Preparation method of a soft tissue tumor specimen incision fixator and its suction cup
By designing a soft tissue tumor specimen incision fixator with suction cups with adjustable height-adjustable mesh tray and adjustment rod-connected suction cups, the problem of fixing and cutting of large soft tissue tumor specimens in the prior art is solved, and the stable fixation and efficient cutting of the specimen is achieved, ensuring the quality and safety of the section.
Patent Information
- Application Number
- CN202011356072.1
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2020-11-26
- Publication Date
- 2025-06-13
- Estimated Expiration
- 2040-11-26
AI Technical Summary
The prior art is difficult to effectively fix and cut large soft tissue tumor specimens, resulting in insufficient fixation, poor section quality, high misdiagnosis rate, and clinicians are prone to injury when processing specimens.
A soft tissue tumor specimen incision fixator is designed, including a mesh tray with adjustable height and a suction cup connected by the adjustment rod, which can adapt to specimens of different sizes and improve production efficiency through an optimized suction cup preparation method.
Stable fixation and cutting of tumor specimens of soft tissues of different sizes is achieved, specimen processing efficiency is improved, sufficient fixation and high-quality sectioning of tissues are ensured, misdiagnosis rate is reduced, and the risk of injury for physicians when processing specimens is reduced.
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Figure CN112268778B_ABST
Abstract
Description
Technical Field
[0001] The present invention belongs to the technical field of medical devices, and particularly relates to a preparation method of a soft tissue tumor specimen incision fixator and its suction cup. Background Art
[0002] After the pathological specimen of soft tissue tumor is removed, it needs to be fixed with 10% formalin in time. For soft tissue tumors with a diameter ≥ 2 cm, it is necessary to make incisions every 1 cm to allow formalin to penetrate into the tumor tissue for sufficient fixation. In clinical work, the soft tissue tumor specimen is often oval, which makes it difficult to clamp the specimen after surgery, difficult to incise the specimen, low efficiency in processing the postoperative specimen, uneven thickness when incising the specimen, resulting in tissue fixation failure. Without sufficient fixation, it can lead to difficult sampling, difficult to obtain high-quality HE sections, causing errors in immunohistochemistry and molecular pathology results, and incorrect pathological diagnosis can interfere with clinical treatment. Clinicians often hold the specimen with one hand and incise the specimen with the other hand, which is prone to blade cutting injuries and cause iatrogenic exposure. At the same time, it is not easy to measure the major axis and minor axis of the tumor after the oval tumor is removed. The base of the present invention has a 1*1 cm grid. After fixing the specimen with the specimen fixing suction cup, the major axis and minor axis of the tumor can be directly read, which is convenient and fast.
[0003] In Patent 201520950579.8, a fixing and cutting device for sectional specimens, which is provided with a plurality of liquid seepage holes on a rectangular chassis, fixing baffles are respectively fixed on two adjacent sides of the chassis, a slideway is arranged in the middle of each baffle, a plurality of vertical baffle knife grooves are arranged on each baffle, a vertical slide plate capable of moving along the slideway is arranged on each slideway, a slide plate fixing device is arranged on the vertical slide plate, a plurality of bars perpendicular to it are arranged on each vertical slide plate, and a plurality of bar knife grooves corresponding to the baffle knife grooves on the opposite baffle are arranged on each bar. A pull-out liquid collection drawer is arranged at the bottom of the chassis. The present invention can fasten the sectional specimen on the chassis, and the sectional specimen can be well and regularly cut by the cutting knives on the baffle knife grooves and bar knife grooves for easy observation, thus improving the teaching effect. Although the above problems are solved, there are still the following problems:
[0004] The fixing and cutting device for sectional specimens can only fix specimens of the same or different sizes. When the specimen is too large, it cannot be used and does not have an adjustment function, making it inconvenient to use.
[0005] In Patent CN201610213972.8, a silicone suction cup, its preparation method, and a pendant including the silicone suction cup; the silicone suction cup comprises the following components: 60 - 105 parts of methyl vinyl silicone rubber; 20 - 50 parts of silica; 1 - 8 parts of hydroxy silicone oil; 2 - 10 parts of dimethyl silicone oil; 0.1 - 0.4 parts of mold release agent; 0.5 - 1.5 parts of vulcanizing agent; the preparation method comprises the following steps: 1) weighing raw materials according to parts by weight; 2) kneading and mixing; 3) adding powder; 4) cold rolling; 5) cooling; 6) evacuating and cooling; 7) open rolling and filtering; 8) rubber mixing; 9) primary vulcanization; 10) secondary vulcanization; a pendant according to the present invention comprises a silicone suction cup, a connecting part, and a cap; the silicone suction cup has the physical property of silicone molecule migration and penetration, and has natural physical adsorption to ceramics, glass, etc.; the pendant is adsorbed on the wall surface in a planar negative pressure manner, and the structure of the pendant can be changed in a detachable manner, which is suitable for use in different occasions. However, there are still the following problems:
[0006] During the preparation of the silicone suction cup, the raw materials need to be added separately according to a specific procedure, which makes it easy to forget the feeding situation during the preparation process, and it also consumes a lot of time, reducing the production efficiency. Summary of the Invention
[0007] The purpose of the present invention is to provide a soft tissue tumor specimen incision fixator to solve the problems raised in the above background technology.
[0008] To achieve the above purpose, the present invention provides the following technical solution: a soft tissue tumor specimen incision fixator, comprising a storage box, one end of the storage box is open, and an adjustable-height grid tray is arranged inside the storage box, a groove is arranged on the inner wall of the storage box, a connecting rod is vertically arranged inside the groove, the grid tray is provided with a connecting head at the groove, a round hole is arranged in the middle of the connecting head, the connecting head is sleeved on the surface of the connecting rod through the round hole and is slidably arranged relative to the connecting rod, and a fastening ring is arranged at the connection between the connecting head and the connecting rod;
[0009] A column is arranged on the upper surface of the storage box, an adjusting rod is rotatably connected to the surface of the column, and a suction cup is arranged at one end of the adjusting rod.
[0010] Preferably, a handle is arranged at the other end of the adjusting rod.
[0011] Preferably in any of the above solutions, the surface of the handle is provided with grooves for increasing the friction force during rotation.
[0012] Preferably in any of the above solutions, the surface of the column is provided with a slot hole, and the inner wall of the slot hole is provided with internal threads.
[0013] Preferably, in any of the above solutions, a male thread is provided on the surface of the adjusting rod for threaded connection with a female thread.
[0014] A method for preparing a suction cup includes the following steps in sequence:
[0015] S1: First, put the silica gel raw material and vulcanizing agent into a blender and stir. At this time, the temperature of the blender is 25°C, stir for 5 minutes, then increase the temperature at a rate of 2°C / min. During the temperature increase, successively add butyl acrylate, fluorinated wax, silicone oil and mold release agent. When the temperature rises to 35°C, stop heating and stir for 10 minutes. Finally, add alumina, raise the temperature to 40°C, stir for 30 minutes, then cool down to 20°C at a rate of 5°C / min, and let it stand for 1 - 2 hours to obtain a mixed material;
[0016] S2: Put the mixed material obtained in the above step into a kneader and perform closed - lid kneading and mixing under the condition that the temperature is 40 - 50°C;
[0017] S3: After the above step is completed, raise the temperature to 60 - 70°C, add silica white, and perform kneading and mixing;
[0018] S4: Then put the sample completed in the above step into a mixer. The temperature of the mixer is set to 80 - 90°C, then add nano - zinc oxide and nano - magnesium oxide for mixing. Mix for 25 - 35 minutes to obtain a shaped rubber compound, and then cool for 8 - 10 hours for standby;
[0019] S5: Put the rubber compound obtained in the above step into an open mill, introduce pure water, set the temperature of the open mill to 80 - 90°C, open - mill until the surface is smooth and in a roll shape, cool for 10 minutes, perform rolling and exhaust, and finally use an 80 - mesh and a 200 - mesh filter screen stacked for filtration to remove impurities and obtain a silica gel raw material;
[0020] S6: Put the silica gel raw material in the above step into a vulcanizer, set the temperature of the vulcanizer to 80 - 90°C, vulcanize for 10 minutes and then standby;
[0021] S7: Put the vulcanized silica gel raw material in the above step on a mold forming machine, set the upper mold temperature to 170 - 200°C, the lower mold temperature to 210 - 220°C, the machine table pressure to: 170 - 175T, and perform silica gel forming under the conditions that the in - mold time is 400 - 450s and the out - of - mold time is 35 - 50s to obtain a raw suction cup;
[0022] S8: After removing the burrs of the above raw suction cup, vulcanize it at 155 - 165°C for 1 - 1.5 hours and cool naturally to obtain a suction cup.
[0023] Preferably, in the step S1, each component includes the following parts by weight: 60-80 parts of silica gel raw material, 5-10 parts of vulcanizing agent, 1-5 parts of butyl acrylate, 1-5 parts of fluorinated wax, 20-40 parts of silicone oil, 1-5 parts of mold release agent, and 8-15 parts of alumina.
[0024] Preferably, in any of the above solutions, in the step S8, the suction cup needs to be detected, and the suction cup without cracks and pore defects on the surface is the finished suction cup.
[0025] Preferably, in any of the above solutions, in the step S1, 20-25 parts of polycaprolactone are further included.
[0026] Technical effects and advantages of the present invention: The soft tissue tumor specimen incision fixator is provided with a liftable grid tray, and the suction cup can be adjusted under the action of the adjusting rod, so as to be applicable to soft tissue tumor specimens of different sizes and is convenient to use;
[0027] The preparation method of the suction cup provided by the present invention first mixes the raw materials that can be mixed to obtain a mixed material, which can avoid forgetting to add materials during the production process on the one hand, and improve the production efficiency and save time on the other hand. BRIEF DESCRIPTION OF THE DRAWINGS
[0028] Figure 1 is a schematic structural diagram of the present invention;
[0029] Figure 2 is a schematic structural diagram of the connection between the suction cup and the adjusting rod of the present invention;
[0030] Figure 3 is a schematic structural diagram of the grid tray of the present invention;
[0031] Figure 4 is a schematic enlarged structural diagram of part A of the present invention;
[0032] Figure 5 is a schematic enlarged structural diagram of part B of the present invention.
[0033] In the figure: 1, storage box; 2, grid tray; 3, groove; 4, suction cup; 5, adjusting rod; 6, column; 7, connecting rod; 8, connecting head; 9, fastening ring; 10, round hole; 11, handle. DETAILED DESCRIPTION OF THE INVENTION
[0034] The following further describes the specific embodiments of the present invention with reference to the drawings. It should be noted here that the description of these embodiments is for helping to understand the present invention, but does not constitute a limitation to the present invention. In addition, the technical features involved in the various embodiments of the present invention described below can be combined with each other as long as they do not conflict with each other.
[0035] In the description of the present invention, it should be understood that the orientation or positional relationship indicated by the terms "center", "longitudinal", "transverse", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise", "axial", "radial", "circumferential", etc. is based on the orientation or positional relationship shown in the drawings. It is only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a specific orientation, be constructed and operated in a specific orientation, and therefore should not be construed as a limitation to the present invention.
[0036] In addition, the terms "first" and "second" are only used for descriptive purposes and should not be construed as indicating or implying relative importance or implicitly specifying the quantity of the indicated technical features. Thus, the features defined with "first" and "second" may explicitly or implicitly include at least one of such features. In the description of the present invention, the meaning of "a plurality" is at least two, such as two, three, etc., unless otherwise specifically defined.
[0037] The present invention provides a soft tissue tumor specimen incision fixator as shown in Figures 1-5 Figure 8, which includes a storage box 1. One end of the storage box 1 is open, and an adjustable-height grid tray 2 is arranged inside the storage box 1. A groove 3 is arranged on the inner wall of the storage box 1. A connecting rod 7 is vertically arranged inside the groove 3. The grid tray 2 is provided with a connecting head 8 at the position of the groove 3. A round hole 10 is arranged in the middle of the connecting head 8. The connecting head 8 is sleeved on the surface of the connecting rod 7 through the round hole 10 and is slidably arranged relative to the connecting rod 7. A fastening ring 9 is arranged at the connection between the connecting head 8 and the connecting rod 7;
[0038] Vertical columns 6 are arranged on the upper surface of the storage box 1. There are 4 vertical columns 6, which are respectively distributed in the middle of the four sides of the storage box 1. An adjusting rod 5 is rotatably connected to the surface of the vertical column 6. A suction cup 4 is arranged at one end of the adjusting rod 5.
[0039] Specifically, a handle 11 is arranged at the other end of the adjusting rod 5.
[0040] Specifically, the surface of the handle 11 is provided with grooves for increasing the friction force during rotation.
[0041] Specifically, the surface of the vertical column 6 is provided with a slot hole, and the inner wall of the slot hole is provided with internal threads.
[0042] Specifically, the surface of the adjusting rod 5 is provided with external threads for threaded connection with the internal threads.
[0043] During the use of the soft tissue tumor specimen incision fixator, first place the soft tissue tumor specimen to be incised on the grid tray 2. Then, according to the size of the soft tissue tumor specimen, press down or pull up the grid tray 2 to adjust the position of the soft tissue tumor specimen so that the suction cup 4 can accurately clamp its middle part. Since the fastening ring 9 is provided on the connecting head 8, the connection between the fastening ring 9 and the connecting rod 7 is tight, and it requires manual pushing to move the grid tray 2. The force during normal cutting will not cause the grid tray 2 to move. Then rotate the adjusting rods 5 in four directions. The notch on the handle 11 facilitates the application of force by hand, enabling the suction cup 4 to fix the soft tissue tumor specimen in the middle, facilitating cutting. The suction cup 4 is small, but has a good fixing effect, and the connection between the suction cup 4 and the adjusting rod 5 is also fixed by the suction cup, facilitating the replacement of suction cups 4 of different models and sizes. The distance between the grids of the grid tray 2 is set, and the long diameter and transverse diameter of the specimen can be directly read after the specimen is fixed, which is convenient for use.
[0044] Example 1:
[0045] The present invention provides a method for preparing a suction cup, which includes the following steps in sequence:
[0046] S1: First, put the silicone raw material and vulcanizing agent into a blender and stir. At this time, the temperature of the blender is 25°C, stir for 5 minutes, and then increase the temperature at a rate of 2°C / min. During the temperature increase, successively add butyl acrylate, fluorinated wax, silicone oil, and mold release agent. When the temperature rises to 35°C, stop heating and stir for 10 minutes. Finally, add alumina, raise the temperature to 40°C, stir for 30 minutes, and then cool at a rate of 5°C / min to 20°C, and let it stand for 1-2 hours to obtain a mixed material;
[0047] S2: Put the mixed material obtained in the above step into a kneader and perform closed-cap kneading and mixing under the condition of a temperature of 40-50°C;
[0048] S3: After the above step is completed, raise the temperature to 60-70°C, add silica to it, and perform kneading and mixing;
[0049] S4: Then put the sample completed in the above step into a mixer. The temperature of the mixer is set to 80-90°C, and then add nano-zinc oxide and nano-magnesium oxide to it for mixing. Mix for 25-35 minutes to obtain a formed rubber compound, and then cool for 8-10 hours for standby;
[0050] S5: Put the rubber compound obtained in the above step into an open mill, pass in pure water, set the temperature of the open mill to 80-90°C, open mill until the surface is smooth and in a roll shape, cool for 10 minutes, perform rolling and exhaust, and finally use 80-mesh and 200-mesh filter screens stacked for filtration to remove impurities and obtain the silicone raw material;
[0051] S6: Put the silicone raw material in the above steps into a vulcanizer, set the temperature of the vulcanizer to 80 - 90 °C, and keep it for 10 minutes for standby after vulcanization;
[0052] S7: Put the vulcanized silicone raw material in the above steps on a mold forming machine, and carry out silicone molding under the conditions that the upper mold temperature is 170 - 200 °C, the lower mold temperature is 210 - 220 °C, the machine pressure is 170 - 175 T, the time inside the forming mold is 400 - 450 s, and the time outside the mold is 35 - 50 s to obtain the original suction cup;
[0053] S8: After removing the burrs of the above original suction cup, vulcanize it for 1 - 1.5 h under the condition of 155 - 165 °C, and cool it naturally to obtain the suction cup.
[0054] Specifically, in step S1, each component includes by weight: 60 parts of silicone raw material, 5 parts of vulcanizing agent, 1 part of butyl acrylate, 1 part of fluorinated wax, 20 parts of silicone oil, 1 part of mold release agent, and 8 parts of alumina.
[0055] Specifically, step S8 requires detecting the suction cup. If there are no cracks and pore defects on the surface of the suction cup, it is a finished suction cup.
[0056] Specifically, step S1 also includes 20 parts of polycaprolactone.
[0057] Example 2:
[0058] The present invention provides a method for preparing a suction cup, which includes the following steps in sequence:
[0059] S1: First, put the silicone raw material and the vulcanizing agent into a blender and stir. At this time, the temperature of the blender is 25 °C, stir for 5 minutes, then increase the temperature at a rate of 2 °C / min. During the temperature increase, successively add butyl acrylate, fluorinated wax, silicone oil, and mold release agent to it. When the temperature rises to 35 °C, stop increasing the temperature and stir for 10 minutes. Finally, add alumina, raise the temperature to 40 °C, stir for 30 minutes, and then cool it at a rate of 5 °C / min to 20 °C, and let it stand for 1 - 2 h to obtain a mixed material;
[0060] S2: Put the mixed material obtained in the above steps into a kneader and carry out closed - lid kneading and mixing under the condition of a temperature of 40 - 50 °C;
[0061] S3: After the above steps are completed, raise the temperature to 60 - 70 °C, add silica to it, and carry out kneading and mixing;
[0062] S4: Then put the sample completed in the above steps into a mixer. Set the temperature of the mixer at 80 - 90 °C, then add nano-zinc oxide and nano-magnesium oxide into it for mixing. Mix for 25 - 35 minutes to obtain the formed rubber compound, and then cool it for 8 - 10 hours for standby;
[0063] S5: Put the rubber compound obtained in the above steps into an open mill, pass in pure water, set the temperature of the open mill at 80 - 90 °C, mill until the surface is smooth and in a roll shape, cool for 10 minutes, conduct rolling and degassing, and finally use a superposition of 80 - mesh and 200 - mesh filters for filtration to remove impurities and obtain the silicone raw material;
[0064] S6: Put the silicone raw material in the above steps into a vulcanizer, set the temperature of the vulcanizer at 80 - 90 °C, and keep it for standby after vulcanizing for 10 min;
[0065] S7: Put the vulcanized silicone raw material in the above steps on a mold forming machine, and conduct silicone molding under the conditions that the upper mold temperature is 170 - 200 °C, the lower mold temperature is 210 - 220 °C, the machine pressure is: 170 - 175 T, the time inside the forming mold is 400 - 450 s, and the time outside the mold is 35 - 50 s to obtain the original suction cup;
[0066] S8: After removing the burrs of the above original suction cup, vulcanize it at 155 - 165 °C for 1 - 1.5 h and cool it naturally to obtain the suction cup.
[0067] Specifically, each component in step S1 includes by weight: 70 parts of silicone raw material, 7 parts of vulcanizing agent, 3 parts of butyl acrylate, 3 parts of fluorinated wax, 30 parts of silicone oil, 3 parts of mold release agent, and 12 parts of alumina.
[0068] Specifically, step S8 requires detecting the suction cup. If there are no crack and pore defects on the surface of the suction cup, it is a finished suction cup.
[0069] Specifically, step S1 also includes 22 parts of polycaprolactone.
[0070] Example 3:
[0071] The present invention provides a method for preparing a suction cup, which includes the following steps in sequence:
[0072] S1: First, put the silicone raw material and the vulcanizing agent into a blender for stirring. At this time, the temperature of the blender is 25 °C, stir for 5 min, then increase the temperature at a rate of 2 °C / min. During the temperature increase process, sequentially add butyl acrylate, fluorinated wax, silicone oil and mold release agent into it. When the temperature rises to 35 °C, stop increasing the temperature and stir for 10 min. Finally, add alumina, raise the temperature to 40 °C, stir for 30 min, and then decrease the temperature at a rate of 5 °C / min to 20 °C, and let it stand for 1 - 2 h to obtain the mixed material;
[0073] S2: Feed the mixed material obtained in the above step into a kneader, and perform closed - cover kneading and mixing at a temperature of 40 - 50 °C;
[0074] S3: After the above step is completed, raise the temperature to 60 - 70 °C, add silica to it, and perform kneading and mixing;
[0075] S4: Then put the sample completed in the above step into a mixer, set the temperature of the mixer to 80 - 90 °C, then add nano - zinc oxide and nano - magnesium oxide to it for mixing, mix for 25 - 35 minutes to obtain the shaped rubber compound, and then cool for 8 - 10 hours for standby;
[0076] S5: Put the rubber compound obtained in the above step into an open mill, introduce pure water, set the temperature of the open mill to 80 - 90 °C, mill until the surface is smooth and in a roll shape, cool for 10 minutes, perform rolling and exhaust, and finally use an 80 - mesh and a 200 - mesh filter screen stacked for filtration to remove impurities to obtain the silica gel raw material;
[0077] S6: Put the silica gel raw material in the above step into a vulcanizer, set the temperature of the vulcanizer to 80 - 90 °C, and keep it for 10 min for standby;
[0078] S7: Put the vulcanized silica gel raw material in the above step on a mold forming machine, set the upper mold temperature to 170 - 200 °C, the lower mold temperature to 210 - 220 °C, the machine table pressure to: 170 - 175 T, and perform silica gel forming under the conditions that the time inside the forming mold is 400 - 450 s and the time outside the mold is 35 - 50 s to obtain the original suction cup;
[0079] S8: After removing the burrs from the above original suction cup, vulcanize it at 155 - 165 °C for 1 - 1.5 h, and cool naturally to obtain the suction cup.
[0080] Specifically, in step S1, each component includes by weight: 80 parts of silica gel raw material, 10 parts of vulcanizing agent, 5 parts of butyl acrylate, 5 parts of fluorinated wax, 40 parts of silicone oil, 5 parts of mold release agent, and 15 parts of alumina.
[0081] Specifically, step S8 requires detecting the suction cup. If there are no crack and pore defects on the surface of the suction cup, it is the finished suction cup.
[0082] Specifically, step S1 also includes 25 parts of polycaprolactone.
[0083] Although the embodiments of the present invention have been shown and described above, it can be understood that the above embodiments are exemplary and should not be construed as limiting the present invention. Those of ordinary skill in the art can make changes, modifications, substitutions, and variations to the above embodiments within the scope of the present invention.
Claims
1. A method for preparing a suction cup of a soft tissue tumor specimen incision fixator, characterized in that: Based on a soft tissue tumor specimen incision fixator, the soft tissue tumor specimen incision fixator includes a storage box (1), one end of the storage box (1) is open, and an adjustable-height grid tray (2) is arranged inside the storage box (1). A groove (3) is arranged on the inner wall of the storage box (1). A connecting rod (7) is vertically arranged inside the groove (3). The grid tray (2) is provided with a connecting head (8) at the position of the groove (3). A round hole (10) is arranged in the middle of the connecting head (8). The connecting head (8) is sleeved on the surface of the connecting rod (7) through the round hole (10) and is slidably arranged relative to the connecting rod (7). A fastening ring (9) is arranged at the connection between the connecting head (8) and the connecting rod (7); A column (6) is arranged on the upper surface of the storage box (1). An adjusting rod (5) rotatably connected to the column (6) is arranged on the surface of the column (6). A suction cup (4) is arranged at one end of the adjusting rod (5); A handle (11) is arranged at the other end of the adjusting rod (5); The surface of the handle (11) is provided with grooves for increasing the friction during rotation; The surface of the column (6) is provided with a slot hole, and the inner wall of the slot hole is provided with female threads; The surface of the adjusting rod (5) is provided with male threads for threaded connection with the female threads; The method for preparing the suction cup of the soft tissue tumor specimen incision fixator, in sequence includes the following steps: S1: First, put silicone raw materials and vulcanizing agents into a blender and stir. At this time, the temperature of the blender is 25°C, stir for 5 minutes, then increase the temperature at a rate of 2°C / min. During the temperature increase, successively add butyl acrylate, fluorinated wax, silicone oil and release agent. When the temperature rises to 35°C, stop heating and stir for 10 minutes. Finally, add alumina, raise the temperature to 40°C, stir for 30 minutes, and then cool at a rate of 5°C / min to 20°C, and let it stand for 1-2 hours to obtain a mixed material; S2: Put the mixed material obtained in the above step into a kneader and perform closed-cap kneading and mixing at a temperature of 40-50°C; S3: After the above step is completed, raise the temperature to 60-70°C, add white carbon black to it, and perform kneading and mixing; S4: Then put the sample completed in the above step into a mixer. The temperature of the mixer is set at 80-90°C, and then add nano-zinc oxide and nano-magnesium oxide to it for mixing. Mix for 25-35 minutes to obtain a formed rubber compound, and then cool for 8-10 hours for standby; S5: Put the rubber compound obtained in the above step into an open mill, introduce pure water, set the temperature of the open mill at 80-90°C, open mill until the surface is smooth and in a roll shape, cool for 10 minutes, perform rolling and exhaust, and finally use an 80-mesh and 200-mesh filter screen stacked for filtration to remove impurities to obtain silicone raw materials; S6: Put the silicone raw materials in the above step into a vulcanizer, set the temperature of the vulcanizer at 80-90°C, and vulcanize for 10 minutes for standby; S7: Put the vulcanized silicone raw material in the above steps on a mold forming machine, and set the upper mold temperature to 170 - 200 °C, the lower mold temperature to 210 - 220 °C, the machine pressure to 170 - 175 T, and the in-mold time to 400 - 450 s and the out-of-mold time to 35 - 50 s to carry out silicone molding to obtain the original suction cup. S8: After removing the burrs from the above original suction cup, vulcanize it at 155 - 165 °C for 1 - 1.5 h and cool it naturally to obtain the suction cup.
2. A method for preparing a suction cup of a soft tissue tumor specimen incision fixator according to claim 1, characterized in that: In the step S1, each component includes by weight: 60 - 80 parts of silicone raw material, 5 - 10 parts of vulcanizing agent, 1 - 5 parts of butyl acrylate, 1 - 5 parts of fluorinated wax, 20 - 40 parts of silicone oil, 1 - 5 parts of mold release agent, and 8 - 15 parts of alumina.
3. A method for preparing a suction cup of a soft tissue tumor specimen incision fixator according to claim 1, characterized in that: In the step S8, the suction cup needs to be detected, and the suction cup without cracks and pore defects on the surface is the finished suction cup.
4. A method for preparing a suction cup of a soft tissue tumor specimen incision fixator according to claim 1, characterized in that: In the step S1, it further includes 20 - 25 parts of polycaprolactone.
Citation Information
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