一种单轴磁场取向制备高取向度Ba5Cu2Ti3Fe12O31铁氧体的方法

By using uniaxial magnetic field orientation technology and Ni2+ ion substitution regulation, the problem of complex equipment in rotating magnetic field orientation technology has been solved, enabling low-cost and high-efficiency production of high-frequency soft magnetic materials, including Ba5Cu2Ti3Fe12O31 ferrite with high orientation degree, high permeability and low magnetic loss.

CN118307315BActive Publication Date: 2026-07-17UNIV OF ELECTRONICS SCI & TECH OF CHINA +1

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
UNIV OF ELECTRONICS SCI & TECH OF CHINA
Filing Date
2024-04-03
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing processes for preparing planar hexagonal ferrites mostly employ rotating magnetic field orientation technology, which involves complex equipment, makes it difficult to achieve industrial-scale production, and results in high costs and low efficiency.

Method used

Uniaxial Cu-18H hexagonal ferrite was synthesized via solid-state reaction using uniaxial magnetic field orientation technology and Ni2+ ion substitution control technology. The uniaxial magnetic field was used to make the grains uniformly aligned in space, and planar CuNi-18H hexagonal ferrite was generated under high-temperature sintering.

Benefits of technology

A high-orientation, low-cost, and high-efficiency production of high-frequency soft magnetic materials has been achieved. Ba5Cu2Ti3Fe12O31 ferrite with high permeability, high natural resonance frequency, and low magnetic loss is suitable for large-scale industrial production.

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Abstract

本发明涉及铁氧体材料技术领域,公开了一种单轴磁场取向制备高取向度平面型六角铁氧体的方法,包括如下步骤:S1按Cu‑18H六角铁氧体的化学计量数,称BaCO3、CuO、TiO2、Fe2O3取原料粉末;S2将原料粉末球磨2‑4h,混合均匀,得到一次球磨混料;S3将一次球磨混料烘干,预烧结,得到Cu‑18H六角铁氧体预烧料;S4向Cu‑18H六角铁氧体预烧料中掺杂NiO,混合均匀;S5将掺杂有NiO的混料进行二次球磨,球磨6‑10h,得到二次球磨混料;S6采用单轴磁场成型压机,将二次球磨混料压制成生坯;S7将生坯进行烧结,得到所述平面型六角铁氧体。本发明利用单轴磁场取向技术,联合Ni2+离子取代调控18H六角铁氧体易磁化轴方向,既能降低生产所需的条件,实现低成本、高效率生产。
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