A high-purity aluminum fluoride condenser
By designing a high-purity aluminum fluoride condenser, the rotation motor drives the rotation of the condensation tube and the coordination of the push block, the problems of insufficient condensation and low efficiency are solved, efficient condensation and automatic discharge of aluminum fluoride crystals are achieved, and the overall condensation efficiency is improved.
Patent Information
- Application Number
- CN202211004828.5
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2022-08-22
- Publication Date
- 2025-08-29
- Estimated Expiration
- 2042-08-22
AI Technical Summary
In the prior art, high-purity aluminum fluoride is not sufficiently condensed and low condensation efficiency.
A high-purity aluminum fluoride condenser is designed. By setting a symmetrically distributed support plate, air pump, condenser tube and rotating motor in the condensation cylinder, the rotating motor is used to drive the condensation tube to rotate, and combined with the design of pushing blocks and elastic rubber ropes, the agitation of the condensed gas and the automatic discharge of crystals are achieved, and the condensation efficiency is improved.
Full condensation of high-purity aluminum fluoride is achieved, condensation efficiency is improved, and the automatic continuous discharge of aluminum fluoride crystals during the condensation process is achieved, improving working efficiency.
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Figure CN115371456B_ABST
Abstract
Description
Technical Field
[0001] The present invention relates to the field of aluminum fluoride production, and in particular to a high-purity aluminum fluoride condenser. Background Art
[0002] With the continuous development of science and technology, people's demand for aluminum is increasing. Aluminum fluoride is an important raw material for aluminum refining. Aluminum fluoride is an inorganic substance, colorless or white crystals, insoluble in water, insoluble in acid and alkali, and can sublime under high temperature conditions. It is mainly used for aluminum refining. High-purity aluminum fluoride can be obtained by heating an aluminum fluoride mixture to sublime the aluminum fluoride under high temperature conditions, and then condensing and crystallizing the high-temperature aluminum fluoride gas obtained by sublimation, thereby obtaining high-purity aluminum fluoride. However, in the existing technology, the condensation of high-purity aluminum fluoride has the problems of insufficient condensation and low condensation efficiency. Summary of the Invention
[0003] In view of the shortcomings of the prior art, the purpose of the present disclosure is to provide a high-purity aluminum fluoride condenser, which solves the problems of insufficient condensation of high-purity aluminum fluoride and low condensation efficiency in the prior art.
[0004] The purpose of this disclosure can be achieved through the following technical solutions:
[0005] A high-purity aluminum fluoride condenser includes a support platform, a pair of symmetrically distributed support plates are fixedly connected to the support platform, an air pump is fixedly connected to the support plates, an air inlet pipe is provided at the air inlet end of the air pump, an on-off valve is provided on the air inlet pipe, an axis tube is provided at the output end of the air pump, the axis tube and the air pump are rotatably connected, a condensing cylinder placed coaxially is provided between the two axis tubes, the condensing cylinder is cylindrical, a condensing air pipe is connected to the peripheral side wall of the condensing cylinder, the condensing air pipe is connected to the inside of the condensing cylinder, a condensing air valve is provided on the condensing air pipe, a first circular through hole is provided on the circular end faces at both ends of the condensing cylinder, one end of the axis tube passes through the first circular through hole, and the axis tube can rotate in the first circular through hole.
[0006] A first condenser tube is provided in the condenser cylinder and is placed coaxially. The diameter of the first condenser tube is larger than that of the shaft tube. Second circular holes are provided on the circular surfaces at both ends of the first condenser tube. The size of the second circular hole is equal to that of the first circular hole. The outer tube wall of the shaft tube is fixedly connected to the wall of the second circular hole.
[0007] A plurality of evenly distributed second condenser tubes are fixedly connected to the upper and lower outer tube walls of the first condenser tube. The second condenser tubes are placed vertically with the first condenser tubes, and the interiors of the second condenser tubes are connected with the interiors of the first condenser tubes.
[0008] The support plate is provided with a fixed plate that is fixedly connected, and the fixed plate is placed in parallel with the circular end surface of the condensing cylinder. A rotating motor is provided on any fixed plate, and the rotating motor is fixedly connected to a side of the fixed plate close to the condensing cylinder. A rotating shaft is provided at the output end of the rotating motor, and a small gear is sleeved on the rotating shaft. The rotating shaft can drive the small gear to rotate, and a large gear is sleeved on the shaft tube on the same side as the small gear. The large gear is fixedly connected to the peripheral side of the shaft tube, and the small gear and the large gear are connected by a belt.
[0009] Furthermore, the first condenser tube is provided with through-hole grooves on the circumferential side surfaces near both ends, and the through-hole grooves pass through the upper and lower circumferential side surfaces of the first condenser tube. A cylindrical pushing block is provided in the first condenser tube, and the circumferential wall of the pushing block is in contact with the inner wall of the first condenser tube. The length of the pushing block is greater than the length of the through-hole groove, and the pushing block can seal and block the through-hole groove.
[0010] Furthermore, a circular plate is provided in each second condenser tube connected to the upper and lower side walls of the first condenser tube. The circular plates are placed coaxially with the second condenser tube, and the circumferential side surfaces of the circular plates are in contact with the inner walls of the second condenser tube. The circular plates in the two coaxially placed second condenser tubes are fixedly connected by elastic rubber ropes, and the rubber ropes are always in a stretched state.
[0011] Furthermore, a fixedly connected positioning pin is provided at one end of the second condenser tube close to the peripheral wall of the first condenser tube.
[0012] Furthermore, two sliding annular sleeves are provided on the tube wall near the two ends of the first condenser tube, and the length of the annular sleeves is greater than the length of the through-hole groove. The annular sleeves can seal and block the through-hole groove. The annular sleeves are fixedly connected to the annular sleeves, and the other ends of the connecting rods are fixedly connected to the first magnet pieces. The first magnet pieces are fitted with the inner wall of the condenser tube, and the two first magnet pieces are fixedly connected by a first guide rod. The length of the first guide rod is less than the distance between the two through-hole grooves.
[0013] Furthermore, the rotating shaft is connected to a threaded rod, which can drive the threaded rod to rotate. The other end of the threaded rod passes through the fixed plate, and the threaded rod and the fixed plate are rotatably connected. Two sliders are provided on the threaded rod, and each slider is provided with a threaded hole. The threaded rod passes through the threaded hole, and the threaded rod and the slider can perform threaded engagement transmission.
[0014] Furthermore, the slider is fixedly connected to the second magnet piece, the second magnet piece is in contact with the outer wall of the condensing cylinder, the position of the second magnet piece corresponds to the first magnet piece, and a second guide rod is fixedly connected between the two second magnet pieces.
[0015] Furthermore, a groove is provided on the peripheral side wall of the rotating shaft, and an automatic telescopic clamping block is fixedly connected in the groove.
[0016] Furthermore, a connecting block is provided between the threaded rod and the rotating shaft, the connecting block is fixedly connected to the rotating shaft, a round hole seat is provided on the connecting block, a rolling bearing is provided in the round hole seat, the outer ring of the rolling bearing is fixedly connected to the circumferential side of the round hole seat, and the threaded rod is fixedly connected to the inner ring of the rolling bearing.
[0017] Furthermore, the threaded rod is provided with a fixedly connected circular plate near the rolling bearing position, and a pair of symmetrically distributed first telescopic cylinders are provided on the circular plate. The bottom of the first telescopic cylinder is fixedly connected to the circular plate, and the telescopic rod of the first telescopic cylinder is fixedly connected to the circular clamp block. The circular clamp block can be inserted between the inner ring and the outer ring of the rolling bearing to clamp and connect the inner ring and the outer ring of the rolling bearing.
[0018] Furthermore, two discharge ports are provided on the side wall around the lower end of the condensing cylinder, and the positions of the discharge ports correspond to the positions of the through-hole grooves at both ends of the first condensing tube. A second telescopic cylinder is provided near the bottom of the condensing cylinder on the support plate, and the bottom of the second telescopic cylinder is fixedly connected to the support plate. The telescopic rod of the second telescopic cylinder is fixedly connected to the discharge baffle, and a storage tank is provided on the support platform.
[0019] Beneficial effects of the present disclosure:
[0020] 1. The present invention aims to overcome the problems of insufficient condensation of high-purity aluminum fluoride and low condensation efficiency in the prior art. A high-purity aluminum fluoride condenser is invented to solve the problems of insufficient condensation of high-purity aluminum fluoride and low condensation efficiency in the prior art. The high-purity aluminum fluoride is fully condensed and the condensation efficiency is improved.
[0021] 2. A high-purity aluminum fluoride condenser invented can stir the condensed gas during the condensation process, diffusing the high-temperature condensed gas after heat exchange from the surface of the condenser tube, allowing the low-temperature condensed gas in the condenser tube to continue condensing, improving the condensation efficiency and increasing the utilization rate of the condensed gas;
[0022] 3. A high-purity aluminum fluoride condenser invented can realize the continuous automatic discharge and collection of aluminum fluoride crystals produced during the condensation and crystallization process, thereby improving work efficiency. BRIEF DESCRIPTION OF THE DRAWINGS
[0023] In order to more clearly illustrate the embodiments of the present disclosure or the technical solutions in the prior art, the following briefly introduces the drawings required for use in the embodiments or the description of the prior art. Obviously, for ordinary technicians in this field, other drawings can be obtained based on these drawings without any creative work.
[0024] Figure 1 It is a schematic diagram of the overall structure and internal parts of the present invention;
[0025] Figure 2Schematic diagram of the overall structure of the present invention from different viewing angles;
[0026] Figure 3 This is a schematic diagram of the internal structure of the condensing cylinder of the present invention;
[0027] Figure 4 This is a schematic structural diagram of a cross-sectional view of the first condenser and the second condenser of the present invention;
[0028] Figure 5 It is a schematic structural diagram of the rotating shaft connection in the present invention;
[0029] Figure 6 It is a schematic diagram of the bottom perspective structure of the condensation cylinder of the present invention. DETAILED DESCRIPTION
[0030] The following will be combined with the accompanying drawings in the embodiments of the present disclosure to clearly and completely describe the technical solutions in the embodiments of the present disclosure. Obviously, the embodiments described are only part of the embodiments of the present disclosure, not all of the embodiments. Based on the embodiments of the present disclosure, all other embodiments obtained by ordinary technicians in this field without making any creative efforts are within the scope of protection of the present disclosure.
[0031] like Figures 1-6As shown, a high-purity aluminum fluoride condenser includes a support platform 1, a pair of symmetrically distributed support plates 2 are fixedly connected to the support platform 1, an air pump 3 is fixedly connected to the support plates 2, an air inlet pipe 4 is provided at the air inlet end of the air pump 3, an on-off valve 41 is provided on the air inlet pipe 4, an output end of the air pump 3 is provided with a shaft tube 5, the shaft tube 5 and the air pump 3 are rotatably connected, a coaxially placed condensing cylinder 6 is provided between the two shaft tubes 5, the condensing cylinder 6 is cylindrical, a condensing air pipe 7 is connected to the peripheral side wall of the condensing cylinder 6, the condensing air pipe 7 is connected to the inside of the condensing cylinder 6, a condensing air valve 71 is provided on the condensing air pipe 7, a first circular through hole is provided on the circular end surface of both ends of the condensing cylinder 6, one end of the shaft tube 5 passes through the first circular through hole, and the shaft tube 5 can rotate in the first circular through hole, a coaxially placed first condensing tube 8 is provided in the condensing cylinder 6, the diameter of the first condensing tube 8 is larger than the shaft tube 5, and a second circular through hole 81 is provided on the circular surface of both ends of the first condensing tube 8. The size of 81 is equal to that of the first circular through hole, the outer tube wall of the shaft tube 5 is fixedly connected to the hole wall of the second circular through hole 81, and the upper and lower tube walls of the outer side of the first condenser tube 8 are fixedly connected with a plurality of evenly distributed second condenser tubes 9, and the second condenser tubes 9 are vertically placed with the first condenser tube 8. The interior of the second condenser tube 9 is connected with the interior of the first condenser tube 8. A fixed plate 10 is fixedly connected to the support plate 2, and the fixed plate 10 is placed in parallel with the circular end surface of the condenser tube 6. A rotating motor 11 is provided on any fixed plate 10, and the rotating motor 11 is fixedly connected to a side of the fixed plate 10 close to the condenser tube 6. A rotating shaft 111 is provided at the output end of the rotating motor 11, and a small gear 12 is sleeved on the rotating shaft 111. The rotating shaft 111 can drive the small gear 12 to rotate, and a large gear 13 is sleeved on the shaft tube 5 on the same side as the small gear 12. The large gear 13 is fixedly connected to the side surface of the shaft tube 5, and the small gear 12 and the large gear 13 are connected by a belt 14;
[0032] Open the condensation valve 71, and let the condensation gas into the condensation tube 6, open the switch valve 41 on any one of the inlet pipes 4, and turn on the air pump 3 connected to the inlet pipe 4, the air pump 3 introduces the high-temperature aluminum fluoride gas into the first condensation tube 8 and the second condensation tube 9, and at the same time turn on the rotating motor 11, the output end of the rotating motor 11 drives the rotating shaft 111, the rotating shaft 111 drives the small gear 12, the small gear 12 drives the belt 14, the belt 14 drives the large gear 13, the large gear 13 drives the shaft tube 5, the shaft tube 5 drives the first condensation tube 8, and the first condensation tube 8 drives the second condensation tube 9 to rotate; the high-temperature fluoride The aluminum gas in the first condenser tube 8 and the second condenser tube 9 is cooled by the condensation of the condensation gas in the condensation tube 6, and the aluminum fluoride gas condenses and crystallizes into aluminum fluoride crystals on the inner walls of the first condenser tube 8 and the second condenser tube 9. At the same time, the rotation of the second condenser tube 9 allows the high-temperature condensation gas formed after the superheat exchange with the high-temperature aluminum fluoride gas to diffuse rapidly, preventing the high-temperature condensation gas from gathering on the outer tube walls of the first condenser tube 8 and the second condenser tube 9, so that the low-temperature condensation gas in the condensation tube 6 can continue to condense, thereby achieving full condensation of the high-temperature aluminum fluoride gas and improving the condensation work efficiency.
[0033] In order to achieve the automatic and continuous discharge of aluminum fluoride crystals condensed in the first condenser tube 8 and prevent the crystals from gathering at one end of the first condenser tube 8 and causing blockage, the first condenser tube 8 is provided with through-hole grooves 82 on the peripheral side surfaces near both ends. The through-hole grooves 82 pass through the upper and lower peripheral sides of the first condenser tube 8. A cylindrical pushing block 83 is provided in the first condenser tube 8. The peripheral wall of the pushing block 83 is in contact with the inner wall of the first condenser tube 8. The length of the pushing block 83 is greater than the length of the through-hole groove 82. The pushing block 83 can seal and block the through-hole groove 82.
[0034] Working principle: First, the first air intake is carried out, the air pump 3 on either side is turned on, the switch valve 41 is opened, and high-temperature aluminum fluoride gas is introduced from one end of the first condenser tube 8. Under the action of gas pressure, the high-temperature aluminum fluoride gas pushes the push block 83 to move along the first condenser tube 8, and the push block 83 slides to the end of the first condenser tube 8 away from the air intake, and then condensation and crystallization are carried out; after the first air intake is fully condensed, the second air intake is carried out, and the air pump 3 on the other side is turned on to introduce high-temperature aluminum fluoride gas into the first condenser tube 8. The gas pushes the push block 83 to move toward the first air intake end. During the movement, the push block 83 drives the crystals produced after the first air intake condensation to move, and discharges the crystals from the through-hole groove 82 near the first air intake end. While the crystals are discharged, the push block 83 also covers the through-hole groove 82 on this side, sealing and blocking the through-hole groove 82; after the second air intake is fully condensed, the air pump 3 at the first air intake end is turned on again, and the third air intake is carried out, and a similar process as the second air intake is carried out. The above process is repeated, and this process is repeated to achieve the automatic and continuous discharge of the aluminum fluoride crystals condensed in the first condensation tube 8, while preventing the crystals from gathering at one end of the first condensation tube 8 to cause blockage.
[0035] In order to realize the automatic discharge of the crystals generated by condensation and crystallization in the second condenser tube 9, a circular plate 91 is provided in each second condenser tube 9 connected to the upper and lower side walls of the first condenser tube 8. The circular plates 91 are placed coaxially with the second condenser tube 9, and the side surfaces of the circular plates 91 are in contact with the inner walls of the second condenser tube 9. The circular plates 91 in the two coaxially placed second condenser tubes 9 are fixedly connected by elastic rubber ropes 92, and the rubber ropes 92 are always in a stretched state; the rotating motor 11 is turned on, and the output end of the rotating motor 11 drives the rotating shaft 111, the rotating shaft 111 drives the small gear 12, the small gear 12 drives the belt 14, the belt 14 drives the large gear 13, the large gear 13 drives the shaft tube 5, the shaft tube 5 drives the first condenser tube 8, and the first condenser tube 8 drives the second condenser tube 9 to rotate. When the rotation speed is high, the centrifugal force generated is greater than the elastic force of the rubber rope 92. Under the action of the centrifugal force, the circular plate 91 moves along the second condenser tube 9 to the end away from the rotation center axis. After sufficient condensation, the rotating motor 11 is turned off, and the second condenser tube 9 starts to rotate slowly until it stops. When the rotation speed of the second condenser tube 9 decreases and the centrifugal force generated is insufficient, the circular plates 91 approach each other under the pull of the elastic force of the rubber rope 92. While the circular plates 91 approach each other, the circular plates 91 scrape the crystallized crystals on the wall of the second condenser tube 9. Driven by the circular plates 91, the crystals move along the second condenser tube 9, and finally the crystals generated in the second condenser tube 9 enter the first condenser tube 8 for easy discharge, thereby achieving the purpose of automatic discharge of the crystals generated by condensation and crystallization in the second condenser tube 9.
[0036] In order to prevent the two coaxial circular plates 91 from entering the same second condenser tube 9, which would result in the inability to effectively discharge the crystals in the second condenser tube 9, a fixedly connected positioning pin 93 is provided at one end of the second condenser tube 9 close to the peripheral wall of the first condenser tube 8, thereby preventing the two coaxial circular plates 91 from entering the same second condenser tube 9.
[0037] In order to prevent the high-temperature aluminum fluoride gas from entering the condenser tube 6 from the through-hole groove 82 at the air inlet end during air intake, and at the same time not hindering the discharge of crystals, two slidable annular sleeves 15 are provided on the tube wall near the two ends of the first condenser tube 8. The length of the annular sleeve 15 is greater than the length of the through-hole groove 82. The annular sleeve 15 can seal and block the through-hole groove 82. A connecting rod 16 is fixedly connected to the annular sleeve 15. The other end of the connecting rod 16 is fixedly connected to the first magnet piece 17. The first magnet piece 17 is fitted with the inner wall of the condenser tube 6. The two first magnet pieces 17 are fixedly connected by a first guide rod 18. The length of the first guide rod 18 is less than the length of the two through-hole grooves. 82, the rotating shaft 111 is connected to a threaded rod 19, the rotating shaft 111 can drive the threaded rod 19 to rotate, the other end of the threaded rod 19 passes through the fixed plate 10, the threaded rod 19 is rotatably connected to the fixed plate 10, the threaded rod 19 is provided with two sliders 20, the sliders 20 are provided with threaded holes, the threaded rod 19 passes through the threaded holes, the threaded rod 19 and the sliders 20 can be threadedly engaged with each other, the sliders 20 are fixedly connected to the second magnet piece 21, the second magnet piece 21 is in contact with the outer wall of the condensing cylinder 6, the position of the second magnet piece 21 corresponds to the first magnet piece 17, and a second guide rod 22 is fixedly connected between the two second magnet pieces 21;
[0038] When air is taken in from either end, the pushing block 83 moves away from the through hole groove 82 at that end under the action of gas pressure. At the same time, the rotating motor 11 is turned on, and the output end of the rotating motor 11 drives the rotating shaft 111, and the rotating shaft 111 drives the threaded rod 19 to rotate. The threaded rod 19 and the slider 20 are threadedly engaged and transmitted. The slider 20 drives the second magnet piece 21. Under the action of magnetic force, the second magnet piece 21 drives the first magnet piece 17, and the first magnet piece 17 drives the connecting rod 16. The connecting rod 16 drives the annular sleeve 15. The annular sleeve 15 moves toward the air inlet end to seal and block the through hole groove 82 near the air inlet end. At the same time, since the length of the first guide rod 18 is less than the distance between the two through hole grooves 82, the through hole groove 82 on the other side will be in an open state, thereby preventing the high-temperature aluminum fluoride gas from entering the condensation tube 6 from the through hole groove 82 at the air inlet end when air is taken in, and at the same time does not hinder the discharge of crystals.
[0039] In order to enable the rotating shaft 111 to selectively drive the pinion 12 and the threaded rod 19, a groove is provided on the circumferential side wall of the rotating shaft 111, and an automatic telescopic block 1111 is fixedly connected in the groove. A connecting block 23 is provided between the threaded rod 19 and the rotating shaft 111, and the connecting block 23 is fixedly connected to the rotating shaft 111. A circular hole seat is provided on the connecting block 23, and a rolling bearing 24 is provided in the circular hole seat. The outer ring of the rolling bearing 24 is fixedly connected to the circumferential side of the circular hole seat, and the threaded rod 19 is fixedly connected to the inner ring of the rolling bearing 24. A fixedly connected circular ring plate 25 is provided at the position of the threaded rod 19 near the rolling bearing 24, and a pair of symmetrically distributed first telescopic cylinders 26 are provided on the circular ring plate 25. The bottom of the first telescopic cylinder 26 is fixedly connected to the circular ring plate 25, and the telescopic rod of the first telescopic cylinder 26 is fixedly connected to the circular block 27. The circular block 27 can be inserted between the inner ring and the outer ring of the rolling bearing 24 to connect the inner ring of the rolling bearing 24 with the outer ring. The outer ring is engaged and connected; when only the rotating shaft 111 needs to drive the pinion 12, the automatic telescopic block 1111 is extended, so that the rotating shaft 111 is engaged with the pinion 12, and the first telescopic cylinder 26 is turned on at the same time. The telescopic rod of the first telescopic cylinder 26 contracts and drives the annular block 27 away from the rolling bearing 24, and the inner and outer rings of the rolling bearing 24 can rotate freely. At this time, rotating the rotating shaft 111 will only drive the pinion 12 to work; when only the rotating shaft 111 needs to drive the threaded rod 19 to rotate, the first telescopic cylinder 26 is turned on, and the telescopic rod of the first telescopic cylinder 26 is extended to drive the annular block 27 close to the rolling bearing 24, so that the annular block 27 engages the inner and outer rings of the rolling bearing 24 for synchronous movement, and at the same time, the automatic telescopic block 1111 is retracted. At this time, rotating the rotating shaft 111 only drives the threaded rod 19 to rotate, thereby achieving the purpose of the rotating shaft 111 selectively driving the pinion 12 and the threaded rod 19.
[0040] In order to facilitate the collection and storage of the discharged aluminum fluoride crystals, two discharge ports 61 are provided on the side wall of the lower end of the condensation cylinder 6. The position of the discharge port 61 corresponds to the position of the through-hole groove 82 at both ends of the first condensation tube 8. The support plate 2 is provided with a second telescopic cylinder 28 near the bottom of the condensation cylinder 6. The bottom of the second telescopic cylinder 28 is fixedly connected to the support plate 2, and the telescopic rod of the second telescopic cylinder 28 is fixedly connected to the discharge baffle 29. A storage groove 30 is provided on the support platform 1; when the aluminum fluoride crystals are discharged from the through-hole groove 82 on one side, the second telescopic cylinder 28 corresponding to the side is opened, and the telescopic rod of the second telescopic cylinder 28 contracts to drive the discharge baffle 29 away from the discharge port 61, so that the discharge port 61 is opened, and the aluminum fluoride crystals discharged from the through-hole groove 82 fall into the storage groove 30 through the discharge port 61, thereby achieving the purpose of conveniently collecting and storing the discharged aluminum fluoride crystals.
[0041] Throughout this specification, references to terms such as "one embodiment," "example," or "specific example" indicate that a specific feature, structure, material, or characteristic described in conjunction with that embodiment or example is included in at least one embodiment or example of the present disclosure. In this specification, schematic representations of these terms do not necessarily refer to the same embodiment or example. Furthermore, the specific features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.
[0042] The above shows and describes the basic principles, main features and advantages of the present disclosure. Those skilled in the art should understand that the present disclosure is not limited to the above embodiments. The above embodiments and descriptions are merely illustrative of the principles of the present disclosure. Various changes and improvements may be made to the present disclosure without departing from the spirit and scope of the present disclosure, and such changes and improvements shall fall within the scope of the present disclosure.
Claims
1. A high-purity aluminum fluoride condenser, comprising a support platform (1), a pair of symmetrically distributed support plates (2) are fixedly connected to the support platform (1), an air pump (3) is fixedly connected to the support plates (2), an air inlet pipe (4) is provided at the air inlet end of the air pump (3), an on-off valve (41) is provided on the air inlet pipe (4), an output end of the air pump (3) is provided with a shaft tube (5), the shaft tube (5) and the air pump (3) are rotatably connected, a condensation cylinder (6) is coaxially arranged between the two shaft tubes (5), the condensation cylinder (6) is cylindrical, a condensation pipe (7) is connected to the peripheral side wall of the condensation cylinder (6), the condensation pipe (7) and the interior of the condensation cylinder (6) are connected, a condensation valve (71) is provided on the condensation pipe (7), and a first circular through hole is provided on the circular end surface of both ends of the condensation cylinder (6), one end of the shaft tube (5) passes through the first circular through hole, and the shaft tube (5) can rotate in the first circular through hole; A first condenser tube (8) is provided in the condenser tube (6) and is coaxially arranged. The diameter of the first condenser tube (8) is larger than that of the shaft tube (5). Second circular through holes (81) are provided on the circular surfaces at both ends of the first condenser tube (8). The size of the second circular through hole (81) is equal to that of the first circular through hole. The outer wall of the shaft tube (5) is fixedly connected to the wall of the second circular through hole (81). A plurality of evenly distributed second condensing tubes (9) are fixedly connected to the upper and lower tube walls of the outer side of the first condensing tube (8), the second condensing tubes (9) are vertically arranged with the first condensing tube (8), and the interior of the second condensing tube (9) is connected to the interior of the first condensing tube (8); The support plate (2) is provided with a fixed plate (10) which is fixedly connected, and the fixed plate (10) is placed in parallel with the circular end surface of the condensing tube (6). A rotating motor (11) is provided on any fixed plate (10), and the rotating motor (11) is fixedly connected to a side surface of the fixed plate (10) close to the condensing tube (6). The output end of the rotating motor (11) is provided with a rotating shaft (111), and a small gear (12) is sleeved on the rotating shaft (111). The rotating shaft (111) can drive the small gear (12) to rotate. A large gear (13) is sleeved on the shaft tube (5) on the same side as the small gear (12), and the large gear (13) is fixedly connected to the peripheral side surface of the shaft tube (5). The small gear (12) and the large gear (13) are connected via a belt (14); The first condenser tube (8) is provided with through-hole grooves (82) on the peripheral side surfaces near both ends, and the through-hole grooves (82) penetrate the upper and lower peripheral side surfaces of the first condenser tube (8). A cylindrical pushing block (83) is provided in the first condenser tube (8), and the peripheral wall of the pushing block (83) is in contact with the inner wall of the first condenser tube (8). The length of the pushing block (83) is greater than the length of the through-hole groove (82), and the pushing block (83) can seal and block the through-hole groove (82); A circular plate (91) is provided in each second condenser tube (9) connected to the upper and lower side walls of the first condenser tube (8), and the circular plates (91) are placed coaxially with the second condenser tube (9), and the circumferential side surface of the circular plate (91) is in contact with the inner wall of the second condenser tube (9), and the circular plates (91) in the two coaxially placed second condenser tubes (9) are fixedly connected by an elastic rubber rope (92), and the rubber rope (92) is always in a stretched state; Two slidable annular sleeves (15) are provided on the tube wall near both ends of the first condensing tube (8), the length of the annular sleeves (15) is greater than the length of the through hole groove (82), and the annular sleeves (15) can seal and block the through hole groove (82), and the annular sleeves (15) are fixedly connected to the connecting rods (16), and the other ends of the connecting rods (16) are fixedly connected to the first magnet pieces (17), and the first magnet pieces (17) are fitted with the inner tube wall of the condensing tube (6), and the two first magnet pieces (17) are fixedly connected by a first guide rod (18), and the length of the first guide rod (18) is less than the distance between the two through hole grooves (82); The rotating shaft (111) is connected to a threaded rod (19), and the rotating shaft (111) can drive the threaded rod (19) to rotate. The other end of the threaded rod (19) passes through the fixed plate (10), and the threaded rod (19) and the fixed plate (10) are rotatably connected. The threaded rod (19) is provided with two sliders (20), and the sliders (20) are each provided with a threaded hole. The threaded rod (19) passes through the threaded hole, and the threaded rod (19) and the slider (20) can perform threaded engagement transmission; The slider (20) is fixedly connected to the second magnet piece (21), the second magnet piece (21) is in contact with the outer wall of the condensing cylinder (6), the position of the second magnet piece (21) corresponds to the first magnet piece (17), and a second guide rod (22) is fixedly connected between the two second magnet pieces (21); A groove is provided on the peripheral side wall of the rotating shaft (111), and an automatic telescopic clamping block (1111) is fixedly connected in the groove; A connecting block (23) is provided between the threaded rod (19) and the rotating shaft (111), the connecting block (23) is fixedly connected to the rotating shaft (111), a circular hole seat is provided on the connecting block (23), a rolling bearing (24) is provided in the circular hole seat, an outer ring of the rolling bearing (24) is fixedly connected to the circumference of the circular hole seat, and the threaded rod (19) is fixedly connected to the inner ring of the rolling bearing (24); The threaded rod (19) is provided with a fixedly connected circular plate (25) near the rolling bearing (24). A pair of first telescopic cylinders (26) are symmetrically distributed on the circular plate (25). The bottom of the first telescopic cylinder (26) is fixedly connected to the circular plate (25). The telescopic rod of the first telescopic cylinder (26) is fixedly connected to the circular clamping block (27). The circular clamping block (27) can be inserted between the inner ring and the outer ring of the rolling bearing (24) to engage and connect the inner ring and the outer ring of the rolling bearing (24).
2. A high-purity aluminum fluoride condenser according to claim 1, characterized in that: A fixedly connected positioning pin (93) is provided at one end of the second condenser tube (9) close to the peripheral wall of the first condenser tube (8).
3. A high-purity aluminum fluoride condenser according to claim 2, characterized in that: Two discharge ports (61) are provided on the side wall of the lower end of the condensing cylinder (6), and the positions of the discharge ports (61) correspond to the positions of the through-hole grooves (82) at both ends of the first condensing tube (8). A second telescopic cylinder (28) is provided at a position near the bottom of the condensing cylinder (6) on the supporting plate (2), the bottom of the second telescopic cylinder (28) is fixedly connected to the supporting plate (2), the telescopic rod of the second telescopic cylinder (28) is fixedly connected to the discharge baffle (29), and a storage tank (30) is provided on the supporting platform (1).
Citation Information
Patent Citations
Condenser applied to anhydrous hydrogen fluoride production
CN212806604U
Novel crystal growing device for aluminum fluoride crystallization
CN213221028U