Carbon preparation device for synthesizing polycrystalline silicon with specific shape from recrystallization waste

Abstract

The invention relates to the technical field of polycrystalline silicon carbon preparation devices, and discloses a preparation device for synthesizing polycrystalline silicon carbon in a specific shape from recrystallization waste, which comprises a reduction furnace, and is characterized in that the top of the reduction furnace is fixedly connected with a protection frame, the interior of the protection frame is fixedly connected with a transmission mechanism, and the transmission mechanism comprises a transmission rod; the outer surface of the transmission rod is movably connected with the stand column, the inner side of the stand column is fixedly connected with the edge, and the inner surface of the edge is fixedly connected with the abrasive disc, so that the reaction can be completed in a shorter time, the reaction efficiency is improved, and meanwhile, the occurrence opportunities of adverse factors such as side reaction and reactant decomposition are reduced. The purity and yield of the product are improved, and the emission of the treated waste gas greatly reduces the peculiar smell and harmful gas concentration in a laboratory, so that a cleaner and safer working environment is provided for workers, and the improvement of the working efficiency and the reduction of occupational diseases are facilitated.

Description

Technical Field

[0001] The present invention relates to the technical field of polycrystalline silicon carbon preparation equipment, and more specifically to a polycrystalline silicon carbon preparation equipment for synthesizing a specific shape from recrystallized waste materials. Background Art

[0002] Recrystallization waste usually refers to the residual material produced in the recrystallization process that has not been effectively utilized or needs to be further processed. Recrystallization is a physical or chemical process that achieves the purpose of purification or separation by dissolving the substance in a solvent and then recrystallizing it. In this process, the main target substance will precipitate from the solution and form crystals, while the remaining non-target substances will also form crystals but are regarded as waste due to their different structures from the target crystals. In order to make the waste effectively utilized, a polycrystalline silicon carbon preparation device is required. It synthesizes polycrystalline silicon carbide materials with specific shapes and sizes by controlling crystal growth conditions such as temperature, pressure and gas. The polycrystalline silicon preparation device usually includes a material handling device, a reduction furnace, a cooling system, and an automation and monitoring system.

[0003] The shortcomings of the existing recrystallization waste synthesis of specific shape polycrystalline silicon carbon preparation device:

[0004] First, the waste material that precipitates from the solution and forms crystals is in a crystalline state. Since the waste material is naturally cooled, its crystals will appear as larger particles. Larger particles mean that the contact area between the unit mass of waste material and the reaction medium is reduced, which may lead to a slower reaction rate, thereby reducing the overall reaction efficiency and output.

[0005] Second: During the preparation of polycrystalline silicon carbon, waste materials and other compounds will produce high-temperature reactions. In this process, in addition to the target product silicon carbide, potentially harmful waste gases may also be generated. These waste gases are directly discharged into the laboratory without treatment. Although these waste gases are harmless to the human body in the short term, they can cause suffocation risks at high concentrations and also have long-term impacts on the environment. Summary of the invention

[0006] In order to overcome the above-mentioned defects of the prior art, the present invention provides a device for preparing polycrystalline silicon carbon of a specific shape by synthesizing polycrystalline silicon carbon from recrystallized waste materials to solve the problems existing in the above-mentioned background technology.

[0007] The present invention provides the following technical solution: a device for preparing polycrystalline silicon carbon of a specific shape by synthesizing recrystallized waste, comprising a reduction furnace, a protective frame fixedly connected to the top of the reduction furnace, a transmission mechanism fixedly connected to the inside of the protective frame, the transmission mechanism comprising a transmission rod, a column movably connected to the outer surface of the transmission rod, an edge fixedly connected to the inner side of the column, a grinding sheet fixedly connected to the inner surface of the edge, a storage box is provided on the top of the grinding sheet, a pressing mechanism is fixedly connected to one side of the storage box, a purification device is fixedly connected to one side of the bottom of the reduction furnace, and a filtering device is movably connected to the inner surface of the purification device;

[0008] Furthermore, the transmission mechanism includes a bracket, a first motor, a first conical tooth, a second conical tooth, a transmission rod, a round block, a first driving rod and a second driving rod. The top of the bracket is fixedly connected to the first motor, the back of the first motor is fixedly connected to the first conical tooth, the top of the outer surface of the first conical tooth is movably connected to the second conical tooth, the top of the second conical tooth is fixedly connected to the transmission rod, the top of the transmission rod is fixedly connected to the round block, one side of the round block is fixedly connected to the first driving rod, the top of the first driving rod is movably connected to the second driving rod, and one side of the second driving rod is fixedly connected to a storage box. The transmission rod drives the round block so that the first driving rod and the second driving rod drive the storage box to rotate on the grinding plate, which can effectively grind the crystalline waste, which is beneficial for completing the reaction in a shorter time, thereby improving the reaction efficiency.

[0009] Furthermore, the outer surface of the grinding plate is fixedly connected with an edge, the middle part is movably connected with a baffle, the top of the baffle is provided with a grinding groove, the bottom of the baffle is fixedly connected with a folding block, the front of the folding block is fixedly connected with a second motor, and the baffle is folded by using the second motor to drive the folding block, so that the ground crystalline waste can be quickly dropped into the reduction furnace to improve work efficiency.

[0010] Furthermore, leakage holes are formed at the bottom of the material storage box, a transfer trough is fixedly connected to the bottom of the material storage box, and a strip groove is provided at the bottom of the transfer trough, so that the crystallized waste can fall onto the grinding disc.

[0011] Furthermore, the pressing mechanism includes a mounting frame, a guide column, a first spring, a pressure plate and a lifting block. The bottom of the mounting frame is fixedly connected to the guide column, the outer surface of the guide column is movably connected to the first spring, the bottom of the first spring is fixedly connected to the pressure plate, and the outer surface of the pressure plate is movably connected to a storage box.

[0012] Furthermore, the purification device includes a first fan, a second fan, a check valve, a Z-shaped groove, a replacement groove, a sealing block, a catalytic decomposition box and a catalytic layer. One end of the purification device is fixedly connected to the first fan, the other end of the purification device is fixedly connected to the second fan, a check valve is provided on one side of the second fan, the top and bottom of the check valve are fixedly connected to the purification device, a Z-shaped groove is provided on the inner surface of the purification device, a replacement groove is provided on the other side of the Z-shaped groove, the inner surface of the replacement groove is movably connected to a sealing block, the middle part of the purification device is fixedly connected to the catalytic decomposition box, and the inner surface of the catalytic decomposition box is movably connected to the catalytic layer, so that the treated exhaust gas emissions will greatly reduce the odor and harmful gas concentration in the laboratory, provide a cleaner and safer working environment for the staff, and help improve work efficiency and reduce the occurrence of occupational diseases.

[0013] Furthermore, the filtering device includes a filter, a clamping block, a second spring, a center block and a groove, wherein the clamping block is fixedly connected to one side of the filter, the second spring is fixedly connected to one end of the clamping block, the center block is fixedly connected to one end of the second spring, and grooves are formed on both sides of the center block.

[0014] Technical effects and advantages of the present invention:

[0015] 1. In the present invention, when the volume of the crystallized waste needs to be reduced, tweezers are used to clamp the lifting block and lift it upward. At this time, the first spring begins to contract, and the setting of the guide column can make the position of the first spring relatively fixed and will not deviate. Then, the crystallized waste is placed under the pressure plate and the tweezers are released. The first spring rebounds and presses the crystallized waste into the storage box through the pressure plate. At this time, the storage box is full of crystallized waste and a leakage hole is opened at the bottom. At this time, the crystallized waste passes through the leakage hole to the transfer groove and the strip groove below to reach the grinding plate. At this time, the first motor is started to make the first conical tooth start to rotate. When the first conical tooth starts to rotate, the second conical tooth starts to rotate. When the second conical tooth starts to rotate, the transmission rod starts to rotate. At this time, the round block on the top of the transmission rod drives the first driving rod to rotate, and the first driving rod is connected to the second driving rod so that the second driving rod drives the storage box to move on the grinding plate. At this time, the crystallized waste material rubs between the grinding plate and the storage box, causing the volume of the crystallized waste material to gradually decrease. Subsequently, the second motor is started to rotate the folding block and fold the baffle downward to cause the crystallized waste material to fall into the reduction furnace, which is conducive to completing the reaction in a shorter time, thereby improving the reaction efficiency. At the same time, since the chances of adverse factors such as side reactions and decomposition of reactants are reduced, the purity and yield of the product will also be improved.

[0016] 2. In the present invention, when the crystallized waste generates a large amount of harmful gas during the reaction, the first fan and the second fan are started to transmit the harmful gas in the reduction furnace to the inside of the purification device. At this time, the harmful air is initially filtered through the filter. Then, the gas continues to move upward to the catalytic decomposition box, decomposes the harmful gas through the catalytic layer and finally transmits it to the outside; when the filter in the filter device needs to be replaced, the bolts on the sealing block are removed and the sealing block is removed, and then the clamp is aligned with the Z-shaped groove and inserted into the groove. At this time, the second spring is unfolded in the Z-shaped groove so that the filter can be quickly installed in the purification device. The treated exhaust gas emissions will greatly reduce the odor and harmful gas concentration in the laboratory, provide a cleaner and safer working environment for the staff, and help improve work efficiency and reduce the occurrence of occupational diseases. BRIEF DESCRIPTION OF THE DRAWINGS

[0017] Figure 1 It is a schematic diagram of the overall structure of the present invention.

[0018] Figure 2 It is an overall schematic diagram of the grinding structure of the present invention.

[0019] Figure 3 It is a schematic diagram of the transmission mechanism structure of the present invention.

[0020] Figure 4 It is a schematic diagram of the structure of the material storage box of the present invention.

[0021] Figure 5 It is a schematic diagram of the structure of the pressing mechanism of the present invention.

[0022] Figure 6 It is a schematic diagram of the structure of the purification device of the present invention.

[0023] Figure 7 It is a schematic diagram of the internal structure of the purification device of the present invention.

[0024] Figure 8 It is a schematic diagram of the structure of the filtering device of the present invention.

[0025] Fig. 9 It is a schematic diagram of the planed structure of the purification device of the present invention.

[0026] The accompanying drawings are marked as follows: 1. reduction furnace; 101. protection frame; 2. transmission mechanism; 201. bracket; 202. first motor; 203. first conical tooth; 204. second conical tooth; 205. transmission rod; 206. round block; 207. first driving rod; 208. second driving rod; 3. column; 301. edge; 302. grinding disc; 303. baffle; 304. folding block; 305. second motor; 4. storage box; 401. leakage hole; 402. transfer slot; 403. strip slot; 5. Pressing mechanism; 501. Mounting frame; 502. Guide column; 503. First spring; 504. Pressing plate; 505. Lifting block; 6. Purification device; 601. First fan; 602. Second fan; 603. Check valve; 604. Z-shaped groove; 605. Replacement groove; 606. Sealing block; 607. Catalytic decomposition box; 608. Catalytic layer; 7. Filtering device; 701. Filter; 702. Clamping block; 703. Second spring; 704. Center block; 705. Groove. DETAILED DESCRIPTION

[0027] The technical solution of the present invention will be clearly and completely described below in conjunction with the drawings in the present invention. In addition, the forms of the various structures described in the following embodiments are only examples. The device for preparing polycrystalline silicon carbon by synthesizing a specific shape of recrystallized waste involved in the present invention is not limited to the structures described in the following embodiments. All other embodiments obtained by ordinary technicians in this field without making creative work belong to the scope of protection of the present invention.

[0028] Reference Figure 1-9 The present invention provides a device for preparing polycrystalline silicon carbon of a specific shape by synthesizing recrystallized waste. A protection frame 101 is fixedly connected to the top of a reduction furnace 1, and a transmission mechanism 2 is fixedly connected to the inside of the protection frame 101. The transmission mechanism 2 includes a transmission rod 205. The outer surface of the transmission rod 205 is movably connected to a column 3, and the inner side of the column 3 is fixedly connected to an edge 301, and the inner surface of the edge 301 is fixedly connected to a grinding sheet 302. A storage box 4 is provided on the top of the grinding sheet 302, and a pressing mechanism 5 is fixedly connected to one side of the storage box 4. A purification device 6 is fixedly connected to one side of the bottom of the reduction furnace 1, and a filtering device 7 is movably connected to the inner surface of the purification device 6.

[0029] In a preferred embodiment, the transmission mechanism 2 includes a bracket 201, a first motor 202, a first conical tooth 203, a second conical tooth 204, a transmission rod 205, a round block 206, a first driving rod 207 and a second driving rod 208. The top of the bracket 201 is fixedly connected to the first motor 202, the back of the first motor 202 is fixedly connected to the first conical tooth 203, the top of the outer surface of the first conical tooth 203 is movably connected to the second conical tooth 204, and the top of the second conical tooth 204 is fixedly connected to the transmission rod 205. The top of the transmission rod 205 is fixedly connected with a round block 206, one side of the round block 206 is fixedly connected with a first driving rod 207, the top of the first driving rod 207 is movably connected with a second driving rod 208, one side of the second driving rod 208 is fixedly connected with a storage box 4, and the transmission rod 205 drives the round block 206 to make the first driving rod 207 and the second driving rod 208 drive the storage box 4 to rotate on the grinding plate 302, which can effectively grind the crystalline waste, which is beneficial to complete the reaction in a shorter time, thereby improving the reaction efficiency.

[0030] In a preferred embodiment, the outer surface of the grinding plate 302 is fixedly connected to the edge 301, and the middle part is movably connected to a baffle 303. The top of the baffle 303 is provided with a grinding groove, the bottom of the baffle 303 is fixedly connected to a folding block 304, and the front of the folding block 304 is fixedly connected to a second motor 305. By using the second motor 305 to drive the folding block 304 to fold the baffle 303, the ground crystalline waste can be quickly dropped into the reduction furnace 1 to improve work efficiency.

[0031] In a preferred embodiment, a leak hole 401 begins to be formed at the bottom of the storage box 4, a transfer trough 402 is fixedly connected to the bottom of the storage box 4, a strip groove 403 is formed at the bottom of the transfer trough 402, and the crystallized waste can fall onto the grinding disc 302 through the setting of the strip groove 403.

[0032] In a preferred embodiment, the pressing mechanism 5 includes a mounting frame 501, a guide column 502, a first spring 503, a pressure plate 504 and a lifting block 505. The bottom of the mounting frame 501 is fixedly connected to the guide column 502, the outer surface of the guide column 502 is movably connected to the first spring 503, the bottom of the first spring 503 is fixedly connected to the pressure plate 504, and the outer surface of the pressure plate 504 is movably connected to the storage box 4.

[0033] In a preferred embodiment, the purification device 6 includes a first fan 601, a second fan 602, a check valve 603, a Z-shaped groove 604, a replacement groove 605, a sealing block 606, a catalytic decomposition box 607 and a catalytic layer 608, one end of the purification device 6 is fixedly connected to the first fan 601, the other end of the purification device 6 is fixedly connected to the second fan 602, a check valve 603 is provided on one side of the second fan 602, the top and bottom of the check valve 603 are fixedly connected to the purification device 6, a Z-shaped groove 604 is provided on the inner surface of the purification device 6, a replacement groove 605 is provided on the other side of the Z-shaped groove 604, the inner surface of the replacement groove 605 is movably connected to the sealing block 606, the middle part of the purification device 6 is fixedly connected to the catalytic decomposition box 607, and the inner surface of the catalytic decomposition box 607 is movably connected to the catalytic layer 608, so that the treated exhaust gas emission will greatly reduce the odor and harmful gas concentration in the laboratory, provide a cleaner and safer working environment for the staff, and help improve work efficiency and reduce the occurrence of occupational diseases.

[0034] In a preferred embodiment, the filtering device 7 includes a filter 701, a clamping block 702, a second spring 703, a center block 704 and a groove 705. The clamping block 702 is fixedly connected to one side of the filter 701, one end of the clamping block 702 is fixedly connected to the second spring 703, one end of the second spring 703 is fixedly connected to the center block 704, and grooves 705 are formed on both sides of the center block 704.

[0035] The working principle of the present invention is as follows: when the volume of the crystallized waste needs to be reduced, tweezers are used to clamp the lifting block 505 and lift it upwards. At this time, the first spring 503 begins to shrink, and the setting of the guide column 502 can make the position of the first spring 503 relatively fixed and will not deviate. Then, the crystallized waste is placed under the pressure plate 504, and then the tweezers are released. The first spring 503 rebounds and presses the crystallized waste through the pressure plate 504 into the storage box 4. At this time, the storage box 4 is full of crystallized waste and a leakage hole 401 is opened at the bottom. When the crystal waste passes through the leak hole 401, the transfer trough 402 and the strip groove 403 below, it reaches the grinding plate 302. At this time, the first motor 202 is started to make the first conical tooth 203 start to rotate. When the first conical tooth 203 starts to rotate, the second conical tooth 204 starts to rotate. When the second conical tooth 204 starts to rotate, the transmission rod 205 starts to rotate. At this time, the round block 206 on the top of the transmission rod 205 drives the first driving rod 207 to rotate, and the first driving rod 207 is connected to the second driving rod 208 so that The second driving rod 208 drives the storage box 4 to move on the grinding disc 302. At this time, the crystallized waste rubs between the grinding disc 302 and the storage box 4, causing the volume of the crystallized waste to gradually decrease. Subsequently, the second motor 305 is started to rotate the folding block 304 and cause the baffle 303 to fold downward to cause the crystallized waste to fall into the reduction furnace 1. When the crystallized waste reacts, a large amount of harmful gas is generated. At this time, the first fan 601 and the second fan 602 are started to transmit the harmful gas in the reduction furnace 1 to the inside of the purification device 6. At this time, there is The harmful air is initially filtered through the filter 701, and then the gas continues to move upward to the catalytic decomposition box 607, where the harmful gas is decomposed through the catalytic layer 608 and finally transmitted to the outside; when the filter 701 in the filter device 7 needs to be replaced, the bolts on the sealing block 606 are removed and the sealing block 606 is removed, and then the clamp 702 is aligned with the Z-shaped groove 604 and inserted into the groove, at which time the second spring 703 is unfolded in the Z-shaped groove 604 so that the filter 701 can be quickly installed inside the purification device 6.

[0036] Finally, a few points should be explained: First, in the description of this application, it should be noted that, unless otherwise specified and limited, the terms "installed", "connected", and "connected" should be understood in a broad sense, which may refer to mechanical connection or electrical connection, or internal communication between two components, or direct connection. "upper", "lower", "left", "right", etc. are only used to indicate relative positional relationships. When the absolute position of the object being described changes, the relative positional relationship may change;

[0037] Secondly: In the drawings of the embodiments disclosed in the present invention, only the structures related to the embodiments disclosed in the present invention are involved, and other structures can refer to the general design. In the absence of conflict, the same embodiment and different embodiments of the present invention can be combined with each other;

[0038] Finally: The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the protection scope of the present invention.

Claims

1. A device for preparing polycrystalline silicon carbon of a specific shape by synthesizing recrystallized waste, comprising a reduction furnace (1), characterized in that: The top of the reduction furnace (1) is fixedly connected to a protection frame (101), the interior of the protection frame (101) is fixedly connected to a transmission mechanism (2), the transmission mechanism (2) comprises a transmission rod (205), the outer surface of the transmission rod (205) is movably connected to a column (3), the inner side of the column (3) is fixedly connected to an edge (301), the inner surface of the edge (301) is fixedly connected to a grinding plate (302), a storage box (4) is provided on the top of the grinding plate (302), one side of the storage box (4) is fixedly connected to a pressing mechanism (5), one side of the bottom of the reduction furnace (1) is fixedly connected to a purification device (6), and the inner surface of the purification device (6) is movably connected to a filtering device (7).

2. The device for preparing polycrystalline silicon carbon of a specific shape by synthesizing recrystallized waste according to claim 1, characterized in that: The transmission mechanism (2) comprises a bracket (201), a first motor (202), a first conical tooth (203), a second conical tooth (204), a transmission rod (205), a round block (206), a first driving rod (207) and a second driving rod (208); the top of the bracket (201) is fixedly connected to the first motor (202); the back of the first motor (202) is fixedly connected to the first conical tooth (203); the top of the outer surface of the first conical tooth (203) is movably connected to the second conical tooth (204); the top of the second conical tooth (204) is fixedly connected to the transmission rod (205); the top of the transmission rod (205) is fixedly connected to the round block (206); one side of the round block (206) is fixedly connected to the first driving rod (207); the top of the first driving rod (207) is movably connected to the second driving rod (208); one side of the second driving rod (208) is fixedly connected to a storage box (4).

3. The device for preparing polycrystalline silicon carbon of a specific shape by synthesizing polycrystalline silicon carbon from recrystallized waste according to claim 1, characterized in that: The outer surface of the grinding plate (302) is fixedly connected to an edge (301), the middle part is movably connected to a baffle (303), a grinding groove is provided on the top of the baffle (303), a folding block (304) is fixedly connected to the bottom of the baffle (303), and a second motor (305) is fixedly connected to the front of the folding block (304).

4. The device for preparing polycrystalline silicon carbon of a specific shape by synthesizing recrystallized waste according to claim 1, characterized in that: A leak hole (401) is formed at the bottom of the material storage box (4), a transfer trough (402) is fixedly connected to the bottom of the material storage box (4), and a strip groove (403) is formed at the bottom of the transfer trough (402).

5. The device for preparing polycrystalline silicon carbon of a specific shape by synthesizing recrystallized waste according to claim 1, characterized in that: The pressing mechanism (5) includes a mounting frame (501), a guide column (502), a first spring (503), a pressure plate (504) and a lifting block (505); the bottom of the mounting frame (501) is fixedly connected to the guide column (502); the outer surface of the guide column (502) is movably connected to the first spring (503); the bottom of the first spring (503) is fixedly connected to the pressure plate (504); and the outer surface of the pressure plate (504) is movably connected to the storage box (4).

6. The device for preparing polycrystalline silicon carbon of a specific shape by synthesizing waste recrystallization materials according to claim 1, characterized in that: The purification device (6) comprises a first fan (601), a second fan (602), a check valve (603), a Z-shaped groove (604), a replacement groove (605), a sealing block (606), a catalytic decomposition box (607) and a catalytic layer (608); one end of the purification device (6) is fixedly connected to the first fan (601), the other end of the purification device (6) is fixedly connected to the second fan (602), and one side of the second fan (602) is provided with a check valve (603). 3), the top and bottom of the check valve (603) are fixedly connected to a purification device (6), the inner surface of the purification device (6) is provided with a Z-shaped groove (604), the other side of the Z-shaped groove (604) is provided with a replacement groove (605), the inner surface of the replacement groove (605) is movably connected to a sealing block (606), the middle part of the purification device (6) is fixedly connected to a catalytic decomposition box (607), and the inner surface of the catalytic decomposition box (607) is movably connected to a catalytic layer (608).

7. The device for preparing polycrystalline silicon carbon of a specific shape by synthesizing waste recrystallization materials according to claim 1, characterized in that: The filtering device (7) comprises a filter (701), a clamping block (702), a second spring (703), a center block (704) and a groove (705); one side of the filter (701) is fixedly connected to the clamping block (702); one end of the clamping block (702) is fixedly connected to the second spring (703); one end of the second spring (703) is fixedly connected to the center block (704); and grooves (705) are formed on both sides of the center block (704).

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