A mixing and stirring device for refining coix seed oil
By designing a mixing and stirring equipment for refining coix seed oil, using technical means such as centrifugal barrels and water-cooled cooling devices, the problem of large amount of water resources during refining is solved, and the reuse of water resources and the environmental protection of the refining process is achieved.
Patent Information
- Application Number
- CN202311137616.9
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2023-09-05
- Publication Date
- 2025-03-14
- Estimated Expiration
- 2043-09-05
AI Technical Summary
The existing coix seed oil refining process is large in water resources and it is difficult to achieve green processing, resulting in waste of water resources.
A mixing and stirring equipment for refining coix seed oil is designed, including a tripod, a reaction device, a separation device and a negative pressure transmission device, and the reaction mixture is separated by a centrifugal barrel, and the water-cooled cooling device and a negative pressure transmission device are used to improve cooling efficiency and water resource utilization.
Effectively reuse water resources, reduce water resources waste, and improve the efficiency and environmental protection of the refining process.
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Figure CN117106520B_ABST
Abstract
Description
Technical Field
[0001] The invention relates to the technical field of coix seed oil refining, and more specifically, to a mixing and stirring device for coix seed oil refining. Background Art
[0002] Coix seed oil is a vegetable oil extracted from coix seeds, also known as coix seed oil. It is rich in various nutrients and bioactive substances, beneficial to human health, and widely used in the field of beauty and health care. However, coix seeds collected in a natural state can only be obtained as crude coix seed oil after simple grinding and distillation. In order to improve the purity and quality of coix seed oil, it is necessary to further refine and extract coix seed oil so that it can be used in food, health products and cosmetics.
[0003] Common methods of refining coix seed oil usually use alkali refining and distillation refining. Alkali refining is to react coix seed oil with an alkali solution of a certain concentration, and then it will undergo deacidification, cooling, separation, decolorization and deodorization to obtain refined coix seed oil. However, in the refining process, each part is carried out almost independently, especially deacidification and decolorization, which require water and water volatile substances to be treated, but in many cases they are provided separately. At the same time, water vapor is also needed to provide water, which increases the use of water resources. It is not possible to achieve green processing and wastes water resources. Summary of the invention
[0004] The purpose of the present invention is to provide a mixing and stirring equipment for refining coix seed oil to solve the problems raised in the above-mentioned background technology: the common coix seed oil refining usually uses two methods, alkali refining and distillation refining, wherein alkali refining is through the coix seed oil and a certain concentration of alkaline solution reaction, and then it will be deacidified, cooled, separated, decolorized and deodorized to obtain refined coix seed oil, but in the refining process each part is almost carried out independently, especially deacidification and decolorization need to use water and water volatile matter treatment, but in many cases they are provided separately, and water vapor needs to be provided at the same time as water, which increases the use of water resources, and cannot achieve green processing well, wasting water resources.
[0005] A mixing and stirring device for refining coix seed oil, comprising a tripod, a reaction device and a separation device, wherein the tripod is installed on the bottom surface of the reaction device, and a negative pressure transmission device is connected to the center of the bottom surface of the reaction device, a decolorization tube is arranged on the negative pressure transmission device, a water cooling device is connected to the negative pressure transmission device, and the top position of the separation device is connected to the negative pressure transmission device, a vacuum extraction device is installed on the upper surface of the separation device, a centrifugal device is arranged inside the separation device, and a collecting device is arranged at the bottom of the separation device;
[0006] Preferably, a movable barrel cover is connected between the separation device and the centrifugal device, and the movable barrel cover includes a movable cover plate, a lifting rod and a sensing block. The lower edge of the movable cover plate is annular in design, and the lower edge of the movable cover plate is 15 cm long. The centrifugal device is provided with a centrifugal bucket, and a plurality of holes are opened in the circumference of the centrifugal bucket at a distance of 10 cm from the top, and an electric heating rod is installed at the bottom of the centrifugal bucket.
[0007] Preferably, the reaction device comprises a reaction barrel and an agitator mounted on a tripod, a feeding port is provided on the top of the reaction barrel, the agitator is arranged in the reaction barrel, and a servo motor is installed on the bottom of the reaction barrel, the servo motor is connected to a ball valve, and the designed reaction device has a simple structure and is easy to operate.
[0008] Preferably, the water cooling device includes a water tank, a controller is installed on the upper surface of the water tank, and water pumps are connected to both sides of the upper surface of the water tank, the water pumps are connected to water pipes, and the water pipes are connected to the negative pressure transmission device. The reaction mixture is cooled by the water cooling device, which shortens the cooling time compared to natural cooling and improves the processing efficiency of the overall device.
[0009] Preferably, the negative pressure transmission device includes a negative pressure pump and a double-layer pipe, the negative pressure pump is connected to a single-layer structure pipe, the double-layer pipe is connected between the single-layer structure pipes, and the decolorization tube is arranged between the double-layer pipe and the single-layer structure pipe. The double-layer pipe arranged by the negative pressure transmission device can extend the time of the reaction mixture in the double-layer pipe, thereby increasing the cooling time of the reaction mixture by the refrigerant, further improving the processing efficiency of the overall device.
[0010] Preferably, the separation device includes a separation barrel and a feed pipe, the feed pipe is connected to the top of the separation barrel, a conical block is provided on the inner bottom surface of the separation barrel, a support column is connected to the lower surface of the separation barrel, and a plurality of feed holes are provided on the circumferential edge of the conical block. The design of the conical block facilitates the separation material to quickly enter the feed hole, and then fall from the feed hole into the collection device, thereby accelerating the outflow of the separation material and improving the efficiency of separation and collection.
[0011] Preferably, the collecting device comprises two symmetrical arc-shaped containing boxes, which are arranged directly below the separating device, and a connecting groove is arranged on the straight side surface of the arc-shaped containing box near the rear end of the separating device, and a connecting column is arranged on the straight side surface of the arc-shaped containing box near the front end of the separating device.
[0012] Preferably, the vacuum extraction device comprises a vacuum tube, which passes through the top of the separation device and is connected to the centrifugal bucket, and the upper end of the vacuum tube is connected to an air pump, and the front of the air pump is connected to an air guide tube.
[0013] Preferably, connecting blocks are fixedly provided on both sides of the movable cover plate, the lifting rod is a threaded rod, and the lifting rod passes through the connecting blocks, the contact surface between the connecting block and the lifting rod is designed with a threaded groove, and the top of the lifting rod is connected to a rotating motor, and the rotating motor is fixedly installed on the top of the separation device, the induction block is arranged directly below the lifting rod, and the induction block is fixedly installed on the inner wall of the separation device, the centrifugal barrel can be sealed by the movable barrel cover, and the vacuum extraction device is triggered to extract the air in the centrifugal barrel, and then the temperature and air pressure are controlled, and vacuum extraction and purification are carried out by the electric heating rod, thereby preliminarily improving the purity of the extracted water vapor.
[0014] Preferably, the centrifugal device comprises a centrifugal bucket, an electric heating rod and holes. The centrifugal bucket is provided with a plurality of holes at a circumference of 1 cm from the top, and an electric heating rod is installed at the bottom of the centrifugal bucket. The electric heating rod is installed at the bottom of the centrifugal bucket, and a rotating shaft is connected to the bottom of the centrifugal bucket. The rotating shaft is connected to a rotating main unit. The water layer and the coix seed oil layer can be effectively separated by the centrifugal device, so that the coix seed oil layer can be collected conveniently.
[0015] Compared with the prior art, the advantages of the present invention are:
[0016] (1) In the present invention, on the basis of alkali refining, a centrifugal bucket is provided to separate the reaction mixture, and the water after separation is reused, volatile steam is generated by heating and distillation through a heating rod, and the volatile steam is extracted and extracted through a vacuum extraction device for further purification, and finally introduced into the separated coix seed oil in the form of water vapor for deodorization, so that water resources are effectively reused, the waste of water resources is reduced, and the processing requirements are met.
[0017] (2) In the present invention, a negative pressure transmission device is provided to transfer the reaction mixture after deacidification, and a water cooling device is combined with the spiral double-layer pipeline of the negative pressure transmission device. Compared with natural cooling, the cooling time is shortened and the processing efficiency of the overall device is improved.
[0018] (3) In the present invention, a movable barrel cover is provided. Before the residual water in the centrifugal barrel is heated, the movable barrel cover can be used to seal the centrifugal barrel and trigger the electric heating rod to start heating, thereby improving the automation of the overall device. BRIEF DESCRIPTION OF THE DRAWINGS
[0019] In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the accompanying drawings required for describing the embodiments will be briefly introduced below. Obviously, the accompanying drawings described below are only some embodiments of the present invention. For ordinary technicians in this field, other accompanying drawings can be obtained based on these accompanying drawings without paying creative work.
[0020] Figure 1 It is a schematic diagram of the overall structure of the present invention;
[0021] Figure 2 It is an enlarged schematic diagram of the reaction device structure of the present invention;
[0022] Figure 3 It is an enlarged schematic diagram of the water cooling device and negative pressure transmission device structure of the present invention;
[0023] Figure 4 It is an enlarged schematic diagram of the separation device structure of the present invention;
[0024] Figure 5 It is an enlarged schematic diagram of the collecting device structure of the present invention;
[0025] Figure 6 It is an enlarged schematic diagram of the movable cylinder cover structure of the present invention;
[0026] Figure 7 It is an enlarged schematic diagram of the centrifugal device structure of the present invention.
[0027] In the accompanying drawings, the components represented by the reference numerals are listed as follows:
[0028] 1. Tripod; 2. Reaction device; 201. Reaction barrel; 202. Feeding port; 203. Agitator; 204. Servo motor; 205. Ball valve; 3. Water cooling device; 301. Water tank; 302. Controller; 303. Water pump; 304. Water pipe; 4. Decolorization pipe; 5. Negative pressure transmission device; 501. Negative pressure pump; 502. Single-layer structure pipeline; 503. Double-layer pipeline; 6. Separation device; 601. Separation barrel; 602. Feeding pipe; 603. Conical block; 604. Feeding hole; 605. 05. Support column; 7. Collecting device; 701. Arc-shaped containing box; 702. Connecting column; 703. Connecting groove; 8. Vacuum extraction device; 801. Vacuum extraction tube; 802. Vacuum pump; 803. Air guide tube; 9. Movable cylinder cover; 901. Rotating motor; 902. Lifting rod; 903. Moving cover plate; 904. Connecting block; 905. Induction block; 10. Centrifugal device; 1001. Centrifugal barrel; 1002. Electric heating rod; 1003. Rotating shaft; 1004. Eyelet; 1005. Rotating host. DETAILED DESCRIPTION
[0029] The technical solutions in the embodiments of the present invention will be described clearly and completely below in conjunction with the accompanying drawings in the embodiments of the present invention.
[0030] See also Figure 1 , Figure 6 and Figure 7As shown, a mixing and stirring device for refining coix seed oil comprises a tripod 1, a reaction device 2 and a separation device 6, wherein the tripod 1 is mounted on the bottom surface of the reaction device 2, and a negative pressure transmission device 5 is connected to the center of the bottom surface of the reaction device 2, a decolorization tube 4 is arranged on the negative pressure transmission device 5, a water cooling device 3 is connected to the negative pressure transmission device 5, and the top position of the separation device 6 is connected to the negative pressure transmission device 5, a vacuum extraction device 8 is mounted on the upper surface of the separation device 6, a centrifugal device 10 is arranged inside the separation device 6, and a collecting device 7 is arranged at the bottom of the separation device 6;
[0031] A movable barrel cover 9 is connected between the separation device 6 and the centrifugal device 10. The movable barrel cover 9 includes a movable cover plate 903, a lifting rod 902 and a sensing block 905. The lower edge of the movable cover plate 903 is annular in design, and the lower edge of the movable cover plate 903 is 15 cm long. The centrifugal device 10 is provided with a centrifugal bucket 1001. The centrifugal bucket 1001 is provided with a plurality of holes 1004 at a distance of 10 cm from the top in the circumferential direction, and an electric heating rod 1002 is installed at the bottom of the centrifugal bucket 1001.
[0032] Among them Figure 2 In this embodiment, the reaction device 2 includes a reaction barrel 201 and an agitator 203 mounted on a tripod 1. A feeding port 202 is provided on the top of the reaction barrel 201, and a cover plate is provided on the feeding port 202. The agitator 203 is arranged in the reaction barrel 201. The agitator 203 is divided into a stirring blade, a rotating shaft and a driving motor. The upper end of the rotating shaft passes through the top of the reaction barrel 201 and is connected to the driving motor, and the lower end of the rotating shaft is connected to the stirring blade. A servo motor 204 is installed on the bottom surface of the reaction barrel 201. The servo motor 204 is driven by the The fixed block is installed on the bottom surface of the reaction barrel 201, the servo motor 204 is connected to the ball valve 205, and the ball valve 205 is arranged on the top of the single-layer structure pipeline 502 at the far left end. The reaction device 2 is used to deacidify the coix seed by pouring the heated coix seed oil into the reaction barrel 201 and then reacting it with a certain concentration of alkaline solution, usually NaOH or Na2CO3, so as to effectively neutralize the free fatty acids in the coix seed oil and generate saponification products such as sodium oleate. The designed reaction device 2 has a simple structure and is easy to operate.
[0033] Among them Figure 3 In this embodiment, the water cooling device 3 includes a water tank 301, a controller 302 is installed on the upper surface of the water tank 301, and water pumps 303 are connected to both sides of the upper surface of the water tank 301, the water pump 303 is connected to a water pipe 304, and the water pipe 304 is connected to the negative pressure transmission device 5, and refrigerant is stored in the water tank 301, and the water pipe 304 is connected to both ends of the double-layer pipe 503 of the negative pressure transmission device 5, and is connected to the interlayer of the double-layer pipe 503, and is not connected to the inner layer of the double-layer pipe 503. The water cooling device 3 is used to cool the reacted mixture, which shortens the cooling time compared to natural cooling and improves the processing efficiency of the overall device.
[0034] Among them Figure 3 In this embodiment, the negative pressure transmission device 5 includes a negative pressure pump 501 and a double-layer pipe 503. The negative pressure pump 501 is connected to a single-layer structure pipe 502. The double-layer pipe 503 is connected between the single-layer structure pipes 502, and the decolorization pipe 4 is arranged between the double-layer pipe 503 and the single-layer structure pipe 502. The single-layer structure pipe 502 connected to the right end of the negative pressure pump 501 is connected to the separation device 6. Activated carbon and white clay are arranged in the decolorization pipe 4 to decolorize the separated coix seed oil and remove the pigments and impurities therein. The negative pressure transmission device 5 is used to transfer the reacted mixture to the separation device 6 for separation treatment. The double-layer pipe 503 arranged by the negative pressure transmission device 5 can extend the time of the reacted mixture in the double-layer pipe 503, thereby increasing the cooling time of the reacted mixture by the refrigerant, and further improving the processing efficiency of the overall device.
[0035] Specifically, first, the heated coix seed oil is poured into the reaction barrel 201 through the feeding port 202, and then a certain concentration of NaOH solution or Na2CO3 solution is poured into the reaction barrel 201 through the feeding port 202 to react with the coix seed oil, effectively neutralize the free fatty acids in the coix seed oil, and generate saponification products such as sodium oleate. The specific concentrations of NaOH solution and Na2CO3 are determined according to the specific alkali refining process and the quality requirements of coix seed oil, and are usually controlled between 1% and 5%. After the reaction is completed, the water cooling device 3 and the negative pressure transmission device 5 are started, and the reaction mixture is extracted by the negative pressure pump 501. The reaction mixture will indirectly contact the refrigerant transmitted by the water cooling device 3 when passing through the double-layer pipe 503, and the reaction mixture will be decolorized through the decolorization tube 4 before passing through the double-layer pipe 503, thereby accelerating the cooling of the reaction mixture and improving the processing efficiency of the overall device.
[0036] Among them Figure 4 In this embodiment, the separation device 6 includes a separation barrel 601 and a feed pipe 602. The feed pipe 602 is connected to the top of the separation barrel 601. A conical block 603 is provided on the bottom surface of the separation barrel 601. A support column 605 is connected to the lower surface of the separation barrel 601, and a plurality of discharge holes 604 are provided on the circumferential edge of the conical block 603. The feed pipe 602 is provided with a pipe cover, and the discharge hole 604 is designed to pass through the lower surface of the separation barrel 601. The design of the conical block 603 facilitates the separation to quickly enter the discharge hole 604, and then fall from the discharge hole 604 into the collection device 7, thereby accelerating the outflow of the separation and improving the efficiency of separation and collection.
[0037] Among them Figure 5In this embodiment, the collecting device 7 includes two symmetrical arc-shaped containing boxes 701, which are arranged directly below the separating device 6. A connecting groove 703 is arranged on the straight side surface of the arc-shaped containing box 701 near the rear end of the separating device 6, and a connecting column 702 is arranged on the straight side surface of the arc-shaped containing box 701 near the front end of the separating device 6. The combination of the connecting column 702 and the connecting groove 703 facilitates the fixed installation of the two arc-shaped containing boxes 701.
[0038] Among them Figure 4 In this embodiment, the vacuum extraction device 8 includes a vacuum suction pipe 801, which passes through the top of the separation device 6 and is connected to the centrifugal barrel 1001. The upper end of the vacuum suction pipe 801 is connected to an air pump 802, and the front of the air pump 802 is connected to an air guide pipe 803. When deodorization treatment is required for the coix seed oil after separation, the air guide pipe 803 is connected to the arc-shaped containing box 701 to remove the odor and volatile substances therein through volatile substances.
[0039] Among them Figure 6 In this embodiment, connecting blocks 904 are fixedly provided on both sides of the movable cover plate 903, the lifting rod 902 is a threaded rod, and the lifting rod 902 penetrates and connects the connecting blocks 904, the contact surface of the connecting block 904 and the lifting rod 902 is designed with a threaded groove, and the top of the lifting rod 902 is connected to a rotating motor 901, and the rotating motor 901 is fixedly installed on the top of the separation device 6, the induction block 905 is arranged directly below the lifting rod 902, and the induction block 905 is fixedly installed on the inner wall of the separation device 6, the single-layer structure pipeline 502 and the feed pipe 602 are both penetrated and connected to the top of the centrifugal bucket 1001, and the single-layer structure pipeline 502, the feed pipe 602 and the movable cover plate 903 are movably connected. When the movable cover plate 903 drops to the lowest point, the single-layer structure pipeline 502 and the feed pipe 602 will not separate from the movable cover plate 903, and the lifting rod 902 is driven to rotate by the rotating motor 901, so that the lifting rod 902 can be rotated by the connecting block 90 The movable cover plate 903 connected to the lifting rod 902 can move up and down, and a trigger block is provided at the bottom of the lifting rod 902. When the lifting rod 902 descends, it will eventually stop due to the resistance of the upper edge of the barrel wall of the separation barrel 601. At this time, the movable cover plate 903 will block the hole 1004, and at the same time, the trigger block at the bottom of the lifting rod 902 will contact and press the sensing block 905, thereby triggering the vacuum extraction device 8 to work, and the air in the centrifugal barrel 1001 is extracted, that is, the acidic neutralizer and the precipitant are added through the feed pipe 602, and then the air in the centrifugal barrel 1001 is extracted by the vacuum pump 802, and the feed pipe 602 is tightly closed. Then, under the premise of ensuring uniform and appropriate heating, the mixed liquid in the centrifugal barrel 1001 is vacuum heated and discharged through the electric heating rod 1002, and then the discharged steam is cooled and extracted again, and finally the purified water is introduced into the arc-shaped containing box 701 in the form of steam to deodorize the separated coix seed oil.
[0040] Among them Figure 7 In this embodiment, the centrifugal device 10 includes a centrifugal bucket 1001, an electric heating rod 1002 and holes 1004. The centrifugal bucket 1001 is provided with a plurality of holes 1004 at a circumferential distance of 10 cm from the top, and the electric heating rod 1002 is installed at the bottom of the centrifugal bucket 1001. The electric heating rod 1002 is installed at the bottom of the centrifugal bucket 1001, and the bottom of the centrifugal bucket 1001 is connected with a rotating shaft 1003, and the rotating shaft 1003 is connected with a rotating host 1005. The rotating shaft 1003 passes through the conical block 603, and the electric heating rod 1002 is provided with a signal receiver for receiving a signal from the induction block 905, and the rotation speed of the rotating host 1005 can be manually controlled and adjusted. The water layer and the coix seed oil layer can be effectively separated by the centrifugal device 10, so as to facilitate the collection of the coix seed oil layer.
[0041] Specifically, the reaction mixture will enter the centrifugal barrel 1001 through the single-layer structure pipe 502, and then brine will be added to the centrifugal device 10 through the feed pipe 602, and the rotating host 1005 will be started to rotate the centrifugal barrel 1001 at a low speed to mix the mixture. The saponification product and other impurities produced will be dissolved in water through the action of the brine, thereby realizing the separation of coix seed oil and the saponification product. At this time, the saponification product and water-soluble impurities in the mixture will be separated from the water phase to form a water layer and a coix seed oil layer, and usually, the coix seed oil layer will be located in the upper layer and the water layer will be located in the lower layer. Then, the speed of the rotating host 1005 is adjusted, and the coix seed oil is made to flow out through the hole 1004 of the centrifugal barrel 1001 by centrifugation. The outflowing coix seed oil will fall into the arc-shaped containing box 701 through the discharge hole 604 of the separation device 6, and then the rotating motor 901 is started to make the movable cylinder cover 9 It drops to the lowest point, at which time the movable cover plate 903 will seal the hole 1004, and then an acidic neutralizer and a precipitant are added through the feed pipe 602 to neutralize the alkali solution and promote the sedimentation of solid particles. Then, the air in the centrifugal barrel 1001 is extracted by the vacuum pump 802, and then the centrifugal barrel 1001 is rotated at a low speed to stir the mixed liquid for sufficient reaction. Then, under the premise of ensuring uniform and appropriate heating, the mixed liquid in the centrifugal barrel 1001 is vacuum heated by the electric heating rod 1002 to perform the first step of purification. In order to improve the purity of the volatile steam, the feed pipe 602 is tightly closed, and the volatile steam is first guided out through the air guide pipe 803 by the vacuum pump 802, and the guided steam is cooled and extracted to further improve the purity of the water in the steam. Finally, the purified water is introduced into the arc-shaped containing box 701 in the form of steam to deodorize the separated coix seed oil.
[0042] The working principle of the present invention is as follows: first, the heated coix seed oil is poured into the reaction barrel 201 through the feeding port 202, and then a certain concentration of NaOH solution or Na2CO3 solution is poured into the reaction barrel 201 through the feeding port 202 to react with the coix seed oil, effectively neutralize the free fatty acids in the coix seed oil, and generate saponification products such as sodium oleate. The specific concentrations of NaOH solution and Na2CO3 are determined according to the specific alkali refining process and the quality requirements of coix seed oil, and are usually controlled between 1% and 5%. After the reaction is completed, the water cooling device 3 and the negative pressure transmission device 5 are started, and the reaction mixture is extracted by the negative pressure pump 501, and the reaction mixture is passed through the double When passing through the double-layer pipe 503, the reaction mixture will indirectly contact the refrigerant transmitted by the water-cooling device 3, and before passing through the double-layer pipe 503, the reaction mixture will be decolorized through the decolorization tube 4, thereby accelerating the cooling of the reaction mixture, and then the reaction mixture will enter the centrifugal bucket 1001 through the single-layer structure pipe 502, and then salt water will be added to the centrifugal device 10 through the feed pipe 602, and the rotating host 1005 will be started to rotate the centrifugal bucket 1001 at a low speed to mix the mixture, and the saponification product and other impurities produced will be dissolved in water by the action of the salt water, thereby realizing the separation of coix seed oil and saponification product. At this time, the saponification product and water-soluble impurities in the mixture will be separated from the water phase to form a A water layer and a coix seed oil layer, and usually, the coix seed oil layer will be located in the upper layer and the water layer will be located in the lower layer. Then, the rotation speed of the rotating host 1005 is adjusted, and the coix seed oil is made to flow out through the hole 1004 of the centrifugal barrel 1001 by centrifugation. The outflowing coix seed oil will fall into the arc-shaped containing box 701 through the discharge hole 604 of the separation device 6. The arc-shaped containing box 701 is heated to remove the water brought in from the washing process from the oil. Then, the rotating motor 901 is started to make the movable cylinder cover 9 drop to the lowest point. At this time, the movable cover plate 903 will seal the hole 1004. Then, the acidic neutralizer and precipitant are added through the feed pipe 602 to neutralize the alkali solution and promote the sedimentation of solid particles. Then The air in the centrifugal barrel 1001 is extracted by the vacuum pump 802, the feed pipe 602 is tightly closed, and the centrifugal barrel 1001 is rotated at a low speed to stir the mixed liquid for sufficient reaction. Then, under the premise of ensuring uniform and moderate heating, the mixed liquid in the centrifugal barrel 1001 is vacuum heated by the electric heating rod 1002 to perform the first step of purification. In order to improve the purity of the volatile vapor, the volatile vapor is first guided out through the air guide pipe 803 by the vacuum pump 802, and the guided vapor is cooled and extracted to further improve the purity of the water in the vapor. Finally, the purified water is introduced into the arc-shaped containing box 701 in the form of vapor, the separated coix seed oil is deodorized, and the mixture is left to stand for a period of time.
[0043] The above shows and describes the basic principles, main features and advantages of the present invention. Those skilled in the art should understand that the present invention is not limited by the above embodiments. The above embodiments and descriptions are only preferred examples of the present invention and are not intended to limit the present invention. Without departing from the spirit and scope of the present invention, the present invention may have various changes and improvements, which fall within the scope of the present invention. The scope of protection of the present invention is defined by the attached claims and their equivalents.
Claims
1. A mixing and stirring device for refining coix seed oil, comprising a tripod (1), a reaction device (2) and a separation device (6), characterized in that: The tripod (1) is installed on the bottom surface of the reaction device (2), and a negative pressure transmission device (5) is connected to the center of the bottom surface of the reaction device (2), a decolorization tube (4) is arranged on the negative pressure transmission device (5), the negative pressure transmission device (5) is connected to a water cooling device (3), and the top position of the separation device (6) is connected to the negative pressure transmission device (5), a vacuum extraction device (8) is installed on the upper surface of the separation device (6), a centrifugal device (10) is arranged inside the separation device (6), and a collecting device (7) is arranged at the bottom of the separation device (6); A movable barrel cover (9) is connected between the separation device (6) and the centrifugal device (10), the movable barrel cover (9) comprising a movable cover plate (903), a lifting rod (902) and a sensing block (905), the lower edge of the movable cover plate (903) being of annular design, and the lower edge of the movable cover plate (903) being 15 cm long, and the centrifugal device (10) being provided with a centrifugal barrel (1001), a plurality of holes (1004) being provided on the centrifugal barrel (1001) at a distance of 10 cm from the top in a circumferential direction, and an electric heating rod (1002) being installed at the bottom of the centrifugal barrel (1001); The separation device (6) comprises a separation barrel (601) and a feed pipe (602), wherein the feed pipe (602) is connected to the top of the separation barrel (601), a conical block (603) is provided on the inner bottom surface of the separation barrel (601), a support column (605) is connected to the lower surface of the separation barrel (601), and a plurality of feed holes (604) are provided on the circumferential edge of the conical block (603); The vacuum extraction device (8) comprises a vacuum extraction tube (801), the vacuum extraction tube (801) passes through the top of the separation device (6) and is connected to the centrifugal bucket (1001), and the upper end of the vacuum extraction tube (801) is connected to an air pump (802), and the front of the air pump (802) is connected to an air guide tube (803); Connecting blocks (904) are fixedly arranged on both sides of the movable cover plate (903); the lifting rod (902) is a threaded rod, and the lifting rod (902) penetrates and connects the connecting blocks (904); the contact surface between the connecting block (904) and the lifting rod (902) is designed with a threaded groove; the top of the lifting rod (902) is connected to a rotating motor (901), and the rotating motor (901) is fixedly installed on the top of the separation device (6); the induction block (905) is arranged directly below the lifting rod (902), and the induction block (905) is fixedly installed on the inner wall of the separation device (6).
2. The mixing and stirring equipment for refining coix seed oil according to claim 1, characterized in that: The reaction device (2) comprises a reaction barrel (201) and a stirrer (203) mounted on a tripod (1); a feeding port (202) is arranged on the top of the reaction barrel (201); the stirrer (203) is arranged in the reaction barrel (201); a servo motor (204) is installed on the bottom surface of the reaction barrel (201); and the servo motor (204) is connected to a ball valve (205).
3. The mixing and stirring equipment for refining coix seed oil according to claim 1, characterized in that: The water cooling device (3) comprises a water tank (301), a controller (302) is installed on the upper surface of the water tank (301), and water pumps (303) are connected to both sides of the upper surface of the water tank (301), the water pump (303) is connected to a water pipe (304), and the water pipe (304) is connected to the negative pressure transmission device (5).
4. The mixing and stirring equipment for refining coix seed oil according to claim 1, characterized in that: The negative pressure transmission device (5) comprises a negative pressure pump (501) and a double-layer pipeline (503), wherein the negative pressure pump (501) is connected to a single-layer structure pipeline (502), the double-layer pipeline (503) is connected between the single-layer structure pipelines (502), and the decolorization tube (4) is arranged between the double-layer pipeline (503) and the single-layer structure pipeline (502).
5. The mixing and stirring equipment for refining coix seed oil according to claim 1, characterized in that: The collecting device (7) comprises two symmetrical arc-shaped containing boxes (701), wherein the symmetrical arc-shaped containing boxes (701) are arranged directly below the separating device (6), a connecting groove (703) is arranged on a straight side surface of the arc-shaped containing box (701) close to the rear end of the separating device (6), and a connecting column (702) is arranged on a straight side surface of the arc-shaped containing box (701) close to the front end of the separating device (6).
6. The mixing and stirring equipment for refining coix seed oil according to claim 1, characterized in that: The centrifugal device (10) comprises a centrifugal bucket (1001), an electric heating rod (1002) and holes (1004); the centrifugal bucket (1001) is provided with a plurality of holes (1004) at a distance of 10 cm from the top in the circumferential direction; the bottom of the centrifugal bucket (1001) is provided with an electric heating rod (1002); the electric heating rod (1002) is installed at the bottom of the centrifugal bucket (1001); the bottom of the centrifugal bucket (1001) is connected to a rotating shaft (1003); and the rotating shaft (1003) is connected to a rotating host (1005).
Citation Information
Patent Citations
Pure steam deodorization refining method for coix seed oil
CN109055005A
Olive oil refining process and system
CN115368967A