A washing device for preparing stannous methanesulfonate crystals and a method of use

By designing an automated stannous methanesulfonate crystal washing device, which utilizes a combination of multiple washing rollers and filters, automated dry and wet washing and air drying of the crystals are achieved, solving the problems of time-consuming and labor-intensive processes in existing technologies and improving washing efficiency and the utilization rate of distilled water.

CN117816641BActive Publication Date: 2026-05-12CHINA TIN NONFERROUS METALS CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
CHINA TIN NONFERROUS METALS CO LTD
Filing Date
2023-12-14
Publication Date
2026-05-12

AI Technical Summary

Technical Problem

Existing stannous methanesulfonate crystal washing devices leave distilled water residue on the crystal surface after washing, requiring manual cleaning and adding a drying process, which is time-consuming and labor-intensive.

Method used

A washing device comprising upper and lower bodies, a filter box, a washing chamber, and a conveying shell was designed. Multiple washing rollers and filters are driven by a programmable controller to achieve automatic sorting, wet and dry washing, and air drying of crystals, reducing manual intervention.

Benefits of technology

The automated washing and drying of stannous methanesulfonate crystals has been achieved, saving time and labor, reducing the workload of subsequent staff, and improving washing efficiency and the recycling rate of distilled water.

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Abstract

The application discloses a kind of stannous methanesulfonate crystal preparation washing device, belong to stannous methanesulfonate crystal preparation technical field, including: up and down fixed upper body and lower body, the upper body top is provided with placing opening, the placing opening inside thread is connected with cover plate, the upper body inside is connected with filter box body just below cover plate, the lower body outer wall is fixed with programmable controller;The application is conveyed by the rotation of multiple washing rollers in upper conveying shell and lower conveying shell to realize the dry and wet washing and dry of stannous methanesulfonate crystal, compared with prior art, without subsequent wiping stannous methanesulfonate crystal surface washing left moisture by staff, time-saving and labor-saving, multiple first filter screens are simultaneously provided, self-classification is carried out to stannous methanesulfonate crystal before washing, reduce the workload of subsequent staff sorting.
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Description

Technical Field

[0001] This invention belongs to the field of stannous methanesulfonate crystal preparation technology, specifically relating to a washing device and method for preparing stannous methanesulfonate crystals. Background Technology

[0002] Stannous methanesulfonate, a white crystalline solid at room temperature, is widely used in electroplating and other electronic industries, including brush plating and bath plating, due to its stable plating solution, low corrosiveness, low toxicity, and low bubble production. However, during the production of stannous methanesulfonate crystals, a washing device is needed to remove surface impurities. Patent No. 202021926809.4 discloses a crystal washing and filtering device, consisting of a washing pot supported by a support frame, a stirring mechanism extending into the washing pot supported by a support base, and a filtering mechanism mounted on the top of the washing pot and extending into the washing pot above the stirring mechanism. During washing and filtering, the crystals are placed inside the filtering structure, and the stirring mechanism is controlled to agitate distilled water, accelerating its flow and removing impurities from the crystal surface. After washing, the filtering mechanism is removed, followed by the crystals. However, this device leaves distilled water residue on the crystal surface after washing, which spills onto the outer surface of the device after removal, requiring manual cleaning. Furthermore, a drying process is added after the crystals are removed, which is time-consuming and labor-intensive, and requires improvement. Summary of the Invention

[0003] The purpose of this invention is to solve the above-mentioned technical problems and provide a washing device and method for preparing stannous methanesulfonate crystals, which is time-saving, labor-saving and reduces the workload of subsequent staff.

[0004] To achieve the above objectives, the technical solution adopted by the present invention is as follows:

[0005] A washing apparatus for preparing stannous methanesulfonate crystals includes: an upper body and a lower body fixedly connected vertically; the upper body has a placement opening at its top, and a cover plate is threaded into the placement opening; a filter box is connected to the interior of the upper body directly below the cover plate; a programmable controller is fixedly connected to the outer wall of the lower body; the lower body has sorting chambers communicating with the material discharge end of the filter box, arranged from near to far from the upper body; multiple connecting openings are equally spaced from top to bottom; and washing chambers are arranged from top to bottom with the same number of connecting openings, each corresponding to the other. A first filter screen is placed above each connecting opening in the sorting chamber; a partition is placed inside each connecting opening; and a receiving slot is provided below each partition in the lower body. Multiple first filters and multiple... A first drive mechanism is assembled between the partition and the lower body to drive multiple first filter screens to rotate, and multiple connecting ports are stored in corresponding storage slots. The washing chamber consists of a front rectangular cavity, a middle inverted trapezoidal cavity containing washing distilled water, and a rear rectangular cavity. A lower conveying shell is fixedly connected to the bottom of the washing chamber. An upper conveying shell is connected to the washing chamber above the lower conveying shell. Multiple washing rollers are placed at equal intervals inside the lower and upper conveying shells. A second drive mechanism is assembled on the lower and upper conveying shells to drive the multiple washing rollers on the lower and upper conveying shells to move in the same direction. A collection box is fixedly connected to the outer wall of the lower body away from the sorting chamber, below each lower conveying shell. The first drive mechanism and the second drive mechanism are connected to the programmable controller by wires.

[0006] Preferably, the first drive mechanism includes a third support plate fixed to the lower body, a plurality of first drive shafts placed inside the sorting chamber in the same number as the first filter screen, and a fourth support plate fixed to one side of the partition. A fourth motor is fixedly connected to the top of the third support plate, and a first conical wheel is fixedly sleeved on the output shaft end of the fourth motor. The first filter screen is fixedly sleeved on the outside of the first drive shaft. One end of the first drive shaft extends through the lower body to the outside. The first drive shaft is connected to the through section of the lower body through a bearing, and the other end of the first drive shaft is connected to the inner wall of the lower body through a bearing. The section extending to the outside is fixedly connected to a first pulley and a third gear from the side closest to the lower body to the side furthest away. A first transmission belt is connected to the multiple first pulleys by frictional transmission. The uppermost first drive shaft extending to the outside is fixedly sleeved with a second conical wheel that meshes with the first conical wheel on the side of the third gear furthest from the first pulley. A slot is opened on the lower body corresponding to each fourth support plate position. Multiple fourth support plates extend to the outside through the corresponding slots and are fixedly connected to the top of a second rack that meshes with the third gear. The fourth motor is connected to the programmable controller by wires.

[0007] Preferably, the second drive module includes a fifth support plate fixedly connected to the lower and upper conveying housings, a plurality of second drive shafts equally spaced within the lower and upper conveying housings, and a plurality of auxiliary shafts connected to the lower and upper conveying housings via bearings for auxiliary operation. A fifth motor is fixedly connected to the fifth support plate, and a third conical wheel is fixedly sleeved at the output shaft end of the fifth motor. One end of the second drive shaft extends through the lower and upper conveying housings to the outside and is fixedly sleeved with a second pulley. The second drive shaft is connected to the through section of the lower and upper conveying housings via bearings, and the other end of the second drive shaft is connected to the inner wall of the lower and upper conveying housings via bearings. A washing roller is fixedly sleeved outside the second drive shaft at the same position. A second transmission belt is frictionally connected between the plurality of second pulleys on the lower and upper conveying housings. A fourth conical wheel, meshing with the third conical wheel, is fixedly sleeved on the second drive shaft on the side of the lower and upper conveying housings closest to the third conical wheel and away from the second pulley. An auxiliary wheel is fixedly sleeved outside the auxiliary shaft. The fifth motor is connected to the programmable controller via wires.

[0008] Preferably, a rotating mechanism is assembled between the filter box and the upper body. A bottom support platform is fixedly connected to the bottom of the filter box inside the upper body. Two impurity outlets are symmetrically opened between the inner wall of the upper body and the bottom support platform at the bottom of the upper body. A closing mechanism is assembled inside the upper body and the bottom support platform to drive the filter box discharge end and the impurity outlet discharge end to open or close. A second support plate is fixedly connected to the outer wall of the lower body at the position of each washing chamber. A first impurity collection box and a first gas collection box are fixedly connected to the rectangular cavity side of the second support plate from near to far from the front of the washing chamber. The pump has an air inlet pipe fixedly connected to the first impurity collection box away from the end wall of the first air pump. A filter is fixedly connected between the first impurity collection box and the first air pump. Multiple air intakes are provided at equal intervals between the lower conveying shell and the upper conveying shell in the rectangular cavity at the front of each washing chamber on the lower body. The two ends of the air intake pipe are respectively connected to the washing chamber. Impurity inlet pipes are fixedly connected to the bottom end of the impurity outlet, the bottom end of the sorting chamber on the lower body, and the bottom end of the first impurity collection box. The other end of the impurity inlet pipe is equipped with a suction collection mechanism. The rotating mechanism, the sealing mechanism, and the suction collection mechanism are connected to the programmable controller by wires.

[0009] Preferably, the rotating mechanism includes a third motor fixed to the top of the upper body, a gear ring fixedly sleeved on the top of the outer wall of the filter box, and two support rings with arc-shaped rolling grooves fixed to the inner wall of the upper body and the outer wall of the filter box. The output shaft of the third motor extends into the interior of the upper body and is fixedly sleeved with a second gear that meshes with the gear ring. Multiple rollers are fixedly and evenly spaced along the circumference in the arc-shaped rolling groove of the support ring on the outer wall of the filter box. Balls extending into the arc-shaped rolling groove of the support ring on the inner wall of the upper body are rolledly connected to the rollers through an open sleeve. The third motor is connected to the programmable controller by wires.

[0010] Preferably, the sealing mechanism includes two second motors fixed to the outer wall of the upper body and a cavity opened inside the bottom support platform. Two third drive shafts are symmetrically placed inside the cavity. One end of the third drive shaft is connected to the output shaft of the second motor through a coupling, and the other end of the third drive shaft is connected to the inner wall of the bottom support platform through a bearing. A first gear is fixedly sleeved on the third drive shaft. Two upper sealing plates for sealing the material discharge end of the filter box are symmetrically placed above the two first gears inside the cavity. Two lower sealing plates for sealing the impurity discharge end of the impurity outlet are symmetrically placed below the two first gears inside the cavity. The bottom end of the upper sealing plate and the top end of the lower sealing plate are respectively provided with an assembly groove, and a first rack that meshes with the first gear on the same side is fixed in the assembly groove. Limiting grooves are respectively opened inside the two upper sealing plates and the two lower sealing plates on the opposite sides. Multiple limiting rods extending into the corresponding limiting grooves are fixed to the inner walls of the upper body and the bottom support platform. The second motors are connected to the programmable controller by wires.

[0011] Preferably, the exhaust and collection mechanism includes a second impurity collection box fixedly connected to the lower body and communicating with the impurity inlet pipe. The top of the second impurity collection box has an adsorption port, and a second filter screen is fixedly connected inside the adsorption port. A second air pump is placed at the top of the second impurity collection box, and the air inlet of the second air pump is connected to the adsorption port. An opening and closing plate is placed at the impurity cleaning end of the second impurity collection box. A connecting shaft is rotatably connected between the top of the opening and closing plate and the second impurity collection box. The second air pump is connected to a programmable controller by a wire.

[0012] Preferably, the first air pump outlet end is fixedly connected to an air outlet pipe, and the lower body has multiple air inlets with both ends connected to the air outlet pipe and the washing chamber respectively, located in the rectangular cavity at the rear of each washing chamber.

[0013] Preferably, a lifting mechanism is assembled between the upper conveying housing and the lower machine body, extending from the outer section of the upper conveying housing. The lifting mechanism includes two first support plates symmetrically fixed to the lower machine body and a movable seat fixed to the side wall of the upper conveying housing. A first motor is fixed to the top of the upper first support plate, and a screw is placed between the two first support plates. One end of the screw is connected to the output shaft of the first motor through a coupling, and the other end of the screw is connected to the inner wall of the lower first support plate through a bearing. The movable seat is driven to the screw through a transmission nut, and the first motor is connected to the programmable controller by wires.

[0014] A method of using a washing apparatus for preparing stannous methanesulfonate crystals includes the following steps:

[0015] S1: Unscrew the cover plate, add an appropriate amount of stannous methanesulfonate crystals into the filter box through the placement port, and tighten the cover plate.

[0016] S2: The third motor is started by the programmable controller. The output shaft of the third motor drives the second gear to rotate, which in turn drives the gear ring to rotate. The gear ring drives the filter box to rotate. Impurities on the surface of the stannous methanesulfonate crystals in the filter box are thrown into the upper body under the action of centrifugal force, achieving preliminary impurity removal. When the set time is up, the third motor is stopped by the programmable controller, and at the same time, the two second motors are started. The output shafts of the two second motors rotate in opposite directions, which in turn drive the two third drive shafts to rotate in opposite directions. The two third drive shafts drive the two first gears to rotate in opposite directions. During the reverse rotation of the two first gears, the two upper sealing plates move away from each other, and the two lower sealing plates move closer to each other, until the set time is reached and they stop. At this time, the filter box discharge port opens and the two impurity outlets open. The stannous methanesulfonate crystals enter the sorting chamber through the discharge port, and the impurities enter the impurity inlet pipe through the impurity outlet.

[0017] S3: The stannous methanesulfonate crystals entering the sorting chamber fall under their own gravity and are sorted by the first filter screens of different mesh sizes. After a set time, the programmable controller activates the fourth motor. The fourth motor drives the output shaft to rotate forward, causing the first conical wheel to rotate forward. The first conical wheel drives the second conical wheel to rotate forward, which in turn drives the connected first drive shaft to rotate forward. The first drive shaft drives the connected third gear, first pulley, and first filter screen to rotate. The connected first pulley drives the first transmission belt to rotate via friction transmission. The first transmission belt drives other first pulleys to rotate via friction transmission, and the other first pulleys drive the connected third gear, first pulley, and first filter screen to rotate. When one drive shaft rotates, other first drive shafts drive the connected third gear and first filter screen to rotate. During the rotation of the third gear, the second rack moves downward, and the second rack moves the fourth support plate in the same direction. The fourth support plate moves the partition in the same direction and stores it in the storage slot. The first drive shaft drives the first filter screen to rotate. When the set time is up, the partition is stored in the storage slot and the inclined bottom end of the first filter screen is flush with the lower conveying housing. That is, the stannous methanesulfonate crystals on the first filter screen roll down between the corresponding lower and upper conveying housings. The programmable controller controls the fifth motor on the lower and upper conveying housings to start. The fifth motor drives the third conical wheel to rotate. The wheel drives the fourth conical wheel to rotate, which in turn drives the connected second drive shaft to rotate. The second drive shaft then drives the connected washing roller and second pulley to rotate. The second pulley, through friction transmission, drives the connected second transmission belt to rotate. This second transmission belt, through friction transmission, drives other second pulleys to rotate. These other second pulleys then drive the connected second drive shaft to rotate, which in turn drives the connected washing roller to rotate. This achieves the unidirectional rotation of multiple washing rollers on the lower and upper conveyor housings, transporting the stannous methanesulfonate crystals along the inner wall curves of the lower and upper conveyor housings. When the stannous methanesulfonate crystals are in the front rectangular cavity, they... The programmable controller controls the start of the first air pump. The first air pump draws air to create a negative pressure state in the filter, the first impurity collection box, and the air inlet pipe. This draws the impurities removed from the stannous methanesulfonate crystals by the washing rollers into the first impurity collection box and into the impurity inlet pipe. When the stannous methanesulfonate crystals are in the middle trapezoidal cavity, distilled water and the washing rollers work together to clean the stubborn stains on the surface. When the stannous methanesulfonate crystals are in the rear rectangular cavity, the rolling washing rollers clean the distilled water remaining on the surface of the stannous methanesulfonate crystals. At the same time, the air from the outlet of the first air pump dries the stannous methanesulfonate crystals and the washing rollers through the outlet pipe and the air inlet. After the process is completed, the crystals fall into the collection box for collection.

[0018] S4: The second air pump is started by the programmable controller. The second air pump draws in the second impurity collection box and the impurity inlet pipe to form a negative pressure. The dust in the impurity inlet pipe enters the second impurity collection box and waits to be cleaned.

[0019] S5: If it is necessary to adjust the height of the upper conveyor housing during the above process, the programmable controller controls the first motor to start. The first motor drives the output shaft to rotate, which in turn drives the screw to rotate. During the rotation of the screw, the movable seat moves on the screw, which in turn moves the upper conveyor housing to achieve adjustment.

[0020] Compared with the prior art, the beneficial effects of the present invention are:

[0021] 1. This invention achieves the conveying, wet washing, and drying of stannous methanesulfonate crystals by rotating multiple washing rollers inside the upper and lower conveying housings. Compared with the prior art, it eliminates the need for workers to wipe the surface of the stannous methanesulfonate crystals to remove the water left by washing, saving time and effort. At the same time, multiple first filters are set up to self-sort the stannous methanesulfonate crystals before washing, reducing the workload of subsequent sorting by workers.

[0022] 2. The present invention provides a communication port between the first filter screen and the washing chamber, and a retractable partition is provided in the communication port. At the same time, a first driving mechanism is provided between the first filter screen and the retractable partition, which can realize the function of automatically retracting the retractable partition when the first filter screen flips and abuts against the lower conveying shell, so as to avoid affecting the filtration effect and facilitate the feeding between the upper and lower conveying shells.

[0023] 3. The filter box of this invention is set to be rotary and has an impurity outlet. Before being sorted, the stannous methanesulfonate crystals are centrifuged by rotation to remove surface impurities. At the same time, an adsorption mechanism is set in the rectangular cavity at the front of the washing chamber to remove surface impurities from the stannous methanesulfonate crystals before they are washed with water. This removes most of the surface impurities from the stannous methanesulfonate crystals before they are washed with water, thereby improving the recycling rate of the washing distilled water.

[0024] 4. The present invention provides a blowing mechanism in the rectangular cavity at the rear of the washing chamber, which can dry the stannous methanesulfonate crystal, improve the drying efficiency of the stannous methanesulfonate crystal, and at the same time dry the washing roller so that the washing roller can roll and wipe away the residual moisture on the surface of the stannous methanesulfonate crystal. Attached Figure Description

[0025] Figure 1 This is a right view of a washing apparatus for preparing stannous methanesulfonate crystals according to the present invention.

[0026] Figure 2 This is a vertical sectional view of a washing apparatus for preparing stannous methanesulfonate crystals according to the present invention;

[0027] Figure 3 This is a vertical sectional view of the upper body of the present invention;

[0028] Figure 4 This is a schematic diagram of the first driving mechanism of the present invention;

[0029] Figure 5 This is a schematic diagram of the second driving mechanism of the present invention;

[0030] Figure 6 For the present invention Figure 5 Right view;

[0031] Figure 7 This is a partial structural rear view of the present invention;

[0032] Figure 8 For the present invention Figure 2 Enlarged view of point A in the middle;

[0033] Reference numerals: 1-Upper body, 2-Lower body, 3-Washing chamber, 4-Collection box, 5-Programmable controller, 6-Screw, 7-First support plate, 8-First air pump, 9-First motor, 10-Second support plate, 11-Outlet pipe, 12-Modible seat, 13-Second motor, 14-Impurity inlet pipe, 15-Classification chamber, 16-First drive shaft, 17-Partition plate, 18-Collection slot, 19-First filter screen, 20-Connecting port, 21-Air inlet, 22-Washing roller, 23-Second drive shaft, 24-Lower conveyor housing, 25-Upper conveyor housing, 26-Air inlet, 27-Ball bearing, 28-Filter box, 29-Bottom support platform, 30-Impurity outlet, 31-Limiting rod, 32-Limiting groove, 33-Lower sealing plate, 34-Third drive shaft, 35-Cavity, 36-First gear, 37-First tooth 38-Upper sealing plate, 39-Support ring, 40-Roller, 41-Second gear, 42-Third motor, 43-Cover plate, 44-Placement port, 45-Gear ring, 46-Third support plate, 47-Fourth motor, 48-First conical wheel, 49-Second conical wheel, 50-First transmission belt, 51-Second rack, 52-Fourth support plate, 53-First pulley, 54-Third gear, 55-Second pulley, 56-Second transmission belt, 57-Fifth motor, 58-Third conical wheel, 59-Fourth conical wheel, 60-Fifth support plate, 61-Auxiliary wheel, 62-Auxiliary shaft, 63-Air inlet pipe, 64-First impurity collection box, 65-Filter, 66-Second impurity collection box body, 67-Adsorption port, 68-Second filter screen, 69-Opening and closing plate, 70-Connecting shaft, 71-Second air pump. Detailed Implementation

[0034] The technical solutions of the present invention will be clearly and completely described below with reference to the accompanying drawings of the embodiments of the present invention. Obviously, the described embodiments are only some embodiments of the present invention, and not all embodiments. Example 1:

[0035] Please see Figure 1-8A washing apparatus for preparing stannous methanesulfonate crystals includes: an upper body 1 and a lower body 2 fixedly connected vertically. The upper body 1 has a placement opening 44 at its top, with a cover plate 43 threadedly connected inside the placement opening 44. A filter box 28 is connected inside the upper body 1 directly below the cover plate 43. A programmable controller 5 is fixedly connected to the outer wall of the lower body 2. The lower body 2 has sorting chambers 15 connected to the material discharge end of the filter box 28, arranged from near to far from the upper body 1, and other chambers spaced at equal intervals from top to bottom. The system includes multiple connecting ports 20 and washing chambers 3 arranged from top to bottom, with the same number of connecting ports 20 and connected to each other. Inside the sorting chamber 15, above each connecting port 20, a first filter screen 19 is placed. The mesh size of the first filter screens 19 decreases sequentially from top to bottom. Inside each connecting port 20, a partition 17 is placed. Inside the lower body 2, below each partition 17, a storage slot 18 is provided. The multiple first filters 19, multiple partitions 17, and the lower body 15... The lower body 2 is equipped with a first drive mechanism that drives multiple first filter screens 19 to rotate and multiple connecting ports 20 to be stored in corresponding storage slots 18. The washing chamber 3 consists of a front rectangular chamber, a middle inverted trapezoidal chamber containing washing distilled water, and a rear rectangular chamber. The lower body 2 is fixed with an inlet pipe and an outlet pipe with valves at the positions corresponding to the middle inverted trapezoidal chamber. The bottom of the washing chamber 3 is fixed with a lower conveying housing 24. The washing chamber 3 is connected to an upper conveying housing 25 above the lower conveying housing 24. Multiple washing rollers 22 are placed at equal intervals inside the lower and upper conveying housings 24 and 25. The lower and upper conveying housings 24 and 25 are respectively equipped with a second drive mechanism that drives the multiple washing rollers 22 on the lower and upper conveying housings 24 and 25 to move in the same direction. The outer wall of the lower body 2 away from the sorting chamber 15 is fixed with a collection box 4 below each lower conveying housing 24. The first drive mechanism and the second drive mechanism are connected to the programmable controller 5 by wires.

[0036] Specifically, the first drive mechanism includes a third support plate 46 fixed to the lower body 2, multiple first drive shafts 16 placed inside the sorting chamber 15 in the same number as the first filter screen 19, and a fourth support plate 52 fixed to one side of the partition plate 17. A fourth motor 47 is fixedly connected to the top of the third support plate 46, and a first conical wheel 48 is fixedly sleeved on the output shaft end of the fourth motor 47. The first filter screen 19 is fixedly sleeved on the outside of the first drive shafts 16. One end of the first drive shaft 16 extends through the lower body 2 to the outside. The first drive shaft 16 is connected to the through section of the lower body 2 through a bearing, and the other end of the first drive shaft 16 is connected to the inner wall of the lower body 2 through a bearing. The shaft 16 extends to the outside and is fixedly connected to the first pulley 53 and the third gear 54 from the side closest to the lower body 2. The first pulleys 53 are connected by friction transmission with the first transmission belt 50. The uppermost first drive shaft 16 extends to the outside and is fixedly sleeved on the side of the third gear 54 away from the first pulley 53 with the second conical wheel 49 meshing with the first conical wheel 48. The lower body 2 has slots corresponding to the positions of each fourth support plate 52. The multiple fourth support plates 52 extend to the outside through the corresponding slots and are fixedly connected to the top of the second rack 51 meshing with the third gear 54. The fourth motor 47 is connected to the programmable controller 5 by wires.

[0037] Specifically, the second drive module includes a fifth support plate 60 fixedly attached to the lower conveying housing 24 and the upper conveying housing 25, a plurality of second drive shafts 23 equally spaced within the lower conveying housing 24 and the upper conveying housing 25, and a plurality of auxiliary shafts 62 connected to the lower conveying housing 24 and the upper conveying housing 25 via bearings for auxiliary operation. A fifth motor 57 is fixedly attached to the fifth support plate 60, and a third conical wheel 58 is fixedly sleeved on the output shaft end of the fifth motor 57. One end of the second drive shaft 23 extends through the lower conveying housing 24 and the upper conveying housing 25 to the outside and is fixedly sleeved with a second pulley 55. The second drive shaft 23 is connected to the lower conveying housing 24 and the upper conveying housing 25 via bearings. The conveying housing 25 is connected through the section. The other end of the second drive shaft 23 is connected to the inner wall of the lower conveying housing 24 and the upper conveying housing 25 through a bearing. The washing roller 22 is fixedly sleeved on the outside of the second drive shaft 23 at the same position. The lower conveying housing 24 and the upper conveying housing 25 are connected by a second transmission belt 56 through friction transmission between multiple second pulleys 55. The lower conveying housing 24 and the upper conveying housing 25 are respectively fixedly sleeved on the second drive shaft 23 on the side away from the second pulley 55, and are respectively engaged with the third conical wheel 58. The auxiliary shaft 62 is fixedly sleeved on the outside of the auxiliary wheel 62. The fifth motor 57 is connected to the programmable controller 5 by wires.

[0038] A method of using a washing apparatus for preparing stannous methanesulfonate crystals includes the following steps:

[0039] S1: Unscrew the cover plate 43, add an appropriate amount of stannous methanesulfonate crystals into the filter box 28 through the placement port 44, and tighten the cover plate 43.

[0040] S2: Stannous methanesulfonate crystals inside the filter housing 28 enter the sorting chamber 15 through the discharge port;

[0041] S3: The stannous methanesulfonate crystals entering the sorting chamber 15 fall under their own gravity and are sorted by the first filter screen 19 of different mesh sizes. After a set time, the programmable controller 5 controls the fourth motor 47 to start. The fourth motor 47 drives the output shaft to rotate forward, causing the first conical wheel 48 to rotate forward. The first conical wheel 48 drives the second conical wheel 49 to rotate forward. The second conical wheel 49 drives the connected first drive shaft 16 to rotate forward. The first drive shaft 16 drives the connected third gear 54, the first pulley 53, and the first filter screen 19 to rotate. The connected first pulley 53 drives the first transmission belt 50 to rotate via friction transmission. Belt 50 drives other first pulleys 53 to rotate via friction transmission. These first pulleys 53 drive the connected first drive shaft 16 to rotate. The first drive shaft 16 drives the connected third gear 54 and first filter screen 19 to rotate. During the rotation of the third gear 54, the second rack 51 moves downwards, causing the fourth support plate 52 to move in the same direction. The fourth support plate 52 then moves the partition 17 in the same direction, allowing it to be stored in the storage groove 18. The first drive shaft 16 drives the first filter screen 19 to rotate. When the set time is reached, the partition 17 is stored in the storage groove 18, and the inclined bottom end of the first filter screen 19 is flush with the lower conveying housing 24. The stannous methanesulfonate crystals roll down between the corresponding lower conveyor housing 24 and upper conveyor housing 25. The programmable controller 5 starts the fifth motor 57 on both the lower and upper conveyor housings. The fifth motor 57 drives the third conical wheel 58 to rotate, which in turn drives the fourth conical wheel 59. The fourth conical wheel 59 drives the connected second drive shaft 23 to rotate, which in turn drives the connected washing roller 22 and the second pulley 55 to rotate. The connected second pulley 55 drives the connected second transmission belt 56 to rotate via friction transmission, and the connected second transmission belt 56 drives the other second pulleys 55 to rotate via friction transmission. The other second pulleys 55 drive the connected second drive shaft 23 to rotate, and the connected second drive shaft 23 drives the connected washing roller 22 to rotate, so that the multiple washing rollers 22 on the lower conveying housing 24 and the upper conveying housing 25 can rotate in the same direction. The stannous methanesulfonate crystals are conveyed along the inner wall curve of the lower conveying housing 24 and the upper conveying housing 25. When the stannous methanesulfonate crystals are in the middle inverted trapezoidal cavity, the distilled water and the washing roller 22 work together to clean the stubborn stains on the surface. When the stannous methanesulfonate crystals are in the rear rectangular cavity, the rolling washing roller 22 cleans the distilled water remaining on the surface of the stannous methanesulfonate crystals. After the cleaning is completed, the crystals fall into the collection box 4 for collection. Example 2:

[0042] The difference between this embodiment and Embodiment 1 is that:

[0043] A rotating mechanism is installed between the filter box 28 and the upper body 1. A bottom support platform 29 is fixedly connected to the bottom of the filter box 28 inside the upper body 1. Two impurity outlets 30 are symmetrically opened between the inner wall of the upper body 1 and the bottom support platform 29 at the bottom of the upper body 1. A closing mechanism is installed inside the upper body 1 and the bottom support platform 29 to drive the opening or closing of the material discharge end of the filter box 28 and the impurity discharge end of the impurity outlets 30. A second support plate 10 is fixedly connected to the outer wall of the lower body 2 at the location of each washing chamber 3. A first impurity collection box 64 and a first air pump 8 are fixedly connected to the rectangular cavity side of the top of the second support plate 10 from near to far from the front of the washing chamber 3. An air inlet pipe 63 is fixedly connected to the end wall of the first impurity collection box 64 away from the first air pump 8. A filter 65 is fixedly connected between an impurity collection box 64 and a first air pump 8. The filter 65 consists of a tubular shell fixed at both ends between the first impurity collection box 64 and the first air pump 8 and a filter screen fixed inside the tubular shell. Multiple air inlets 21 are provided at equal intervals between the lower conveying shell 24 and the upper conveying shell 25 in the rectangular cavity at the front of each washing chamber 3 on the lower body 2. The two ends of the air inlet 21 are respectively connected to the air inlet pipe 63 and the washing chamber 3. Impurity inlet pipes 14 are fixedly connected to the bottom of the impurity outlet 30, the bottom of the sorting chamber 15 on the lower body 2, and the bottom of the first impurity collection box 64. The other end of the impurity inlet pipe 14 is equipped with a suction collection mechanism. The rotating mechanism, the sealing mechanism, and the suction collection mechanism are connected by wires to the programmable controller 5.

[0044] The rotating mechanism includes a third motor 42 fixed to the top of the upper body 1, a gear ring 45 fixedly sleeved on the top of the outer wall of the filter box 28, and two support rings 39 with arc-shaped rolling grooves fixed to the inner wall of the upper body 1 and the outer wall of the filter box 28. The output shaft of the third motor 42 extends into the interior of the upper body 1 and is fixedly sleeved with a second gear 41 that meshes with the gear ring 45. Multiple rollers 40 are fixedly and evenly spaced along the circumference in the arc-shaped rolling groove of the support ring 39 on the outer wall of the filter box 28. Roller balls 27 extending into the arc-shaped rolling groove of the support ring 39 on the inner wall of the upper body 1 are rolled on the rollers 40 by means of open sleeve connection. The third motor 42 is connected to the programmable controller 5 by wires.

[0045] The sealing mechanism includes two second motors 13 fixed to the outer wall of the upper body 1 and a cavity 35 opened inside the bottom support platform 29. Two third drive shafts 34 are symmetrically placed inside the cavity 35. One end of each third drive shaft 34 is connected to the output shaft of the second motor 13 via a coupling, and the other end is connected to the inner wall of the bottom support platform 29 via a bearing. A first gear 36 is fixedly sleeved on each third drive shaft 34. Two upper sealing plates 38 for the material discharge ends of the sealed filter boxes 28 are symmetrically placed above the two first gears 36 inside the cavity 35. Inside the upper closed plate 38, two closed impurity outlets 30 with impurity dropping ends are symmetrically placed below the two first gears 36. The bottom of the upper closed plate 38 and the top of the lower closed plate 33 are respectively provided with assembly grooves, and the first rack 37 that meshes with the first gear 36 on the same side is fixed in the assembly grooves. Limiting grooves 32 are respectively provided in the interior of the two upper closed plates 38 and the lower closed plate 33 on the side away from each other. Multiple limiting rods 31 extending into the corresponding limiting grooves 32 are fixed to the inner walls of the upper body 1 and the bottom support platform 29. The second motor 13 is connected to the programmable controller 5 by wires.

[0046] The exhaust collection mechanism includes a second impurity collection box 66 fixedly connected to the lower body 2 and connected to the impurity inlet pipe 14. The top of the second impurity collection box 66 is provided with an adsorption port 67. A second filter screen 68 is fixedly connected inside the adsorption port 67. A second air pump 71 is placed at the top of the second impurity collection box 66. The air inlet of the second air pump 71 is connected to the adsorption port 67. An opening and closing plate 69 is placed at the impurity cleaning end of the second impurity collection box 66. A connecting shaft 70 is rotatably connected between the top of the opening and closing plate 69 and the second impurity collection box 66. The second air pump 71 is connected to the programmable controller 5 by wires.

[0047] A method of using a washing apparatus for preparing stannous methanesulfonate crystals further includes the following steps:

[0048] S1: Before the stannous methanesulfonate crystals enter the sorting chamber 15, the third motor 42 is started by the programmable controller 5. The third motor 42 drives the output shaft to rotate, which in turn drives the second gear 41 to rotate. The second gear 41 drives the gear ring 45 to rotate, which in turn drives the filter box 28 to rotate. Impurities on the surface of the stannous methanesulfonate crystals in the filter box 28 are propelled through the filter box 28 into the upper body 1 by centrifugal force. When the set time is up, the programmable controller 5 stops the third motor 42 and simultaneously starts the two second motors 13. 13 Drive output shaft rotates in the opposite direction, driving two third drive shafts 34 to rotate in the opposite direction. The two third drive shafts 34 drive two first gears 36 to rotate in the opposite direction. During the reverse rotation of the two first gears 36, the two upper sealing plates 38 move away from each other, and the two lower sealing plates 33 move closer to each other until the set time is reached and they stop. At this time, the material inlet of the filter box 28 opens and the two impurity outlets 30 open. Stannous methanesulfonate crystals enter the sorting chamber 15 through the material inlet, and impurities enter the impurity inlet pipe 14 through the impurity outlet 30, thus achieving preliminary impurity removal.

[0049] S2: When the stannous methanesulfonate crystal is in the front rectangular cavity, the programmable controller 5 controls the first air pump 8 to start. The first air pump 8 draws and makes the filter 65, the first impurity collection box 64 and the air inlet pipe 63 present a negative pressure state, adsorbing the impurities cleaned off by the washing roller 22 into the first impurity collection box 64 and into the impurity inlet pipe 14.

[0050] S3: The second air pump 71 is started by controlling the programmable controller 5. The second air pump 71 draws to create a negative pressure in the second impurity collection box 66 and the impurity inlet pipe 14. The dust in the impurity inlet pipe 14 enters the second impurity collection box 66 and waits to be cleaned. Example 3:

[0051] The difference between this embodiment and embodiment 2 is that:

[0052] Specifically, the first air pump 8 is fixedly connected to the air outlet pipe 11, and the lower body 2 has multiple air inlets 26 at equal intervals between the lower conveying housing 24 and the upper conveying housing 25 located in the rectangular cavity at the rear of each washing chamber 3. The air inlets are connected to the air outlet pipe 11 and the washing chamber 3 at their respective ends.

[0053] A method of using a washing apparatus for preparing stannous methanesulfonate crystals further includes the following steps:

[0054] S1: Air from the outlet of the first air pump 8 is used to dry the stannous methanesulfonate crystal and the washing roller 22 through the outlet pipe 11 and the inlet 26. Example 4:

[0055] The difference between this embodiment and embodiment 3 is that:

[0056] Specifically, a lifting mechanism is installed between the upper conveying housing 25 and the lower body 2, extending from the outer section of the upper conveying housing 25. The lifting mechanism includes two first support plates 7 symmetrically fixed to the lower body 2 and a movable seat 12 fixed to the side wall of the upper conveying housing 25. A first motor 9 is fixed to the top of the upper first support plate 7. A screw 6 is placed between the two first support plates 7. One end of the screw 6 is connected to the output shaft of the first motor 9 through a coupling, and the other end of the screw 6 is connected to the inner wall of the lower first support plate 7 through a bearing. The movable seat 12 is connected to the screw 6 through a transmission nut. The first motor 9 is connected to the programmable controller 5 by wires.

[0057] A method of using a washing apparatus for preparing stannous methanesulfonate crystals further includes the following steps:

[0058] S1: If it is necessary to adjust the height of the upper conveying housing 25 during the above process, the programmable controller 5 controls the first motor 9 to start. The first motor 9 drives the output shaft to rotate, which in turn drives the screw 6 to rotate. During the rotation of the screw 6, the movable seat 12 moves on the screw 6, which in turn drives the upper conveying housing 25 to move to achieve adjustment.

[0059] In the description of this invention, it should be understood that the terms "center," "longitudinal," "lateral," "front," "rear," "upper," "lower," "left," "right," "head," "tail," "vertical," "horizontal," "top," "bottom," "inner," and "outer," etc., indicating orientation or positional relationships, are based on the orientation or positional relationships shown in the accompanying drawings and are only for the convenience of describing this invention and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific orientation, or be constructed and operated in a specific orientation. Therefore, they should not be construed as limiting the scope of protection of this invention. It should also be noted that, unless otherwise explicitly specified and limited, terms such as "connected" and "linked" should be interpreted broadly. For example, it can refer to a fixed connection; a detachable connection; a point connection; a direct connection; or an indirect connection through an intermediate medium, which can enable communication between the internal parts of two elements. Those skilled in the art can understand the specific meaning of the above terms in this invention based on the specific circumstances. Device connection methods not described in detail in this invention are understood according to conventional connection methods in the art.

[0060] The above embodiments are merely specific examples to further illustrate the purpose, technical solution, and beneficial effects of the present invention, and the present invention is not limited thereto. Any modifications, equivalent substitutions, improvements, etc., made within the scope of the disclosure of the present invention are included within the protection scope of the present invention.

Claims

1. A washing apparatus for preparing stannous methanesulfonate crystals, characterized in that, include: An upper and lower body are fixedly connected. The upper body has a placement opening at its top, with a cover threaded into the opening. A filter box is connected to the interior of the upper body directly below the cover. A programmable controller is fixed to the outer wall of the lower body. Inside the lower body, from the side closest to the upper body, there are sorting chambers communicating with the material discharge end of the filter box; multiple connecting ports are equally spaced from top to bottom; and a washing chamber, the same number as the connecting ports, is also formed from top to bottom. A first filter screen is placed above each connecting port inside the sorting chamber, with the screen diameter decreasing sequentially from top to bottom. A partition is placed inside each connecting port. A storage slot is formed below each partition inside the lower body, housing multiple first filters and multiple... A first drive mechanism is assembled between the partition and the lower body to drive multiple first filter screens to rotate, and multiple connecting ports are stored in corresponding storage slots. The washing chamber is composed of a front rectangular cavity, a middle inverted trapezoidal cavity containing washing distilled water, and a rear rectangular cavity. A lower conveying shell is fixedly connected to the bottom of the washing chamber. An upper conveying shell is connected to the washing chamber above the lower conveying shell. Multiple washing rollers are placed at equal intervals inside the lower and upper conveying shells. A second drive mechanism is assembled on the lower and upper conveying shells to drive the multiple washing rollers on the lower and upper conveying shells to move in the same direction. A collection box is fixedly connected to the outer wall of the lower body away from the sorting chamber and below each lower conveying shell. The first drive mechanism and the second drive mechanism are connected to the programmable controller by wires. A rotating mechanism is assembled between the filter housing and the upper body. A bottom support platform is fixedly connected to the bottom of the filter housing inside the upper body. Two impurity outlets are symmetrically opened between the inner wall of the upper body and the bottom support platform at the bottom of the upper body. A closing mechanism is assembled inside the upper body and the bottom support platform to drive the opening or closing of the material discharge end of the filter housing and the impurity discharge end of the impurity outlet. A second support plate is fixedly connected to the outer wall of the lower body at the location of each washing chamber. A first impurity collection box and a first air pump are fixedly connected to the rectangular cavity side of the second support plate from near to far from the front of the washing chamber. An air inlet pipe is fixedly connected to the first impurity collection box away from the end wall of the first air pump. A filter is fixedly connected between the first impurity collection box and the first air pump. Multiple air intakes are provided at equal intervals between the lower conveying shell and the upper conveying shell in the rectangular cavity at the front of each washing chamber on the lower body. The two ends of the air intake pipe are respectively connected to the washing chamber. Impurity inlet pipes are fixedly connected to the bottom end of the impurity outlet, the bottom end of the sorting chamber on the lower body, and the bottom end of the first impurity collection box. An exhaust collection mechanism is installed at the other end of the impurity inlet pipe. The rotating mechanism, the sealing mechanism, and the exhaust collection mechanism are connected to the programmable controller by wires.

2. The washing apparatus for preparing stannous methanesulfonate crystals according to claim 1, characterized in that: The first drive mechanism includes a third support plate fixed to the lower body, multiple first drive shafts (the same number as the first filter screen) placed inside the sorting chamber, and a fourth support plate fixed to one side of the partition. A fourth motor is fixed to the top of the third support plate, and a first conical wheel is fixedly sleeved on the output shaft end of the fourth motor. The first filter screen is fixedly sleeved on the outside of the first drive shaft. One end of the first drive shaft extends through the lower body to the outside and is connected to the through section of the lower body through a bearing. The other end of the first drive shaft is connected to the inner wall of the lower body through a bearing. A first pulley and a third gear are fixedly connected to the section of the first drive shaft extending to the outside from the side closest to the lower body to the side away from the lower body, respectively. A first transmission belt is connected to the multiple first pulleys through friction transmission. A second conical wheel, meshing with the first conical wheel, is fixedly sleeved on the uppermost section of the first drive shaft extending to the outside, located on the side of the third gear away from the first pulley. A slot is opened on the lower body corresponding to each fourth support plate position. Multiple fourth support plates extend through the corresponding slots to the outside and are fixedly connected to the top of a second rack that meshes with the third gear. The fourth motor is connected to the programmable controller by wires.

3. The washing apparatus for preparing stannous methanesulfonate crystals according to claim 1, characterized in that: The second drive mechanism includes a fifth support plate fixed to the lower and upper conveying housings, multiple second drive shafts evenly spaced within the lower and upper conveying housings, and multiple auxiliary shafts connected to the lower and upper conveying housings via bearings for auxiliary operation. A fifth motor is fixed to the fifth support plate, and a third conical wheel is fixedly sleeved on the output shaft end of the fifth motor. One end of the second drive shaft extends through the lower and upper conveying housings to the outside and is fixedly sleeved with a second pulley. The second drive shaft is connected to the through section of the lower and upper conveying housings via bearings, and the other end of the second drive shaft is connected to the inner wall of the lower and upper conveying housings via bearings. A washing roller is fixedly sleeved outside the second drive shaft at the same position. A second transmission belt is frictionally connected between the multiple second pulleys on the lower and upper conveying housings. On the side of the second drive shaft near the third conical wheel on the lower and upper conveying housings, and away from the second pulley, fourth conical wheels that mesh with the third conical wheel are fixedly sleeved on the side of the second drive shaft away from the second pulley on the lower and upper conveying housings. An auxiliary wheel is fixedly sleeved outside the auxiliary shaft. The fifth motor is connected to the programmable controller via wires.

4. The washing apparatus for preparing stannous methanesulfonate crystals according to claim 1, characterized in that: The rotating mechanism includes a third motor fixed to the top of the upper body, a gear ring fixedly sleeved on the top of the outer wall of the filter box, and two support rings with arc-shaped rolling grooves fixed to the inner wall of the upper body and the outer wall of the filter box. The output shaft of the third motor extends into the interior of the upper body and is fixedly sleeved with a second gear that meshes with the gear ring. Multiple rollers are fixedly and evenly spaced along the circumference in the arc-shaped rolling groove of the support ring on the outer wall of the filter box. Balls extending into the arc-shaped rolling groove of the support ring on the inner wall of the upper body are rolledly connected to the rollers through an open sleeve. The third motor is connected to the programmable controller by wires.

5. The washing apparatus for preparing stannous methanesulfonate crystals according to claim 1, characterized in that: The sealing mechanism includes two second motors fixed to the outer wall of the upper body and a cavity inside the bottom support platform. Two third drive shafts are symmetrically placed inside the cavity. One end of each third drive shaft is connected to the output shaft of a second motor via a coupling, and the other end is connected to the inner wall of the bottom support platform via a bearing. A first gear is fixedly sleeved on each third drive shaft. Two upper sealing plates, representing the material discharge end of the sealed filter box, are symmetrically placed above the two first gears inside the cavity. Two lower sealing plates, representing the impurity discharge end of the sealed impurity outlet, are symmetrically placed below the two first gears inside the cavity. Assembly slots are respectively provided at the bottom of the upper sealing plate and the top of the lower sealing plate, and a first rack is fixed within each assembly slot to mesh with the first gear on the same side. Limiting slots are respectively provided on the sides of the two upper and lower sealing plates that are furthest from each other. Multiple limiting rods extending into the corresponding limiting slots are fixed to the inner walls of the upper body and the bottom support platform. The second motors are connected to a programmable controller via wires.

6. The washing apparatus for preparing stannous methanesulfonate crystals according to claim 1, characterized in that: The exhaust and collection mechanism includes a second impurity collection box fixedly connected to the lower body and connected to the impurity inlet pipe. The top of the second impurity collection box has an adsorption port, and a second filter screen is fixedly connected inside the adsorption port. A second air pump is placed at the top of the second impurity collection box, and the air inlet of the second air pump is connected to the adsorption port. An opening and closing plate is placed at the impurity cleaning end of the second impurity collection box. A connecting shaft is rotatably connected between the top of the opening and closing plate and the second impurity collection box. The second air pump is connected to a programmable controller by wires.

7. The washing apparatus for preparing stannous methanesulfonate crystals according to claim 1, characterized in that: The first air pump has an air outlet pipe fixedly connected to its air outlet end. The lower body has multiple air inlets at equal intervals between the lower conveying housing and the upper conveying housing in the rectangular cavity at the rear of each washing chamber. The air inlets are connected to the air outlet pipe and the washing chamber at their respective ends.

8. The washing apparatus for preparing stannous methanesulfonate crystals according to claim 1, characterized in that: The upper conveying housing extends to the lower body and is equipped with a lifting mechanism between the upper and lower body sections. The lifting mechanism includes two first support plates symmetrically fixed to the lower body and a movable seat fixed to the side wall of the upper conveying housing. A first motor is fixed to the top of the upper first support plate. A screw is placed between the two first support plates. One end of the screw is connected to the output shaft of the first motor through a coupling, and the other end of the screw is connected to the inner wall of the lower first support plate through a bearing. The movable seat is connected to the screw through a transmission nut. The first motor is connected to the programmable controller by wires.