A phosphorus pentachloride feeding station
By designing the automated operation and nitrogen protection environment of the phosphorus pentachloride feeding station, the problems of easy damage to the equipment and toxic gas leakage during the phosphorus pentachloride feeding process were solved, and safe and efficient phosphorus pentachloride treatment was achieved.
Patent Information
- Application Number
- CN202111083427.9
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2021-09-16
- Publication Date
- 2025-10-10
- Estimated Expiration
- 2041-09-16
AI Technical Summary
In the prior art, during the phosphorus pentachloride feeding process, the corrosiveness of phosphorus pentachloride causes the device to be easily damaged, the risk of toxic gas leakage is high, and the operators are exposed to a dangerous environment.
A phosphorus pentachloride feeding station was designed, including a guide rail bracket, a waste bag collection room, an unpacking room, and a feeding room. An electric hoist and a self-locking hook are used for automated operation. A nitrogen-protected environment and a carbon steel frame are combined to reduce the contact between phosphorus pentachloride and air and avoid leakage.
The automated processing of phosphorus pentachloride packaging bags is achieved, which reduces the diffusion of toxic gases, protects the health of operators, and extends the service life of the device.
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Figure CN113650901B_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the field of toxic raw material feeding devices, in particular to a phosphorus pentachloride feeding station. Background Art
[0002] Phosphorus pentachloride is an important industrial raw material and one of the important raw materials for lithium battery electrolytes. Phosphorus pentachloride has strong toxicity and corrosiveness. If it is dispersed in the air, it will seriously pollute the environment and harm people's health. Therefore, the feeding of phosphorus pentachloride in industry is a technical problem. In the prior art, when phosphorus pentachloride is added, all the devices involved will be placed in a fully enclosed vacuum environment, relying on vacuum pipes, vacuum containers and pressure regulating valves to achieve. Although such operation can temporarily seal the toxic gas, due to the highly corrosive nature of phosphorus pentachloride, the number of devices contacted is large and the time is long, which is very easy to cause damage, and on the contrary easily causes the leakage of toxic gas. Summary of the Invention
[0003] To solve the above problems, the present invention provides the following technical solution: a phosphorus pentachloride feeding station, comprising a feeding station frame; the feeding station frame is divided into a guide rail bracket, a waste bag collection chamber, an unpacking chamber and a feeding chamber, the guide rail bracket is located at the top of the feeding station frame, and a baffle is provided on the bottom; the waste bag collection chamber, the feeding chamber and the unpacking chamber are interconnected and arranged in sequence from left to right directly below the guide rail bracket.
[0004] Preferably, a guide rail is fixed laterally on the top of the guide rail bracket, and a movable groove parallel to the guide rail is provided at the baffle; it also includes an electric hoist and a bag hanging device, the electric hoist is installed on the guide rail, and the bag hanging device is connected to the electric hoist and is located below the movable groove.
[0005] Preferably, the bag hanging device has four bag hanging brackets, and each bag hanging bracket end is connected to a self-locking hook; the self-locking hook includes a fixed block, a hook and a self-locking block, the fixed block is movably connected to the hook, and the self-locking block is movably connected to the hook.
[0006] Preferably, the upper end of the fixing block has a triangular protrusion, and a through slot is provided inside the fixing block, and a cylindrical limiting rod is connected between the through slots; one end of the hook is a triangular limiting block, an arc-shaped slot is provided near the limiting block, and the other end is a solid hook tail; the upper half of the self-locking block also has the through slot, the limiting rod is connected between the through slots, the lower half is solid, and a self-locking slot is provided at the bottom.
[0007] Preferably, a discharge port is provided inside the feeding chamber, an outer closed room is formed below the discharge port by the baffle, a vibration bucket is fixed in the outer closed room, and a nitrogen room is provided below the vibration bucket; an iris valve and a partition valve are also included, and the iris valve and the partition valve are respectively fixed to the lower end of the vibration bucket and the upper end of the nitrogen room.
[0008] Preferably, the nitrogen room has a discharge pipe at the bottom, a glove operation port at the side, and two opposite bag pressing cylinders at the inner side of the top; it also includes a material cut-off ball valve and a bag beating device, the material cut-off ball valve is connected to the bottom end of the discharge pipe, and the bag beating device is dispersedly arranged above the discharge port.
[0009] Preferably, a waste bag collecting frame is placed at the bottom of the waste bag collecting chamber, and a liftable pressure plate is provided on the side.
[0010] Preferably, the feeding station frame is a carbon steel frame, and the baffles are arranged around it.
[0011] Preferably, the baffle is made of PE board.
[0012] Preferably, the waste bag collection chamber and the bottom of the unpacking chamber are both provided with automatic doors.
[0013] Compared with the prior art, the present invention has the following beneficial effects:
[0014] 1. Delaying the unpacking time of phosphorus pentachloride bags reduces the time that phosphorus pentachloride comes into contact with air and reduces the space where phosphorus pentachloride is exposed, thus solving the problem of toxic gas diffusion from the root.
[0015] 2. The hooking of the phosphorus pentachloride packaging bag and the final packaging bag recovery can be operated automatically without manual contact, thus avoiding exposure of phosphorus pentachloride to the environment where the operator is located.
[0016] 3. The bag unpacking and unloading space is a fully nitrogen-protected environment, effectively preventing the material from coming into contact with air.
[0017] 4. It adopts carbon steel frame and is enclosed with non-metallic plates inside, which is suitable for high corrosion environment. BRIEF DESCRIPTION OF THE DRAWINGS
[0018] Figure 1 It is the overall structural diagram of the present invention;
[0019] Figure 2 Schematic diagram of the internal structure of the present invention;
[0020] Figure 3 It is an enlarged view of the feeding chamber of the present invention;
[0021] Figure 4 It is a partial cross-sectional view of the feeding chamber of the present invention;
[0022] Figure 5 This is a diagram showing the locking state of the self-locking hook of the present invention;
[0023] Figure 6 This is a diagram of the natural state of the self-locking hook of the present invention;
[0024] In the figure: 1 feeding station frame, 2 guide rail bracket, 3 waste bag collection chamber, 4 unpacking chamber, 5 feeding chamber, 6 baffle, 7 guide rail, 8 movable groove, 9 electric hoist, 10 bag hanging device, 11 bag hanging bracket, 12 self-locking hook, 13 fixed block, 1301 protrusion, 1302 through-notch, 14 hook, 1401 limit block, 1402 arc-shaped notch, 1403 hook tail, 15 self-locking block, 1501 self-locking groove, 16 limit rod, 17 unloading port, 18 external closed room, 19 vibration bucket, 20 nitrogen room, 21 iris valve, 22 isolation valve, 23 discharge pipe, 24 glove operation port, 25 bag pressing cylinder, 26 material cut-off ball valve, 27 bag patting device, 28 waste bag collection frame, 29 pressure plate, 30 automatic door. DETAILED DESCRIPTION
[0025] The following will clearly and completely describe the technical solutions in the embodiments of the present invention in conjunction with the accompanying drawings. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative efforts are within the scope of protection of the present invention.
[0026] Reference Figure 1-6 A phosphorus pentachloride feeding station includes a feeding station frame 1; the feeding station frame 1 is divided into a guide rail bracket 2, a waste bag collection chamber 3, an unpacking chamber 4 and a feeding chamber 5, the guide rail bracket 2 is located at the top of the feeding station frame 1, and a baffle 6 is provided on the bottom; the waste bag collection chamber 3, the feeding chamber 5 and the unpacking chamber 4 are interconnected, and are arranged in sequence from left to right directly below the guide rail bracket 2.
[0027] A guide rail 7 is laterally fixed to the top of the guide rail bracket 2, and a movable groove 8 parallel to the guide rail 7 is formed on the baffle 6. The system also includes an electric hoist 9 and a bag hanging device 10. The electric hoist 9 is installed on the guide rail 7, and the bag hanging device 10 is connected to the electric hoist 9 and is located below the movable groove 8. Since the waste bag collection chamber 3, the unpacking chamber 4 and the feeding chamber 5 are connected, the electric hoist 9 can drive the bag hanging device 10 to move freely among the three chambers, thereby driving the phosphorus pentachloride packaging bags to the required workstation.
[0028] In order to reduce manual operation and realize the automation of bag hanging and bag removal, and at the same time reduce the automation cost, the bag hanging device 10 has four bag hanging brackets 11 to maintain balance, and each of the bag hanging brackets 11 is connected to a self-locking hook 12 at the end thereof for hooking the bottom of the phosphorus pentachloride bag to facilitate subsequent unbundling and feeding; the self-locking hook 12 includes a fixed block 13, a hook 14 and a self-locking block 15, the fixed block 13 is movably connected to the hook 14, and the self-locking block 15 is movably connected to the hook 14; the upper end of the fixed block 13 has a triangular protrusion 1301, and the interior of the fixed block 13 is provided with a through slot 1302, the through slot A cylindrical limiting rod 16 is connected between 1302; one end of the hook 14 is a triangular limiting block 1401, an arc-shaped notch 1402 is provided near the limiting block 1401, and the other end is a solid hook tail 1403; the upper part of the self-locking block 15 is also provided with the through-notch 1302, the limiting rod 16 is connected between the through-notch 1302, the lower part is solid, and a self-locking groove 1501 is provided at the bottom; the limiting rod 16 inside the fixed block 13 passes through the arc-shaped notch 1402 of the hook 14, so that the hook 14 can slide back and forth, and the limiting rod 16 inside the self-locking block 15 passes through the triangular limiting block 1401, so that the self-locking block 15 can rotate.
[0029] The working principle of the self-locking hook 12 is as follows: when the self-locking hook 12 is in an unused state, the heavier self-locking block 15 drives the limit block 1401 to fall together. At this time, the hook tail 1403 at the other end of the hook 14 immediately rises. By simply lowering the self-locking hook 12 as a whole, the hook tail 1403 can be easily inserted into the bag ring at the bottom of the phosphorus pentachloride packaging bag specifically provided for feeding. At this time, the bag hanging device 10 rises, and the weight borne by the hook tail 1403 exceeds the weight of the self-locking block 15. Therefore, the hook tail 1403 falls, and the limit rod 16 at the fixed block 13 moves forward and slides toward the end of the through-notch 1302 near the limit block 1401. At the same time, the self-locking block 15 begins to rotate under the action of gravity, and the self-locking groove 1501 at the bottom contacts the hook tail 1403, achieving a closed and locked state. When the packaging bag needs to be removed from the self-locking hook 12, the hook tail 1403 is pressed down to contact an object, and the limiting rod 16 on the fixed block 13 is moved back to the end of the through-notch 1302 closer to the hook tail 1403. The triangular protrusion 1301 on the upper end of the fixed block 13 prevents the self-locking block 15 from becoming rigid and rotating. When the self-locking block 15 is at an angle greater than 45° to the horizontal, the protrusion 1301 pushes it downward, helping it to fall back and close.
[0030] The feeding chamber 5 is provided with a discharge port 17 inside. Below the discharge port 17, an outer sealed room 18 is formed by the baffle 6. A vibrating hopper 19 is fixed in the outer sealed room 18, and a nitrogen room 20 is provided below the vibrating hopper 19. The chamber also includes an iris valve 21 and a shutoff valve 22, which are respectively fixed to the lower end of the vibrating hopper 19 and the upper end of the nitrogen room 20. A discharge pipe 23 is connected to the bottom of the nitrogen room 20, a glove operation port 24 is provided on the side, and two opposing bag pressing cylinders 25 are provided on the inner side of the top. The chamber also includes a material cut-off ball valve 26 and a bag-beating device 27. The material cut-off ball valve 26 is connected to the bottom end of the discharge pipe 23 to facilitate controlling the direction of the material by opening or closing the material cut-off ball valve 26. The bag-beating device 27 is dispersed above the discharge port 17. A waste bag collecting frame 28 is placed at the bottom of the waste bag collecting chamber 3, and a liftable pressure plate 29 is provided on the side.
[0031] When the bag hanging device 10 brings the phosphorus pentachloride packaging bag to the feeding chamber 5, the phosphorus pentachloride packaging bag is still in an upside-down state, with the bag opening at the lower end tied tightly. At this time, the packaging bag slowly descends, passes through the discharge port 17 used for positioning, and contacts the vibrating bucket 19. The vibrating bucket 19 is equipped with a weighing sensor. After sensing the weight of the material, it stops descending. The iris valve 21 at the lower end of the vibrating bucket 19 and the isolation valve 22 at the upper end of the nitrogen room 20 are opened at the same time, so that the bag opening is inside the nitrogen room 20. At this time, the operator puts the bag opening onto the pipe openings of the loading and unloading pipes 23 through the glove operation port 24 sealed by the rubber glove, and presses the belts on both sides. The cylinder 25 pushes forward to tighten, and at the same time unties the bag opening and replaces the nitrogen from the outside through the vent and outlet below the nitrogen room 20. After completion, the pressing cylinder 25 withdraws the system to start unloading. During this process, the vibrating bucket 19 will vibrate to help unload the material, and the bag-beating devices 27 around it will also push and squeeze the packaging bag to help empty it. When the weighing sensor detects that the material has been emptied, the system will prompt the operator to tie the bag opening, and the bag hanging device 10 will bring the packaging bag to the waste bag collection chamber 3, press down on the waste bag collection frame 28 to achieve automatic unhooking, and the pressure plate 29 on the side will compact the waste bag, and the feeding is completed.
[0032] In order to improve the corrosion resistance of the entire device and extend its service life, the feeding station frame 1 is made of carbon steel frame and is surrounded by baffles 6. The baffles 6 are made of PE plates.
[0033] In order to close the device in time, automatic doors 30 are provided at the bottom of the waste bag collecting chamber 3 and the unpacking chamber 4 .
[0034] While embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions, and variations may be made to these embodiments without departing from the principles and spirit of the invention, and that the scope of the invention is defined by the appended claims and their equivalents.
Claims
1. A phosphorus pentachloride feeding station, comprising a feeding station frame (1); characterized in that: The feeding station frame (1) is divided into a guide rail bracket (2), a waste bag collection chamber (3), an unpacking chamber (4) and a feeding chamber (5); the guide rail bracket (2) is located at the top of the feeding station frame (1), and a baffle (6) is provided on the bottom surface; the waste bag collection chamber (3), the feeding chamber (5) and the unpacking chamber (4) are interconnected and arranged in sequence from left to right directly below the guide rail bracket (2); a guide rail (7) is fixed transversely to the top of the guide rail bracket (2), and a movable groove (8) parallel to the guide rail (7) is provided at the baffle (6); an electric hoist (9) and a bag hanging device (10) are also included, and the electric hoist (9) is installed on the guide rail (7). The bag hanging device (10) is connected to the electric hoist (9) and is located below the movable groove (8); the bag hanging device (10) has four bag hanging brackets (11), and each of the bag hanging brackets (11) is connected to a self-locking hook (12) at the end; the self-locking hook (12) includes a fixed block (13), a hook (14) and a self-locking block (15), the fixed block (13) is movably connected to the hook (14), and the self-locking block (15) is movably connected to the hook (14); the upper end of the fixed block (13) has a triangular protrusion (1301), and the interior of the fixed block (13) is provided with a through slot (1302), and the through slot (1302) ) are connected with a cylindrical limiting rod (16); one end of the hook (14) is a triangular limiting block (1401), and an arc-shaped notch (1402) is provided near the limiting block (1401), and the other end is a solid hook tail (1403); the upper half of the self-locking block (15) is also provided with the through notch (1302), the limiting rod (16) is connected between the through notch (1302), the lower half is solid, and a self-locking groove (1501) is provided at the bottom; a discharge port (17) is provided inside the feeding chamber (5), and an outer closed room (18) is formed below the discharge port (17) by the baffle (6), and a vibration A dynamic bucket (19), a nitrogen room (20) is provided below the vibration bucket (19); an iris valve (21) and a shutoff valve (22), the iris valve (21) and the shutoff valve (22) being fixed to the lower end of the vibration bucket (19) and the upper end of the nitrogen room (20), respectively; a discharge pipe (23) is introduced into the bottom of the nitrogen room (20), a glove operation port (24) is provided on the side, and two opposite bag pressing cylinders (25) are provided on the inner side of the top; a material cutting ball valve (26) and a bag beating device (27) are also provided, the material cutting ball valve (26) is connected to the bottom end of the discharge pipe (23), and the bag beating device (27) is dispersedly provided above the discharge port (17).
2. The phosphorus pentachloride feeding station according to claim 1, wherein: A waste bag collection frame (28) is placed at the bottom of the waste bag collection chamber (3), and a liftable pressure plate (29) is provided on the side.
3. The phosphorus pentachloride feeding station according to claim 1, wherein: The feeding station frame (1) is a carbon steel frame, and the baffles (6) are arranged around it.
4. The phosphorus pentachloride feeding station according to claim 3, wherein: The baffle (6) is made of PE board.
5. The phosphorus pentachloride feeding station according to claim 1, wherein: Automatic doors (30) are provided at the bottoms of the waste bag collection chamber (3) and the unpacking chamber (4).
Citation Information
Patent Citations
Ton bag opening and feeding station
CN113264250A
Phosphorus pentachloride feeding station
CN215623268U
Automatic hook
JP1996277086A