Heat-preservation stirring device for preparing dextro-phenylethylamine

Abstract

The utility model relates to the technical field of phenylethylamine preparation, in particular to a heat-preservation stirring device for dextro-phenylethylamine preparation, which comprises a box body, the box body is of a cavity structure, two through holes are formed in the box body, a liquid inlet pipe and a liquid outlet pipe are respectively and fixedly arranged in the two through holes, a drying box and a filter box are fixedly arranged on the outer wall of the box body, and the filter box is arranged in the box body. A cover plate is arranged at the upper part of the box body, a detachable driving motor is mounted at the upper part of the cover plate, a fixed rod is fixedly connected with a stirring blade, and a cooling pipe and a heating wire are arranged between the outer wall of the reaction tank and the inner wall of the box body. The first rotating rod rotates to drive the vertical bevel gear on the lower portion to rotate, then the second rotating rod and the third rotating rod can rotate, the connecting rods on the two sides can do circular motion with the second rotating rod and the third rotating rod as the circle center, and therefore stirring rods at the two ends of the connecting rods can stir stirring liquid up and down; the upper and lower temperatures of the reaction liquid are more balanced.

Description

Technical Field

[0001] The utility model relates to the technical field of phenethylamine preparation, in particular to a heat-insulating stirring device for preparing dextrorotatory phenethylamine. Background Art

[0002] Phenylethylamine (PEA), also known as β-phenylethylamine and 2-phenylethylamine, has a molecular formula of C8H11N. It is an alkaloid and monoamine neurotransmitter that can increase the level of dopamine in the extracellular fluid while inhibiting dopamine nerve activation to treat depression.

[0003] There are many existing technologies, such as a heat-insulating and stirring device for preparing dextrorotatory phenylethylamine disclosed in publication number CN215139714U. This technology includes a catalyst box, the top and bottom of the catalyst box are respectively connected to a feed rod and a discharge rod, the inner cavity of the catalyst box is fixedly installed with a heat-insulating layer, the left side of the catalyst box is fixedly connected to a hot air blower with one end penetrating into the inner cavity of the catalyst box, the bottom of the right side of the catalyst box is connected to an exhaust rod, and the top of the catalyst box is fixedly installed with a catalytic mechanism with the bottom penetrating into the inner cavity of the catalyst box. The chemical materials of this technology are fed into the material through the feed rod, and the hot air blower blows the hot air flow into the cavity, thereby achieving a heat-insulating effect inside the catalytic device as a whole. The catalytic mechanism is started to stir and catalyze the materials inside the catalyst box. However, the following problems exist in use:

[0004] When the above technology is used, the pendulum arm rotates horizontally by rotating the rotating rod. During the rotation process, the temperature of the stirring liquid cannot be kept consistent between the upper and lower parts, which easily causes uneven temperature of the stirring liquid in the upper and lower parts, resulting in a decrease in the reaction effect. In addition, the water droplets on the inner wall cannot be scraped off, which easily leads to incomplete reaction. Utility Model Content

[0005] The utility model aims to solve the problems of temperature imbalance and incomplete reaction in the prior art, and proposes a heat-insulating and stirring device for preparing dextrorotatory phenylethylamine.

[0006] In order to achieve the above purpose, the present invention adopts the following technical solutions:

[0007] A heat-insulating stirring device for preparing dextrorotatory phenylethylamine comprises a box body, the box body being a hollow structure, the box body being provided with two through holes, a liquid inlet pipe and a liquid outlet pipe being fixedly installed in the two through holes, a drying box and a filter box being fixedly installed on the outer wall of the box body, a cover plate being provided on the upper portion of the box body, a detachable drive motor being installed on the upper portion of the cover plate, a drive end of the drive motor being fixedly connected to a first rotating rod, an outer wall of the first rotating rod being fixedly connected to a fixing rod, and a stirring blade being fixedly connected to the fixing rod, a reaction tank being provided inside the box body, a cooling pipe and a heating wire being provided between the outer wall of the reaction tank and the inner wall of the box body, and the liquid inlet pipe and the liquid outlet pipe being fixedly connected to the cooling pipe, respectively.

[0008] Preferably, two handles and a vacuum pump are fixedly mounted on the upper portion of the cover plate, four limiting clamps for limiting positioning are clamped between the upper portion of the cover plate and the upper end of the box body, and a pipeline is provided on the movable sleeve of the vacuum pump.

[0009] Preferably, the outer wall of the first rotating rod is fixedly connected to a sleeve, the lower part of the first rotating rod is fixedly connected to a vertical bevel gear, the lower part of the sleeve is rotatably connected to a pipe fitting, the second rotating rod and the third rotating rod are rotatably connected inside the pipe fitting, and the second rotating rod and the third rotating rod are respectively rotatably connected to the inner wall of the reaction tank.

[0010] Preferably, the second rotating rod is fixedly connected to the first transverse bevel gear, the third rotating rod is fixedly connected to the second transverse bevel gear, the first transverse bevel gear and the second transverse bevel gear are meshed and connected with the vertical bevel gear, the second rotating rod and the third rotating rod are respectively fixedly connected to the connecting rod, and the two ends of the connecting rod are respectively fixedly connected to stirring rods.

[0011] Preferably, the drying box and the filter box are connected to a pipeline, and the sleeve is rotatably connected to the cover plate.

[0012] Preferably, the four limiting clamps are equidistantly distributed on the cover plate, nuts and screws are respectively provided inside the four limiting clamps, and the two handles are horizontally symmetrically distributed on the cover plate.

[0013] Compared with the prior art, the present invention has the following advantages:

[0014] 1. The utility model rotates the first rotating rod to drive the vertical bevel gear at the bottom to rotate, thereby rotating the first transverse gear and the second transverse gear meshed and linked on both sides of the vertical bevel gear, and then the second rotating rod and the third rotating rod will rotate. When the second rotating rod and the third rotating rod rotate, the connecting rods on both sides thereof will make circular motions with the second rotating rod and the third rotating rod as the center, respectively, so that the stirring rods at both ends of the connecting rods will stir the stirring liquid up and down, so that the temperature of the reaction liquid is more balanced.

[0015] 2. In the present invention, when the first rotating rod rotates, the fixed rod is driven to rotate with the first rotating rod as the center, thereby driving the stirring blade to rotate. When the stirring blade rotates, the water droplets in the reaction tank will be scraped off, thereby making the reaction more complete. BRIEF DESCRIPTION OF THE DRAWINGS

[0016] Figure 1 This is a schematic structural diagram of a heat-insulating and stirring device for preparing dextrorotatory phenylethylamine proposed in the present invention;

[0017] Figure 2This is a schematic front cross-sectional view of a heat-insulating and stirring device for preparing dextrorotatory phenylethylamine proposed in the present invention;

[0018] Figure 3 This is a schematic diagram of a first transmission rod and stirring blade of a heat-insulating stirring device for preparing dextrorotatory phenylethylamine proposed in the present invention;

[0019] Figure 4 The present invention provides a schematic diagram of a cooling tube and a heating tube of a heat-insulating stirring device for preparing dextrorotatory phenylethylamine.

[0020] In the figure: 1. Box body; 2. Liquid inlet pipe; 3. Liquid outlet pipe; 4. Limiting clamp; 5. Cover plate; 6. Handle; 7. Vacuum pump; 8. Pipe; 9. Drying box; 10. Filter box; 11. Drive motor; 12. First rotating rod; 13. Pipe fitting; 14. Second rotating rod; 15. Third rotating rod; 16. Connecting rod; 17. Stirring rod; 18. Sleeve; 19. Fixed rod; 20. Stirring blade; 21. Cooling tube; 22. Heating wire; 23. Reactor; 24. Vertical bevel gear; 25. First horizontal bevel gear; 26. Second horizontal bevel gear. DETAILED DESCRIPTION

[0021] The technical solutions in the embodiments of the present invention will be described clearly and completely below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, rather than all the embodiments.

[0022] Reference Figures 1-4 , a heat-insulating stirring device for preparing dextrorotatory phenylethylamine, comprising a box body 1, the box body 1 being a cavity structure, the box body 1 being provided with two through holes, the two through holes being fixedly mounted with a liquid inlet pipe 2 and a liquid outlet pipe 3, the outer wall of the box body 1 being fixedly mounted with a drying box 9 and a filter box 10, a cover plate 5 being provided on the upper part of the box body 1, a detachable driving motor 11 being mounted on the upper part of the cover plate 5, when the cover plate 5 needs to be opened, the driving motor 11 is first removed, and then the cover plate 5 is taken out, the driving end of the driving motor 11 is fixedly connected with a first rotating rod 12, the outer wall of the first rotating rod 12 is fixedly connected with a fixing rod 19, the fixing rod 19 is fixedly connected with a stirring blade 20, a reaction tank 23 is provided inside the box body 1, a cooling pipe 21 and a heating wire 22 are provided between the outer wall of the reaction tank 23 and the inner wall of the box body 1, the liquid inlet pipe 2 and the liquid outlet pipe 3 are respectively fixedly connected with the cooling pipe 21;

[0023] Two handles 6 and a vacuum pump 7 are fixedly installed on the upper part of the cover plate 5. Four limiting clamps 4 are clamped between the upper part of the cover plate 5 and the upper end of the box body 1 for limiting the position. When the cover plate 5 is to be opened, the nuts in the limiting clamps 4 are screwed to reduce the limiting force of the limiting clamps 4 on the cover plate 5. A pipe 8 is provided in a movable sleeve of the vacuum pump 7.

[0024] The outer wall of the first rotating rod 12 is fixedly connected with a sleeve 18, and the sleeve 18 is provided with a through hole, in which a fixing rod 19 is provided. The lower part of the first rotating rod 12 is fixedly connected with a vertical bevel gear 24, and the lower part of the sleeve 18 is rotatably connected with the pipe fitting 13, and the second rotating rod 14 and the third rotating rod 15 are rotatably connected in the pipe fitting 13. The second rotating rod 14 and the third rotating rod 15 are respectively rotatably connected to the inner wall of the reaction tank 23. When the driving motor 11 drives the first rotating rod 12 to rotate, the sleeve 18 will rotate accordingly. The pipe fitting 13 rotatably connected at the lower part of the sleeve 18 is kept stable by being rotatably connected to the second rotating rod 14 on the reaction tank 23. Therefore, when the vertical bevel gear 24 rotates, the first transverse bevel gear 25 and the second transverse bevel gear 26 meshing with the vertical bevel gear 24 rotate accordingly;

[0025] The second rotating rod 14 is fixedly connected to the first transverse bevel gear 25, and the third rotating rod 15 is fixedly connected to the second transverse bevel gear 26. The first transverse bevel gear 25 and the second transverse bevel gear 26 are meshed and connected with the vertical bevel gear 24. The second rotating rod 14 and the third rotating rod 15 are respectively fixedly connected to the connecting rod 16, and the two ends of the connecting rod 16 are respectively fixedly connected to the stirring rod 17;

[0026] The drying box 9 and the filter box 10 are connected to the pipe 8, and the sleeve 18 is rotatably connected to the cover plate 5. When the drive motor 11 rotates, the first rotating rod 12 rotates accordingly, thereby driving the sleeve 18 to rotate. The pipe 13 is rotatably connected to the lower end of the sleeve 18. The pipe 13 is fixed by rotating the second rotating rod 14 connected to the inner wall of the reaction tank 23. Therefore, when the sleeve 18 rotates, the pipe 13 remains stationary;

[0027] Four limiting clamps 4 are equidistantly distributed on the cover plate 5 circumference, nuts and screws are respectively provided inside the four limiting clamps 4 , and two handles 6 are horizontally symmetrically distributed on the cover plate 5 .

[0028] The functional principle of this utility model can be explained through the following operation modes:

[0029] Open the limiting clamp 4, remove the cover plate 5 through the handle 6, then add the stirring liquid, turn on the vacuum pump 7, and allow air to enter the vacuum pump 7 from the pipe 8, and then enter the reaction tank 23 through the vacuum pump 7. When the air enters from the pipe 8, it will first pass through the drying box 9 to dry the moisture in the air, and then enter the filter box 10 to filter out the gas in the air that may interfere with the reaction, and finally enter the reaction tank 23;

[0030] Turn on the drive motor 11, so that the driving end of the drive motor 11 drives the first rotating rod 12 to rotate. When the first rotating rod 12 rotates, it drives the vertical bevel gear 24 at the bottom to rotate. When the vertical bevel gear 24 rotates, the first transverse bevel gear 25 and the second transverse bevel gear 26 on both sides of it that are meshed and linked will rotate accordingly, and when rotating, the second rotating rod 14 and the third rotating rod 15 on both sides are driven to rotate. When the second rotating rod 14 and the third rotating rod 15 rotate, the connecting rods 16 on both sides thereof will make circular motions with the second rotating rod 14 and the third rotating rod 15 as the center, respectively. Therefore, the stirring rods 17 at both ends of the connecting rod 16 will stir the stirring liquid up and down, so that the temperature of the stirring liquid in the upper and lower parts is more balanced.

[0031] When the stirring liquid reacts to a certain extent, small water droplets will be generated on the inner wall of the reaction tank 23. There will be some stirring liquid in the small water droplets, which will be scraped off by the stirring blade 20 to allow the reaction to proceed fully.

[0032] The heating wire 22 is turned on to maintain a certain temperature of the heating wire 22, so that the reaction tank 23 will maintain the same temperature as the heating wire 22, thereby achieving the effect of heat preservation. When the reaction tank 23 needs to be cooled, the coolant enters the cooling pipe 21 from the liquid inlet pipe 2 and then flows out from the liquid outlet pipe 3. During the outflow process of the coolant, the heat will be taken away, thereby achieving the cooling effect.

[0033] The above is only a preferred specific implementation method of the present invention, but the protection scope of the present invention is not limited to this. Any technician familiar with the technical field within the technical scope disclosed by the present invention can make equivalent replacements or changes based on the technical solution and utility model concept of the present invention, which should be covered by the protection scope of the present invention.

Claims

1. A heat-insulating stirring device for preparing dextrorotatory phenylethylamine, comprising a housing (1), characterized in that: The box body (1) is a cavity structure. The box body (1) is provided with two through holes. A liquid inlet pipe (2) and a liquid outlet pipe (3) are fixedly installed in the two through holes respectively. A drying box (9) and a filter box (10) are fixedly installed on the outer wall of the box body (1). A cover plate (5) is provided on the upper part of the box body (1). A detachable driving motor (11) is installed on the upper part of the cover plate (5). The driving end of the driving motor (11) is fixedly connected to a first rotating rod (12). The outer wall of the first rotating rod (12) is fixedly connected to a fixing rod (19). The fixing rod (19) is fixedly connected to a stirring blade (20). A reaction tank (23) is provided inside the box body (1). A cooling pipe (21) and a heating wire (22) are provided between the outer wall of the reaction tank (23) and the inner wall of the box body (1). The liquid inlet pipe (2) and the liquid outlet pipe (3) are fixedly connected to the cooling pipe (21) respectively.

2. A heat-insulating and stirring device for preparing dextrorotatory phenylethylamine according to claim 1, characterized in that, Two handles (6) and a vacuum pump (7) are fixedly mounted on the upper portion of the cover plate (5); four limiting clamps (4) for limiting are clamped between the upper portion of the cover plate (5) and the upper end of the box body (1); and a pipe (8) is movably sleeved on the vacuum pump (7).

3. A heat-insulating and stirring device for preparing dextrorotatory phenylethylamine according to claim 1, characterized in that, The outer wall of the first rotating rod (12) is fixedly connected to a sleeve (18), the lower part of the first rotating rod (12) is fixedly connected to a vertical bevel gear (24), the lower part of the sleeve (18) is rotatably connected to a pipe (13), the inside of the pipe (13) is rotatably connected to a second rotating rod (14) and a third rotating rod (15), and the second rotating rod (14) and the third rotating rod (15) are respectively rotatably connected to the inner wall of the reaction tank (23).

4. A heat-insulating and stirring device for preparing dextrorotatory phenylethylamine according to claim 3, characterized in that, The second rotating rod (14) is fixedly connected to a first transverse bevel gear (25), and the third rotating rod (15) is fixedly connected to a second transverse bevel gear (26). The first transverse bevel gear (25) and the second transverse bevel gear (26) are meshed and connected with the vertical bevel gear (24). The second rotating rod (14) and the third rotating rod (15) are respectively fixedly connected to a connecting rod (16), and both ends of the connecting rod (16) are respectively fixedly connected to stirring rods (17).

5. A heat-insulating and stirring device for preparing dextrorotatory phenylethylamine according to claim 2, characterized in that, The drying box (9) and the filter box (10) are connected to the pipeline (8), and the sleeve (18) is rotatably connected to the cover plate (5).

6. A heat-insulating and stirring device for preparing dextrorotatory phenylethylamine according to claim 2, characterized in that, The four limiting clamps (4) are equidistantly distributed on the cover plate (5), and nuts and screws are respectively provided inside the four limiting clamps (4). The two handles (6) are horizontally and symmetrically distributed on the cover plate (5).

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