An optimized design of a butyl rubber granule water conveying system
By optimizing the granule water conveying system of the butyl rubber production unit, and by adopting a closed impeller pump and specific parameter design, the problem of unstable granule water circulation was solved, thus achieving stable operation of the unit and improved product quality.
Patent Information
- Application Number
- CN202210734550.0
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2022-06-27
- Publication Date
- 2025-12-02
- Estimated Expiration
- 2042-06-27
AI Technical Summary
In existing butyl rubber production facilities, the instability and frequent blockages caused by the reliance on pumps for rubber particle water circulation affect production continuity and capacity.
The colloidal water delivery system is optimized by using a closed-loop impeller pump. Through specific equipment connection sequence and parameter design, including improvements to the impeller and pump casing of the closed-loop impeller pump, the risk of clogging is reduced and the stable operation time of the system is extended.
This reduced the frequency of production and shutdowns caused by pump blockages, extended the stable operation time of the equipment, and improved the product qualification rate.
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Figure CN115143118B_ABST
Abstract
Description
Technical Field
[0001] This invention belongs to the technical field of butyl rubber preparation equipment, and relates to a granule water conveying system in a butyl rubber production device, and more particularly to an optimized design of a granule water conveying system for a butyl rubber device. Background Technology
[0002] In butyl rubber plants, the granule water plays a crucial role as the carrier for the movement of granules throughout the entire production process. As a carrier, the granule water receives granules in the polymerization unit and is then pumped to the halogenation unit, where the granules are released. The filtered water is then pumped back to the polymerization unit to collect granules again, forming a complete cycle.
[0003] In actual operation, the smoothness of the colloidal water circulation becomes a crucial factor restricting production. The existing colloidal water circulation system relies entirely on pumps for power; if the pumps malfunction, the colloidal water circulation will be terminated. This disrupts the circulation system, forcing a production shutdown and severely limiting the plant's capacity.
[0004] Therefore, finding a suitable way to solve the problems existing in the current butyl rubber production process and ensure the stable operation of the production process has become one of the urgent problems to be solved by many front-line researchers in this field. Summary of the Invention
[0005] In view of this, the technical problem to be solved by the present invention is to provide a granule water conveying system in a butyl rubber production unit, and more particularly, an optimized design of a granule water conveying system for a butyl rubber unit. The present invention further optimizes the conveying of granule water, avoiding production stoppages due to pump blockage, thus preventing disruption to the stable operation of the unit, reducing the frequency of pump blockages, and laying a foundation for extending the reaction cycle.
[0006] This invention provides a granule water conveying system in a butyl rubber production apparatus, wherein the conveying system is connected between the polymerization unit and the halogenation unit of butyl rubber;
[0007] The conveying system includes:
[0008] Flash tank of the polymerization unit;
[0009] A first colloidal water impeller pump connected to the liquid phase outlet pipeline of the flash tank;
[0010] The stripping tower of the polymerization unit connected to the outlet of the first colloid pump;
[0011] A second colloidal water impeller pump connected to the liquid phase outlet pipeline of the stripping tower;
[0012] A halogenation unit connected to the outlet of the second colloidal water pump;
[0013] A third colloidal water impeller pump is connected to the filtered process water outlet pipeline of the halogenation unit.
[0014] The polymerization unit is connected to the outlet of the third granule water pump;
[0015] The first and second colloid water impeller pumps are closed impeller pumps.
[0016] Preferably, the impeller of the closed-loop impeller pump is a rear-mounted impeller;
[0017] The volute height radius of the closed impeller pump is 245mm;
[0018] The volute width of the closed impeller pump is 175mm.
[0019] Preferably, the clearance between the impeller and the pump casing of the closed-loop impeller pump is 1.5 mm;
[0020] The closed impeller pump is equipped with an impeller sealing ring at the impeller inlet end;
[0021] The closed impeller pump is equipped with a pump body sealing ring at the impeller inlet end.
[0022] Preferably, the halogenation unit includes a first storage tank, a first medium transfer pump, a second storage tank, a second medium transfer pump, and a third storage tank connected in sequence.
[0023] The filtered process water outlet pipeline after the third storage tank of the halogenation unit is connected to the third colloidal water impeller pump.
[0024] The first medium transfer pump and / or the second medium transfer pump are closed impeller pumps.
[0025] This invention also provides a process for transporting butyl rubber particles in water, comprising the following steps:
[0026] 1) The colloidal water from the flash tank of the polymerization unit is transported to the stripping tower of the polymerization unit via the first colloidal water impeller pump;
[0027] 2) The butyl rubber granule water from the stripping tower is transported to the halogenation unit via the second granule water impeller pump;
[0028] 3) The filtered process water obtained after treatment in the halogenation unit is returned to the polymerization unit via the third colloidal water impeller pump.
[0029] The first and second colloid water impeller pumps are closed impeller pumps.
[0030] Preferably, in step 1), the conveying flow rate is 130-150 T / h;
[0031] In step 1), the conveying temperature is 68–74°C;
[0032] In step 1), the dwell time of the conveying is 40 to 60 minutes;
[0033] In step 1), the colloidal content of the colloidal water is 4% to 6%.
[0034] Preferably, in step 2), the conveying flow rate is 130-150 T / h;
[0035] In step 2), the conveying temperature is 68–74°C;
[0036] In step 2), the dwell time of the conveying is 40 to 60 minutes;
[0037] In step 2), the colloidal content of the colloidal water is 4% to 6%.
[0038] Preferably, the halogenation unit includes a first storage tank, a second storage tank, and a third storage tank arranged sequentially;
[0039] The first storage tank and the second storage tank are connected by a first medium transfer pump;
[0040] The first medium transfer pump includes a closed impeller pump;
[0041] The flow rate between the first and second storage tanks is 130-150 T / h;
[0042] The transport temperature between the first and second storage tanks is 68–74°C;
[0043] The transfer dwell time between the first storage tank and the second storage tank is 40 to 60 minutes;
[0044] The colloidal content of the water between the first and second storage tanks is 4% to 6%.
[0045] Preferably, the second storage tank and the third storage tank are connected by a second medium transfer pump;
[0046] The second medium transfer pump includes a closed-loop impeller pump;
[0047] The transfer flow rate between the second and third storage tanks is 130-140 T / h;
[0048] The transport temperature between the second and third storage tanks is 60–65°C;
[0049] The transfer dwell time between the second and third storage tanks is 60-70 minutes;
[0050] The colloidal content of the water between the second and third storage tanks is 4% to 6%.
[0051] Preferably, the filtered process water is obtained after the third storage tank;
[0052] The flow rate between the third storage tank and the polymerization unit is 130-140 T / h;
[0053] The conveying temperature between the third storage tank and the polymerization unit is 60-65℃;
[0054] The conveying and residence time between the third storage tank and the polymerization unit is 40-60 minutes;
[0055] The particle content of the process water between the third storage tank and the polymerization unit is 0.
[0056] This invention provides a granule water conveying system in a butyl rubber production apparatus. The conveying system connects the polymerization unit and the halogenation unit of the butyl rubber. The conveying system includes: a flash tank of the polymerization unit; a first granule water impeller pump connected to the liquid phase outlet pipeline of the flash tank; a stripping tower of the polymerization unit connected to the outlet of the first granule water pump; a second granule water impeller pump connected to the liquid phase outlet pipeline of the stripping tower; a halogenation unit connected to the outlet of the second granule water pump; a third granule water impeller pump connected to the filtered process water outlet pipeline of the halogenation unit; and a polymerization unit connected to the outlet of the third granule water pump. The first and second granule water impeller pumps are closed-loop impeller pumps. Compared with existing technologies, this invention argues that, based on the cationic polymerization reaction of butyl rubber, which requires a vigorous reaction at extremely low temperatures to generate the desired rubber, uneven granule size can occur when the reaction is unstable. Due to the small impeller clearance and high granule viscosity, large granules can cause pump blockage and reduced flow. These particles, due to pressure, will become larger and accumulate more within the pump chamber. This causes blockage in the water circulation, ultimately leading to a halt in the reaction and abnormal production.
[0057] Based on this, the present invention has specially designed a new colloidal water conveying system, which adopts a specific equipment connection sequence and a closed impeller pump designed with specific parameters. By setting the operating parameters of the entire conveying system, the conveying of colloidal water is optimized, avoiding equipment shutdowns and stoppages due to pump blockage, thus reducing the frequency of pump blockage and laying a good foundation for extending the reaction cycle.
[0058] Based on the actual working conditions and connection sequence of specific devices before and after, this invention adjusts and replaces the impeller form and pump body parameter design, optimizes the conveying form of granulated water, extends the stable operation cycle of the granulated water system, reduces the frequency of pump blockage and cleaning, and naturally reduces the risk of device shutdown caused by the cessation of granulated water circulation, thus extending the stable operation time of the device, reducing the output of defective granulated water, and improving the product qualification rate. Attached Figure Description
[0059] Figure 1 Equipment layout diagram showing the structure and dimensions of the closed impeller pump provided by the present invention;
[0060] Figure 2 This is a partial screenshot of the statistical ledger of all device anomaly analysis in 2020 provided by the present invention. Detailed Implementation
[0061] To further understand the present invention, preferred embodiments of the present invention are described below in conjunction with examples. However, it should be understood that these descriptions are only for further illustrating the features and advantages of the present invention and not for limiting the claims of the present invention.
[0062] There are no particular restrictions on the source of any raw materials used in this invention; they can be purchased from the market or prepared using conventional methods known to those skilled in the art.
[0063] There are no particular restrictions on the purity of any of the raw materials used in this invention. Preferably, industrial-grade pure or conventionally used purity in the production and preparation of butyl rubber is sufficient.
[0064] All terms and abbreviations used in this invention are conventional terms and abbreviations in the field. Each term and abbreviation is clear and distinct in its relevant application area, and those skilled in the art can understand it clearly, accurately, and uniquely based on the terms and abbreviations.
[0065] This invention provides a butyl rubber granule water conveying system, wherein the conveying system is connected between the polymerization unit and the halogenation unit of butyl rubber;
[0066] The conveying system includes:
[0067] Flash tank of the polymerization unit;
[0068] A first colloidal water impeller pump connected to the liquid phase outlet pipeline of the flash tank;
[0069] The stripping tower of the polymerization unit connected to the outlet of the first colloid pump;
[0070] A second colloidal water impeller pump connected to the liquid phase outlet pipeline of the stripping tower;
[0071] A halogenation unit connected to the outlet of the second colloidal water pump;
[0072] A third colloidal water impeller pump is connected to the filtered process water outlet pipeline of the halogenation unit.
[0073] The polymerization unit is connected to the outlet of the third granule water pump;
[0074] The first and second colloid water impeller pumps are closed impeller pumps.
[0075] In this invention, the impeller of the closed impeller pump is preferably a rear-mounted impeller.
[0076] In this invention, the volute height radius of the closed impeller pump is preferably 245 mm.
[0077] In this invention, the volute width of the closed impeller pump is preferably 175 mm.
[0078] In this invention, the clearance between the impeller and the pump casing of the closed impeller pump is preferably 1.5 mm.
[0079] In this invention, the impeller inlet end of the closed impeller pump is preferably provided with an impeller sealing ring.
[0080] In this invention, the impeller inlet end of the closed impeller pump is preferably provided with a pump body sealing ring.
[0081] See Figure 1 , Figure 1 The equipment layout diagram shows the structure and dimensions of the closed impeller pump provided by the present invention.
[0082] Depend on Figure 1 It can be seen that the closed impeller pump used in this invention has a larger volute height (245mm) and volute width (175mm), which increases the gap between the impeller and the volute. Combined with the overall system optimization design, it makes it easier for granules to pass through smoothly.
[0083] Furthermore, this invention employs a closed impeller with a maximum impeller clearance of 1.5mm. The impeller inlet end features both an impeller sealing ring and a pump body sealing ring. This structure can accommodate larger particles, allowing them to pass through smoothly. It reduces the squeezing force between the impeller and the volute, decreasing the likelihood of particles agglomerating and thus lowering the frequency of pump blockage.
[0084] The closed-loop impeller pump provided by this invention features an enlarged volute volume and a changed impeller design, resulting in looser, less caking granules after pump blockage. This facilitates cleaning after pump shutdown and allows for rapid removal of granules from the pump chamber. This reduces processing time and improves work efficiency.
[0085] In this invention, the halogenation unit preferably includes a first storage tank, a first medium transfer pump, a second storage tank, a second medium transfer pump, and a third storage tank connected in sequence.
[0086] In this invention, the filtered process water outlet pipeline after the third storage tank of the halogenation unit is preferably connected to the third colloidal water impeller pump.
[0087] In this invention, the first medium delivery pump and / or the second medium delivery pump are preferably closed impeller pumps, and more preferably both the first medium delivery pump and the second medium delivery pump are the aforementioned closed impeller pumps.
[0088] This invention provides a process for transporting butyl rubber particles to water, comprising the following steps:
[0089] 1) The colloidal water from the flash tank of the polymerization unit is transported to the stripping tower of the polymerization unit via the first colloidal water impeller pump;
[0090] 2) The butyl rubber granule water from the stripping tower is then transported to the halogenation unit via the second granule water impeller pump;
[0091] 3) The filtered process water obtained after treatment in the halogenation unit is returned to the polymerization unit via the third colloidal water impeller pump.
[0092] The first and second colloid water impeller pumps are closed impeller pumps.
[0093] The present invention first transports the colloidal water from the flash tank of the polymerization unit to the stripping tower of the polymerization unit via a first colloidal water impeller pump.
[0094] In this invention, in step 1), the conveying flow rate is preferably 130-150 T / h, more preferably 134-146 T / h, and even more preferably 138-142 T / h.
[0095] In this invention, in step 1), the conveying temperature is preferably 68-74°C, more preferably 69-73°C, and even more preferably 70-72°C.
[0096] In this invention, in step 1), the dwell time of the conveying is preferably 40-60 min, more preferably 44-56 min, and even more preferably 48-52 min.
[0097] In this invention, in step 1), the colloidal content of the colloidal water is preferably 4% to 6%, more preferably 4.4% to 5.6%, and even more preferably 4.8% to 5.2%.
[0098] The present invention further transports the butyl rubber granules water from the stripping tower to the halogenation unit via a second granule water impeller pump.
[0099] In this invention, in step 2), the conveying flow rate is preferably 130-150 T / h, more preferably 134-146 T / h, and even more preferably 138-142 T / h.
[0100] In this invention, in step 2), the conveying temperature is preferably 68-74°C, more preferably 69-73°C, and even more preferably 70-72°C.
[0101] In this invention, in step 2), the dwell time of the conveying is preferably 40-60 min, more preferably 44-56 min, and even more preferably 48-52 min.
[0102] In this invention, in step 2), the colloidal content of the colloidal water is preferably 4% to 6%, more preferably 4.4% to 5.6%, and even more preferably 4.8% to 5.2%.
[0103] Finally, the filtered process water obtained after halogenation unit treatment is returned to polymerization unit via a third colloidal water impeller pump.
[0104] In this invention, the first granular water impeller pump and the second granular water impeller pump are preferably closed impeller pumps.
[0105] In this invention, the halogenation unit preferably includes a first storage tank, a second storage tank, and a third storage tank arranged sequentially.
[0106] In this invention, the first storage tank and the second storage tank are preferably connected by a first medium transfer pump.
[0107] In this invention, the first medium delivery pump preferably includes the above-mentioned closed impeller pump.
[0108] In this invention, the preferred flow rate between the first storage tank and the second storage tank is 130-150 T / h, more preferably 134-146 T / h, and even more preferably 138-142 T / h.
[0109] In this invention, the preferred conveying temperature between the first storage tank and the second storage tank is 68-74°C, more preferably 69-73°C, and even more preferably 70-72°C.
[0110] In this invention, the preferred transport dwell time between the first storage tank and the second storage tank is 40-60 min, more preferably 44-56 min, and even more preferably 48-52 min.
[0111] In this invention, the colloidal content of the colloidal water between the first storage tank and the second storage tank is preferably 4% to 6%, more preferably 4.4% to 5.6%, and even more preferably 4.8% to 5.2%.
[0112] In this invention, the second storage tank and the third storage tank are preferably connected by a second medium transfer pump.
[0113] In this invention, the second medium delivery pump preferably includes a closed impeller pump.
[0114] In this invention, the preferred flow rate between the second and third storage tanks is 130-140 T / h, more preferably 132-138 T / h, and even more preferably 134-136 T / h.
[0115] In this invention, the conveying temperature between the second storage tank and the third storage tank is preferably 60-65°C, more preferably 61-64°C, and even more preferably 62-63°C.
[0116] In this invention, the preferred transport dwell time between the second and third storage tanks is 60-70 min, more preferably 62-68 min, and even more preferably 64-66 min.
[0117] In this invention, the colloidal content of the colloidal water between the second and third storage tanks is preferably 4% to 6%, more preferably 4.4% to 5.6%, and even more preferably 4.8% to 5.2%.
[0118] In this invention, filtered process water is obtained after the third storage tank. Specifically, the effluent from the third storage tank can be filtered to obtain filtered process water.
[0119] In this invention, the flow rate between the third storage tank and the polymerization unit is 130-140 T / h, more preferably 132-138 T / h, and even more preferably 134-136 T / h.
[0120] In this invention, the conveying temperature between the third storage tank and the polymerization unit is 60-65°C, more preferably 61-64°C, and even more preferably 62-63°C.
[0121] In this invention, the conveying dwell time between the third storage tank and the polymerization unit is 40-60 min, more preferably 44-56 min, and even more preferably 48-52 min.
[0122] In this invention, the particle content of the process water between the third storage tank and the polymerization unit is preferably 0.
[0123] The above steps of the present invention provide an optimized design for a butyl rubber granule water conveying system. This granule water conveying system adopts a specific equipment connection sequence and a closed impeller pump designed with specific parameters. By setting the operating parameters of the entire conveying system, the conveying of granule water is optimized, avoiding equipment shutdowns due to pump blockage, affecting the stable operation of the equipment, reducing the frequency of pump blockage, and laying a good foundation for extending the reaction cycle.
[0124] Based on the actual working conditions and connection sequence of specific devices before and after, this invention adjusts and replaces the impeller form and pump body parameter design, optimizes the conveying form of granulated water, extends the stable operation cycle of the granulated water system, reduces the frequency of pump blockage and cleaning, and naturally reduces the risk of device shutdown caused by the cessation of granulated water circulation, thus extending the stable operation time of the device, reducing the output of defective granulated water, and improving the product qualification rate.
[0125] To further illustrate the present invention, the following describes in detail a rubber granule water conveying system in a butyl rubber production apparatus provided by the present invention with reference to embodiments. However, it should be understood that these embodiments are implemented under the premise of the technical solution of the present invention, and provide detailed implementation methods and specific operating procedures. They are only for further illustrating the features and advantages of the present invention, and are not intended to limit the scope of the claims of the present invention. The scope of protection of the present invention is not limited to the following embodiments.
[0126] Example 1
[0127] Butyl rubber granule water conveying system in butyl rubber production plant:
[0128] Polymerization section: Flash tank V135 / 145 / 155, Stripping tower V148 / V160;
[0129] Halogenation section: T500, P500, T501, P501, T505, P505;
[0130] In this context, T represents the storage tank, i.e., T500 represents storage tank 500 and T501 represents storage tank 501.
[0131] P represents a pump, meaning P500 represents a medium transfer pump for storage tank 500.
[0132] The system process is as follows:
[0133] Flash evaporator V135 / 145 / 155 → Glue pump → Stripping tower V148 / V160 → Glue pump → T500 → P500 → T501 → P501 → T505 → P505 → Flash evaporator V135 / 145 / 155
[0134] Among them, the granule water pump, P500 and P501 are all closed impeller pumps.
[0135] The structure and dimensions of a closed impeller pump are as follows: Figure 1 As shown.
[0136] See Table 1, which shows the specific parameters of the rubber granule water conveying system in the butyl rubber production apparatus provided by the present invention.
[0137] Table 1
[0138] process flow temperature Duration of stay Pipeline Dimensions Particle content Flash tank to stripping tower 130-150T / h 68-74℃ 40-60min DN150 4%-6% Stripping tower to T500 130-150T / h 68-74℃ 40-60min DN150 4%-6% T500 to T501 130-150T / h 68-74℃ 60-70min DN150 4%-6% T501 to T505 130-140T / h 60-65℃ 60-70min DN150 4%-6% T505 to flash tank 130-140T / h 60-65℃ 40-60min DN150 0
[0139] The granule water conveying system provided by this invention in the production of butyl rubber was actually verified.
[0140] Before the optimized design of the conveyor system, the production system experienced a total of 22 anomalies in the first three quarters of 2020, 12 of which were due to pump blockage. After the optimization, the total number of anomalies in the fourth quarter (starting in October) was 10, with 2 of them being due to pump blockage. In the following year, 2021, only one pump blockage occurred. Furthermore, disassembly and inspection revealed that the rubber blocks inside the pump chamber were relatively loose, and the processing speed was significantly improved compared to before.
[0141] See Figure 2 , Figure 2 This is a partial screenshot of the statistical ledger of all device anomaly analysis in 2020 provided by the present invention.
[0142] It should be noted that cleaning a clogged pump takes approximately one hour. During this time, the produced adhesive will be classified as Grade B (normally Grade A; Grade A is supplied to large customers, and Grade B is supplied to smaller customers with less stringent requirements). This portion of adhesive will be separately marked and tested. If it passes the test, it will be classified as Grade B; otherwise, it will be classified as defective. This affects the product pass rate by approximately 0.5%, meaning the product pass rate can be improved by about 0.5%.
[0143] The above provides a detailed description of the optimized design of a butyl rubber granule water conveying system provided by the present invention. Specific examples have been used to illustrate the principles and implementation methods of the invention. The descriptions of these embodiments are merely for the purpose of helping to understand the method and core ideas of the present invention, including the best mode, and also to enable any person skilled in the art to practice the invention, including manufacturing and using any device or system, and implementing any combined method. It should be noted that for those skilled in the art, several improvements and modifications can be made to the invention without departing from the principles of the invention, and these improvements and modifications also fall within the protection scope of the claims. The scope of protection of this patent is defined by the claims and may include other embodiments that can be conceived by those skilled in the art. If these other embodiments have structural elements that are not different from the wording of the claims, or if they include equivalent structural elements that are not substantially different from the wording of the claims, then these other embodiments should also be included within the scope of the claims.
Claims
1. A process for conveying butyl rubber granules to water, characterized in that, Includes the following steps: 1) The colloidal water from the flash tank of the polymerization unit is transported to the stripping tower of the polymerization unit via the first colloidal water impeller pump; 2) The butyl rubber granule water from the stripping tower is transported to the halogenation unit via the second granule water impeller pump; 3) The filtered process water obtained after treatment in the halogenation unit is returned to the polymerization unit via the third colloidal water impeller pump; The first and second colloidal water impeller pumps are closed impeller pumps; In step 1), the conveying flow rate is 130~150T / h; In step 2), the conveying flow rate is 130~150T / h; The conveying process includes a granule water conveying system, which is connected between the polymerization unit and the halogenation unit of butyl rubber. The conveying system includes: Flash tank of the polymerization unit; A first colloidal water impeller pump connected to the liquid phase outlet pipeline of the flash tank; The stripping tower of the polymerization unit connected to the outlet of the first colloid pump; A second colloidal water impeller pump connected to the liquid phase outlet pipeline of the stripping tower; A halogenation unit connected to the outlet of the second colloidal water pump; A third colloidal water impeller pump is connected to the filtered process water outlet pipeline of the halogenation unit. The polymerization unit is connected to the outlet of the third granule water pump; The impeller of the closed-type impeller pump is a rear-mounted impeller; The clearance between the impeller and the pump casing of the closed-loop impeller pump is 1.5 mm. The closed impeller pump is equipped with an impeller sealing ring at the impeller inlet end; The closed impeller pump is equipped with a pump body sealing ring at the impeller inlet end; The volute height radius of the closed impeller pump is 245mm; The volute width of the closed impeller pump is 175mm; The halogenation unit includes a first storage tank, a first medium transfer pump, a second storage tank, a second medium transfer pump, and a third storage tank connected in sequence. The filtered process water outlet pipeline after the third storage tank of the halogenation unit is connected to the third colloidal water impeller pump. The first medium transfer pump and / or the second medium transfer pump are closed impeller pumps.
2. The colloidal water conveying process according to claim 1, characterized in that, In step 1), the conveying temperature is 68~74℃; In step 1), the dwell time of the conveying is 40~60 minutes; In step 1), the colloidal content of the colloidal water is 4%~6%.
3. The colloidal water conveying process according to claim 1, characterized in that, In step 2), the conveying temperature is 68~74℃; In step 2), the dwell time of the conveying is 40-60 minutes; In step 2), the colloidal content of the colloidal solution is 4% to 6%.
4. The colloidal water conveying process according to claim 3, characterized in that, The halogenation unit includes a first storage tank, a second storage tank, and a third storage tank arranged sequentially. The first storage tank and the second storage tank are connected by a first medium transfer pump; The first medium transfer pump includes a closed impeller pump; The flow rate between the first and second storage tanks is 130~150T / h; The transport temperature between the first and second storage tanks is 68~74℃; The transfer dwell time between the first storage tank and the second storage tank is 40~60 minutes; The colloidal content of the water between the first and second storage tanks is 4% to 6%.
5. The colloidal water conveying process according to claim 4, characterized in that, The second and third storage tanks are connected by a second medium transfer pump; The second medium transfer pump includes a closed-loop impeller pump; The flow rate between the second and third storage tanks is 130~140T / h; The transport temperature between the second and third storage tanks is 60~65℃; The transfer dwell time between the second and third storage tanks is 60-70 minutes; The colloidal content of the water between the second and third storage tanks is 4% to 6%.
6. The colloidal water conveying process according to claim 4, characterized in that, The filtered process water is obtained after the third storage tank; The flow rate between the third storage tank and the polymerization unit is 130~140T / h; The conveying temperature between the third storage tank and the polymerization unit is 60~65℃; The conveying and residence time between the third storage tank and the polymerization unit is 40-60 minutes; The particle content of the process water between the third storage tank and the polymerization unit is 0.
Citation Information
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