Extraction and purification equipment and purification method for efficient extraction of furanol

By designing the heating and shunt cooling system in the furolol purification equipment, the problem of impurity residue in the existing equipment is solved, efficient furolol purification is achieved, and product purity and quality are improved.

CN118873991BActive Publication Date: 2024-12-20JIANGSU SANJILI CHEM
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Patent Information

Application Number
CN202411355118.6
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2024-09-27
Publication Date
2024-12-20
Estimated Expiration
2044-09-27

AI Technical Summary

Technical Problem

In existing furothol purification equipment, more impurities remain in the product, resulting in low product purity and affecting product quality.

Method used

An extraction and purification equipment including a bottom tank, extraction tower, extraction mixing assembly and product cooling assembly was designed. The product evaporates and enters the shunt tube by heating, and uses the special structure and cooling mechanism of the shunt tube to quickly cool the gaseous product into liquid. , thereby improving the purity of the product.

Benefits of technology

Through this equipment and method, the purification efficiency of furothol is significantly improved, impurity residues are reduced, and the purity and quality of the product are improved.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention relates to the technical field of furanol purification, and in particular to an extraction and purification device and a purification method for efficient extraction of furanol, comprising a bottom tank, an extraction tower, an extraction mixing component and a product cooling component, wherein the top of the bottom tank is provided with an extraction tower, one side of the top of the extraction tower is connected with a product cooling component, the product cooling component is used to cool the product, and the product cooling component also liquefies the gaseous product into liquid, the product cooling component comprises a cooling tank and a cooling mechanism, a top plate is provided in the cooling tank, the bottom of the top plate is connected with a shunt pipe, the bottom of the shunt pipe is connected with a bottom plate, and the top of the top plate is connected with a first pipeline, the invention heats the product to an evaporation temperature to vaporize the product, and then the vaporized product enters the shunt pipe, and the product in the shunt pipe is liquefied through the special structure of the shunt pipe, thereby improving the purity of the product.
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Description

Technical Field

[0001] The invention relates to the technical field of furanol purification, in particular to extraction and purification equipment and a purification method for efficient extraction of furanol. Background Art

[0002] Furanol is an important chemical intermediate. It is easily soluble in organic solvents such as benzene, toluene, methanol, ethanol, and chloroform. It is slightly soluble in water, but soluble in strong alkaline solutions. It is stable at room temperature and pressure, but will be oxidized if exposed to air for a long time. Pure furanol is a colorless liquid with specific physical and chemical parameters such as boiling point, density, viscosity, and specific heat capacity. Furanol generally needs to be purified by extraction. When purifying furanol, an extractant is generally added to separate the furanol and the extractant.

[0003] Chinese patent application CN118079453A discloses a high-yield furanol purification device and process based on an extraction process, which relates to the field of extraction technology, and comprises an extraction tower and a distillation kettle, wherein one side of the top of the extraction tower is connected to the distillation kettle through an oil phase material delivery pipeline, the middle of the extraction tower is connected to a raw material delivery pipeline, a mixer is installed on the raw material delivery pipeline, a NaHCO solution delivery pipeline is provided on the top of the raw material delivery pipeline, a washing water delivery pipeline is provided on the top of the NaHCO solution delivery pipeline, a flow guide device is provided inside the extraction tower, the flow guide device passes through a stratification zone, a one-way valve is installed on the flow guide device, a neutralizer delivery pipeline is provided on the top of the stratification zone, an oil phase delivery pipeline is connected to one side of the stratification zone, one end of the oil phase delivery pipeline is connected to a cyclization liquid desolventizing section, the cyclization liquid desolventizing section is connected to the extraction tower through a xylene delivery pipeline, the bottom of the extraction tower is connected to a washing water delivery pipeline, and the washing water delivery pipeline is also connected to an interstitial desalter.

[0004] In the above structure, the xylene treatment section in the original furanol production device is used to carry out stratification and then extract the material, which belongs to the device coupling scheme and reduces the increase of equipment. However, in the above structure, various reagents are used for reaction and extraction. During separation, a large amount of impurities will still remain in the product, resulting in low purity of the product and affecting the quality of the product. Summary of the invention

[0005] The object of the present invention is to provide an extraction and purification device and a purification method for efficient extraction of furanol, by heating the product to the evaporation temperature to vaporize the product, and then the vaporized product enters the diverter pipe, and the special structure of the diverter pipe makes the product in the diverter pipe liquefied, thereby improving the purity of the product.

[0006] In order to solve the problems of the prior art, the present invention provides an extraction and purification device, comprising a bottom tank, an extraction tower, an extraction mixing component and a product cooling component, wherein the top of the bottom tank is provided with an extraction tower, and one side of the top of the extraction tower is connected to a product cooling component, wherein the product cooling component is used to cool the product, and the product cooling component also liquefies the gaseous product into

[0007] Liquid, the product cooling component includes a cooling tank and a cooling mechanism, a top plate is arranged in the cooling tank, a shunt pipe is connected to the bottom of the top plate, a bottom of the shunt pipe is connected to the bottom plate, a first pipe is connected to the top of the top plate, one end of the first pipe passes through the cooling tank and is connected to the top of the extraction tower, the top plate is hollow inside, the shunt pipe is vertically inserted into the bottom of the top plate, and a plurality of shunt pipes are evenly arranged between the top plate and the bottom plate, a plurality of annular protrusions are also arranged on the outside of each shunt pipe, the shunt pipe is used to shunt the product flowing into the top plate, the shunt pipe increases the contact area with the heat conductor in the external cooling tank to quickly cool the product.

[0008] Preferably, the interior of the cooling tank is hollow and filled with a heat conductor, the top plate, the shunt pipe and the bottom plate are inserted into the cooling tank, the bottom of the bottom plate is connected to a second pipe, and the second pipe passes through the cooling tank and extends out.

[0009] Preferably, the product cooling assembly also includes a cooling mechanism, which includes a protective shell, and the protective shell is arranged on the outside of the bottom tank, and a cooler is installed inside the protective shell; the cooler includes a heat conducting plate and a heat conducting pipe, and the heat conducting plate is formed by stacking a number of metal plates to increase the heat conducting area, and a number of heat conducting pipes are coiled between the heat conducting plates, and the heat conducting pipes are made of metal pipes, and the heat conducting pipes are arranged in a "snake" shape in the heat conducting plate to increase the heat conducting area.

[0010] Preferably, the cooling mechanism also includes a pump body, one end of the pump body is fixedly connected to the heat conducting pipe through a pipe, and one end of the heat conducting pipe is connected to a second circulation pipe, one end of the second circulation pipe extends to the upper part of the cooling tank and extends into the cooling tank, the other end of the pump body is connected to the first circulation pipe, and one end of the first circulation pipe passes through the protective shell and is connected to the lower part of the cooling tank and extends into the cooling tank, the pump body is used for the flow of heat conducting agent in the cooling tank, the heat conducting agent flows into the heat conducting pipe, and heat is introduced into the heat conducting plate.

[0011] Preferably, a plurality of heat dissipation slots for dissipating heat are provided on the outside of the protective shell, and at least one heat dissipation fan is fixed on the outside of the protective shell, and the heat dissipation fan is used to flow air in the protective shell and remove heat from the heat conductive sheet.

[0012] Preferably, the bottom tank is used to store the liquid to be extracted, the extraction tower is used to extract the liquid, and an extraction mixing assembly is arranged in the extraction tower; the extraction mixing assembly includes a rotating drive member and a rotating rod, the rotating drive member is fixed on the top of the extraction tower, the rotating rod is vertically rotatably arranged in the extraction tower, and one end of the rotating rod extends into the bottom tank and is fixed with a stirring blade for stirring the liquid in the bottom tank, the other end of the rotating rod passes through the top of the extraction tower and is fixedly connected to the output end of the rotating drive member, and the rotation of the rotating drive member is used to drive the rotating rod to rotate and simultaneously drive the stirring blade to rotate.

[0013] Preferably, the extraction and mixing assembly includes a fixed ring, a rotating disk and blades, and the rotating disk is evenly distributed on the rotating rod, and the blades are also evenly distributed on the rotating rod, and the fixed ring is evenly fixed on the inner wall of the extraction tower, the rotating disk is arranged between the two fixed rings, and the blades and the fixed ring are in the same plane.

[0014] Preferably, the interlayer inside the extraction tower is equipped with a plurality of heating coils, and the heating coils adopt the principle of electromagnetic induction.

[0015] The internal metal elements are heated and then the heat is transferred to the liquid inside the extraction tower. The bottom tank and the extraction tower are also provided with temperature sensors for detecting the temperature of the liquid. The bottom tank and the extraction tower are provided with a liquid inlet outside, and the liquid inlet is connected to a first solenoid valve. The bottom tank is also provided with a heavy liquid outlet outside, and the heavy liquid outlet is connected to a second solenoid valve. The bottom tank and the extraction tower are also provided with a maintenance platform for maintenance by staff. A safety valve is also provided on the top of the extraction tower.

[0016] The present application also relates to a purification method for efficient extraction of furanol, comprising an extraction and purification device as described in the above scheme, comprising the following steps:

[0017] S1: The extractant and the product to be extracted are introduced into the bottom tank and the extraction tower from two liquid inlets. The rotary drive member is started, and the rotary drive member rotates the rotary rod, and the rotary rod rotates the turntable and the blades. In this process, the components in the mixture will fully contact and form different solubilities, which is conducive to separation. As the turntable rotates, the mixture will be brought to the top of the tower body and then gradually flow downward. In this process, due to the difference in solubility of the components in different solvents, they will gradually separate, thereby achieving separation of the mixture;

[0018] S2: In order to make the product after extraction higher in purity, the product in the extraction tower is heated to make the temperature in the product reach the evaporation temperature of the product, and then the product evaporates and enters the top plate from the first pipeline, and then the product enters the diversion pipe, and multiple diversion pipes are used to increase the contact area with the heat conductive agent, so that the gas is cooled into liquid;

[0019] S3: By starting the pump body, the pump body makes the heat conductive agent in the cooling tank flow, and the heat conductive agent flows into the heat conductive pipe. Since the heat conductive sheet is arranged outside the heat conductive pipe, the heat is introduced into the heat conductive sheet. By starting the cooling fan, the cooling fan makes the air flow, so that the heat conductive agent is cooled;

[0020] S4: The liquefied product flows out from the second pipeline, while the extractant and other impurities flow out from the heavy liquid outlet and the second solenoid valve, completing the purification.

[0021] Compared with the prior art, the invention has the beneficial effects that the extraction and purification equipment and the purification method for efficient extraction of furanol are reasonable in structure and have the following advantages:

[0022] After being layered through the bottom tank and the extraction tower, the internal liquid is energized through the heating coil. According to the principle of electromagnetic induction, the internal components are heated, and then the heat is introduced into the liquid, thereby evaporating the product into a gaseous state. The gaseous product then enters the diversion pipe. The special structure of the diversion pipe increases the heat conduction area, thereby cooling the gaseous product into a liquid, thereby increasing the purity of the product and achieving higher purification efficiency. BRIEF DESCRIPTION OF THE DRAWINGS

[0023] FIG. 1 is a schematic diagram of the three-dimensional structure of an extraction and purification device.

[0024] FIG. 2 is a schematic diagram of the front view of the extraction and purification equipment.

[0025] FIG. 3 is a schematic diagram of the top view of the structure of an extraction and purification device.

[0026] FIG. 4 is a schematic diagram of the left side structure of an extraction and purification device.

[0027] Fig. 5 is a schematic diagram of the first internal stereoscopic structure of an extraction and purification device. Fig. 6 is a schematic diagram of the internal structure of a cooling tank of an extraction and purification device.

[0028] Fig. 7 is a schematic diagram of the three-dimensional structure of the heat conducting sheet and the heat conducting pipe of an extraction and purification device. Fig. 8 is a schematic diagram of the second internal three-dimensional structure of an extraction and purification device.

[0029] FIG. 9 is a schematic diagram of the right side view of an extraction and purification device.

[0030] FIG. 10 is an enlarged schematic diagram of the structure of point A in FIG. 5 of an extraction and purification device.

[0031] The numbers in the figure are: 1, bottom tank; 2, extraction tower; 3, maintenance platform; 4, extraction mixing component; 401, rotating drive member; 402, rotating rod; 403, fixing ring; 404, turntable; 405, blade; 406, stirring blade; 5, first solenoid valve; 6, liquid inlet; 7, second solenoid valve; 8, heavy liquid outlet; 9, safety valve; 10, product cooling component; 1001, first pipeline; 1002, cooling tank; 1003, second pipeline; 1004, top plate; 1005, shunt pipe; 1006, bottom plate; 102, cooling mechanism; 1021, protective shell; 1022, first circulation pipe; 1023, second circulation pipe; 1024, cooler; 10241, heat conducting sheet; 10242, Heat pipe; 1025, pump body; 1026, cooling fan; 11, heating coil. DETAILED DESCRIPTION

[0032] In order to further understand the features, technical means, specific objectives and functions of the present invention, the present invention is further described in detail below in conjunction with the accompanying drawings and specific implementation methods.

[0033] 1 to 10 , the present invention provides: an extraction and purification device, comprising a bottom tank 1, an extraction tower 2, an extraction mixing assembly 4 and a product cooling assembly 10. The bottom tank 1 is the main part of the device, and is usually used to store raw materials or solvents to be extracted. The bottom tank 1 needs to have sufficient capacity and strength to withstand the pressure and temperature fluctuations that may occur during the extraction process. An extraction tower 2 is arranged on the top of the bottom tank 1, and a product cooling assembly 10 is connected to one side of the top of the extraction tower 2. The product cooling assembly 10 is used to cool the product, and the product cooling assembly 10 also liquefies the gaseous product into liquid. The product cooling assembly 10 includes a cooling tank 1002 and a cooling mechanism 102. The cooling tank 1002 is the main part of the cooling assembly and is used to accommodate a cooling medium. A top plate 1004 is arranged in the cooling tank 1002, and a shunt pipe 1005 is connected to the bottom of the top plate 1004, and a bottom plate 1006 is connected to the bottom of the shunt pipe 1005. A first pipe 1001 is connected to the top of the top plate 1004, and one end of the first pipe 1001 passes through the cooling tank 1002 and is connected to the top of the extraction tower 2. The top plate 1004 and the bottom plate 1006 together with the shunt pipe 1005 form a distribution system for evenly distributing the gaseous product in the cooling tank 1002. In order to improve the cooling efficiency.

[0034] In this embodiment, the product is evaporated into gaseous state, and the gaseous product enters into the shunt pipe 1005. The special structure in the shunt pipe 1005 increases the heat conduction area, so that the gaseous product is cooled into liquid, thereby increasing the purity of the product and improving the purification efficiency.

[0035] The top plate 1004 is hollow inside, and the diverter pipe 1005 is vertically inserted into the bottom of the top plate 1004. The top plate 1004 is the initial contact point for the product to enter the cooling tank 1002, and plays a role in preliminary cooling and dispersion of the product. There are several diverter pipes 1005 evenly arranged between the top plate 1004 and the bottom plate 1006, and each diverter pipe 1005 is also provided with several annular protrusions on the outside. The diverter pipe 1005 is used to divert the product flowing into the top plate 1004. The diverter pipe 1005 increases the contact area with the heat transfer agent in the external cooling tank 1002 to quickly cool the product. These protrusions not only increase the contact area between the diverter pipe 1005 and the heat transfer agent in the cooling tank 1002, but also accelerate the cooling process of the product by increasing the contact area with the heat transfer agent.

[0036] In this embodiment, the high-temperature product enters the top plate 1004 through the first pipe 1001 and flows into the diverter pipe 1005. The diverter pipe 1005 evenly diverts the product to different areas of the cooling tank 1002 and increases the contact area with the heat transfer agent through the annular protrusion on its outside, thereby accelerating the cooling process of the product.

[0037] The cooling tank 1002 is hollow inside and filled with a heat conductor. The top plate 1004, the shunt pipe 1005 and the bottom plate 1006 are inserted into the cooling tank 1002. The bottom of the bottom plate 1006 is connected with a second pipe 1003, and the second pipe 1003 passes through the cooling tank 1002 and extends out.

[0038] The product cooling assembly 10 also includes a cooling mechanism 102, which includes a protective shell 1021, and the protective shell 1021 is arranged outside the bottom tank 1, and the protective shell 1021 is used to protect the cooling mechanism 102 from being directly affected by the external environment, while improving the cooling efficiency. A cooler 1024 is installed inside the protective shell 1021; the cooler 1024 includes a heat conductive sheet 10241 and a heat conductive pipe 10242, and the heat conductive sheet 10241 is formed by stacking a number of metal sheets to increase the heat conduction area. The design of the heat conductive sheet 10241 can significantly increase the contact area with the cooling medium (such as cooling water or refrigerant), thereby improving the heat conduction efficiency. The main function of the heat conductive sheet 10241 is to conduct the heat emitted from the gaseous product to the liquid product, and quickly disperse it to a larger area, so as to more effectively exchange heat with the cooling medium. A plurality of heat conducting pipes 10242 are coiled between the heat conducting sheets 10241, and the heat conducting pipes 10242 are made of metal pipes, and the heat conducting pipes 10242 are arranged in a "snake" shape in the heat conducting sheets 10241 to increase the heat conducting area. The design of the heat conducting pipes 10242 further increases the contact area with the heat conducting sheets 10241, thereby improving the heat conduction efficiency. At the same time, the "snake" shape arrangement is also conducive to increasing the flow path of the fluid in the pipe, thereby improving the heat exchange efficiency.

[0039] In this embodiment, the heat conductor circulates in the cooler 1024 in the protective shell 1021. When the heat emitted by the gaseous product converted into a liquid product is conducted to the cooler 1024, the heat conductive sheet 10241 quickly disperses the heat to a larger area and exchanges heat with the heat pipe 10242. Due to the special design of the heat conductive sheet 10241 and the heat pipe 10242 (such as the stacked metal sheets and the "snake"-shaped arrangement of the heat pipe 10242), the heat conduction and heat exchange efficiency are significantly improved, thereby achieving rapid cooling of the product.

[0040] The cooling mechanism 102 further includes a pump body 1025, which is a key component in the cooling mechanism 102 and is responsible for driving the heat transfer agent in the cooling tank 1002 to flow. One end of the pump body 1025 is fixedly connected to the heat transfer pipe 10242 through a pipeline, and one end of the heat transfer pipe 10242 is connected to the second circulation pipe 1023, one end of the second circulation pipe 1023 extends to the upper part of the cooling tank 1002 and extends into the cooling tank 1002, the other end of the pump body 1025 is connected to the first circulation pipe 1022, and one end of the first circulation pipe 1022 passes through the protective shell 1021 and is connected to the lower part of the cooling tank 1002 and extends into the cooling tank 1002. The pump body 1025 is used for the heat transfer agent in the cooling tank 1002 to flow, and the heat transfer agent flows into the heat transfer pipe 10242 to introduce heat to the heat conductive sheet 10241.

[0041] In this embodiment, by starting the pump body 1025, the internal heat conductor is driven to flow. The heat conductor is driven by the pump body 1025, flows through the heat pipe 10242, and exchanges heat with the heat conductive sheet 10241. The cooled heat conductor enters the pump body 1025 again through the first circulation pipe 1022 to form a complete circulation loop.

[0042] The protective shell 1021 has a plurality of heat dissipation slots for heat dissipation on its exterior. At least one heat dissipation fan 1026 is also fixed on the exterior of the protective shell 1021 . The heat dissipation fan 1026 is used to circulate air in the protective shell 1021 and remove heat from the heat conducting sheet 10241 .

[0043] In this embodiment, when the heat dissipation fan 1026 is started, it will inhale external air through the heat dissipation slots. The air will blow through the heat conductive sheet 10241 and the heat conductive pipe 10242. In this way, the heat will be taken away from the protective shell 1021, thereby cooling the internal heat conductive agent.

[0044] The bottom tank 1 is used to store the liquid to be extracted, the extraction tower 2 is used to extract the liquid, and an extraction mixing component 4 is arranged in the extraction tower 2; the extraction mixing component 4 includes a rotating driving member 401 and a rotating rod 402, the rotating driving member 401 is fixed on the top of the extraction tower 2, the rotating rod 402 is vertically rotated and arranged in the extraction tower 2, and one end of the rotating rod 402 extends into the bottom tank 1 and is fixed with a stirring blade 406 for stirring the liquid in the bottom tank 1, the other end of the rotating rod 402 passes through the top of the extraction tower 2 and is fixedly connected to the output end of the rotating driving member 401, and the rotating driving member 401 rotates to drive the rotating rod 402 to rotate and simultaneously drives the stirring blade 406 to rotate.

[0045] In this embodiment, the rotary drive member 401 starts to work, and the rotary drive member 401 drives the rotary rod 402, and the entire rotary rod 402 starts to rotate. As the rotary rod 402 rotates, the stirring blade 406 also starts to rotate, thereby stirring the liquid in the bottom tank 1. This stirring action helps to evenly mix the liquid, making the extraction process more effective.

[0046] The extraction mixing assembly 4 includes a fixed ring 403, a rotating disk 404 and blades 405, and the rotating disk 404 is evenly distributed on the rotating rod 402, and the blades 405 are also evenly distributed on the rotating rod 402, and the fixed ring 403 is evenly fixed on the inner wall of the extraction tower 2, the rotating disk 404 is arranged between the two fixed rings 403, and the blades 405 and the fixed ring 403 are in the same plane.

[0047] In this embodiment, when the rotary drive member 401 starts to work, it drives the rotary rod 402 to rotate. As the rotary rod 402 rotates, the turntable 404 and the blade 405 also rotate together. In this process, the turntable 404 and the blade 405 generate shear force and turbulence through the contact of their surfaces with the liquid during rotation, which promotes the mixing and extraction of the liquid. The components in the mixture will fully contact and form different solubilities, which is conducive to separation. As the turntable 404 rotates, the mixture will be brought to the top of the tower body and then gradually flow downward. In this process, due to the difference in solubility of each component in different solvents, they will gradually separate out, thereby achieving separation of the mixture.

[0048] The interlayer inside the extraction tower 2 is equipped with several heating coils 11, and the heating coils 11 use the electromagnetic induction principle to heat the internal metal components. The heating coils 11 use the electromagnetic induction principle to heat the internal metal components through the action of the electromagnetic field. This heating method has the characteristics of high efficiency, rapidity, and contactlessness, and can quickly transfer heat to the liquid inside the extraction tower 2 to maintain or adjust the temperature of the liquid. Then, the heat is transferred to the liquid inside the extraction tower 2. The bottom tank 1 and the extraction tower 2 are also provided with temperature sensors for detecting the temperature of the liquid; the bottom tank 1 and the extraction tower 2 are externally equipped with a liquid inlet 6, and the liquid inlet 6 is connected to the first electromagnetic valve 5. The bottom tank 1 is also externally equipped with a heavy liquid outlet 8, and the heavy liquid outlet 8 is connected to the second electromagnetic valve 7. The bottom tank 1 and the extraction tower 2 are also externally equipped with an inspection platform 3 for staff to inspect. The inspection platform 3 provides a safe and convenient inspection and maintenance space for the staff. The staff can inspect, repair and replace the bottom tank 1, extraction tower 2 and related components on the inspection platform 3. A safety valve 9 is also provided on the top of the extraction tower 2 to protect the extraction tower 2 from damage under overpressure or other abnormal conditions. When the pressure inside the extraction tower 2 exceeds the set safety value, the safety valve 9 will automatically open to release the internal pressure to prevent the extraction tower 2 from explosion or leakage.

[0049] Working principle: When in use, the liquid inlet pipe is connected to the two first solenoid valves 5, the liquid outlet pipe is connected to the second solenoid valve 7 and the second pipeline 1003, and then connected to other equipment, and then the liquid is passed into the bottom tank 1 and the extraction tower 2. At this time, by starting the rotating drive member 401, the rotating drive member 401 rotates the rotating rod 402, and the rotating rod 402 rotates the turntable 404 and the blade 405. In this process, the components in the mixture will fully contact and form different solubilities, which is conducive to separation. As the turntable 404 rotates, the mixture will be brought to the top of the tower body and then gradually flow downward. In this process, due to the difference in solubility of each component in different solvents, they will gradually separate out, thereby achieving separation of the mixture. In order to make the product purer, the product in the extraction tower 2 is heated to make the temperature in the product reach the evaporation temperature of the product, and then the product evaporates and enters the top plate 1004 from the first pipeline 1001, and then the product enters the branch pipe 1005. A plurality of branch pipes 1005 are used to increase the contact area with the heat conductor, so that the gas is cooled into liquid. By starting the pump body 1025, the pump body 1025 makes the heat conductor in the cooling tank 1002 flow, and the heat conductor flows into the heat pipe 10242. Since the heat pipe 10242 is provided with a heat conducting sheet 10241 on the outside, heat is introduced into the heat conducting sheet 10241. By starting the cooling fan 1026, the cooling fan 1026 makes the air flow, so that the heat conductor is cooled, and the liquefied product is discharged from the second pipeline 1003. The extractant and other impurities flow out from the heavy liquid outlet 8 and the second solenoid valve 7 to another device for processing, thereby completing the purification.

[0050] The above embodiments only express one or several implementation modes of the present invention, and the description thereof is relatively specific and detailed, but it cannot be understood as limiting the scope of the present invention. It should be pointed out that, for a person of ordinary skill in the art, several variations and improvements can be made without departing from the concept of the present invention, and these all belong to the protection scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the attached claims.

Claims

1. An extraction and purification device, Features: The invention comprises a bottom tank (1), an extraction tower (2), an extraction mixing component (4) and a product cooling component (10), wherein the top of the bottom tank (1) is provided with an extraction tower (2), one side of the top of the extraction tower (2) is connected with a product cooling component (10), the product cooling component (10) is used to cool the product, and the product cooling component (10) can also liquefy the gaseous product into liquid, the product cooling component (10) comprises a cooling tank (1002) and a cooling mechanism (102), a top plate (1004) is provided in the cooling tank (1002), a shunt pipe (1005) is connected to the bottom of the top plate (1004), a bottom of the shunt pipe (1005) is connected to the bottom plate (1006), a first pipe (1001) is connected to the top of the top plate (1004), one end of the first pipe (1001) passes through the cooling tank (1002) and is connected to the top of the extraction tower (2); The top plate (1004) is hollow inside, the diverter pipe (1005) is vertically inserted into the bottom of the top plate (1004), and a plurality of diverter pipes (1005) are evenly arranged between the top plate (1004) and the bottom plate (1006), and a plurality of annular protrusions are arranged outside each diverter pipe (1005). The diverter pipe (1005) is used to divert the product flowing into the top plate (1004), and the diverter pipe (1005) increases the contact area with the heat transfer agent in the external cooling tank (1002) to quickly cool the product; The interior of the cooling tank (1002) is hollow and filled with a heat conductor. The top plate (1004), the shunt pipe (1005) and the bottom plate (1006) are inserted into the cooling tank (1002). The bottom of the bottom plate (1006) is connected to a second pipe (1003), and the second pipe (1003) passes through the cooling tank (1002) and extends out. The product cooling assembly (10) further comprises a cooling mechanism (102), wherein the cooling mechanism (102) comprises a protective shell (1021), and the protective shell (1021) is arranged outside the bottom tank (1), and a cooler (1024) is installed inside the protective shell (1021); The cooler (1024) comprises a heat conducting sheet (10241) and a heat conducting pipe (10242), wherein the heat conducting sheet (10241) is formed by stacking a plurality of metal sheets to increase the heat conducting area, and a plurality of heat conducting pipes (10242) are coiled between the heat conducting sheets (10241), and the heat conducting pipes (10242) are made of metal pipes, and the heat conducting pipes (10242) are arranged in a "snake" shape in the heat conducting sheet (10241) to increase the heat conducting area; The cooling mechanism (102) further comprises a pump body (1025), one end of the pump body (1025) is fixedly connected to the heat conducting pipe (10242) through a pipeline, and one end of the heat conducting pipe (10242) is connected to a second circulation pipe (1023), one end of the second circulation pipe (1023) extends to the upper part of the cooling tank (1002) and extends into the cooling tank (1002), the other end of the pump body (1025) is connected to the first circulation pipe (1022), and one end of the first circulation pipe (1022) passes through the protective shell (1021) and is connected to the lower part of the cooling tank (1002) and extends into the cooling tank (1002), the pump body (1025) is used for the heat conducting agent in the cooling tank (1002) to flow, the heat conducting agent flows into the heat conducting pipe (10242), and heat is introduced into the heat conducting sheet (10241); The bottom tank (1) is used to store the liquid to be extracted, the extraction tower (2) is used to extract the liquid, and the extraction tower (2) is provided with an extraction mixing component (4); The extraction and mixing assembly (4) comprises a rotary drive member (401) and a rotary rod (402), wherein the rotary drive member (401) is fixed on the top of the extraction tower (2), and the rotary rod (402) is vertically rotatably arranged in the extraction tower (2), and one end of the rotary rod (402) extends into the bottom tank (1) and is fixed with a stirring blade (406) for stirring the liquid in the bottom tank (1), and the other end of the rotary rod (402) passes through the top of the extraction tower (2) and is fixedly connected to the output end of the rotary drive member (401), and the rotary drive member (401) rotates to drive the rotary rod (402) to rotate and simultaneously drives the stirring blade (406) to rotate; The extraction and mixing assembly (4) comprises a fixed ring (403), a rotating disk (404) and blades (405), wherein the rotating disk (404) is evenly distributed on the rotating rod (402), and the blades (405) are also evenly distributed on the rotating rod (402), and the fixed ring (403) is evenly fixed on the inner wall of the extraction tower (2), the rotating disk (404) is arranged between the two fixed rings (403), and the blades (405) and the fixed ring (403) are in the same plane; A plurality of heating coils (11) are installed in the interlayer inside the extraction tower (2), and the heating coils (11) use the electromagnetic induction principle to heat the metal components inside, thereby transferring the heat to the liquid inside the extraction tower (2), and temperature sensors for detecting the temperature of the liquid are also arranged inside the bottom tank (1) and the extraction tower (2); The bottom tank (1) and the extraction tower (2) are provided with a liquid inlet (6) on the outside, and the liquid inlet (6) is connected to a first solenoid valve (5). The bottom tank (1) is also provided with a heavy liquid outlet (8) on the outside, and the heavy liquid outlet (8) is connected to a second solenoid valve (7). The bottom tank (1) and the extraction tower (2) are also provided with a maintenance platform (3) for maintenance by staff on the outside, and a safety valve (9) is also provided on the top of the extraction tower (2).

2. An extraction and purification device according to claim 1, Features: The protective shell (1021) is provided with a plurality of heat dissipation slots for dissipating heat on the outside. At least one heat dissipation fan (1026) is also fixed on the outside of the protective shell (1021). The heat dissipation fan (1026) is used to flow air in the protective shell (1021) and remove heat from the heat conductive sheet (10241).

3. A method for efficiently extracting furanol, comprising: using an extraction and purification device according to any one of claims 1 to 2. Features: The following steps are involved: S1: The extractant and the product to be extracted are introduced into the bottom tank (1) and the extraction tower (2) from the two liquid inlets (6). The rotary drive member (401) is started, and the rotary drive member (401) rotates the rotary rod (402), and the rotary rod (402) rotates the rotating disk (404) and the blades (405). In this process, the components in the mixture will fully contact each other and form different solubilities, which is conducive to separation. As the rotating disk (404) rotates, the mixture will be brought to the top of the tower body and then gradually flow downward. In this process, due to the difference in solubility of the components in different solvents, they will gradually separate, thereby achieving separation of the mixture; S2: In order to make the product after extraction more pure, the product in the extraction tower (2) is heated to make the temperature in the product reach the evaporation temperature of the product, and then the product evaporates and enters the top plate (1004) from the first pipeline (1001), and then the product enters the diversion pipe (1005). A plurality of diversion pipes (1005) are used to increase the contact area with the heat conductive agent, so that the gas is cooled into liquid; S3: By starting the pump body (1025), the pump body (1025) causes the heat conductive agent in the cooling tank (1002) to flow, and the heat conductive agent flows into the heat conductive pipe (10242). Since a heat conductive sheet (10241) is provided outside the heat conductive pipe (10242), heat is introduced into the heat conductive sheet (10241). By starting the heat dissipation fan (1026), the heat dissipation fan (1026) causes air to flow, thereby cooling the heat conductive agent; S4: The liquefied product flows out from the second pipeline (1003), while the extractant and other impurities flow out from the heavy liquid outlet (8) and the second solenoid valve (7), completing the purification.