Dendrimer network structure gel nanosuspension preparation apparatus

Abstract

The utility model discloses dendritic polymer network structure gel nano slurry preparation equipment belongs to the technical field of grinding equipment, including frame, stand, the frame is assembled with the grinding assembly that can grind dendritic polymer network structure gel into nano slurry, through adopting nanometer level partition spacing design, forms gradient shear field, can tear the gel network gradually and break, and the cooperation drive component can make the grinding roller reciprocating movement and grind the gel into nanometer level particle, has improved grinding efficiency and quality significantly, push part can push the gel after grinding evenly to the grinding area and grind again through the reciprocating motion of lifting plate and vertical board, ensures its full grinding.

Description

Technical Field

[0001] This utility model relates to the field of grinding equipment technology, and in particular to equipment for preparing dendritic polymer network structure gel nanoparticle slurry. Background Technology

[0002] Dendritic polymers, with their highly branched three-dimensional spherical structure, abundant terminal functional groups, and low viscosity, have shown great application potential in high-end fields such as conductive pastes, drug carriers, and functional coatings. However, traditional grinding equipment can only achieve micron-level dispersion and cannot be further broken down to the nanoscale, resulting in low efficiency of conductive / thermal / mechanical enhancement in downstream applications.

[0003] However, existing grinding equipment has insufficient shear strength and cannot effectively destroy the chemical cross-linking network of dendritic polymers, resulting in larger particle sizes after grinding and making it difficult to obtain uniform nanoscale particles. Utility Model Content

[0004] The purpose of this invention is to solve the problem that the existing grinding equipment has insufficient shear strength, resulting in large particle size after grinding, and to propose a dendritic polymer network structure gel nanoslurry preparation device.

[0005] To achieve the above objectives, the present invention employs the following technology: a dendritic polymer network structure gel nanoslurry preparation equipment, comprising a frame and a column, wherein the frame is equipped with a grinding component capable of grinding the dendritic polymer network structure gel into a nanoslurry; The grinding assembly includes a movable frame disposed at the top of the frame, a grinding rack disposed at the top of the movable frame, a grinding groove formed on the grinding rack, several partitions fixedly installed in the middle of the grinding groove, and the two sides of the grinding groove being set as inclined surfaces, a grinding roller disposed on a column, a pushing component that can push the ground gel to reciprocate for grinding on the grinding rack, a driving component that can drive the grinding roller to grind the gel on the column, and a movable component that can move the grinding rack out on the frame.

[0006] As a further description of the above technical solution: the pushing component includes a lifting plate that is slidably installed on the grinding tank, several vertical plates that are fixedly installed on the lifting plate and located between several partitions, a rectangular frame that is fixedly installed at the bottom of the grinding frame, an electric push rod that is fixedly installed on the rectangular frame, and the lifting plate that is fixedly installed on the output end of the electric push rod.

[0007] As a further description of the above technical solution: the rectangular frame is slidably mounted on the movable frame, the electric push rod two is fixedly mounted on the movable frame, the rectangular frame is fixedly connected to the output end of the electric push rod two, and the vibrator is set on the grinding frame.

[0008] As a further description of the above technical solution: the drive assembly includes a lead screw and a motor mounted on the column, a support frame threaded onto the lead screw and slidably connected to the column, a slide mounted slidably on the support frame, a motor fixedly mounted on the slide, and an electric actuator fixedly connected between the slide and the support frame.

[0009] As a further description of the above technical solution: the lead screw is fixedly connected to the output end of the motor, the grinding roller is rotatably mounted on the slide, and a belt is provided between the grinding roller and the output end of the motor.

[0010] As a further description of the above technical solution: the size of the grinding roller is adapted to the grinding groove, and a scraper is fixedly installed on the slide, and the scraper is in contact with the surface of the grinding roller.

[0011] As a further description of the above technical solution: the moving component includes a limiting rod and a lead screw 2 symmetrically arranged on the frame. The moving frame is threadedly installed on the two lead screws 2 and slidably connected with the limiting rod. A synchronous belt meshes between the two lead screws 2, and one of the lead screws 2 is fixedly connected to the output end of the motor 3.

[0012] In summary, due to the adoption of the above technical solution, the beneficial effects of this utility model are: By employing a nanoscale partition spacing design, a gradient shear field is formed, which can tear and break the gel network step by step. Combined with the drive component, the grinding roller can reciprocate to grind the gel into nanoscale particles, significantly improving grinding efficiency and quality. The pushing component, through the reciprocating motion of the lifting plate and the vertical plate, can evenly push the ground gel to the grinding area for further grinding, ensuring that it is fully ground. The electric push rod two works with the vibrator to make the grinding frame vibrate, causing the gel to shake, thereby preventing accumulation. The vibration can also loosen and remove gel particles adhering to the grinding tank or partition. Attached Figure Description

[0013] Figure 1 An overall schematic diagram according to an embodiment of the present utility model is shown; Figure 2 A schematic diagram of a grinding assembly provided according to an embodiment of the present invention is shown; Figure 3 A cross-sectional view of a grinding frame provided according to an embodiment of the present invention is shown; Figure 4 A schematic diagram of a pusher component according to an embodiment of the present invention is shown; Figure 5 A schematic diagram of a drive component provided according to an embodiment of the present invention is shown; Figure 6 The present invention provides an embodiment of the present invention. Figure 5Another perspective view.

[0014] Legend: 10. Frame; 11. Column; 20. Grinding assembly; 21. Moving frame; 22. Grinding frame; 23. Grinding tank; 24. Partition plate; 25. Grinding roller; 26. Pushing component; 261. Lifting plate; 262. Vertical plate; 263. Rectangular frame; 264. Electric actuator one; 265. Electric actuator two; 266. Vibrator; 30. Drive assembly; 31. Lead screw one; 32. Motor one; 33. Support frame; 34. Carriage; 35. Motor two; 36. Electric actuator three; 40. Moving component; 41. Lead screw II; 42. Synchronous belt; 43. Motor III. Detailed Implementation

[0015] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those skilled in the art without creative effort are within the protection scope of the present utility model.

[0016] Reference Figure 1 - Figure 6 The dendritic polymer network structure gel nanoslurry preparation equipment provided in this embodiment includes a frame 10 and a column 11. The frame 10 is equipped with a grinding component 20 that can grind the dendritic polymer network structure gel into nanoslurry. The grinding assembly 20 includes a movable frame 21 disposed at the top of the frame 10, a grinding frame 22 disposed at the top of the movable frame 21, and a grinding tank 23 disposed on the grinding frame 22. The dendritic polymer network structure gel can be ground in the grinding tank 23. The dendritic polymer network structure gel is obtained by first adding ethylenediamine and methyl acrylate to a solvent to react and obtain a colorless and transparent liquid; then adding the liquid to the solvent with ethylenediamine to react and obtain a pale yellow viscous liquid; then adding nicotinic acid or isonicotinic acid and reacting in the presence of a catalyst to remove the white precipitate, and precipitating in diethyl ether to obtain a viscous liquid; finally, washing the obtained viscous liquid, dissolving it with distilled water, evaporating the solution to obtain a yellow solid, i.e., dendritic polymer. By placing the yellow solid in the grinding tank 23 for grinding, it forms a nano-slurry. The nano-sized particles can provide more conductive pathways. In conductive composite materials, nanoparticles can be more tightly filled in the matrix to form a continuous conductive network, thereby improving the conductivity of the material. Several partitions 24 are fixedly installed in the middle of the grinding tank 23. The distance between the partitions 24 is at the nanometer level. The two sides of the grinding tank 23 are set as inclined surfaces. The inclined surfaces can prevent accumulation and grinding dead corners. The grinding roller 25 is set on the column 11. The grinding frame 22 is also equipped with a pushing component 26 that can push the ground gel to grind it back and forth. The column 11 is equipped with a driving component 30 that can drive the grinding roller 25 to grind the gel. The frame 10 is also equipped with a moving component 40 that can move the grinding frame 22 out.

[0017] Reference Figure 2 Specifically, in order to drive the movable frame 21 to move the top grinding frame 22 for loading and unloading, a movable assembly 40 is provided. The movable assembly 40 includes a limiting rod and two lead screws 41 symmetrically arranged on the frame 10. The movable frame 21 is threaded onto the two lead screws 41, which are rotatably connected to the frame 10. The movable frame 21 can move by rotating the lead screws 41 and is slidably connected to the limiting rods. While the movable frame 21 moves, it is kept stable by the limiting rods. A synchronous belt 42 meshes between the two lead screws 41. The meshing transmission of 2 enables the two lead screws 41 to rotate synchronously. One of the lead screws 41 is fixedly connected to the output end of the motor 43. In use, the dendritic polymer network structure gel is placed in the grinding tank 23, and then the motor 43 is started. The motor 43 drives the rotation of the lead screw 41 connected to it. Through the meshing transmission of the synchronous belt 42, the two lead screws 41 can rotate synchronously, which in turn causes the moving frame 21 to move the top grinding frame 22 to below the grinding roller 25, where grinding can be performed.

[0018] Reference Figure 5 - Figure 6 Specifically, in order to enable the grinding roller 25 to grind the dendritic polymer network structure gel, a drive assembly 30 is provided. The drive assembly 30 includes a lead screw 31 and a motor 32 mounted on the column 11. A support frame 33 is threaded onto the lead screw 31 and slidably connected to the column 11. The rotation of the lead screw 31 allows the support frame 33 to be raised and lowered, and it is kept stable by the column 11. A slide 34 is slidably mounted on the support frame 33. A motor 35 is fixedly mounted on the slide 34. An electric actuator 36 is fixedly connected between the slide 34 and the support frame 33. The electric actuator 36 can drive the slide 34 to move on the support frame 33.

[0019] In more detail, the lead screw 31 is fixedly connected to the output end of the motor 32. The motor 32 can drive the lead screw 31 to rotate. The grinding roller 25 is rotatably mounted on the slide 34. A belt is provided between the grinding roller 25 and the output end of the motor 35. When the output end of the motor 35 rotates, the grinding roller 25 will also rotate through the belt drive.

[0020] In more detail, the size of the grinding roller 25 is adapted to the grinding groove 23, allowing the grinding roller 25 to descend into the grinding groove 23. A scraper is fixedly installed on the slide 34, and the scraper is in contact with the surface of the grinding roller 25. The scraper can prevent residue from remaining on the surface of the grinding roller 25. When the moving frame 21 moves the top grinding frame 22 to below the grinding roller 25, the motor 32 is started, which drives the lead screw 31 to rotate, causing the support frame 33 to lower the grinding roller 25 into the grinding groove 23. Then, the motor 35 is started. When the output end of the motor 35 rotates, the grinding roller 25 will also rotate through the belt drive. At the same time, the electric actuator 36 is started. The electric actuator 36 drives the carriage 34 to move on the support frame 33, thereby enabling the grinding roller 25 to reciprocate within the grinding groove 23. This continuously grinds the dendritic polymer network structure gel at the top of the partition 24. Since the distance between the partitions 24 is on the nanometer scale, this nanometer-scale spacing generates extremely high shear force, which helps to efficiently break down the three-dimensional network structure of the dendritic polymer network structure gel, thus grinding it into smaller particles and achieving a nanometer-scale dispersion effect. This keeps the size of the ground particles within the target range. Secondly, the nanometer-scale spacing of the partitions 24 forces the material to pass through uniformly, reducing particle inhomogeneity and missed areas during grinding, and improving grinding efficiency. Furthermore, this design can also create numerous "shear hot spots" at the microscale, allowing the grinding process to more specifically target the chemical bonds or physical network of the dendritic polymer network structure gel, further enhancing the grinding effect.

[0021] Reference Figure 2 - Figure 4Specifically, in order to make the dendritic polymer network structure gel more thoroughly ground, a pushing component 26 is provided. The pushing component 26 includes a lifting plate 261 slidably mounted on the grinding tank 23, and several vertical plates 262 fixedly mounted on the lifting plate 261 and located between several partitions 24. The lifting plate 261 can drive the vertical plates 262 to rise and fall, thereby pushing out the dendritic polymer network structure gel between the partitions 24. At this time, the vertical plates 262 fill the nanometer-level distance between the partitions 24 to form a complete plane, so that the pushed-out dendritic polymer network structure gel can be ground again. This process is repeated. A rectangular frame 263 is fixedly mounted on the bottom of the grinding frame 22, and an electric push rod 264 is fixedly mounted on the rectangular frame 263. The lifting plate 261 is fixedly mounted on the output end of the electric push rod 264. The electric push rod 264 can reciprocate to drive the lifting plate 261 to drive the vertical plates 262 to rise and fall.

[0022] In more detail, the rectangular frame 263 is slidably mounted on the movable frame 21, and the electric push rod 265 is fixedly mounted on the movable frame 21. The rectangular frame 263 is fixedly connected to the output end of the electric push rod 265. The vibrator 266 (model YBZD series) is set on the grinding frame 22. The electric push rod 265 can drive the movable frame 21 to move back and forth in a small amplitude during grinding. In conjunction with the vibrator 266, the grinding frame 22 is vibrated, which can shake the dendritic polymer network structure gel inside the grinding frame 22 to prevent it from accumulating.

[0023] The above description is only a preferred embodiment of the present utility model, but the protection scope of the present utility model is not limited thereto. Any equivalent substitutions or changes made by those skilled in the art within the technical scope disclosed in the present utility model, based on the technical solution and the inventive concept of the present utility model, should be included within the protection scope of the present utility model.

Claims

1. A device for preparing dendritic polymer network structure gel nanoparticle slurry, comprising a frame (10) and a column (11), characterized in that, The frame (10) is equipped with a grinding component (20) capable of grinding dendritic polymer network structure gel into nano-slurry. The grinding assembly (20) includes a movable frame (21) disposed at the top of the frame (10), a grinding frame (22) disposed at the top of the movable frame (21), a grinding groove (23) disposed on the grinding frame (22), a plurality of partitions (24) fixedly installed in the middle of the grinding groove (23), and the two sides of the grinding groove (23) are set as inclined surfaces, a grinding roller (25) disposed on a column (11), a pushing component (26) that can push the ground gel to grind it back and forth is also mounted on the grinding frame (22), a driving component (30) that can drive the grinding roller (25) to grind the gel is mounted on the column (11), and a movable component (40) that can move the grinding frame (22) out is also mounted on the frame (10).

2. The apparatus for preparing dendritic polymer network structure gel nanoparticles according to claim 1, characterized in that, The pushing component (26) includes a lifting plate (261) slidably mounted on the grinding tank (23), several vertical plates (262) fixedly mounted on the lifting plate (261) and located between several partitions (24), a rectangular frame (263) fixedly mounted on the bottom end of the grinding frame (22), an electric push rod (264) fixedly mounted on the rectangular frame (263), and the lifting plate (261) fixedly mounted on the output end of the electric push rod (264).

3. The apparatus for preparing dendritic polymer network structure gel nanoparticles according to claim 2, characterized in that, The rectangular frame (263) is slidably mounted on the movable frame (21), the electric push rod two (265) is fixedly mounted on the movable frame (21), the rectangular frame (263) is fixedly connected to the output end of the electric push rod two (265), and the vibrator (266) is set on the grinding frame (22).

4. The apparatus for preparing dendritic polymer network structure gel nanoparticles according to claim 1, characterized in that, The drive assembly (30) includes a lead screw (31) and a motor (32) mounted on the column (11). A support frame (33) is threaded onto the lead screw (31) and slidably connected to the column (11). A slide (34) is slidably mounted on the support frame (33). A motor (35) is fixedly mounted on the slide (34). An electric actuator (36) is fixedly connected between the slide (34) and the support frame (33).

5. The apparatus for preparing dendritic polymer network structure gel nanoparticles according to claim 4, characterized in that, The lead screw (31) is fixedly connected to the output end of the motor (32), the grinding roller (25) is rotatably mounted on the slide (34), and a belt is provided between the grinding roller (25) and the output end of the motor (35).

6. The apparatus for preparing dendritic polymer network structure gel nanoparticles according to claim 5, characterized in that, The size of the grinding roller (25) is adapted to the grinding groove (23), and a scraper is fixedly installed on the slide (34), and the scraper is in contact with the surface of the grinding roller (25).

7. The apparatus for preparing dendritic polymer network structure gel nanoparticles according to claim 1, characterized in that, The moving component (40) includes a limiting rod and a lead screw (41) symmetrically arranged on the frame (10). The moving frame (21) is threaded onto the two lead screws (41) and slidably connected to the limiting rod. A synchronous belt (42) meshes between the two lead screws (41). One of the lead screws (41) is fixedly connected to the output end of the motor (43).

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