Method and equipment for preparing and processing deuterium-depleted water

Through superconducting quantum cutting technology and precise deuterium content detection, the problems of low efficiency and high cost in the preparation of deuterium-depleted water have been solved, and efficient, low-cost and environmentally friendly deuterium-depleted water preparation has been achieved, which is suitable for large-scale industrial production.

CN120733563APending Publication Date: 2025-10-03WANYUAN ZHINONG TECHNOLOGY DEVELOPMENT (BEIJING) CO LTD
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Patent Information

Application Number
CN202510917170.4
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-07-03
Publication Date
2025-10-03

AI Technical Summary

Technical Problem

Existing methods for preparing deuterium-depleted water are inefficient, costly, complex to operate, energy-intensive, and difficult to precisely control the deuterium content, thus failing to meet market demand.

Method used

Using superconducting quantum cutting devices, superconducting energy extraction windings and quantum energy generation devices, combined with multi-layer filtration, ion exchange resins and reverse osmosis technology, superconducting quantum fields are used to separate protium and deuterium, and the deuterium content is detected and controlled in real time through a mass spectrometer to achieve precise preparation.

Benefits of technology

The highly efficient preparation of deuterium-depleted water is achieved, with efficiency increased several times, cost reduced, compact equipment, environmental protection and energy saving, and precise control of deuterium content, making it suitable for large-scale industrial production.

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Abstract

The invention discloses a deuterium-depleted water preparing and processing method and equipment, and belongs to the technical field of deuterium-depleted water preparation.The equipment comprises a superconducting quantum cutting device, a superconducting energy leading-out winding and a quantum energy generating device.Pretreated purified water is conveyed into a reaction cavity of the superconducting quantum cutting device, a low-temperature cooling system is started, and the quantum energy generating device is started; cooling the superconducting quantum cutting device to a low-temperature environment required by the superconducting material, enabling the superconducting coil to enter a superconducting state, starting the quantum energy generating device, generating a superconducting quantum field with specific frequency and strength, performing quantum cutting on water molecules in the reaction cavity, separating protium and deuterium in the water molecules under the action of the superconducting quantum field, and performing quantum cutting on the water molecules. Water with low deuterium content gradually gathers in a specific area of the reaction cavity, protium and deuterium can be efficiently separated in a short time, the preparation efficiency of deuterium-depleted water is greatly improved, the equipment cost and the energy consumption are reduced, meanwhile, the preparation process is simplified, and the operation steps and the maintenance cost are reduced.
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Description

Technical Field

[0001] The present invention relates to the technical field of deuterium-depleted water preparation, and in particular to a deuterium-depleted water preparation and processing method and equipment. Background Art

[0002] Deuterium-depleted water (DDW) is water with a deuterium volume fraction of less than 0.015%, also known as deuterium-depleted water or ultra-light water. Deuterium-depleted water carries a large amount of kinetic energy, rapid movement, high penetrating power, and strong dissolving power. Once inside the human body, it continuously activates cells and carries more beneficial nutrients, minerals, and oxygen, promoting cell growth and development and making them more vigorous. It also fully dissolves and excretes nutrients that cannot be fully absorbed by cells, as well as accumulated fat, cholesterol, and other substances, thereby enhancing the body's detoxification capacity. Deuterium-depleted water also exhibits a range of biological effects, such as anti-tumor, antioxidant, hypoglycemic, and antidepressant properties, and can influence the biochemical metabolic processes of living organisms. It is easy to use, has no adverse reactions, and can be used as an adjuvant in clinical treatment.

[0003] Currently, the main methods for artificially preparing deuterium-depleted water include distillation, electrolysis, adsorption, and membrane separation. However, these traditional methods generally suffer from low efficiency, high cost, complex operation, bulky equipment, high energy consumption, and difficulty in accurately controlling the deuterium content. For example, distillation requires a large amount of heat energy to achieve water evaporation and condensation, which consumes extremely high energy; electrolysis has stringent requirements for electrode materials, and the electrodes are easily corroded, resulting in high equipment maintenance costs; the adsorption capacity of the adsorbent in the adsorption method is limited, and the adsorbent needs to be frequently replaced, increasing production costs; membrane separation has low separation efficiency, and the membrane material is easily contaminated, resulting in a short service life. With the increasing demand for deuterium-depleted water and the increasing requirements for its quality, the market urgently needs a deuterium-depleted water preparation technology that is efficient, low-cost, easy to operate, can accurately control the deuterium content, and is environmentally friendly.

[0004] Therefore, it is necessary to provide a deuterium-depleted water preparation and processing method and equipment to solve the above technical problems. Summary of the Invention

[0005] The object of the present invention is to provide a method and equipment for preparing deuterium-depleted water to solve the problems raised in the above background technology.

[0006] To achieve the above objectives, the present invention solves the above technical problems as follows: a method for preparing and processing deuterium-depleted water, which is based on a superconducting quantum cutting device, a superconducting energy extraction winding, and a quantum energy generation device, and comprises the following steps:

[0007] S1. Water pretreatment: Ordinary water is passed through a multi-layer filtration device to remove impurities, microorganisms, and macromolecular organic matter. Ion exchange resins are then used to remove metal ions and other charged impurities. Finally, reverse osmosis technology is used to further remove tiny particles and soluble substances in the water, resulting in high-purity purified water, which provides a high-quality water source for the subsequent superconducting quantum cutting process to prepare deuterium-depleted water.

[0008] S2. Superconducting quantum cutting: The pretreated purified water is transported to the reaction chamber of the superconducting quantum cutting device. The low-temperature cooling system is activated to cool the superconducting quantum cutting device to the low temperature environment required for superconducting materials, so that the superconducting coil enters the superconducting state. The quantum energy generator is turned on to generate a superconducting quantum field of specific frequency and intensity, which performs quantum cutting on the water molecules in the reaction chamber. Under the action of the superconducting quantum field, the protium and deuterium in the water molecules are separated, and the water with lower deuterium content gradually accumulates in a specific area of ​​the reaction chamber.

[0009] S3. Deuterium content detection and control: During the superconducting quantum cutting process, the mass spectrometer of the deuterium content detection and control system is used to detect the deuterium content in the water in the reaction chamber in real time. The central control system compares and analyzes the detected deuterium content data with the preset target deuterium content value. If the detected deuterium content is higher than the target value, the central control system automatically adjusts the parameters of the quantum field generator to enhance the intensity of the superconducting quantum field or adjust its frequency to improve the separation effect of protium and deuterium and reduce the deuterium content in the water. If the detected deuterium content is lower than the target value, the intensity of the superconducting quantum field is appropriately reduced or the frequency is adjusted to ensure that the deuterium content of the prepared low-deuterium water is precisely controlled within the target range.

[0010] S4. Collection and storage of deuterium-depleted water: After superconducting quantum cutting and precise control of deuterium content, deuterium-depleted water that meets the target deuterium content is transported through pipelines to the storage tank of the collection and storage device for storage. During the storage process, the liquid level of the deuterium-depleted water in the storage tank is monitored in real time by a liquid level sensor. When the liquid level reaches the set upper limit, the transportation is automatically stopped. At the same time, the quality of the stored deuterium-depleted water is regularly tested using quality inspection equipment to ensure the stable and reliable quality of the deuterium-depleted water.

[0011] A deuterium-depleted water preparation and processing device is used to complete the method steps in the self-pressurized liquid nitrogen tank claimed in the claim. A self-pressurized liquid nitrogen tank is provided on one side of the superconducting quantum cutting device. A superconducting energy extraction winding and a quantum energy generating device are provided inside the self-pressurized liquid nitrogen tank. A superconducting microparticle energy extraction winding that cooperates with the superconducting energy extraction winding is provided inside the superconducting quantum cutting device. A stainless steel pipeline is connected between the self-pressurized liquid nitrogen tank and the superconducting quantum cutting device, and multiple superconducting quantum cutting devices are connected through the stainless steel pipeline.

[0012] As a further solution of the present invention, a pipeline booster pump connected to the self-pressurized liquid nitrogen tank through a pipeline is provided on one side of the self-pressurized liquid nitrogen tank provided inside the superconducting quantum cutting device.

[0013] As a further solution of the present invention, water forward and backwash solenoid valves are installed on the pipeline between the pipeline booster pump and the self-pressurized liquid nitrogen tank.

[0014] As a further solution of the present invention, manual control valves are installed on the pipelines at the bottom of the self-pressurized liquid nitrogen tank and the superconducting quantum cutting device.

[0015] As a further solution of the present invention, a remote G flow controller is provided on the output pipeline of the superconducting quantum cutting device.

[0016] As a further solution of the present invention, ether disturbance field coils are provided inside the superconducting quantum cutting device and the self-pressurized liquid nitrogen tank.

[0017] Compared with the prior art, the present invention has the following beneficial effects:

[0018] 1. High efficiency: Superconducting quantum cutting technology can achieve efficient separation of protium and deuterium in a short time, greatly improving the preparation efficiency of low-deuterium water. Compared with traditional methods, the preparation efficiency can be increased by several times or even dozens of times.

[0019] 2. Low cost: The use of new high-temperature superconducting materials and advanced refrigeration technology reduces equipment costs and energy consumption; at the same time, it simplifies the preparation process, reduces operating steps and maintenance costs, and significantly reduces the production cost of deuterium-depleted water.

[0020] 3. Precise control: Through the deuterium content detection and control system, the deuterium content of deuterium-depleted water can be accurately detected and controlled in real time. Deuterium-depleted water with a deuterium content within a specific range can be prepared according to different application requirements to meet the diverse needs of the market.

[0021] 4. Environmental protection and energy saving: The entire preparation process does not require the use of chemical reagents and will not cause environmental pollution; it also has low energy consumption and meets the requirements of sustainable development.

[0022] 5. Compact equipment: The equipment of the present invention has a compact structure, occupies a small area, is easy to install and maintain, and is suitable for large-scale industrial production. BRIEF DESCRIPTION OF THE DRAWINGS

[0023] The present invention will be further described below with reference to the accompanying drawings and embodiments:

[0024] Figure 1 Schematic diagram of the method flow of the present invention;

[0025] Figure 2This is a schematic diagram of the structure of the device for preparing deuterium-depleted water using the superconducting quantum cutting technology of the present invention.

[0026] In the accompanying drawings, the components represented by the reference numerals are as follows:

[0027] 1. Self-pressurized liquid nitrogen tank; 2. Superconducting quantum cutting device; 3. Superconducting energy extraction winding; 4. Quantum energy generation device; 5. Superconducting microparticle energy extraction winding; 6. Water flow forward and backwash solenoid valves; 7. Manual control valve; 8. Remote 4G flow controller; 9. Stainless steel pipeline; 10. Pipeline booster pump; 11. Ether disturbance field coil. DETAILED DESCRIPTION

[0028] The present invention will be further described below with reference to the embodiments.

[0029] See also Figure 1-2 The present invention provides a method for preparing and processing deuterium-depleted water. The method is based on a superconducting quantum cutting device 2, a superconducting energy extraction winding 3, and a quantum energy generating device 4. The method comprises the following steps:

[0030] S1. Water pretreatment: Ordinary water is passed through a multi-layer filtration device to remove impurities, microorganisms, and macromolecular organic matter. Ion exchange resins are then used to remove metal ions and other charged impurities. Finally, reverse osmosis technology is used to further remove tiny particles and soluble substances in the water, resulting in high-purity purified water, which provides a high-quality water source for the subsequent superconducting quantum cutting process to prepare deuterium-depleted water.

[0031] S2. Superconducting quantum cutting: The pretreated pure water is transported to the reaction chamber of the superconducting quantum cutting device 2. The low-temperature cooling system is activated to cool the superconducting quantum cutting device 2 to the low temperature environment required for superconducting materials, so that the superconducting coil enters the superconducting state. The quantum energy generator 4 is turned on to generate a superconducting quantum field of specific frequency and intensity, which performs quantum cutting on the water molecules in the reaction chamber. Under the action of the superconducting quantum field, the protium and deuterium in the water molecules are separated, and the water with lower deuterium content gradually accumulates in a specific area of ​​the reaction chamber.

[0032] S3. Deuterium content detection and control: During the superconducting quantum cutting process, the mass spectrometer of the deuterium content detection and control system is used to detect the deuterium content in the water in the reaction chamber in real time. The central control system compares and analyzes the detected deuterium content data with the preset target deuterium content value. If the detected deuterium content is higher than the target value, the central control system automatically adjusts the parameters of the quantum field generator to enhance the intensity of the superconducting quantum field or adjust its frequency to improve the separation effect of protium and deuterium and reduce the deuterium content in the water. If the detected deuterium content is lower than the target value, the intensity of the superconducting quantum field is appropriately reduced or the frequency is adjusted to ensure that the deuterium content of the prepared low-deuterium water is precisely controlled within the target range.

[0033] S4. Collection and storage of deuterium-depleted water: After superconducting quantum cutting and precise control of deuterium content, deuterium-depleted water that meets the target deuterium content is transported through pipelines to the storage tank of the collection and storage device for storage. During the storage process, the liquid level of the deuterium-depleted water in the storage tank is monitored in real time by a liquid level sensor. When the liquid level reaches the set upper limit, the transportation is automatically stopped. At the same time, the quality of the stored deuterium-depleted water is regularly tested using quality inspection equipment to ensure the stable and reliable quality of the deuterium-depleted water.

[0034] Further as Figure 2 As shown, it is worth mentioning in detail that a deuterium-depleted water preparation and processing equipment is used to complete the method steps in the self-pressurized liquid nitrogen tank 1 claimed in the claim, and a self-pressurized liquid nitrogen tank 1 is provided on one side of the superconducting quantum cutting device 2. The interior of the self-pressurized liquid nitrogen tank 1 is provided with a superconducting energy extraction winding 3 and a quantum energy generating device 4, and the interior of the superconducting quantum cutting device 2 is provided with a superconducting microparticle energy extraction winding 5 coordinated with the superconducting energy extraction winding 3. A stainless steel pipeline 9 is connected between the self-pressurized liquid nitrogen tank 1 and the superconducting quantum cutting device 2, and multiple superconducting quantum cutting devices 2 are connected through the stainless steel pipeline 9. The stainless steel pipeline 9 can be a 63mm diameter stainless steel pipeline.

[0035] Further as Figure 2 As shown, it is worth mentioning that the superconducting quantum cutting device 2 is provided with a self-pressurized liquid nitrogen tank 1 inside and a pipeline booster pump 10 connected to the self-pressurized liquid nitrogen tank 1 through a pipeline is provided on one side.

[0036] Further as Figure 2 As shown, it is worth noting that a water flow forward and backwash solenoid valve 6 is installed on the pipeline between the pipeline booster pump 10 and the self-pressurized liquid nitrogen tank 1.

[0037] Further as Figure 2 As shown, it is worth noting that manual control valves 7 are installed on the pipelines at the bottom of the self-pressurized liquid nitrogen tank 1 and the superconducting quantum cutting device 2.

[0038] Further as Figure 2 As shown, it is worth noting that a remote 4G flow controller 8 is provided on the output end pipeline of the superconducting quantum cutting device 2.

[0039] Further as Figure 2 As shown, it is worth noting that both the superconducting quantum cutting device 2 and the self-pressurized liquid nitrogen tank 1 are provided with ether disturbance field coils 11, and the ether disturbance field coils 11 can be selected in 6 sets, 12 per set, for a total of 72 disturbance field coils.

[0040] Example 1

[0041] Equipment Preparation: A set of equipment using superconducting quantum cutting technology to prepare deuterium-depleted water was selected. The superconducting coils of the superconducting quantum cutting device are made of YBCO (yttrium barium copper oxide) high-temperature superconducting material, and the quantum field generator can generate a superconducting quantum field with a frequency range of 10-100 MHz and an intensity range of 0-5 T. The cryogenic cooling system uses liquid nitrogen refrigeration combined with pulse tube refrigeration technology to cool the superconducting quantum cutting device to below 77K. The water supply system is equipped with a high-precision gear pump with a flow control accuracy of ±0.1L / min, which can deliver pretreated water to the reaction chamber at a stable flow rate. The deuterium content detection and control system uses a time-of-flight mass spectrometer with a resolution of 0.01ppm to monitor the deuterium content in the water in real time. The collection and storage system includes five 1000L stainless steel storage tanks with special anti-corrosion treatment.

[0042] Water pretreatment: 1000L of ordinary tap water is filtered through a 5μm PP cotton filter, an activated carbon filter, and a 0.1μm ultrafiltration membrane filter in sequence to remove impurities, odors, and microorganisms. The water is then filtered through a strong acid cation exchange resin and a strong base anion exchange resin to remove metal ions and other charged impurities. Finally, a reverse osmosis device is used for deep treatment to obtain high-purity purified water with a conductivity of less than 1μS / cm.

[0043] Preparation of deuterium-depleted water by superconducting quantum cutting: 500L of pretreated pure water is delivered to the reaction chamber of the superconducting quantum cutting device via the water supply system. The cryogenic cooling system is activated, cooling the superconducting quantum cutting device to 70K within 30 minutes, causing the superconducting coil to enter a superconducting state. The quantum field generator is turned on, with the superconducting quantum field frequency set to 50MHz and the intensity to 3T, to perform quantum cutting on the water molecules in the reaction chamber. During the cutting process, the deuterium content in the water is monitored in real time using the mass spectrometer of the deuterium content detection and control system. After two hours of cutting, the deuterium content in the water was detected to have dropped to 50ppm, reaching the preset target value.

[0044] Deuterium-depleted water collection and storage: The prepared deuterium-depleted water is transported through pipelines to the storage tanks of the collection and storage device for storage. The liquid level and quality are monitored in real time during the storage process to ensure the storage safety and stable quality of the deuterium-depleted water.

[0045] Example 2

[0046] Equipment adjustment: Adjust the parameters of the quantum field generator of the superconducting quantum cutting device so that it can generate a superconducting quantum field with a frequency range of 20-150MHz and an intensity range of 0-8T; at the same time, optimize the control program of the low-temperature cooling system to improve the accuracy of temperature control and ensure that the superconducting quantum cutting device operates in a stable low-temperature environment of 65K.

[0047] Water pretreatment and preparation: Repeat the water pretreatment steps in Example 1 to obtain high-purity purified water. 600 L of pretreated purified water was transferred to the reaction chamber of the superconducting quantum cutting device, and the device was activated for superconducting quantum cutting. The superconducting quantum field frequency was set to 80 MHz and the intensity to 5 T. After 1.5 hours of cutting, the deuterium content in the water was detected by the deuterium content detection and control system and dropped to 30 ppm, meeting the requirements for preparing higher-purity, low-deuterium water.

[0048] Collection and storage: The prepared deuterium-depleted water is collected and stored in a storage tank. The quality of the stored deuterium-depleted water is regularly tested according to the quality inspection standards. The results show that the quality of the deuterium-depleted water is stable and meets the relevant standards.

[0049] It can be seen from the above examples that the method and equipment for preparing deuterium-depleted water using superconducting quantum cutting technology of the present invention can efficiently and accurately prepare deuterium-depleted water with different deuterium contents, and has good application prospects and economic benefits.

Claims

1. A method for preparing deuterium-depleted water, characterized in that: The deuterium-depleted water preparation and processing method is based on a superconducting quantum cutting device, a superconducting energy extraction winding, and a quantum energy generation device, and the preparation and processing method includes the following steps: S1. Water pretreatment: Ordinary water is passed through a multi-layer filtration device to remove impurities, microorganisms, and macromolecular organic matter. Ion exchange resins are then used to remove metal ions and other charged impurities. Finally, reverse osmosis technology is used to further remove tiny particles and soluble substances in the water, resulting in high-purity purified water, which provides a high-quality water source for the subsequent superconducting quantum cutting process to prepare deuterium-depleted water. S2. Superconducting quantum cutting: The pretreated purified water is transported to the reaction chamber of the superconducting quantum cutting device. The low-temperature cooling system is activated to cool the superconducting quantum cutting device to the low temperature environment required for superconducting materials, so that the superconducting coil enters the superconducting state. The quantum energy generator is turned on to generate a superconducting quantum field of specific frequency and intensity, which performs quantum cutting on the water molecules in the reaction chamber. Under the action of the superconducting quantum field, the protium and deuterium in the water molecules are separated, and the water with lower deuterium content gradually accumulates in a specific area of ​​the reaction chamber. S3. Deuterium content detection and control: During the superconducting quantum cutting process, the mass spectrometer of the deuterium content detection and control system is used to detect the deuterium content in the water in the reaction chamber in real time. The central control system compares and analyzes the detected deuterium content data with the preset target deuterium content value. If the detected deuterium content is higher than the target value, the central control system automatically adjusts the parameters of the quantum field generator to enhance the intensity of the superconducting quantum field or adjust its frequency to improve the separation effect of protium and deuterium and reduce the deuterium content in the water. If the detected deuterium content is lower than the target value, the intensity of the superconducting quantum field is appropriately reduced or the frequency is adjusted to ensure that the deuterium content of the prepared low-deuterium water is precisely controlled within the target range. S4. Collection and storage of deuterium-depleted water: After superconducting quantum cutting and precise control of deuterium content, deuterium-depleted water that meets the target deuterium content is transported through pipelines to the storage tank of the collection and storage device for storage. During the storage process, the liquid level of the deuterium-depleted water in the storage tank is monitored in real time by a liquid level sensor. When the liquid level reaches the set upper limit, the transportation is automatically stopped. At the same time, the quality of the stored deuterium-depleted water is regularly tested using quality inspection equipment to ensure the stable and reliable quality of the deuterium-depleted water.

2. A deuterium-depleted water preparation and processing equipment, which is used to complete the method steps in the claim from a pressurized liquid nitrogen tank, characterized in that: A self-pressurized liquid nitrogen tank is provided on one side of the superconducting quantum cutting device, and a superconducting energy extraction winding and a quantum energy generating device are provided inside the self-pressurized liquid nitrogen tank. A superconducting microparticle energy extraction winding that cooperates with the superconducting energy extraction winding is provided inside the superconducting quantum cutting device. A stainless steel pipeline is connected between the self-pressurized liquid nitrogen tank and the superconducting quantum cutting device, and multiple superconducting quantum cutting devices are connected through stainless steel pipelines.

3. The deuterium-depleted water preparation and processing equipment according to claim 2, characterized in that: The deuterium-depleted water preparation and processing equipment according to the superconducting quantum cutting device is characterized in that a self-pressurizing liquid nitrogen tank is provided inside the superconducting quantum cutting device, and a pipeline booster pump connected to the self-pressurizing liquid nitrogen tank through a pipeline is provided on one side.

4. The deuterium-depleted water preparation and processing equipment according to claim 3, characterized in that: Water flow forward and backwash solenoid valves are installed on the pipeline between the pipeline booster pump and the self-pressurized liquid nitrogen tank.

5. The deuterium-depleted water preparation and processing equipment according to claim 4, characterized in that: Manual control valves are installed on the pipelines at the bottom of the self-pressurized liquid nitrogen tank and the superconducting quantum cutting device.

6. The deuterium-depleted water preparation and processing equipment according to claim 5, characterized in that: A remote 4G flow controller is provided on the output end pipeline of the superconducting quantum cutting device.

7. The deuterium-depleted water preparation and processing equipment according to claim 5, characterized in that: The superconducting quantum cutting device and the self-pressurized liquid nitrogen tank are both provided with ether disturbance field coils.