Anti-dandruff shampoo soap and preparation method thereof
The specially formulated anti-dandruff shampoo soap solves the problems of traditional shampoo soaps such as easy residue, poor foaming and poor dandruff removal effect, and achieves the effects of efficient dandruff removal and itching relief as well as safe carrying.
Patent Information
- Application Number
- CN202510532964.9
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-04-25
- Publication Date
- 2025-09-19
AI Technical Summary
Traditional shampoo soap is difficult to spread, easily leaves residue, has poor foaming effect, is not ideal for removing dandruff, and the shampoo liquid is not easy to carry.
The anti-dandruff shampoo soap is made from ingredients such as sodium lauryl sulfate, guar hydroxypropyltrimonium chloride, cetearyl alcohol, shea butter, coconut oil, sodium cocoyl glutamate, pyridone ethanolamine salt, polyvinyl pyrrolidone, ganoderma lucidum extract, soapberry peel extract, ginseng root extract, angelica extract, cypress leaf extract and polygonum multiflorum extract through a specific proportion and preparation method.
It can effectively remove dandruff and relieve itching. The formula is natural and safe, reduces the risk of skin allergies, has good foaming effect, and is easy to carry.
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Abstract
Description
Technical Field
[0001] The present invention relates to the technical field of daily necessities, in particular to an anti-dandruff shampoo soap and a preparation method thereof. Background Art
[0002] Dandruff, a seemingly minor problem that clings to the scalp and hair and causes massive shedding, often plagues people in all aspects of their lives, including work, daily life, and social life. Dandruff not only causes physical distress but also causes internal and emotional distress. Frequently finding a head and shoulders covered in dandruff not only affects one's image but can also hinder career choices. Therefore, a shampoo specifically targeting dandruff has been developed.
[0003] Traditional concepts such as anti-dandruff, anti-hair loss, sun protection, hair treatment, conditioner, no-wash, silicone-free, natural extraction, plant essence, and Chinese herbal conditioning have also penetrated into the field of shampoo, becoming a new highlight of shampoo. However, shampoo is a liquid and is not easy to carry when traveling, and it takes up space. Shampoo soap came into being, but the current shampoo soap is not easy to spread, easy to leave residue, has poor foaming effect, and the anti-dandruff effect is not ideal. Summary of the Invention
[0004] In order to solve the above technical problems or at least partially solve the above technical problems, the present application provides an anti-dandruff shampoo soap and a preparation method thereof.
[0005] In a first aspect, the present application provides an anti-dandruff shampoo soap, wherein the raw material components include, by mass percentage: Sodium lauryl sulfate 45% to 50%; Guar gum hydroxypropyltrimonium chloride 3% to 6%; Cetearyl alcohol 4% to 6%; Shea butter 11% to 13%; Coconut oil 0.8%-1%; Sodium cocoyl glutamate 10%-12%; Pyridone ethanolamine salt 3% to 5%; Polyvinylpyrrolidone 4% to 5%; Ganoderma lucidum extract 0.4% to 1%; Soapberry peel extract 0.3%-1%; Ginseng root extract 0.2%-1%; Angelica extract 0.1% to 1%; Platycladus orientalis leaf extract 0.5%-1%; Polygonum multiflorum extract 0.8%-1%; The balance is water.
[0006] In one possible embodiment, the raw material components include, by mass percentage: Sodium lauryl sulfate 50%; Guar hydroxypropyltrimonium chloride 4%; Cetearyl alcohol 5%; Shea butter 12%; Coconut oil 1%; Sodium cocoyl glutamate 12%; Pyridone ethanolamine salt 5%; Polyvinylpyrrolidone 5%; Ganoderma lucidum extract 1%; Soapberry peel extract 1%; Ginseng root extract 1%; Angelica extract 1%; Platycladus orientalis leaf extract 1%; Polygonum multiflorum extract 1%; The balance is water.
[0007] In one possible embodiment, the preparation method of the Polygonum multiflorum extract is as follows: Wash the Polygonum multiflorum and grind it into 80-100 meshes after drying to obtain Polygonum multiflorum powder; Adding Polygonum multiflorum powder to a 75% to 85% ethanol aqueous solution with a volume concentration of 7 to 9 times its weight, and soaking at room temperature for 6 to 8 hours; The extract of Polygonum multiflorum is obtained by treating the extract with 35-45 kHz ultrasonic oscillation at 50-60° C. for 40-50 minutes, centrifuging and collecting the supernatant, and concentrating under reduced pressure to an extract with a relative density of 1.15-1.25.
[0008] In one possible embodiment, the preparation method of the soapberry peel extract is as follows: Select ripe soapberry fruits, peel them, wash them and dry them; Grinding the dried peel into 40-60 mesh to obtain soapberry peel powder; The soapberry peel powder is added to a solvent at a material-liquid ratio of 1:10 to 1:15, and the extraction is performed 2 to 3 times under controlled temperature. The filtrate is then treated with a spiral evaporator to obtain the soapberry peel extract.
[0009] In one possible embodiment, the preparation method of the Ganoderma lucidum extract is as follows: Ultrafine grinding the dried Ganoderma lucidum to 80-100 mesh to obtain Ganoderma lucidum powder; Adding Ganoderma lucidum powder to a solvent at a temperature of 90-100° C. at a material-liquid ratio of 1:15, and performing reflux extraction 2-3 times to obtain a mixed solution; The mixed solution is concentrated to obtain the Ganoderma lucidum extract.
[0010] In one possible embodiment, the preparation method of the angelica extract is as follows: Wash the angelica root with water, cut it into thin slices, and then put the slices into a drying oven at a temperature of 80-100℃ to dry; The dried angelica slices were added to a solvent at a solid-liquid ratio of 1:10 to 1:15, and microwave extraction was performed at a power of 80 to 120 W for 30 minutes, followed by filtration to obtain a filtrate. The filtrate was concentrated to obtain an angelica extract.
[0011] In one possible embodiment, the Platycladus orientalis leaf extract is prepared using the same method as the Angelica sinensis extract.
[0012] In a second aspect, the present application also provides a method for preparing an anti-dandruff shampoo soap. In a possible implementation, the following steps are included: (1) Preparation of component A: Sodium lauryl sulfate is added to a stirring pot and stirred for a first preset time, then guar gum hydroxypropyltrimonium chloride and Polygonum multiflorum extract are added and stirred for a second preset time, and then sodium cocoyl glutamate, pyridone ethanolamine salt, polyvinyl pyrrolidone, Ganoderma lucidum extract, Sapindus mukorossi peel extract, Panax ginseng root extract, Angelica sinensis extract and Platycladus orientalis leaf extract are added and stirred to obtain component A; (2) Preparation of component B: cetearyl alcohol and shea butter are added to a solvent for dissolution, and placed in an insulated box at a preset temperature for insulation to obtain component B; (3) Add component B to component A and mix and stir. After stirring for a third preset time, add coconut oil and stir evenly. Then dry the mixture to obtain the target anti-dandruff shampoo soap.
[0013] In a possible implementation manner, the first preset time is 2 to 3 minutes, the second preset time is 20 to 25 minutes, the third preset time is 15 to 18 minutes, and the preset temperature is 65 to 70°C.
[0014] In a possible embodiment, in step (3), the mixing and stirring is performed at a rotation speed of 600 to 800 rpm and a temperature of 25 to 35°C.
[0015] The above technical solution provided by the embodiment of the present application has the following advantages compared with the prior art: The present invention adds functional ingredients such as sodium lauryl sulfate, guar hydroxypropyltrimonium chloride, cetearyl alcohol, shea butter, coconut oil, sodium cocoyl glutamate, pyridone ethanolamine salt, polyvinyl pyrrolidone, ganoderma lucidum extract, soapberry peel extract, ginseng root extract, angelica extract, orientalis leaf extract and polygonum multiflorum extract. Experiments have shown that the present invention has significant anti-dandruff and antipruritic effects, and the natural plant formula prepared with the functional ingredients is healthier for the human body and has a health-care effect on hair. The formula is safer, has less toxic side effects and irritation, and is less likely to cause skin allergies, inflammation and other skin microecological system disorders. DETAILED DESCRIPTION
[0016] In order to better understand the technical content of the present invention, specific examples are provided below to further illustrate the present invention.
[0017] Unless otherwise specified, the experimental methods used in the examples of the present invention are all conventional methods.
[0018] Unless otherwise specified, the materials, reagents, etc. used in the examples of the present invention can be obtained from commercial sources.
[0019] Example 1 1. Weigh the raw materials according to Table 1 and set aside.
[0020] 2. Add sodium lauryl sulfate to a stirring pot and stir for 2 minutes. Then add guar gum hydroxypropyltrimonium chloride and Polygonum multiflorum extract and stir for 20 minutes. Then add sodium cocoyl glutamate, pyridone ethanolamine salt, polyvinyl pyrrolidone, Ganoderma lucidum extract, Sapindus mukorossi peel extract, Panax ginseng root extract, Angelica sinensis extract and Platycladus orientalis leaf extract and stir to obtain component A.
[0021] 3. Add cetearyl alcohol and shea butter to a solvent to dissolve them, and place them in an insulated box at 65° C. to obtain component B.
[0022] 4. Add component B to component A and mix well. After stirring for 15 minutes, add coconut oil and stir evenly. Then dry the mixture to obtain the target anti-dandruff shampoo soap.
[0023] Table 1
[0024] Example 2 1. Weigh the raw materials according to Table 2 and set aside.
[0025] 2. Add sodium lauryl sulfate to a stirring pot and stir for 2.5 minutes. Then add guar gum hydroxypropyltrimonium chloride and Polygonum multiflorum extract and stir for 22 minutes. Then add sodium cocoyl glutamate, pyridone ethanolamine salt, polyvinyl pyrrolidone, Ganoderma lucidum extract, Sapindus mukorossi peel extract, Panax ginseng root extract, Angelica sinensis extract and Platycladus orientalis leaf extract and stir to obtain component A.
[0026] 3. Add cetearyl alcohol and shea butter to a solvent to dissolve them, and place them in an insulated box at 67° C. to obtain component B.
[0027] Component B was added to component A and mixed. After stirring for 16 minutes, coconut oil was added and stirred evenly. The mixture was then dried to obtain the target anti-dandruff shampoo soap.
[0028] Table 2
[0029] Example 3 1. Weigh the raw materials according to Table 3 and set aside.
[0030] 2. Add sodium lauryl sulfate to a stirring pot and stir for 3 minutes. Then add guar gum hydroxypropyltrimonium chloride and Polygonum multiflorum extract and stir for 25 minutes. Then add sodium cocoyl glutamate, pyridone ethanolamine salt, polyvinyl pyrrolidone, Ganoderma lucidum extract, Sapindus mukorossi peel extract, Panax ginseng root extract, Angelica sinensis extract and Platycladus orientalis leaf extract and stir to obtain component A.
[0031] 3. Add cetearyl alcohol and shea butter to a solvent to dissolve them, and place them in an insulated box at 70° C. to obtain component B.
[0032] Component B was added to component A and mixed. After stirring for 18 minutes, coconut oil was added and stirred evenly. The mixture was then dried to obtain the target anti-dandruff shampoo soap.
[0033] Table 3
[0034] Clinical trial section Animal testing of anti-dandruff shampoo; Experimental animals: Guinea pigs, weighing 250-400 g; Experimental reagents: Sanwei Qingre Zhiyang Lotion and samples of Example 1, Example 2, and Example 3 of this patent; Test Method: Effect of histamine phosphate on the antipruritic response in guinea pigs. 120 healthy guinea pigs weighing 250-400g were randomly divided into 12 groups, 10 in each group, half male and half female. A blank control group (0.1ml / 100g distilled water) and a positive control group (0.1ml / 100g Sanwei Qingre Zhiyang Lotion) were used. Each example was tested at three doses: 0.2ml / g, 0.1ml / g, and 0.05ml / g.
[0035]
[0036] The test results show that external application of each dose of Example 1, Example 2, and Example 3 (0.05 ml / 100 g, 0.1 ml / 100 g, 0.2 ml / 100 g) and the Sanwei Qingre Zhiyang Lotion group (0.1 ml / 100 g) can significantly increase the itch threshold of histamine phosphate on guinea pigs, and it can be clearly seen from the test results that the itch thresholds of Examples 1, Example 2, and Example 3 on guinea pigs are all higher than that of the Sanwei Qingre Zhiyang Lotion group, indicating that Examples 1, Example 2, and Example 3 all have obvious antipruritic effects.
[0037] In addition, using soapberry extract as a plant-derived surfactant reduces the use of traditional chemical surfactants, reduces the irritation of chemical surfactants, and can reduce the potential risk substance dioxin brought in by such surfactants, thereby improving safety.
[0038] Here, it should be noted that the Polygonum multiflorum extract, Sapindus mukorossi peel extract, Ganoderma lucidum extract, Angelica sinensis extract and Platycladus orientalis leaf extract in the above-mentioned Examples 1, 2 and 3 can be prepared by the following methods. The specific preparation methods are as follows: In one embodiment, the preparation method of the Polygonum multiflorum extract is as follows: the Polygonum multiflorum is washed and crushed to 80-100 mesh after drying to obtain the Polygonum multiflorum powder; the Polygonum multiflorum powder is added to a 75%-85% ethanol aqueous solution with a volume concentration of 7 to 9 times its weight, and soaked at room temperature for 6 to 8 hours; the powder is treated with 35-45 kHz ultrasonic oscillation at 50 to 60° C. for 40 to 50 minutes, the supernatant is collected by centrifugation, and the powder is concentrated under reduced pressure to an extract with a relative density of 1.15 to 1.25, thereby obtaining the Polygonum multiflorum extract.
[0039] In one embodiment, the preparation method of Ganoderma lucidum extract is as follows: the dried Ganoderma lucidum is ultrafinely ground to 80-100 mesh to obtain Ganoderma lucidum powder; the Ganoderma lucidum powder is added to a solvent at a temperature of 90-100°C at a material-liquid ratio of 1:15, and reflux extraction is performed 2-3 times to obtain a mixed solution; the mixed solution is concentrated to obtain Ganoderma lucidum extract.
[0040] In one embodiment, the preparation method of angelica extract is as follows: the angelica root is cleaned with water, and the cleaned angelica root is cut into thin slices, and then the slices are placed in a drying oven with a temperature range of 80 to 100°C for drying; the dried angelica slices are added with a solvent at a material-liquid ratio of 1:10 to 1:15, and microwave extraction is performed at a power of 80 to 120 W for an extraction time of 30 minutes, and then filtered to obtain a filtrate; the filtrate is concentrated to obtain the angelica extract.
[0041] In one embodiment, the Platycladus orientalis leaf extract is prepared in the same manner as the Angelica sinensis extract. The preparation method of the Platycladus orientalis leaf extract can refer to the preparation method of the Angelica sinensis extract, which will not be described in detail.
[0042] The above is only a preferred embodiment of the present invention. It should be pointed out that for ordinary technicians in this technical field, several improvements and substitutions can be made without departing from the technical principles of the present invention. These improvements and substitutions should also be regarded as the scope of protection of the present invention.
Claims
1. An anti-dandruff shampoo soap, characterized in that: In terms of mass percentage, the raw material components include: Sodium lauryl sulfate 45% to 50%; Guar gum hydroxypropyltrimonium chloride 3% to 6%; Cetearyl alcohol 4% to 6%; Shea butter 11% to 13%; Coconut oil 0.8%-1%; Sodium cocoyl glutamate 10%-12%; Pyridone ethanolamine salt 3% to 5%; Polyvinylpyrrolidone 4% to 5%; Ganoderma lucidum extract 0.4% to 1%; Soapberry peel extract 0.3%-1%; Ginseng root extract 0.2%-1%; Angelica extract 0.1% to 1%; Platycladus orientalis leaf extract 0.5%-1%; Polygonum multiflorum extract 0.8%-1%; The balance is water.
2. The anti-dandruff shampoo soap according to claim 1, characterized in that In terms of mass percentage, the raw material components include: Sodium lauryl sulfate 50%; Guar hydroxypropyltrimonium chloride 4%; Cetearyl alcohol 5%; Shea butter 12%; Coconut oil 1%; Sodium cocoyl glutamate 12%; Pyridone ethanolamine salt 5%; Polyvinylpyrrolidone 5%; Ganoderma lucidum extract 1%; Soapberry peel extract 1%; Ginseng root extract 1%; Angelica extract 1%; Platycladus orientalis leaf extract 1%; Polygonum multiflorum extract 1%; The balance is water.
3. The anti-dandruff shampoo soap according to claim 1 or 2, characterized in that: The preparation method of the Polygonum multiflorum extract is as follows: Wash the Polygonum multiflorum and grind it into 80-100 meshes after drying to obtain Polygonum multiflorum powder; Adding Polygonum multiflorum powder to a 75% to 85% ethanol aqueous solution with a volume concentration of 7 to 9 times its weight, and soaking at room temperature for 6 to 8 hours; The extract of Polygonum multiflorum is obtained by treating the extract with 35-45 kHz ultrasonic oscillation at 50-60° C. for 40-50 minutes, centrifuging and collecting the supernatant, and concentrating under reduced pressure to an extract with a relative density of 1.15-1.
25.
4. The anti-dandruff shampoo soap according to claim 1, characterized in that The preparation method of the soapberry peel extract is as follows: Select ripe soapberry fruits, peel them, wash them and dry them; Grinding the dried peel into 40-60 mesh to obtain soapberry peel powder; The soapberry peel powder is added to a solvent at a material-liquid ratio of 1:10 to 1:15, and the extraction is performed 2 to 3 times under controlled temperature. The filtrate is then treated with a spiral evaporator to obtain the soapberry peel extract.
5. The anti-dandruff shampoo soap according to claim 1, characterized in that The preparation method of the Ganoderma lucidum extract is as follows: Ultrafine grinding the dried Ganoderma lucidum to 80-100 mesh to obtain Ganoderma lucidum powder; Adding Ganoderma lucidum powder to a solvent at a temperature of 90-100° C. at a material-liquid ratio of 1:15, and performing reflux extraction 2-3 times to obtain a mixed solution; The mixed solution is concentrated to obtain the Ganoderma lucidum extract.
6. The anti-dandruff shampoo soap according to claim 1, characterized in that The preparation method of the angelica extract is as follows: Wash the angelica root with water, cut it into thin slices, and then put the slices into a drying oven at a temperature of 80-100℃ to dry; The dried angelica slices were added to a solvent at a solid-liquid ratio of 1:10 to 1:15, and microwave extraction was performed at a power of 80 to 120 W for 30 minutes, followed by filtration to obtain a filtrate. The filtrate was concentrated to obtain an angelica extract.
7. The anti-dandruff shampoo soap according to claim 6, characterized in that The Platycladus orientalis leaf extract is prepared in the same manner as the Angelica sinensis extract.
8. The method for preparing the anti-dandruff shampoo according to any one of claims 1 to 7, characterized in that: The following steps are involved: (1) Preparation of component A: Sodium lauryl sulfate is added to a stirring pot and stirred for a first preset time, then guar gum hydroxypropyltrimonium chloride and Polygonum multiflorum extract are added and stirred for a second preset time, and then sodium cocoyl glutamate, pyridone ethanolamine salt, polyvinyl pyrrolidone, Ganoderma lucidum extract, Sapindus mukorossi peel extract, Panax ginseng root extract, Angelica sinensis extract and Platycladus orientalis leaf extract are added and stirred to obtain component A; (2) Preparation of component B: cetearyl alcohol and shea butter are added to a solvent for dissolution, and placed in an insulated box at a preset temperature for insulation to obtain component B; (3) Add component B to component A and mix and stir. After stirring for a third preset time, add coconut oil and stir evenly. Then dry the mixture to obtain the target anti-dandruff shampoo soap.
9. The method for preparing the anti-dandruff shampoo soap according to claim 8, characterized in that: The first preset time is 2 to 3 minutes, the second preset time is 20 to 25 minutes, the third preset time is 15 to 18 minutes, and the preset temperature is 65 to 70°C.
10. The method for preparing the anti-dandruff shampoo soap according to claim 8, characterized in that: In the step (3), the mixing and stirring speed is 600-800 rpm and the temperature is 25-35°C.