A detection device and method for heavy metal content of traditional Chinese medicine products
By using a space extrusion sleeve and a drive motor to drive the rotation of the extrusion plate in the heavy metal content detection equipment for traditional Chinese medicine products, the problem of slow temperature rise and low mixing degree caused by mixture accumulation is solved, and the complete digestion and detection efficiency of traditional Chinese medicine products are achieved. improvement.
Patent Information
- Application Number
- CN202410621271.2
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- Filing Date
- 2024-05-20
- Publication Date
- 2025-01-24
- Estimated Expiration
- 2044-05-20
AI Technical Summary
During the use of existing heavy metal content detection equipment for traditional Chinese medicine products, the temperature rises slowly due to the accumulation of mixture, and the degree of mixing between nitric acid, hydrogen peroxide and powdered traditional Chinese medicine products is low, so it cannot ensure complete digestion.
A testing equipment for heavy metal content in traditional Chinese medicine products is designed. It uses a space extrusion sleeve and a drive motor to drive the extrusion plate to rotate, ensuring that the mixture is fully stirred and flowing, accelerating the temperature and pressure raising process, and thus achieving complete digestion.
Through sufficient stirring and flow, the temperature and pressure raising process of the mixture is significantly accelerated, ensuring the complete digestion of traditional Chinese medicine products and improving the use value of the testing equipment.
Smart Images

Figure CN118330008B_ABST
Abstract
Description
Technical Field
[0001] The present invention relates to the technical field of heavy metal content detection, and in particular to a device and method for detecting the heavy metal content of a traditional Chinese medicine product. Background Art
[0002] Heavy metals refer to metals with a density greater than 4.5g / cm3, including gold, silver, copper, iron, mercury, lead, cadmium, etc. When heavy metals accumulate in the human body to a certain level, they will cause chronic poisoning. During the production process of Chinese medicine products, their heavy metal content needs to be tested.
[0003] During use, the existing heavy metal content detection equipment for traditional Chinese medicine products mixes the powdered traditional Chinese medicine product with nitric acid and hydrogen peroxide, and then introduces it into a microwave digester. When the temperature and pressure of the mixture inside the digestion tank are increased, the mixture accumulates in the digestion tank and the temperature increases from the outside to the inside, resulting in a slow temperature increase. At the same time, the degree of mixing between nitric acid, hydrogen peroxide and the powdered traditional Chinese medicine product is low, and it is impossible to ensure that they are digested completely, thereby reducing the use value of the detection equipment. Summary of the invention
[0004] The invention discloses a detection device for the heavy metal content of a traditional Chinese medicine product, and aims to solve the technical problem that in the existing detection device for the heavy metal content of traditional Chinese medicine products, after a powdered traditional Chinese medicine product is mixed with nitric acid and hydrogen peroxide, the mixture is introduced into a microwave digestion instrument during use, and when the temperature and pressure of the mixture in a digestion tank are increased, the mixture is accumulated in the digestion tank, and the temperature is increased from the outside to the inside, resulting in a slow temperature increase, and at the same time, the mixing degree between nitric acid, hydrogen peroxide and the powdered traditional Chinese medicine product is low, and the complete digestion thereof cannot be ensured.
[0005] In order to achieve the above object, the present invention adopts the following technical solutions:
[0006] A detection device for heavy metal content of traditional Chinese medicine products comprises a digestion instrument body and a mass spectrometer body, wherein a placement frame is fixedly connected to the bottom inner wall of the digestion instrument body, and a limiting ring plate is fixedly connected to the interior of the placement frame, a digestion tank is placed inside the placement frame, a space extrusion sleeve is provided inside the digestion tank, and the space extrusion sleeve comprises a plurality of extrusion plates, an upper fixed plate is fixedly connected to the top of the digestion tank at the top, and a driving motor is fixedly connected to the top of the upper fixed plate, the output shaft of the driving motor is fixedly connected to the driving shaft through a coupling, a blocking ring plate is fixedly connected to the inner wall of the digestion tank at the bottom end of the driving shaft, the bottom end of the driving shaft is connected to the top of the blocking ring plate through a bearing, the extrusion plates are annularly distributed on the outer side wall of the driving shaft, and the bottom of the extrusion plates contacts the top of the blocking ring plate.
[0007] By providing a space extrusion sleeve, when the powdered traditional Chinese medicine product is mixed with nitric acid and hydrogen peroxide, all of them are introduced into the digestion tank, and a placement cavity is formed between each extrusion plate and the digestion tank, thereby limiting the storage range of the mixture. When the temperature and pressure are increased, the drive motor is started, and the drive motor drives each extrusion plate and the sealing airbag to rotate, so as to fully stir the mixture, accelerate the flow of the mixture, and make it heat up and pressurize faster, so as to achieve the effect of thorough digestion.
[0008] In a preferred solution, stirring plates are fixedly connected to the outside of the extrusion plate at equal distances, and the side walls of every two adjacent extrusion plates are fixedly connected to the same sealing airbag, the outside of the drive shaft is fixedly connected to a pump frame, the inside of the pump frame is fixedly connected to an air pump, each sealing airbag has a connecting hole on the side wall facing the drive shaft, each connecting hole has a connecting tube fixedly connected to the inside, the ends of the multiple connecting tubes are fixedly connected to the same annular air pipe, the air delivery end of the air pump is connected to the inside of the annular air pipe through a pipeline, and the air inlet end of the air pump is located on the outside of the upper fixed plate.
[0009] In a preferred embodiment, the sealing ring plate is provided with a material unloading auxiliary component, and the material unloading auxiliary component includes an annular guide rail, which is fixedly connected to the inner wall of the digestion tank, and the interior of the annular guide rail is equidistantly slidably connected with a follower slide rod, and the bottom of each follower slide rod is fixedly connected to a baffle plate, and the baffle plate is connected to the top of the sealing ring plate, and the sealing ring plate is provided with a through hole under each baffle plate.
[0010] By providing a material unloading auxiliary component, when the mixture is unloaded after digestion is completed, electromagnet two is closed and electromagnet one is turned on, then electromagnet one adsorbs iron block one, and when the driving motor drives the driving shaft to rotate, iron block one drives the shielding plate to slide in the annular guide rail, so that the through hole under the shielding plate is exposed to the outside, and the mixture falls into the placement frame below along the through hole, and the unloading operation is successfully completed. At the same time, the rotating shielding plate has a pushing effect on the mixture, thereby improving the unloading efficiency.
[0011] In a preferred solution, the top of each follower slide rod of the annular guide rail is fixedly connected to a mounting block 2, the bottom of each mounting block 2 is fixedly connected to an electromagnet 2, and the top of each baffle plate near the electromagnet 2 is fixedly connected to an iron block 2, and the iron block 2 is in contact with the electromagnet 2.
[0012] In a preferred embodiment, the side wall of each extrusion plate near the bottom end is fixedly connected to a mounting block 1, and the bottom of each mounting block 1 is fixedly connected to an electromagnet 1, and the top of the baffle plate located below the electromagnet 1 is fixedly connected to an iron block 1, and the iron block 1 is in contact with the electromagnet 1.
[0013] In a preferred embodiment, a feeding hole is provided at the top of the upper fixed plate, and a feeding pipe is fixedly connected to the inside of the feeding hole; a discharge hole is provided at the bottom of the digestion tank, a discharge pipe is fixedly connected to the inside of the discharge hole, and a discharge valve is connected to the outside of the discharge pipe via a flange.
[0014] In a preferred embodiment, both ends of the bottom of the digester body are fixedly connected to grounding sockets, and a mounting frame is fixedly connected to one side of the digester body, a mixing cylinder is fixedly connected to the inside of the mounting frame, an introduction hole is opened at the bottom of the mixing cylinder, an introduction tube is fixedly connected to the inside of the introduction hole, the introduction tube is inserted into the interior of the mass spectrometer body, and the outside of the introduction tube is connected to a pipe valve through a flange.
[0015] In a preferred embodiment, a step-by-step mixing element is provided inside the mixing cylinder, and the step-by-step mixing element includes a spray nozzle, and spray holes are equidistantly provided at the bottom of the spray nozzle. A fixed ring plate is fixedly connected to the inner wall of the mixing cylinder above the spray nozzle, and two electric telescopic rods are fixedly connected to the bottom of the fixed ring plate, and the output ends of the two electric telescopic rods are fixedly connected to the outside of the spray nozzle.
[0016] By providing a gradual mixing piece, the digested mixture needs to be mixed with pure water before being introduced into the mass spectrometer. During the mixing process, the electric telescopic rod is adjusted to drive the spray nozzle to move to the bottom of the mixing barrel, and pure water is slowly introduced into the mixing barrel. The extraction pump is started, and the extraction pump introduces the mixture into the spray nozzle, and the mixture is evenly spread in the introduced pure water through the spray hole. As the amount of pure water introduced increases, the electric telescopic rod drives the spray nozzle to gradually rise, thereby realizing layer-by-layer spraying and mixing, thereby improving the uniformity of mixing of pure water and the mixture.
[0017] In a preferred embodiment, an extraction pump is fixedly connected to the top of the mounting frame, and an extraction end of the extraction pump is fixedly connected to an extraction pipe, which is inserted into the interior of the placement frame; a telescopic connecting pipe is fixedly connected to the top inner wall of the mixing cylinder, which is inserted into the interior of the spray nozzle; a delivery end of the extraction pump is fixedly connected to a delivery pipe, which is inserted into the interior of the telescopic connecting pipe; a water adding hole is opened on the side wall of the mixing cylinder, a pure water adding pipe is fixedly connected to the interior of the water adding hole, and a control valve is connected to the outer side of the pure water adding pipe near the bottom through a flange.
[0018] A method for detecting the heavy metal content of a traditional Chinese medicine product, using the above-mentioned device for detecting the heavy metal content of a traditional Chinese medicine product, the method comprising the following steps:
[0019] Step 1: Mix the powdered Chinese medicine with nitric acid and hydrogen peroxide. After the mixing is completed, put the digestion tank into the digestion instrument body, the digestion instrument body starts to work, and the drive motor is started. The drive motor drives each extrusion plate and the sealing airbag to rotate, so as to fully stir the mixture, accelerate the flow of the mixture, and make it heat up and increase the pressure faster;
[0020] Step 2: After the digestion is completed, the electromagnet 2 is turned off and the electromagnet 1 is turned on. Then the electromagnet 1 adsorbs the iron block 1. When the driving motor drives the driving shaft to rotate, the iron block 1 drives the shielding plate to slide in the annular guide rail, and the through hole under the shielding plate is exposed to the outside. The mixture falls into the placement frame below along the through hole, and the extraction pump is started to guide the mixture into the spray nozzle;
[0021] Step 3: Adjust the electric telescopic rod to drive the spray nozzle to move to the bottom of the mixing barrel. Pure water is slowly introduced into the mixing barrel. The mixture is evenly spread in the introduced pure water through the spray hole. As the amount of pure water introduced increases, the electric telescopic rod drives the spray nozzle to gradually rise to achieve layer-by-layer spraying and mixing. After the mixing is completed, open the pipe valve, and the liquid enters the mass spectrometer body along the introduction pipe, and the mass spectrometer body starts to work.
[0022] As can be seen from the above, the detection equipment and method for the heavy metal content of traditional Chinese medicine products provided by the present invention have the characteristics of introducing all the powdered traditional Chinese medicine products into a digestion tank when mixing them with nitric acid and hydrogen peroxide, forming a placement cavity between each extrusion plate and the digestion tank, thereby limiting the storage range of the mixture, and starting the drive motor when heating and pressurizing it, and the drive motor drives each extrusion plate and the sealing airbag to rotate, so as to fully stir the mixture, accelerate the flow of the mixture, and make it heat up and pressurize faster, so as to achieve the technical effect of thorough digestion. BRIEF DESCRIPTION OF THE DRAWINGS
[0023] Figure 1 This is a schematic diagram of the overall structure of a device for detecting the heavy metal content of traditional Chinese medicine products proposed by the present invention.
[0024] Figure 2 This is a schematic diagram of the combined structure of a digestion tank and a mixing cylinder of a device for detecting heavy metal content in traditional Chinese medicine products proposed by the present invention.
[0025] Figure 3 This is a cross-sectional view of the structure of a digestion tank of a device for detecting the heavy metal content of traditional Chinese medicine products proposed by the present invention.
[0026] Figure 4 This is a schematic diagram of the structure of a space extrusion sleeve of a device for detecting heavy metal content in traditional Chinese medicine products proposed by the present invention.
[0027] Figure 5 This is a schematic diagram of the auxiliary material feeding components of a device for detecting the heavy metal content of traditional Chinese medicine products proposed by the present invention.
[0028] Figure 6 This is a cross-sectional view of the sealing ring plate structure of a device for detecting the heavy metal content of traditional Chinese medicine products proposed by the present invention.
[0029] Figure 7This is a schematic diagram of the structure of the step-by-step mixing components of a device for detecting the heavy metal content of traditional Chinese medicine products proposed by the present invention.
[0030] In the figure: 1. digestion instrument body; 2. delivery pipe; 3. mixing cylinder; 4. pure water adding pipe; 5. mounting frame; 6. mass spectrometer body; 7. grounding seat; 8. digestion tank; 9. placement frame; 10. limit ring plate; 11. extraction pipe; 12. introduction pipe; 13. pipe valve; 14. extraction pump; 15. space extrusion sleeve; 1501. drive motor; 1502. stirring plate; 1503. extrusion plate; 1504. connecting pipe; 1505. annular air pipe; 1506. pump frame; 1507. air pump; 1508. sealing air bag; 1509. drive shaft; 16. Material pipe; 17, upper fixed plate; 18, discharge pipe; 19, discharge valve; 20, sealing ring plate; 21, material unloading auxiliary component; 2101, baffle plate; 2102, electromagnet one; 2103, iron block one; 2104, annular guide rail; 2105, mounting block one; 2106, electromagnet two; 2107, follow-up slide rod; 2108, through hole; 2109, iron block two; 2110, mounting block two; 22, step-by-step mixing element; 2201, spray nozzle; 2202, spray hole; 2203, electric telescopic rod; 2204, fixed ring plate; 2205, telescopic connecting pipe. DETAILED DESCRIPTION
[0031] The technical solutions in the embodiments of the present invention will be described clearly and completely below in conjunction with the drawings in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, rather than all the embodiments.
[0032] The invention discloses a detection device for the heavy metal content of a traditional Chinese medicine product, which is mainly applied to the existing detection device for the heavy metal content of a traditional Chinese medicine product. During use, a powdered traditional Chinese medicine product is mixed with nitric acid and hydrogen peroxide, and then introduced into a microwave digestion instrument. When the temperature and pressure of the mixture inside the digestion tank are increased, the temperature is increased from the outside to the inside due to the accumulation of the mixture in the digestion tank, resulting in a slow temperature increase. At the same time, the degree of mixing between nitric acid, hydrogen peroxide and the powdered traditional Chinese medicine product is low, and a complete digestion scenario cannot be ensured.
[0033] Reference Figure 1-Figure 7A detection device for the heavy metal content of a traditional Chinese medicine product comprises a digestion instrument body 1 and a mass spectrometer body 6. The bottom inner wall of the digestion instrument body 1 is fixedly connected with a placement frame 9, and the interior of the placement frame 9 is fixedly connected with a limiting ring plate 10. A digestion tank 8 is placed inside the placement frame 9. The interior of the digestion tank 8 is provided with a space extrusion sleeve 15, and the space extrusion sleeve 15 comprises a plurality of extrusion plates 1503. The digestion tank 8 is fixedly connected with an upper fixed plate 17 at the top, and the top of the upper fixed plate 17 is fixedly connected with a driving motor 1501. The output shaft of the driving motor 1501 is fixedly connected with a driving shaft 1509 through a coupling. The inner wall of the digestion tank 8 at the bottom end of the driving shaft 1509 is fixedly connected with a blocking ring plate 20. The bottom end of the driving shaft 1509 is connected to the top of the blocking ring plate 20 through a bearing. The extrusion plates 1503 are distributed in an annular manner. On the outer wall of the driving shaft 1509, the bottom of the extrusion plate 1503 contacts the top of the sealing ring plate 20, the outer side of the extrusion plate 1503 is fixedly connected with a stirring plate 1502 at an equal distance, and the side walls of each adjacent two extrusion plates 1503 are fixedly connected with the same sealing air bag 1508, the outer side of the driving shaft 1509 is fixedly connected with a pump frame 1506, and the inside of the pump frame 1506 is fixedly connected with an air pump 1507, each sealing air bag 1508 has a connecting hole on the side wall facing the driving shaft 1509, and the inside of each connecting hole is fixedly connected with a connecting pipe 1504, and the ends of the multiple connecting pipes 1504 are fixedly connected with the same annular air pipe 1505, the air delivery end of the air pump 1507 is connected to the inside of the annular air pipe 1505 through a pipeline, and the air inlet end of the air pump 1507 is located on the outside of the upper fixed plate 17.
[0034] In a specific application scenario, when powdered Chinese medicine products are mixed with nitric acid and hydrogen peroxide, they are all introduced into the digestion tank 8, and a placement cavity is formed between each extrusion plate 1503 and the digestion tank 8, thereby limiting the storage range of the mixture. When the temperature and pressure are increased, the drive motor 1501 is started, and the drive motor 1501 drives each extrusion plate 1503 and the sealing airbag 1508 to rotate, so as to fully stir the mixture, accelerate the flow of the mixture, and make it heat up and pressurize faster, thereby achieving the effect of thorough digestion.
[0035] Specifically, during the digestion process, if the amount of the mixture is small, the air pump 1507 is started. The air pump 1507 fills the sealed air bag 1508 with gas to expand the sealed air bag 1508, and compresses the space where the mixture is stacked by the expansion, so that the mixture contacts the inner wall of the digestion tank 8 more frequently, further improving the efficiency of heating and pressurizing.
[0036] Reference Figure 1 , Figure 2 , Figure 5 and Figure 6In a preferred embodiment, a material unloading auxiliary component 21 is provided on the sealing ring plate 20, and the material unloading auxiliary component 21 includes an annular guide rail 2104, the annular guide rail 2104 is fixedly connected to the inner wall of the digestion tank 8, and the inner part of the annular guide rail 2104 is equidistantly slidably connected with a follower slide bar 2107, and the bottom of each follower slide bar 2107 is fixedly connected with a shielding plate 2101, and the shielding plate 2101 is connected to the top of the sealing ring plate 20, and the sealing The blocking ring plate 20 is located below each baffle plate 2101 and has a through hole 2108. The annular guide rail 2104 is located at the top of each follow-up slide rod 2107 and is fixedly connected to a mounting block 2110. The bottom of each mounting block 2110 is fixedly connected to an electromagnet 2106. The top of each baffle plate 2101 near the electromagnet 2106 is fixedly connected to an iron block 2109, and the iron block 2109 is in contact with the electromagnet 2106.
[0037] It should be noted that after the mixture is digested and discharged, electromagnet 2 2106 is turned off and electromagnet 1 2102 is turned on, then electromagnet 1 2102 adsorbs iron block 1 2103, and when the driving motor 1501 drives the driving shaft 1509 to rotate, the iron block 1 2103 drives the baffle plate 2101 to slide in the annular guide rail 2104, and the through hole 2108 under the baffle plate 2101 is exposed to the outside, and the mixture falls into the placement frame 9 below along the through hole 2108, and the discharge operation is successfully completed. At the same time, the rotating baffle plate 2101 has a pushing effect on the mixture, thereby improving the discharge efficiency.
[0038] In the present invention, the side wall of each extrusion plate 1503 near the bottom end is fixedly connected to a mounting block 2105, and the bottom of each mounting block 2105 is fixedly connected to an electromagnet 2102, the top of the baffle plate 2101 located below the electromagnet 2102 is fixedly connected to an iron block 2103, the iron block 2103 is in contact with the electromagnet 2102, a feeding hole is provided at the top of the upper fixed plate 17, and a feeding pipe 16 is fixedly connected inside the feeding hole, a discharge hole is provided at the bottom of the digestion tank 8, a discharge pipe 18 is fixedly connected inside the discharge hole, and a discharge valve 19 is connected to the outside of the discharge pipe 18 through a flange.
[0039] Reference Figure 1 , Figure 2 and Figure 3 In a preferred embodiment, both ends of the bottom of the digester body 1 are fixedly connected to a grounding seat 7, and a mounting frame 5 is fixedly connected to one side of the digester body 1, a mixing cylinder 3 is fixedly connected to the inside of the mounting frame 5, an introduction hole is opened at the bottom of the mixing cylinder 3, an introduction pipe 12 is fixedly connected to the inside of the introduction hole, the introduction pipe 12 is inserted into the inside of the mass spectrometer body 6, and a pipe valve 13 is connected to the outside of the introduction pipe 12 through a flange.
[0040] Reference Figure 1 , Figure 2 and Figure 7 In a preferred embodiment, a step-by-step mixing element 22 is provided inside the mixing cylinder 3, and the step-by-step mixing element 22 includes a spray nozzle 2201, and spray holes 2202 are opened at equal distances at the bottom of the spray nozzle 2201. A fixed ring plate 2204 is fixedly connected to the inner wall of the mixing cylinder 3 above the spray nozzle 2201, and two electric telescopic rods 2203 are fixedly connected to the bottom of the fixed ring plate 2204. The output ends of the two electric telescopic rods 2203 are fixedly connected to the outside of the spray nozzle 2201. The top of the mounting frame 5 is fixedly connected to an extraction pump. 14, and the extraction end of the extraction pump 14 is fixedly connected with the extraction pipe 11, the extraction pipe 11 is inserted into the interior of the placement frame 9, the top inner wall of the mixing cylinder 3 is fixedly connected with the telescopic connecting pipe 2205, the telescopic connecting pipe 2205 is inserted into the interior of the spray nozzle 2201, the delivery end of the extraction pump 14 is fixedly connected with the delivery pipe 2, the delivery pipe 2 is inserted into the interior of the telescopic connecting pipe 2205, the side wall of the mixing cylinder 3 is opened with a water adding hole, the interior of the water adding hole is fixedly connected with a pure water adding pipe 4, and the outer side of the pure water adding pipe 4 near the bottom is connected to a control valve through a flange.
[0041] Specifically, before the digested mixture is introduced into the mass spectrometer, it needs to be mixed with pure water. During the mixing process, the electric telescopic rod 2203 is adjusted to drive the spray nozzle 2201 to move to the bottom of the mixing barrel 3, and pure water is slowly introduced into the mixing barrel 3. The extraction pump 14 is started, and the extraction pump 14 introduces the mixture into the spray nozzle 2201, and evenly spreads it in the introduced pure water through the spray hole 2202. As the amount of pure water introduced increases, the electric telescopic rod 2203 drives the spray nozzle 2201 to gradually rise, realizing layer-by-layer spraying and mixing, thereby improving the uniformity of mixing of pure water and the mixture.
[0042] A method for detecting the heavy metal content of a traditional Chinese medicine product, using the above-mentioned device for detecting the heavy metal content of a traditional Chinese medicine product, the detection method comprises the following steps:
[0043] Step 1: Mix the powdered Chinese medicine with nitric acid and hydrogen peroxide. After the mixing is completed, put the digestion tank 8 into the digestion instrument body 1, and the digestion instrument body 1 starts to work, and starts the drive motor 1501. The drive motor 1501 drives each extrusion plate 1503 and the sealing airbag 1508 to rotate, so as to fully stir the mixture, accelerate the flow of the mixture, and make it heat up and increase the pressure faster;
[0044] Step 2: After the digestion is completed, the electromagnet 2106 is turned off and the electromagnet 1 2102 is turned on. Then the electromagnet 1 2102 adsorbs the iron block 1 2103. When the driving motor 1501 drives the driving shaft 1509 to rotate, the iron block 1 2103 drives the shielding plate 2101 to slide in the annular guide rail 2104. Then the through hole 2108 below the shielding plate 2101 is exposed to the outside, and the mixture falls into the lower placement frame 9 along the through hole 2108. The extraction pump 14 is started, and the extraction pump 14 guides the mixture into the spray nozzle 2201.
[0045] Step three: adjust the electric telescopic rod 2203 to drive the spray nozzle 2201 to move to the bottom of the mixing barrel 3, and slowly introduce pure water into the mixing barrel 3. The mixture is evenly spread in the introduced pure water through the spray hole 2202. As the amount of pure water introduced increases, the electric telescopic rod 2203 drives the spray nozzle 2201 to gradually rise to achieve layer-by-layer spraying and mixing. After the mixing is completed, open the pipe valve 13, and the liquid enters the mass spectrometer body 6 along the introduction pipe 12, and the mass spectrometer body 6 starts to work.
[0046] The above description is only a preferred specific implementation manner of the present invention, but the protection scope of the present invention is not limited thereto. Any technician familiar with the technical field can make equivalent replacements or changes according to the technical scheme and inventive concept of the present invention within the technical scope disclosed by the present invention, which should be covered by the protection scope of the present invention.
Claims
1. A device for detecting the heavy metal content of a traditional Chinese medicine product, comprising a digestion instrument body (1) and a mass spectrometer body (6), characterized in that: The bottom inner wall of the digestion instrument body (1) is fixedly connected to a placement frame (9), and the interior of the placement frame (9) is fixedly connected to a limiting ring plate (10), a digestion tank (8) is placed inside the placement frame (9), a space extrusion sleeve (15) is provided inside the digestion tank (8), and the space extrusion sleeve (15) includes a plurality of extrusion plates (1503), an upper fixed plate (17) is fixedly connected to the top of the digestion tank (8), and a driving electric motor is fixedly connected to the top of the upper fixed plate (17). The machine (1501) comprises an output shaft of a driving motor (1501) fixedly connected to a driving shaft (1509) via a coupling, an inner wall of a digestion tank (8) located at the bottom end of the driving shaft (1509) is fixedly connected to a blocking ring plate (20), the bottom end of the driving shaft (1509) is connected to the top of the blocking ring plate (20) via a bearing, and an extrusion plate (1503) is distributed in an annular shape on the outer wall of the driving shaft (1509), and the bottom of the extrusion plate (1503) is in contact with the top of the blocking ring plate (20); The outer side of the extrusion plate (1503) is fixedly connected with stirring plates (1502) at equal distances, and the side walls of each two adjacent extrusion plates (1503) are fixedly connected with the same sealing airbag (1508), the outer side of the driving shaft (1509) is fixedly connected with a pump frame (1506), and the inside of the pump frame (1506) is fixedly connected with an air pump (1507), and each sealing airbag (1508) has a connecting hole on the side wall facing the driving shaft (1509), and the inside of each connecting hole is fixedly connected with a connecting pipe (1504), and the ends of the multiple connecting pipes (1504) are fixedly connected with the same annular air pipe (1505), and the air delivery end of the air pump (1507) is connected to the inside of the annular air pipe (1505) through a pipeline, and the air inlet end of the air pump (1507) is located on the outer side of the upper fixed plate (17).
2. The device for detecting heavy metal content in traditional Chinese medicine products according to claim 1, characterized in that: The blocking ring plate (20) is provided with a material unloading auxiliary component (21), and the material unloading auxiliary component (21) comprises an annular guide rail (2104), the annular guide rail (2104) is fixedly connected to the inner wall of the digestion tank (8), and the inside of the annular guide rail (2104) is equidistantly slidably connected with a follower slide bar (2107), and the bottom of each follower slide bar (2107) is fixedly connected with a baffle plate (2101), and the baffle plate (2101) is in contact with the top of the blocking ring plate (20), and the blocking ring plate (20) is provided with a through hole (2108) below each baffle plate (2101).
3. A device for detecting heavy metal content in traditional Chinese medicine products according to claim 2, characterized in that: The annular guide rail (2104) is fixedly connected to a second mounting block (2110) at the top of each follower slide bar (2107), and the bottom of each second mounting block (2110) is fixedly connected to a second electromagnet (2106). The top of each shielding plate (2101) close to the second electromagnet (2106) is fixedly connected to a second iron block (2109), and the second iron block (2109) is in contact with the second electromagnet (2106).
4. The device for detecting heavy metal content in traditional Chinese medicine products according to claim 3, characterized in that: The side wall of each extrusion plate (1503) close to the bottom end is fixedly connected to a mounting block 1 (2105), and the bottom of each mounting block 1 (2105) is fixedly connected to an electromagnet 1 (2102), and the top of the shielding plate (2101) located below the electromagnet 1 (2102) is fixedly connected to an iron block 1 (2103), and the iron block 1 (2103) is in contact with the electromagnet 1 (2102).
5. The device for detecting heavy metal content in traditional Chinese medicine products according to claim 4, characterized in that: The top of the upper fixed plate (17) is provided with a feeding hole, and a feeding pipe (16) is fixedly connected to the inside of the feeding hole. The bottom of the digestion tank (8) is provided with a discharge hole, and a discharge pipe (18) is fixedly connected to the inside of the discharge hole. The outer side of the discharge pipe (18) is connected to a discharge valve (19) via a flange.
6. The device for detecting heavy metal content in traditional Chinese medicine products according to claim 5, characterized in that: Both ends of the bottom of the digestion instrument body (1) are fixedly connected to grounding seats (7), and one side of the digestion instrument body (1) is fixedly connected to a mounting frame (5), the interior of the mounting frame (5) is fixedly connected to a mixing cylinder (3), the bottom of the mixing cylinder (3) is provided with an introduction hole, the interior of the introduction hole is fixedly connected to an introduction pipe (12), the introduction pipe (12) is plugged into the interior of the mass spectrometer body (6), and the outer side of the introduction pipe (12) is connected to a pipe valve (13) via a flange.
7. The device for detecting heavy metal content in traditional Chinese medicine products according to claim 6, characterized in that: The mixing cylinder (3) is provided with a step-by-step mixing element (22) inside, and the step-by-step mixing element (22) comprises a spray nozzle (2201), the bottom of the spray nozzle (2201) is provided with spray holes (2202) at equal intervals, the inner side wall of the mixing cylinder (3) located above the spray nozzle (2201) is fixedly connected to a fixed ring plate (2204), the bottom of the fixed ring plate (2204) is fixedly connected to two electric telescopic rods (2203), and the output ends of the two electric telescopic rods (2203) are both fixedly connected to the outside of the spray nozzle (2201).
8. The device for detecting heavy metal content in traditional Chinese medicine products according to claim 7, characterized in that: The top of the mounting frame (5) is fixedly connected to an extraction pump (14), and the extraction end of the extraction pump (14) is fixedly connected to an extraction pipe (11), the extraction pipe (11) is plugged into the interior of the placement frame (9), the top inner wall of the mixing cylinder (3) is fixedly connected to a telescopic connecting pipe (2205), the telescopic connecting pipe (2205) is plugged into the interior of the spray nozzle (2201), the delivery end of the extraction pump (14) is fixedly connected to a delivery pipe (2), the delivery pipe (2) is plugged into the interior of the telescopic connecting pipe (2205), a water adding hole is opened on the side wall of the mixing cylinder (3), the interior of the water adding hole is fixedly connected to a pure water adding pipe (4), and the outer side of the pure water adding pipe (4) near the bottom is connected to a control valve via a flange.
9. A method for detecting heavy metal content in a traditional Chinese medicine product, using the device for detecting heavy metal content in a traditional Chinese medicine product as claimed in claim 8, characterized in that: The detection method comprises the following steps: Step 1: Powdered Chinese medicine is mixed with nitric acid and hydrogen peroxide. After the mixing is completed, a digestion tank (8) is placed in a digestion instrument body (1). The digestion instrument body (1) starts to work and a drive motor (1501) is started. The drive motor (1501) drives each extrusion plate (1503) and a sealing air bag (1508) to rotate, thereby fully stirring the mixture, accelerating the flow of the mixture, and causing the mixture to heat up and increase pressure more quickly. Step 2: After digestion is completed, electromagnet 2 (2106) is turned off and electromagnet 1 (2102) is turned on, so that electromagnet 1 (2102) adsorbs iron block 1 (2103). When the driving motor (1501) drives the driving shaft (1509) to rotate, iron block 1 (2103) drives the shielding plate (2101) to slide in the annular guide rail (2104), so that the through hole (2108) below the shielding plate (2101) is exposed to the outside, and the mixture falls into the lower placement frame (9) along the through hole (2108), and the extraction pump (14) is started, and the extraction pump (14) guides the mixture into the spray nozzle (2201); Step 3: Adjust the electric telescopic rod (2203) to drive the spray nozzle (2201) to move to the bottom of the mixing barrel (3), and slowly introduce pure water into the mixing barrel (3). The mixture is evenly spread in the introduced pure water through the spray hole (2202). As the amount of pure water introduced increases, the electric telescopic rod (2203) drives the spray nozzle (2201) to gradually rise, so as to achieve layer-by-layer spraying and mixing. After the mixing is completed, open the pipe valve (13), and the liquid enters the mass spectrometer body (6) along the introduction pipe (12), and the mass spectrometer body (6) starts to work.
Citation Information
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