin 7. Before the tray 2 is pushed into the discharge bin 7, the seventh vacancy detection device transmits the signal of whether there is a tray 2 placed in the discharge bin 7 collected to the control system 40, and the control system 40 controls the action of the third push rod 39 corresponding to the valve of the cooling bin 6. Specifically, when the seventh vacancy detection device detects that there is a tray 2 placed in the discharge bin 7, after receiving this signal, the control system 40 controls the third push rod 39 corresponding to the valve of the cooling bin 6 not to act. When the seventh vacancy detection device detects that there is no tray 2 in the discharge bin 7, after receiving this signal, the control system 40 controls the third push rod 39 corresponding to the valve of the cooling bin 6 to enter the discharge bin 7 to push the tray 2 on the first transmission device of the first steering mechanism four 33 placed at the rightmost end of the cooling bin 6 and transmit it into the discharge bin 7.
[0073] Step S53: Repeat the above steps S51 to S52, and multiple carbonized, graphitized, and purified fourth materials can be pushed into the discharge bin 7 and then taken out.
[0074] Step S6: Repeat the above steps S1 to S5 to realize the continuous production of carbonization, graphitization, and purification of the first material.
[0075] The rotation angle of the steering mechanism 38 in this embodiment is 90°, and those skilled in the art can adjust the rotation angle according to the specific implementation environment.
[0076] The first vacancy detection device, the second vacancy detection device, the third vacancy detection device, the fourth vacancy detection device, the fifth vacancy detection device, the sixth vacancy detection device, and the seventh vacancy detection device in this embodiment can adopt the same type of vacancy detection device. The specifications and models of the vacancy detection device are not limited here, as long as it can collect the signal of whether there is a tray 2 at the position to be detected.
[0077] The computer program stored on the readable storage medium provided by the present invention, when executed by a processor, realizes the method steps of the above continuous carbonization, graphitization, and purification.
[0078] Regarding the specific structure of the present invention, it should be noted that the connection relationships between the various component modules adopted by the present invention are definite and achievable. Except for the special descriptions in the embodiments, the specific connection relationships can bring corresponding technical effects, and on the premise of not relying on the execution of corresponding software programs, the technical problems proposed by the present invention can be solved. The models of the components, modules, and specific components, the connection methods therebetween, and the conventional usage methods and predictable technical effects brought by the above technical features, except for the specific descriptions, all belong to the publicly disclosed contents in patents, journal papers, technical manuals, technical dictionaries, and textbooks that those skilled in the art can obtain before the filing date, or belong to the prior arts such as conventional technologies and common general knowledge in the art, and do not need to be elaborated. Thus, the technical solution provided in this case is clear, complete, and achievable, and the corresponding physical product can be reproduced or obtained according to this technical means.
[0079] Finally, it should be noted that: the above embodiments are only used to illustrate the technical solutions of the present invention, rather than to limit it; although the present invention has been described in detail with reference to the foregoing embodiments, those of ordinary skill in the art should understand that: they can still modify the technical solutions recorded in the foregoing embodiments, or perform equivalent replacements on some or all of the technical features; and these modifications or replacements do not cause the essence of the corresponding technical solutions to deviate from the scope of the technical solutions of the embodiments of the present invention.
Claims
1. Continuous carbonization, graphitization, and purification equipment, characterized in that, It includes a first vacuum pump (1), a number of processing chambers and a number of transition chambers. The processing chambers are connected through the transition chambers in pairs. At least one first steering mechanism (38) is provided on each of the processing chambers, and at least one second steering mechanism is provided on each of the transition chambers. The first steering mechanism (38) cooperates with the second steering mechanism; The multiple processing chambers are respectively a carbonization and graphitization chamber (4), a purification chamber (5) and a cooling chamber (6). The carbonization and graphitization chamber (4), the purification chamber (5) and the cooling chamber (6) are connected in sequence. The carbonization and graphitization chamber (4) is also connected to a feeding chamber (3), and the cooling chamber (6) is also connected to a discharging chamber (7); At least one propulsion component (14) is movably connected to the feeding chamber (3), the transition chambers and the multiple processing chambers respectively. The propulsion component (14) acts on the tray (2); The carbonization and graphitization chamber (4) includes a carbonization zone and a graphitization zone. The carbonization zone and the graphitization zone are partitioned. A number of first transmission components are provided in the carbonization zone, and a number of second transmission components are provided in the graphitization zone. The first transmission components and the second transmission components cooperate with each other; The first transmission components, the second transmission components cooperate with the first steering mechanism (38); The third transmission component provided in the purification chamber (5) cooperates with the first steering mechanism (38) and the second steering mechanism; The fourth transmission component provided in the cooling chamber (6) cooperates with the first steering mechanism (38) and the second steering mechanism; The feeding chamber (3) and the carbonization zone are connected to the first vacuum pump (1) through a cyclone filter device (16) provided in the suction pipeline; 2. The continuous carbonization, graphitization, and purification equipment according to claim 1, characterized in that, The multiple transition chambers are respectively a first transition chamber (8) and a second transition chamber (9). The first transition chamber (8) is provided between the carbonization and graphitization chamber (4) and the purification chamber (5), and the second transition chamber (9) is provided between the purification chamber (5) and the cooling chamber (6).
3. The continuous carbonization, graphitization, and purification equipment according to claim 1, characterized in that, A first flap valve (10) is provided between the feeding chamber (3) and the carbonization and graphitization chamber (4) and between the cooling chamber (6) and the discharging chamber (7). A second flap valve (11) is provided between the processing chamber and the transition chamber.
4. The continuous carbonization, graphitization, and purification equipment according to claim 1, characterized in that, A first transmission device is provided on the first steering mechanism (38), and a second transmission device is provided on the second steering mechanism. The first transmission device cooperates with the second transmission device.
5. The continuous carbonization, graphitization, and purification equipment according to claim 1, characterized in that, The first steering mechanism (38) includes a lifting mechanism and a commutation mechanism. The lifting mechanism includes a first rotating shaft (203) and a lifting shaft (205). The first rotating shaft (203) and the lifting shaft (205) are connected to each other. The first rotating shaft (203) is connected to the output end of a lifting motor (201). The lifting shaft (205) is rotatably connected to a second rotating shaft (210) of the commutation mechanism. The second rotating shaft (210) is connected to the processing chamber through a first magneto-rheological fluid sealing assembly (209). The second rotating shaft (210) is further connected with a pulley (206) and a bottom plate (211). The pulley (206) is connected to the output end of a rotating motor (208) through a belt (207). A material tray (2) is placed on the bottom plate (211). The structure of the second steering mechanism is the same as that of the first steering mechanism (38). The second rotating shaft (210) of the second steering mechanism is connected to the transition chamber through a second magneto-rheological fluid sealing assembly.
6. The continuous carbonization, graphitization, and purification equipment according to claim 1, characterized in that, Third plug valves (12) are movably connected to both the carbonization and graphitization chamber (4) and the purification chamber (5). The third plug valves (12) cooperate with the propulsion components (14).
7. The continuous carbonization, graphitization, and purification equipment according to claim 2, characterized in that, The first transition chamber (8) and the purification chamber (5) are connected to a second vacuum pump (23) through a first filter tank (24) provided in a first vacuum pipeline (26). The first vacuum pipeline (26) is connected among the first transition chamber (8), the purification chamber (5) and the second vacuum pump (23). The second transition chamber (9) and the cooling chamber (6) are connected to the output end of a strong cooling fan (25) through a second filter tank (42) provided in a second vacuum pipeline (41). The second vacuum pipeline (41) is connected among the second transition chamber (9), the cooling chamber (6) and the output end of the strong cooling fan (25).
8. The continuous carbonization, graphitization, and purification equipment according to claim 1, wherein A first heating system and a first temperature measuring system (34) are installed in the carbonization area. The first heating system and the first temperature measuring system (34) are electrically connected to form a feedback loop to control the temperature in the carbonization area to meet the carbonization requirements. A second heating system and a second temperature measuring system (35) are installed in the graphitization area. The second heating system and the second temperature measuring system (35) are electrically connected to form a feedback loop to control the temperature in the graphitization area to meet the graphitization requirements. A third heating system and a third temperature measuring system (36) are installed in the purification chamber (5). The third heating system and the third temperature measuring system (36) are electrically connected to form a feedback loop to control the temperature in the purification chamber (5) to meet the purification requirements. A fourth temperature measuring system (37) and a strong cooling fan (25) are installed in the cooling chamber (6). The fourth temperature measuring system (37) and the strong cooling fan (25) are electrically connected to form a feedback loop to ensure that the material (15) placed in the cooling chamber (6) meets the discharge temperature requirements before being transferred to the discharge bin (7).
9. Continuous carbonization, graphitization, and purification method, characterized in that, Using the continuous carbonization, graphitization, purification equipment according to any one of claims 1-8, comprising the following steps: Step S1: Place the first material to be carbonized, graphitized, and purified into the feeding bin (3), and perform vacuum pumping on the feeding bin (3) through a first vacuum pump (1). Step S2: Open the first plug valve (10) between the feeding bin (3) and the carbonization and graphitization bin (4), feed the first material into the carbonization zone of the carbonization and graphitization bin (4) for carbonization treatment to obtain the second material, and then the first transmission member and the second transmission member cooperate with each other to feed the second material into the graphitization zone of the carbonization and graphitization bin (4) for graphitization treatment to obtain the third material; Step S3: Open the second plug valve (11) provided between the carbonization and graphitization bin (4) and the first transition bin (8) and the second plug valve (11) provided between the first transition bin (8) and the purification bin (5), and feed the third material into the purification bin (5) for purification treatment to obtain the fourth material; Step S4: Open the second plug valve (11) provided between the purification bin (5) and the second transition bin (9) and the second plug valve (11) provided between the second transition bin (9) and the cooling bin (6), and feed the fourth material into the cooling bin (6) for cooling treatment; Step S5: Open the first plug valve (10) provided between the cooling bin (6) and the discharge bin (7), and feed the fourth material after cooling treatment into the discharge bin (7) and then take it out; Step S6: Repeat the above steps S1 to S5 to realize the continuous production of carbonization, graphitization and purification of the first material.
10. A readable storage medium, characterized in that, The computer program is stored on the readable storage medium, and when the computer program is executed by the processor, the method steps described in claim 9 are realized.
Citation Information
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