Polymerization reactor for continuous production of spandex and polymerization reaction method thereof

By designing a vertical consecutive polymerization reactor including the L -shaped board, the horizontal and vertical mixed rotation is achieved, which solves the problem of uneven distribution and layered phenomenon in the existing technology, and significantly improves the uniformity of chemical reactions. Sexuality and efficiency reduce the cost of cleaning and maintenance.

CN119346041APending Publication Date: 2025-01-24HANGZHOU SHUERZI SPANDEX CO LTD
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Patent Information

Application Number
CN202411325192.3
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-09-23
Publication Date
2025-01-24

AI Technical Summary

Technical Problem

The existing polymerization reactor for continuous production of spandex is mixed by lateral agitation and vertical flip, resulting in uneven distribution of materials and stratification, which affects the uniformity and efficiency of chemical reactions.

Method used

Design a vertical consecutive production polymerization reactor including the L -shaped board, drive the first rotation rotor by the setting motor, driver rod, first gear, and second gear to drive Mixing the vertical direction to avoid layering.

Benefits of technology

Through horizontal and vertical mixing and rotation, the uniform distribution of materials is significantly improved, the uniformity and efficiency of chemical reactions are improved, the formation of gel and scaling is reduced, and the cleaning frequency and maintenance costs of the reactor are reduced.

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Abstract

The invention discloses a polymerization reactor for continuous production of spandex and a polymerization reaction method.The polymerization reactor comprises an L-shaped plate, a production mechanism for spandex production is arranged at the transverse top of the L-shaped plate, and the production mechanism comprises a transverse mixing assembly, a second mixing assembly and a third mixing assembly, a first rotating rod is rotationally connected to the reactor body through a first rotating hole, a stirring wheel is connected to the bottom of the first rotating rod through a vibration assembly, and a first rectangular plate is arranged on the vertical side wall of an L-shaped plate. The reactor solves the problems that in the prior art, materials are generally mixed through transverse stirring and cannot be turned over vertically, so that the materials are possibly distributed unevenly, the layering phenomenon occurs, and the uniformity and efficiency of chemical reaction are affected.
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Description

Technical Field

[0001] The invention relates to the technical field of spandex production, in particular to a polymerization reactor for continuous spandex production and a polymerization reaction method thereof. Background Art

[0002] The polymerization reactor for continuous production of spandex is a device specially used for spandex fiber production. It is used to convert raw materials (such as diisocyanate and polyester polyol) into spandex polymer through polymerization reaction. This reactor is usually used in the continuous polymerization process of spandex. Compared with the traditional intermittent polymerization process, the continuous polymerization process can provide more uniform product quality, simplify the production process, reduce energy consumption, and improve production efficiency.

[0003] The existing reactors still have the following problems. Reference publication number CN105170066B discloses a continuous polymerization reactor for producing mesophase carbon microspheres, including a shell and a rapid temperature raising device and a double stirring transmission device arranged on the top of the shell; the shell is provided with a nitrogen port, a discharge port and a jacket, and a frame agitator and a split-flow main agitator are arranged inside the shell; the bottom of the rapid temperature raising device is provided with a material inlet and a material outlet; the frame agitator is fixed with a scraper group and a horizontal baffle; the blade group of the split-flow main agitator is cross-arranged with the horizontal baffle. The reactor of the invention rotates in reverse to make part of the material move to the upper part of the shell, and the reaction polymerization effect becomes more uniform as the reaction time increases, which promotes the uniform and rapid growth of the mesophase carbon microspheres, and achieves the purpose of efficient, energy-saving, low-cost and continuous production of mesophase carbon microspheres.

[0004] However, the above technology cannot solve the problem in the prior art that the reactor generally only mixes the materials by horizontal stirring and cannot be turned vertically, which may lead to uneven distribution of the materials and stratification, thereby affecting the uniformity and efficiency of the chemical reaction. To this end, the present invention provides a polymerization reactor for continuous production of spandex and a polymerization reaction method thereof. Summary of the invention

[0005] In view of the deficiencies in the prior art, the present invention provides a polymerization reactor for continuous production of spandex and a polymerization reaction method thereof, which solves the problem in the prior art that the reactor generally only mixes the materials by horizontal stirring and cannot be turned vertically, which may lead to uneven distribution of the materials, causing stratification and affecting the uniformity and efficiency of the chemical reaction.

[0006] To achieve the above object, the present invention is implemented by the following technical scheme: A polymerization reactor for continuous production of spandex, comprising an L-shaped plate, wherein a production mechanism for spandex production is arranged on the top of the L-shaped plate, and the production mechanism comprises:

[0007] A transverse mixing assembly, comprising a reactor body to which the transverse top of an L-shaped plate is fixed via a group of fixing columns, a first rotating rod is rotatably connected to the reactor body via a first rotating hole, a stirring wheel is connected to the bottom of the first rotating rod via a vibration assembly, a first rectangular plate is disposed on the vertical side wall of the L-shaped plate, and a driving assembly for driving the first rotating rod to rotate is disposed on the first rectangular plate;

[0008] A vertical mixing assembly comprises a pair of circular blocks fixed on a first rotating rod, a pair of circular block side walls are rotatably connected to a flipping rod, a pair of flipping rods are fixed to a first arc plate, a pair of flipping rods are fixed to a second arc plate, a first annular groove is provided on the inner wall of the reactor body, and a flipping assembly for driving a pair of flipping rods to rotate is arranged in the first annular groove.

[0009] Preferably, the flip assembly includes an annular plate rotatably connected between the relative groove walls of the first annular groove through a pair of second annular grooves, and the annular plate is rotatably connected to a pair of flip rods through a pair of second rotating holes, a pair of flip rods are fixedly connected to a third gear at one end, a gear ring is fixed in the first annular groove, and a pair of third gears are meshingly connected to the gear ring.

[0010] Preferably, the vibration assembly includes a rectangular groove opened on the first rotating rod, a rectangular block is slidably connected in the rectangular groove, a sliding tube is fixed on the rectangular block, and the sliding tube is slidably connected to the first rotating rod, and the stirring wheel is fixed on the sliding tube.

[0011] Preferably, an eccentric block is fixedly connected to the flip rod, an eccentric groove is opened on the side wall of the eccentric block, an L-shaped rod is fixedly connected to the top of the sliding tube, one lateral end of the L-shaped rod is slidably connected in the eccentric groove, a rectangular box is fixedly connected to the first rotating rod, both sides of the rectangular box are rotatably connected to the flip rod through the third rotating hole, and the bottom of the rectangular box is slidably connected to the sliding tube through the sliding hole.

[0012] Preferably, the driving assembly includes a second rectangular plate, the second rectangular plate is fixed to the vertical side wall of the L-shaped plate, a motor is fixed to the bottom of the second rectangular plate, a driving rod is provided at the output end of the motor, the bottom of the driving rod is rotatably connected to the top of the first rectangular plate, a first gear is fixed to the driving rod, a second gear is fixed to the first rotating rod, and the first gear is meshingly connected to the second gear.

[0013] Preferably, a group of arc-shaped through grooves are opened on the inner wall of the reactor body, a first flow groove is opened on the top of the first rotating rod, a pair of the circular blocks are each provided with a first through groove, a pair of the flipping rods are each provided with a second flow groove, and a group of first inclined grooves are opened on the pair of the flipping rods.

[0014] Preferably, an annular block is fixedly connected in the second flow groove, a blocking block is fixedly connected to the side wall of the annular block via a spring, and a group of second inclined grooves are formed on the blocking block.

[0015] Preferably, a water pump is fixedly connected to the bottom of the second rectangular plate, an input end of the water pump is connected to a connecting pipe, an output end of the water pump is connected to a fixed pipe, and the fixed pipe is rotatably connected to the top of the first rotating rod.

[0016] Preferably, an outlet valve is installed at the bottom outlet of the reactor body, and an inlet valve is installed at the top inlet of the reactor body.

[0017] The polymerization reaction method of the polymerization reactor for continuous production of spandex specifically comprises the following steps:

[0018] S1: The first rotating rod is driven to rotate by the driving assembly, and the first rotating rod drives a pair of flipping rods to rotate;

[0019] S2: The flip assembly drives the flip rod to rotate, thereby driving the first arc plate and the second arc plate to rotate;

[0020] S3: The stirring wheel can be driven to rotate by rotating the first rotating rod, and the stirring wheel can be driven to vibrate up and down by the vibration component.

[0021] Beneficial Effects

[0022] The present invention provides a polymerization reactor for continuous production of spandex and a polymerization reaction method thereof. Compared with the prior art, it has the following beneficial effects:

[0023] (1) The reactor can drive the first rotating rod to rotate through the motor, driving rod, first gear and second gear, thereby driving the stirring wheel to rotate, and the flip rod is rotatably connected to the side wall of the circular block, and one end of the flip rod extends into the first annular groove. Through the third gear and gear ring, the first rotating rod can drive the stirring wheel to rotate for mixing while driving the flip rod to rotate. The flip rod is meshed with the gear ring through the third gear, so that the flip rod can rotate simultaneously, so that it can rotate vertically while rotating horizontally, avoiding the problem of simple horizontal rotation for mixing and stirring in the prior art, which makes the mixing efficiency slow and cannot ensure sufficient uniformity.

[0024] (2) The reactor is provided with an eccentric block fixedly connected to the first rotating rod and capable of driving the sliding tube to vibrate by means of an L-shaped rod having one lateral end slidably connected to an eccentric groove provided on the side wall of the eccentric block, thereby driving the stirring wheel to rotate and vibrate at the same time. Since vibration during stirring can reduce the formation of gel and scale, the cleaning frequency and maintenance cost of the reactor can be reduced, and the gel can be prevented from adhering to the inner wall of the reactor body and being inconvenient to clean.

[0025] (3) The reactor can prevent the raw materials from flowing into the first annular groove and being unable to flow out during spandex production by setting up a group of arc-shaped grooves, thereby preventing the raw materials from flowing into the first annular groove and being unable to flow out, thereby causing material loss and making it impossible to produce spandex that requires precise control of the raw material ratio. When cleaning the inside of the reactor body, in order to avoid the inconvenience of cleaning the gear ring and the third gear being located in the first annular groove, the first rotating rod, the circular block and the flipping rod are connected by opening a first flow groove, a first through groove and a second flow groove, so that during cleaning, water can be connected to the water pipe through a connecting pipe and transported by a water pump, so that it can be flushed through a group of first inclined grooves opened on the flipping rod. The blocking block is connected by a spring, so that the blocking block can be moved under the impact of the water flow driven by the water pump, so that the second inclined groove and the first inclined groove are connected, so that the cleaning water can clean the gear and the gear ring, and can flow into the reactor body through the arc-shaped through groove. BRIEF DESCRIPTION OF THE DRAWINGS

[0026] Figure 1 A perspective view of the present invention;

[0027] Figure 2 It is a schematic diagram of the outlet valve of the present invention;

[0028] Figure 3 It is a horizontal cross-sectional view of the reactor body of the present invention;

[0029] Figure 4 It is a vertical cross-sectional view of the reactor body of the present invention;

[0030] Figure 5 is a schematic diagram of a first rotating rod of the present invention;

[0031] Figure 6 It is the exploded view of the circular block of the present invention;

[0032] Figure 7 It is an exploded view of a rectangular block of the present invention;

[0033] Figure 8 A partial cross-sectional view of the flip rod of the present invention;

[0034] Fig. 9 For the present invention Figure 4 A magnified view of middle;

[0035] Fig.10 For the present invention Figure 5 Enlarged view of B.

[0036] In the figure: 1, L-shaped plate; 2, reactor body; 3, first rotating rod; 4, stirring wheel; 5, first rectangular plate; 6, circular block; 7, flip rod; 8, first arc plate; 9, second arc plate; 10, first annular groove; 11, annular plate; 12, third gear; 13, gear ring; 14, rectangular groove; 15, rectangular block; 16, sliding pipe; 17, eccentric block; 18, eccentric groove; 19, L-shaped rod; 20, rectangular box; 21, second rectangular plate; 22, motor; 23, driving rod; 24, first gear; 25, second gear; 26, arc through groove; 27, first flow groove; 28, first through groove; 29, second flow groove; 30, first inclined groove; 31, annular block; 32, blocking block; 33, second inclined groove; 34, water pump; 35, connecting pipe; 36, fixed pipe; 37, outlet valve; 38, inlet valve. DETAILED DESCRIPTION

[0037] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0038] See also Figure 1-10 , the present invention provides a technical solution:

[0039] Embodiment 1: A polymerization reactor for continuous production of spandex and a polymerization reaction method thereof, comprising an L-shaped plate 1, wherein a production mechanism for spandex production is arranged at the lateral top of the L-shaped plate 1, and the production mechanism comprises: a lateral mixing assembly, comprising a reactor body 2 fixedly connected to the lateral top of the L-shaped plate 1 by a group of fixed columns, a first rotating rod 3 rotatably connected to the reactor body 2 through a first rotating hole, a stirring wheel 4 connected to the bottom of the first rotating rod 3 through a vibration assembly, a first rectangular plate 5 is arranged on the vertical side wall of the L-shaped plate 1, and a driving assembly for driving the first rotating rod 3 to rotate is arranged on the first rectangular plate 5; a vertical mixing assembly, comprising a pair of circular blocks 6 fixedly connected to the first rotating rod 3, a The side walls of the circular blocks 6 are rotatably connected with flip rods 7, a first arc plate 8 is fixedly connected to a pair of flip rods 7, a second arc plate 9 is fixedly connected to a pair of flip rods 7, a first annular groove 10 is provided on the inner wall of the reactor body 2, a flip assembly for driving the pair of flip rods 7 to rotate is arranged in the first annular groove 10, the flip assembly includes an annular plate 11 rotatably connected between the first annular groove 10 and the groove wall through a pair of second annular grooves, and the annular plate 11 is rotatably connected to the pair of flip rods 7 through a pair of second rotating holes, a third gear 12 is fixedly connected to one end of the pair of flip rods 7, a gear ring 13 is fixedly connected in the first annular groove 10, and a pair of third gears 12 are meshed and connected to the gear ring 13. On the ring 13, the driving assembly includes a second rectangular plate 21, the second rectangular plate 21 is fixedly connected to the vertical side wall of the L-shaped plate 1, a motor 22 is fixedly connected to the bottom of the second rectangular plate 21, and a driving rod 23 is provided at the output end of the motor 22. The bottom of the driving rod 23 is rotatably connected to the top of the first rectangular plate 5, a first gear 24 is fixedly connected to the driving rod 23, and a second gear 25 is fixedly connected to the first rotating rod 3. The first gear 24 is meshed with the second gear 25. An outlet valve 37 is installed at the bottom outlet of the reactor body 2, and an inlet valve 38 is installed at the top inlet of the reactor body 2; the motor 22, the driving rod 23, the first gear 24 and the second gear 25 can be driven by the first rotating rod 3. The movable rod 3 rotates, thereby driving the set stirring wheel 4 to rotate, and is rotatably connected to the side wall of the circular block 6 through the set flipping rod 7, and one end of the flipping rod 7 extends into the first annular groove 10. Through the arrangement of the third gear 12 and the gear ring 13, the first rotating rod 3 can drive the stirring wheel 4 to rotate for mixing while driving the flipping rod 7 to rotate, and the flipping rod 7 is engaged with the gear ring 13 through the third gear 12, so that the flipping rod 7 can be rotated at the same time, so that it can be rotated vertically while rotating horizontally, avoiding the problem that the prior art only performs simple horizontal rotation for mixing and stirring, resulting in slow mixing efficiency and failure to ensure sufficient uniformity.

[0040] Embodiment 2: The vibration assembly includes a rectangular groove 14 provided on the first rotating rod 3, a rectangular block 15 is slidably connected in the rectangular groove 14, a sliding tube 16 is fixedly connected to the rectangular block 15, and the sliding tube 16 is slidably connected to the first rotating rod 3, the stirring wheel 4 is fixedly connected to the sliding tube 16, an eccentric block 17 is fixedly connected to the flip rod 7, an eccentric groove 18 is provided on the side wall of the eccentric block 17, an L-shaped rod 19 is fixedly connected to the top of the sliding tube 16, and one lateral end of the L-shaped rod 19 is slidably connected to the eccentric groove 18, a rectangular box 20 is fixedly connected to the first rotating rod 3, and the two sides of the rectangular box 20 are respectively connected by the third rotating The hole is rotatably connected to the flip rod 7, and the bottom of the rectangular box 20 is slidably connected to the sliding tube 16 through the sliding hole; an L-shaped rod 19 with an eccentric block 17 fixedly connected to the first rotating rod 3 and one lateral end of which is slidably connected to the eccentric groove 18 opened on the side wall of the eccentric block 17 drives the sliding tube 16 to vibrate, thereby driving the stirring wheel 4 to rotate and vibrate at the same time. Since vibration during stirring can reduce the formation of gel and scaling, the cleaning frequency and maintenance cost of the reactor can be reduced, and the gel can be prevented from adhering to the inner wall of the reactor body 2 and being inconvenient to clean.

[0041] Embodiment 3: A group of arcuate through grooves 26 are provided on the inner wall of the reactor body 2, a first flow groove 27 is provided on the top of the first rotating rod 3, a pair of circular blocks 6 are provided with first through grooves 28, a pair of flipping rods 7 are provided with second flow grooves 29, a pair of flipping rods 7 are provided with a group of first inclined grooves 30, an annular block 31 is fixedly connected in the second flow groove 29, a blocking block 32 is fixedly connected to the side wall of the annular block 31 through a spring, a group of second inclined grooves 33 are provided on the blocking block 32, a water pump 34 is fixedly connected to the bottom of the second rectangular plate 21, a connecting pipe 35 is connected to the input end of the water pump 34, and a fixed pipe 36 is connected to the output end of the water pump 34, and the fixed pipe 36 is rotatably connected to the top of the first rotating rod 3; by setting a group of arcuate through grooves 26, it is possible to prevent the raw materials from flowing into the first annular groove 10 and being unable to flow out during the production of spandex, thereby causing material loss, without The method allows the production of spandex that requires precise control of the raw material ratio to be carried out, and when cleaning the inside of the reactor body 2, in order to avoid the inconvenience of cleaning of the gear ring 13 and the third gear 12 located in the first annular groove 10, the first rotating rod 3, the circular block 6 and the flip rod 7 are connected by opening a first flow groove 27, a first through groove 28 and a second flow groove 29, so that during cleaning, the water pipe can be connected through a connecting pipe 35 and transported through a water pump 34, so that it can be flushed through a group of first inclined grooves 30 opened on the flip rod 7, and the blocking block 32 is connected by a spring, so that the blocking block 32 can be moved under the impact of the water flow driven by the water pump 34, so that the second inclined groove 33 and the first inclined groove 30 are connected, so that the cleaning water can clean the gear and the gear ring 13, and can flow into the reactor body 2 through the arc through groove 26.

[0042] Meanwhile, the contents not described in detail in this specification belong to the prior art known to those skilled in the art.

[0043] During operation, the motor 22, the driving rod 23, the first gear 24 and the second gear 25 can drive the first rotating rod 3 to rotate, thereby driving the stirring wheel 4 to rotate, and the flipping rod 7 is rotatably connected to the side wall of the circular block 6, and one end of the flipping rod 7 extends into the first annular groove 10. Through the third gear 12 and the gear ring 13, the first rotating rod 3 can drive the stirring wheel 4 to rotate for mixing, and drive the flipping rod 7 to rotate, and the flipping rod 7 is meshed with the gear ring 13 through the third gear 12, so that the flipping rod 7 can be turned. 7 is rotated simultaneously, so that it can rotate vertically while rotating horizontally, avoiding the problem that the mixing and stirring in the prior art is only performed by simple horizontal rotation, which makes the mixing efficiency slow and cannot ensure sufficient uniformity. The sliding tube 16 is driven to vibrate by an L-shaped rod 19 with an eccentric block 17 fixedly connected to the first rotating rod 3 and one end of which can be slidably connected to the eccentric groove 18 opened on the side wall of the eccentric block 17, thereby driving the stirring wheel 4 to vibrate while rotating. Since vibration during stirring can reduce the formation of gel and scaling Therefore, the cleaning frequency and maintenance cost of the reactor can be reduced, and the gel can be prevented from adhering to the inner wall of the reactor body 2 and being inconvenient to clean. The set of arc-shaped through grooves 26 can prevent the raw materials from flowing into the first annular groove 10 and being unable to flow out during the spandex production, thereby causing material loss and making it impossible to produce spandex that requires precise control of the raw material ratio. When cleaning the inside of the reactor body 2, in order to prevent the gear ring 13 and the third gear 12 from being located in the first annular groove 10 and being inconvenient to clean, the first rotating rod 3, the circular block 6 and the flipping rod 7 are opened through the first rotating rod 3, the circular block 6 and the flipping rod 7. A flow groove 27, a first through groove 28 and a second flow groove 29 are connected, so that during cleaning, a water pipe can be connected through a connecting pipe 35 and transported through a water pump 34, so that flushing can be carried out through a group of first inclined grooves 30 opened on the flip rod 7. The blocking block 32 is connected by a spring, and the blocking block 32 can be moved under the impact of the water flow driven by the water pump 34, so that the second inclined groove 33 and the first inclined groove 30 are connected, so that the cleaning water can clean the gear and the gear ring 13, and can flow into the reactor body 2 through the arc-shaped through groove 26.

[0044] A polymerization reaction method of a polymerization reactor for continuous production of spandex, specifically comprising the following steps:

[0045] S1: The first rotating rod 3 is driven to rotate by the driving assembly, and the first rotating rod 3 drives a pair of flipping rods 7 to rotate;

[0046] S2: The flipping assembly drives the flipping rod 7 to rotate, thereby driving the first arc plate 8 and the second arc plate 9 to rotate;

[0047] S3: The first rotating rod 3 is rotated to drive the stirring wheel 4 to rotate, and the vibration component drives the stirring wheel 4 to vibrate up and down.

[0048] It should be noted that, in this article, relational terms such as first and second, etc. are only used to distinguish one entity or operation from another entity or operation, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Moreover, the terms "include", "comprise" or any other variants thereof are intended to cover non-exclusive inclusion, so that a process, method, article or device including a series of elements includes not only those elements, but also other elements not explicitly listed, or also includes elements inherent to such process, method, article or device.

[0049] Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A polymerization reactor for continuous production of spandex, comprising an L-shaped plate (1), characterized in that: The L-shaped plate (1) is provided with a production mechanism for spandex production at the top thereof, and the production mechanism comprises: A transverse mixing assembly comprises a reactor body (2) fixedly connected to the transverse top of an L-shaped plate (1) via a group of fixing columns, a first rotating rod (3) rotatably connected to the reactor body (2) via a first rotating hole, a stirring wheel (4) connected to the bottom of the first rotating rod (3) via a vibration assembly, a first rectangular plate (5) provided on the vertical side wall of the L-shaped plate (1), and a driving assembly for driving the first rotating rod (3) to rotate is provided on the first rectangular plate (5); A vertical mixing assembly comprises a pair of circular blocks (6) fixedly connected to a first rotating rod (3), the side walls of the pair of circular blocks (6) are both rotatably connected to a flipping rod (7), the pair of flipping rods (7) are both fixedly connected to a first arc plate (8), the pair of flipping rods (7) are both fixedly connected to a second arc plate (9), a first annular groove (10) is provided on the inner wall of the reactor body (2), and a flipping assembly for driving the pair of flipping rods (7) to rotate is arranged in the first annular groove (10).

2. A polymerization reactor for continuous production of spandex according to claim 1, characterized in that: The flip assembly comprises an annular plate (11) rotatably connected between the first annular groove (10) and the groove wall via a pair of second annular grooves, and the annular plate (11) is rotatably connected to a pair of flip rods (7) via a pair of second rotating holes, a third gear (12) is fixedly connected to one end of the pair of flip rods (7), a gear ring (13) is fixedly connected to the first annular groove (10), and a pair of the third gears (12) are meshingly connected to the gear ring (13).

3. The polymerization reactor for continuous production of spandex according to claim 1, characterized in that: The vibration assembly comprises a rectangular groove (14) formed on a first rotating rod (3), a rectangular block (15) being slidably connected in the rectangular groove (14), a sliding tube (16) being fixedly connected to the rectangular block (15), and the sliding tube (16) being slidably connected to the first rotating rod (3), and the stirring wheel (4) being fixedly connected to the sliding tube (16).

4. A polymerization reactor for continuous production of spandex according to claim 3, characterized in that: An eccentric block (17) is fixedly connected to the flip rod (7), and an eccentric groove (18) is provided on the side wall of the eccentric block (17). An L-shaped rod (19) is fixedly connected to the top of the sliding tube (16), and one lateral end of the L-shaped rod (19) is slidably connected in the eccentric groove (18). A rectangular box (20) is fixedly connected to the first rotating rod (3), and both sides of the rectangular box (20) are rotatably connected to the flip rod (7) through third rotating holes, and the bottom of the rectangular box (20) is slidably connected to the sliding tube (16) through sliding holes.

5. The polymerization reactor for continuous production of spandex according to claim 1, characterized in that: The driving assembly comprises a second rectangular plate (21), the second rectangular plate (21) is fixedly connected to the vertical side wall of the L-shaped plate (1), a motor (22) is fixedly connected to the bottom of the second rectangular plate (21), a driving rod (23) is provided at the output end of the motor (22), the bottom of the driving rod (23) is rotatably connected to the top of the first rectangular plate (5), a first gear (24) is fixedly connected to the driving rod (23), a second gear (25) is fixedly connected to the first rotating rod (3), and the first gear (24) is meshingly connected to the second gear (25).

6. The polymerization reactor for continuous production of spandex according to claim 1, characterized in that: A group of arc-shaped through grooves (26) are provided on the inner wall of the reactor body (2), a first flow groove (27) is provided on the top of the first rotating rod (3), a pair of the circular blocks (6) are provided with first through grooves (28), a pair of the flipping rods (7) are provided with second flow grooves (29), and a group of first inclined grooves (30) are provided on the pair of the flipping rods (7).

7. A polymerization reactor for continuous production of spandex according to claim 6, characterized in that: An annular block (31) is fixedly connected inside the second circulation groove (29), a blocking block (32) is fixedly connected to the side wall of the annular block (31) via a spring, and a group of second inclined grooves (33) are formed on the blocking block (32).

8. The polymerization reactor for continuous production of spandex according to claim 5, characterized in that: A water pump (34) is fixedly connected to the bottom of the second rectangular plate (21); the input end of the water pump (34) is connected to a connecting pipe (35); the output end of the water pump (34) is connected to a fixed pipe (36); and the fixed pipe (36) is rotatably connected to the top of the first rotating rod (3).

9. The polymerization reactor for continuous production of spandex according to claim 1, characterized in that: An outlet valve (37) is installed at the bottom outlet of the reactor body (2), and an inlet valve (38) is installed at the top inlet of the reactor body (2).

10. The polymerization method of a polymerization reactor for continuous production of spandex according to any one of claims 1 to 9, characterized in that: The specific steps include: S1: the first rotating rod (3) is driven to rotate by the driving assembly, and the first rotating rod (3) drives the pair of flipping rods (7) to rotate; S2: The turning rod (7) is driven to rotate by the turning assembly, thereby driving the first arc plate (8) and the second arc plate (9) to rotate; S3: The first rotating rod (3) is rotated to drive the stirring wheel (4) to rotate, and the vibration component is used to drive the stirring wheel (4) to vibrate up and down.

Citation Information

Patent Citations

  • A Continuous Polymerization Reactor for the Production of Mesophase Carbon Microspheres

    CN105170066B