Micro-arc oxidation solution for titanium alloy strontium-containing biological coating and application of micro-arc oxidation solution

A bio-coating and micro-arc oxidation technology, applied in the field of materials science, can solve the problems of low biological activity of titanium alloys, and achieve the effect of increasing osteoinductive properties, low price, and firm bonding

CN106435690AActive Publication Date: 2017-02-22上海理微医疗科技发展有限公司
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Publication Date
2017-02-22

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Abstract

The invention discloses a micro-arc oxidation solution for a titanium alloy strontium-containing biological coating. The micro-arc oxidation solution contains Sr(OH)2 with the concentration being 1-3 g / L or Sr(OH)2.8H2O with the concentration being 2-6 g / L, Na2SiO3 with the concentration being 4-8 g / L, NaH2PO4 with the concentration being 2-4 g / L, triethanolamine with the concentration being 2-4 g / L, Na2B4O7 with the concentration being 1-2 g / L and glycerol with the concentration being 5-10 ml / L, and a solvent is deionized water. The invention further provides application of the micro-arc oxidation solution. Titanium alloy is added into the micro-arc oxidation solution, a direct current pulse power source is adopted, voltage is controlled at 200-600 V, the current density is 0.1-0.4 A / dm<2>, the solution temperature is lower than 60 DEG C, time is 20-120 min, and the strontium-containing biological coating is formed on the surface of the titanium alloy. Compared with other medial titanium alloy surface treatment technology, the micro-arc oxidation solution has the beneficial effects of being high in treatment efficiency, firm in combination of a film layer and a base body and the like. Besides, because strontium, phosphorus and other active elements are added into the film layer, the biological activity is superior to that of an existing titanium alloy micro-arc oxidation treatment method.
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Description

technical field

[0001] The invention belongs to the field of materials science and relates to a titanium alloy, in particular to a micro-arc oxidation solution of a strontium-containing biological coating on a titanium alloy and an application thereof. Background technique

[0002] Bone defects and fractures have become a serious social problem affecting people's health and life. At present, the number of biomaterials for bone repair is small, the varieties and specifications are not complete, and it is difficult to meet the needs of clinical operations. Therefore, the research and development of bone repair materials can not only heal the body of the disabled, but also have huge social and economic benefits. Among the materials used for bone repair and replacement are metals and alloys, bioceramics, polymers, composites, and derivatives of human and animal bone. Under the complex stress conditions of the bone and joint system, it is not only required that the repair mater...

Examples

Embodiment 1

[0055] A micro-arc oxidation solution for strontium-containing biocoatings on titanium alloys containing 1 g of Sr(OH) per liter of solution 2 , 4 g of Na 2 SiO 3 , 2 g of NaH 2 PO 4 , 2 g of triethanolamine, 1 g of Na 2 B 4 o 7 and 5 ml / L of glycerin, prepared into a solution with deionized water and stirred evenly.

Embodiment 2

[0067] A micro-arc oxidation solution for strontium-containing biocoatings on titanium alloys containing 3 g of Sr(OH) per liter of solution 2 , 8 g of Na 2 SiO 3 , 4 g of NaH 2 PO 4 , 4 g of triethanolamine, 2 g of Na 2 B 4 o 7 and 10 ml / L of glycerol, prepared into a solution with deionized water and stirred evenly.