Fermented oil for hair, hair care agent as well as preparation method and application of fermented oil

Abstract

The invention relates to the technical field of daily chemicals, in particular to fermented oil for hair, a hair care agent as well as a preparation method and application of the fermented oil. The fermented oil for hair is prepared from the following raw materials: prunus amygdalus dulcis, macadamia nut seeds, rhizoma anemarrhenae roots and citron fruits. The fermented oil is added into the hair care agent, so that the hair care effect and nutrient substances are increased, the hair care agent is light and easy to smear, hair is glossy, and light and comfortable feelings are brought while hair is moistened and protected. Meanwhile, the function of maintaining the hair dyeing effect is achieved.

Description

Technical Field

[0001] The invention relates to the technical field of daily chemicals, and in particular to a fermented oil for hair, a hair conditioner and a preparation method and application thereof. Background Art

[0002] Hair care essential oils have the basic effect of moisturizing and nourishing hair. Most of the hair care oils on the market achieve smooth care through silicone oil film, and then add a single oil care, which will have a sticky film or relatively moist feeling. At present, the hair care essential oils on the market are mainly aimed at the problem of hair moisturizing and repairing. In daily life, hair often has to withstand various tests, such as hot hair drying, dyeing and perming, ultraviolet damage, etc., which makes people's hair easily damaged, frizzy, split, dry, difficult to comb, high friction, and dull luster. However, the existing hair care essential oils cannot meet people's hair care needs well.

[0003] In order to solve the above problems, the present invention provides a fermented oil for hair, a hair conditioner and a preparation method and application thereof. Summary of the invention

[0004] In order to solve the above technical problems, the present invention provides a fermented oil for hair use, and the raw materials for preparing the oil include: sweet almond, macadamia nut seeds, rhizome of Anemarrhena asphodeloides, and citron fruit.

[0005] As an embodiment of the present invention, the mass ratio of the sweet almond, macadamia nut seeds, Anemarrhena asphodeloides root, and Citron fruit is 1:1:1:1.

[0006] A hair conditioner comprising the fermented oil for hair.

[0007] As an embodiment of the present invention, the raw materials for preparing the hair conditioner include: a hair conditioner, a moisturizer, a fragrance, a hair conditioner, a moisturizer and an antioxidant.

[0008] As an embodiment of the present invention, the hair conditioner described herein comprises, by weight, the following raw materials:

[0009] Cyclopentasiloxane 50-60

[0010] Dimethicone, Dimethiconol 35-45

[0011] Isohexadecane 4-5

[0012] Fragrance 0.8-1

[0013] Caprylic / capric triglyceride 0.1-1

[0014] Fermented oil for hair 0.1-1

[0015] MAURITIA FLEXUOSA FRUIT OIL 0.1-1

[0016] Macadamia ternifolia seed oil 0.1-1

[0017] Sweet almond (PRUNUS AMYGDALUSDULCIS) oil 0.1-1

[0018] Jojoba (SIMMONDSIA CHINENSIS) seed oil 0.1-1

[0019] Tocopheryl acetate 0.02-0.06.

[0020] As an embodiment of the present invention, the raw materials for preparation thereof include, by weight:

[0021] Cyclopentasiloxane 53

[0022] Dimethicone, Dimethiconol 42

[0023] Isohexadecane 4

[0024] Fragrance 0.9

[0025] Caprylic / capric triglyceride 0.7

[0026] Fermented oil for hair1

[0027] MAURITIA FLEXUOSA FRUIT OIL 0.3

[0028] Macadamia ternifolia seed oil 0.2

[0029] Sweet almond (PRUNUS AMYGDALUSDULCIS) oil 0.5

[0030] Jojoba (SIMMONDSIA CHINENSIS) seed oil 0.5

[0031] Tocopheryl acetate 0.05.

[0032] A method for preparing the hair conditioner comprises the following steps:

[0033] (1) Add cyclopentasiloxane, polydimethylsiloxane and polydimethylsiloxane alcohol into a stirring emulsifier, start stirring, and stir until the mixture is uniform and transparent;

[0034] (2) Add isohexadecane, flavor, caprylic / capric triglyceride into an emulsifier and keep stirring;

[0035] (3) Add fermented oil, MAURITIA FLEXUOSA fruit oil, MACADAMIATERNIFOLIA seed oil, PRUNUS AMYGDALUS DULCIS oil, jojoba seed oil, and tocopherol acetate, stir evenly until the mixture is evenly mixed and discharged.

[0036] As an embodiment of the present invention, the hair conditioner is applied in the field of daily chemicals.

[0037] By adopting the above technical solution, the present invention has the following beneficial effects:

[0038] Fermented oil is added to the hair conditioner to increase its hair care effect and nutrients. It is light and easy to apply, giving hair luster, moisturizing and providing a light and comfortable feeling. It also has the function of maintaining the effect of hair dyeing. BRIEF DESCRIPTION OF THE DRAWINGS

[0039] In order to more clearly illustrate the specific implementation methods of the present invention or the technical solutions in the prior art, the drawings required for use in the specific implementation methods or the description of the prior art will be briefly introduced below. Obviously, the drawings in the following description are some implementation methods of the present invention. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying creative work.

[0040] Figure 1 This is a photo of hair scales (Example 1);

[0041] Figure 2 This is a photo of hair scales (control group). DETAILED DESCRIPTION

[0042] The technical solution of the present invention will be described clearly and completely below. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of them. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0043] A hair conditioner, wherein the raw materials for its preparation comprise, by weight:

[0044] Cyclopentasiloxane 53

[0045] Polydimethylsiloxane, polydimethylsiloxane alcohol (mass ratio is 1:1) 42

[0046] Isohexadecane 4

[0047] Fragrance 0.9

[0048] Caprylic / capric triglyceride 0.7

[0049] Fermented oil for hair1

[0050] MAURITIA FLEXUOSA FRUIT OIL 0.3

[0051] Macadamia ternifolia seed oil 0.2

[0052] Sweet almond (PRUNUS AMYGDALUSDULCIS) oil 0.5

[0053] Jojoba (SIMMONDSIA CHINENSIS) seed oil 0.5

[0054] Tocopheryl acetate 0.05.

[0055] A method for preparing the hair conditioner comprises the following steps:

[0056] (1) Add cyclopentasiloxane, polydimethylsiloxane and polydimethylsiloxane alcohol into a stirring emulsifier, start stirring, and stir until the mixture is uniform and transparent;

[0057] (2) Add isohexadecane, flavor, caprylic / capric triglyceride into an emulsifier and keep stirring;

[0058] (3) Add fermented oil, MAURITIA FLEXUOSA fruit oil, MACADAMIATERNIFOLIA seed oil, PRUNUS AMYGDALUS DULCIS oil, jojoba seed oil, and tocopherol acetate, stir evenly until the mixture is evenly mixed and discharged.

[0059] The raw materials for preparing the fermented oil for hair use include: sweet almonds, macadamia seeds, rhizomes of Anemarrhena asphodeloides and citron fruits.

[0060] In the present invention, the preparation method of the fermented oil for hair is as follows:

[0061] (1) The freshly harvested raw materials are stored at 0-5°C for 72 hours, taken out, mixed and chopped, placed in a culture solution, and inoculated with strain A for culture; the fermentation temperature is 30°C and the time is 72 hours.

[0062] (2) After the fermentation in step (1) is completed, a new strain B is inoculated and the fermentation is continued; centrifugation is performed, and the supernatant is removed and an equal volume of methyl tert-butyl ether is added;

[0063] (3) After operating at a temperature of 30° C. and a rotation speed of 300 r / min for 40 min, the solvent phase is separated by centrifugation at 10,000 r / min for 3 min at room temperature, and then an equal volume of 0.1 wt % NaCl solution is added to wash the solvent phase, and the methyl tert-butyl ether is removed by rotary evaporation after drying over anhydrous sodium sulfate, and then the oil is dried to obtain the oil.

[0064] Wherein, in step (1), the components of the culture solution are: casein peptone (trypsin digestion) 10.0g, beef extract powder 10.0g, yeast extract powder 10.0g, glucose 25.0g, Tween 80 1.0g, sodium acetate 5.0g, ammonium citrate tribasic 2.0g, K2HPO4 2.0g, MgSO4·7H2O 0.2g, MnSO4·H2O 0.05g, agar 15.0g, and distilled water 1000.0mL.

[0065] The strain A is: Bacillus glucanolyticus (China Industrial Microbiological Culture Collection Administration Center, CICC 23909) and Pediococcus pentosaceus (China Industrial Microbiological Culture Collection Administration Center, CICC 22228), with an inoculation amount of 5 vol% and an inoculation ratio of 3:2.

[0066] The strain B is: Issaffron orientalis (China Industrial Microbiological Culture Collection Center, CICC 32866), the inoculation amount is 5 vol%, the fermentation temperature is 37° C., and the fermentation time is 48 h.

[0067] The present invention is further explained below in conjunction with specific implementation modes.

[0068] Example 1

[0069] This embodiment provides a hair conditioner, and the raw materials for its preparation include, by weight:

[0070] Cyclopentasiloxane 53

[0071] Polydimethylsiloxane, polydimethylsiloxane alcohol (mass ratio is 1:1) 42

[0072] Isohexadecane 4

[0073] Fragrance 0.9

[0074] Caprylic / capric triglyceride 0.7

[0075] Fermented oil for hair1

[0076] MAURITIA FLEXUOSA FRUIT OIL 0.3

[0077] Macadamia ternifolia seed oil 0.2

[0078] Sweet almond (PRUNUS AMYGDALUSDULCIS) oil 0.5

[0079] Jojoba (SIMMONDSIA CHINENSIS) seed oil 0.5

[0080] Tocopheryl acetate 0.05.

[0081] A method for preparing the hair conditioner comprises the following steps:

[0082] (1) Add cyclopentasiloxane, polydimethylsiloxane and polydimethylsiloxane alcohol into a stirring emulsifier, start stirring, and stir until the mixture is uniform and transparent;

[0083] (2) Add isohexadecane, flavor, caprylic / capric triglyceride into an emulsifier and keep stirring;

[0084] (3) Add fermented oil, MAURITIA FLEXUOSA fruit oil, MACADAMIATERNIFOLIA seed oil, PRUNUS AMYGDALUS DULCIS oil, jojoba seed oil, and tocopherol acetate, stir evenly until the mixture is evenly mixed and discharged.

[0085] The raw materials for preparing the fermented oil for hair use include: sweet almonds, macadamia seeds, rhizomes of Anemarrhena asphodeloides and citron fruits, with a mass ratio of 1:1:1:1.

[0086] The preparation method of the fermented oil for hair is as follows:

[0087] (1) The freshly harvested raw materials are stored at 0-5°C for 72 hours, taken out, mixed and chopped, placed in a culture solution, and inoculated with strain A for culture; the fermentation temperature is 30°C and the time is 72 hours.

[0088] (2) After the fermentation in step (1) is completed, a new strain B is inoculated and the fermentation is continued; centrifugation is performed, and the supernatant is removed and an equal volume of methyl tert-butyl ether is added;

[0089] (3) After operating at a temperature of 30° C. and a rotation speed of 300 r / min for 40 min, the solvent phase is separated by centrifugation at 10,000 r / min for 3 min at room temperature, and then an equal volume of 0.1 wt % NaCl solution is added to wash the solvent phase, and the methyl tert-butyl ether is removed by rotary evaporation after drying over anhydrous sodium sulfate, and then the oil is dried to obtain the oil.

[0090] Wherein, in step (1), the components of the culture solution are: casein peptone (trypsin digestion) 10.0g, beef extract powder 10.0g, yeast extract powder 10.0g, glucose 25.0g, Tween 80 1.0g, sodium acetate 5.0g, ammonium citrate tribasic 2.0g, K2HPO4 2.0g, MgSO4·7H2O 0.2g, MnSO4·H2O 0.05g, agar 15.0g, and distilled water 1000.0mL.

[0091] The strain A is: Bacillus glucanolyticus (China Industrial Microbiological Culture Collection Administration Center, CICC 23909) and Pediococcus pentosaceus (China Industrial Microbiological Culture Collection Administration Center, CICC 22228), with an inoculation amount of 5 vol% and an inoculation ratio of 3:2.

[0092] The strain B is: Issaffron orientalis (China Industrial Microbiological Culture Collection Center, CICC 32866), the inoculation amount is 5 vol%, the fermentation temperature is 37° C., and the fermentation time is 48 h.

[0093] Example 2

[0094] This embodiment provides a hair conditioner, and the raw materials for its preparation include, by weight:

[0095] Cyclopentasiloxane 53

[0096] Polydimethylsiloxane, polydimethylsiloxane alcohol (mass ratio is 1:1) 42

[0097] Isohexadecane 4

[0098] Fragrance 0.9

[0099] Caprylic / capric triglyceride 0.7

[0100] Fermented oil for hair1

[0101] MAURITIA FLEXUOSA FRUIT OIL 0.3

[0102] Macadamia ternifolia seed oil 0.2

[0103] Sweet almond (PRUNUS AMYGDALUSDULCIS) oil 0.5

[0104] Jojoba (SIMMONDSIA CHINENSIS) seed oil 0.5

[0105] Tocopheryl acetate 0.05.

[0106] A method for preparing the hair conditioner comprises the following steps:

[0107] (1) Add cyclopentasiloxane, polydimethylsiloxane and polydimethylsiloxane alcohol into a stirring emulsifier, start stirring, and stir until the mixture is uniform and transparent;

[0108] (2) Add isohexadecane, flavor, caprylic / capric triglyceride into an emulsifier and keep stirring;

[0109] (3) Add fermented oil, MAURITIA FLEXUOSA fruit oil, MACADAMIATERNIFOLIA seed oil, PRUNUS AMYGDALUS DULCIS oil, jojoba seed oil, and tocopherol acetate, stir evenly until the mixture is evenly mixed and discharged.

[0110] The raw materials for preparing the fermented oil for hair include: sweet almond (PRUNUS AMYGDALUS DULCIS) oil, macadamia (MACADAMIA TERNIFOLIA) seed oil, Anemarrhena (ANEMARRHENA ASPHODELOIDES) root extract, and citron (CITRUS MEDICA LIMONUM) fruit oil, with a mass ratio of 1:1:1:1.

[0111] The preparation method of the fermented oil for hair is as follows:

[0112] (1) Prunus amygdalus dulcis oil, macadamia ternifolia seed oil, anemarrhena asphodeloides root extract, and citron oil were mixed and placed in a culture medium, and strain B was inoculated for culture; the fermentation temperature was 30°C and the time was 72 h.

[0113] (2) after the fermentation in step (1) is completed, centrifuge, remove the supernatant and add an equal volume of methyl tert-butyl ether;

[0114] (3) After operating at a temperature of 30° C. and a rotation speed of 300 r / min for 40 min, the solvent phase is separated by centrifugation at 10,000 r / min for 3 min at room temperature, and then an equal volume of 0.1 wt % NaCl solution is added to wash the solvent phase, and the methyl tert-butyl ether is removed by rotary evaporation after drying over anhydrous sodium sulfate, and then the oil is dried to obtain the oil.

[0115] Wherein, in step (1), the components of the culture solution are: casein peptone (trypsin digestion) 10.0g, beef extract powder 10.0g, yeast extract powder 10.0g, glucose 25.0g, Tween 80 1.0g, sodium acetate 5.0g, ammonium citrate tribasic 2.0g, K2HPO4 2.0g, MgSO4·7H2O 0.2g, MnSO4·H2O 0.05g, agar 15.0g, and distilled water 1000.0mL.

[0116] The strain B is: Issaffron orientalis (China Industrial Microbiological Culture Collection Center, CICC 32866), the inoculation amount is 5 vol%, the fermentation temperature is 37° C., and the fermentation time is 48 h.

[0117] Example 3

[0118] This embodiment provides a hair conditioner, and the raw materials for its preparation include, by weight:

[0119] Cyclopentasiloxane 53

[0120] Polydimethylsiloxane, polydimethylsiloxane alcohol (mass ratio is 1:1) 42

[0121] Isohexadecane 4

[0122] Fragrance 0.9

[0123] Caprylic / capric triglyceride 0.7

[0124] Fermented oil for hair1

[0125] MAURITIA FLEXUOSA FRUIT OIL 0.3

[0126] Macadamia ternifolia seed oil 0.2

[0127] Sweet almond (PRUNUS AMYGDALUSDULCIS) oil 0.5

[0128] Jojoba (SIMMONDSIA CHINENSIS) seed oil 0.5

[0129] Tocopheryl acetate 0.05.

[0130] A method for preparing the hair conditioner comprises the following steps:

[0131] (1) Add cyclopentasiloxane, polydimethylsiloxane and polydimethylsiloxane alcohol into a stirring emulsifier, start stirring, and stir until the mixture is uniform and transparent;

[0132] (2) Add isohexadecane, flavor, caprylic / capric triglyceride into an emulsifier and keep stirring;

[0133] (3) Add fermented oil, MAURITIA FLEXUOSA fruit oil, MACADAMIATERNIFOLIA seed oil, PRUNUS AMYGDALUS DULCIS oil, jojoba seed oil, and tocopherol acetate, stir evenly until the mixture is evenly mixed and discharged.

[0134] The raw materials for preparing the fermented oil for hair use include: sweet almonds, macadamia seeds, rhizomes of Anemarrhena asphodeloides and citron fruits, with a mass ratio of 1:1:1:1.

[0135] The preparation method of the fermented oil for hair is as follows:

[0136] (1) The freshly harvested raw materials are placed at 0-5°C for 72 hours, taken out, mixed and chopped, placed in a culture solution, and inoculated with strain B for culture; the fermentation temperature is 30°C, and the fermentation time is 72 hours; centrifugation is performed, the supernatant is removed, and an equal volume of methyl tert-butyl ether is added;

[0137] (2) After operating at a temperature of 30° C. and a rotation speed of 300 r / min for 40 min, the solvent phase is separated by centrifugation at 10,000 r / min for 3 min at room temperature, and then an equal volume of 0.1 wt % NaCl solution is added to wash the solvent phase, and the methyl tert-butyl ether is removed by rotary evaporation after drying over anhydrous sodium sulfate, and then the oil is dried to obtain the oil.

[0138] Wherein, in step (1), the components of the culture solution are: casein peptone (trypsin digestion) 10.0g, beef extract powder 10.0g, yeast extract powder 10.0g, glucose 25.0g, Tween 80 1.0g, sodium acetate 5.0g, ammonium citrate tribasic 2.0g, K2HPO4 2.0g, MgSO4·7H2O 0.2g, MnSO4·H2O 0.05g, agar 15.0g, and distilled water 1000.0mL.

[0139] The strain B is: Issaffron orientalis (China Industrial Microbiological Culture Collection Center, CICC 32866), the inoculation amount is 5 vol%, the fermentation temperature is 37° C., and the fermentation time is 48 h.

[0140] Example 4

[0141] This embodiment provides a hair conditioner, and the raw materials for its preparation include, by weight:

[0142] Cyclopentasiloxane 53

[0143] Polydimethylsiloxane, polydimethylsiloxane alcohol (mass ratio is 1:1) 42

[0144] Isohexadecane 4

[0145] Fragrance 0.9

[0146] Caprylic / capric triglyceride 0.7

[0147] Fermented oil for hair1

[0148] MAURITIA FLEXUOSA FRUIT OIL 0.3

[0149] Macadamia ternifolia seed oil 0.2

[0150] Sweet almond (PRUNUS AMYGDALUSDULCIS) oil 0.5

[0151] Jojoba (SIMMONDSIA CHINENSIS) seed oil 0.5

[0152] Tocopheryl acetate 0.05.

[0153] A method for preparing the hair conditioner comprises the following steps:

[0154] (1) Add cyclopentasiloxane, polydimethylsiloxane and polydimethylsiloxane alcohol into a stirring emulsifier, start stirring, and stir until the mixture is uniform and transparent;

[0155] (2) Add isohexadecane, flavor, caprylic / capric triglyceride into an emulsifier and keep stirring;

[0156] (3) Add fermented oil, MAURITIA FLEXUOSA fruit oil, MACADAMIATERNIFOLIA seed oil, PRUNUS AMYGDALUS DULCIS oil, jojoba seed oil, and tocopherol acetate, stir evenly until the mixture is evenly mixed and discharged.

[0157] The raw materials for preparing the fermented oil for hair use include: sweet almonds, macadamia seeds, rhizomes of Anemarrhena asphodeloides and citron fruits, with a mass ratio of 1:1:1:1.

[0158] The preparation method of the fermented oil for hair is as follows:

[0159] (1) The freshly harvested raw materials are stored at 0-5°C for 72 hours, taken out, mixed and chopped, placed in a culture solution, and inoculated with strain A for culture; the fermentation temperature is 30°C and the time is 72 hours.

[0160] (2) After the fermentation in step (1) is completed, a new strain B is inoculated and the fermentation is continued; centrifugation is performed, and the supernatant is removed and an equal volume of methyl tert-butyl ether is added;

[0161] (3) After operating at a temperature of 30° C. and a rotation speed of 300 r / min for 40 min, the solvent phase is separated by centrifugation at 10,000 r / min for 3 min at room temperature, and then an equal volume of 0.1 wt % NaCl solution is added to wash the solvent phase, and the methyl tert-butyl ether is removed by rotary evaporation after drying over anhydrous sodium sulfate, and then the oil is dried to obtain the oil.

[0162] Wherein, in step (1), the components of the culture solution are: casein peptone (trypsin digestion) 10.0g, beef extract powder 10.0g, yeast extract powder 10.0g, glucose 25.0g, Tween 80 1.0g, sodium acetate 5.0g, ammonium citrate tribasic 2.0g, K2HPO4 2.0g, MgSO4·7H2O 0.2g, MnSO4·H2O 0.05g, agar 15.0g, and distilled water 1000.0mL.

[0163] The strain A is: Bacillus glucanolyticus (China Industrial Microbiological Culture Collection Center, CICC23909), with an inoculation amount of 5 vol%.

[0164] The strain B is: Issaffron orientalis (China Industrial Microbiological Culture Collection Center, CICC 32866), the inoculation amount is 5 vol%, the fermentation temperature is 37° C., and the fermentation time is 48 h.

[0165] Example 5

[0166] This embodiment provides a hair conditioner, and the raw materials for its preparation include, by weight:

[0167] Cyclopentasiloxane 53

[0168] Polydimethylsiloxane, polydimethylsiloxane alcohol (mass ratio is 1:1) 42

[0169] Isohexadecane 4

[0170] Fragrance 0.9

[0171] Caprylic / capric triglyceride 0.7

[0172] Fermented oil for hair1

[0173] MAURITIA FLEXUOSA FRUIT OIL 0.3

[0174] Macadamia ternifolia seed oil 0.2

[0175] Sweet almond (PRUNUS AMYGDALUSDULCIS) oil 0.5

[0176] Jojoba (SIMMONDSIA CHINENSIS) seed oil 0.5

[0177] Tocopheryl acetate 0.05.

[0178] A method for preparing the hair conditioner comprises the following steps:

[0179] (1) Add cyclopentasiloxane, polydimethylsiloxane and polydimethylsiloxane alcohol into a stirring emulsifier, start stirring, and stir until the mixture is uniform and transparent;

[0180] (2) Add isohexadecane, flavor, caprylic / capric triglyceride into an emulsifier and keep stirring;

[0181] (3) Add fermented oil, MAURITIA FLEXUOSA fruit oil, MACADAMIATERNIFOLIA seed oil, PRUNUS AMYGDALUS DULCIS oil, jojoba seed oil, and tocopherol acetate, stir evenly until the mixture is evenly mixed and discharged.

[0182] The raw materials for preparing the fermented oil for hair use include: sweet almonds, macadamia seeds, rhizomes of Anemarrhena asphodeloides and citron fruits, with a mass ratio of 1:1:1:1.

[0183] The preparation method of the fermented oil for hair is as follows:

[0184] (1) The freshly harvested raw materials are stored at 0-5°C for 72 hours, taken out, mixed and chopped, placed in a culture solution, and inoculated with strain A for culture; the fermentation temperature is 30°C and the time is 72 hours.

[0185] (2) After the fermentation in step (1) is completed, a new strain B is inoculated and the fermentation is continued; centrifugation is performed, and the supernatant is removed and an equal volume of methyl tert-butyl ether is added;

[0186] (3) After operating at a temperature of 30° C. and a rotation speed of 300 r / min for 40 min, the solvent phase is separated by centrifugation at 10,000 r / min for 3 min at room temperature, and then an equal volume of 0.1 wt % NaCl solution is added to wash the solvent phase, and the methyl tert-butyl ether is removed by rotary evaporation after drying over anhydrous sodium sulfate, and then the oil is dried to obtain the oil.

[0187] Wherein, in step (1), the components of the culture solution are: casein peptone (trypsin digestion) 10.0g, beef extract powder 10.0g, yeast extract powder 10.0g, glucose 25.0g, Tween 80 1.0g, sodium acetate 5.0g, ammonium citrate tribasic 2.0g, K2HPO4 2.0g, MgSO4·7H2O 0.2g, MnSO4·H2O 0.05g, agar 15.0g, and distilled water 1000.0mL.

[0188] The strain A is Pediococcus pentosaceus (China Industrial Microbiological Culture Collection Center, CICC 22228), with an inoculation amount of 5 vol%.

[0189] The strain B is: Issaffron orientalis (China Industrial Microbiological Culture Collection Center, CICC 32866), the inoculation amount is 5 vol%, the fermentation temperature is 37° C., and the fermentation time is 48 h.

[0190] Example 6

[0191] This embodiment provides a hair conditioner, and the raw materials for its preparation include, by weight:

[0192] Cyclopentasiloxane 53

[0193] Polydimethylsiloxane, polydimethylsiloxane alcohol (mass ratio is 1:1) 42

[0194] Isohexadecane 4

[0195] Fragrance 0.9

[0196] Caprylic / capric triglyceride 0.7

[0197] Fermented oil for hair1

[0198] MAURITIA FLEXUOSA FRUIT OIL 0.3

[0199] Macadamia ternifolia seed oil 0.2

[0200] Sweet almond (PRUNUS AMYGDALUSDULCIS) oil 0.5

[0201] Jojoba (SIMMONDSIA CHINENSIS) seed oil 0.5

[0202] Tocopheryl acetate 0.05.

[0203] A method for preparing the hair conditioner comprises the following steps:

[0204] (1) Add cyclopentasiloxane, polydimethylsiloxane and polydimethylsiloxane alcohol into a stirring emulsifier, start stirring, and stir until the mixture is uniform and transparent;

[0205] (2) Add isohexadecane, flavor, caprylic / capric triglyceride into an emulsifier and keep stirring;

[0206] (3) Add fermented oil, MAURITIA FLEXUOSA fruit oil, MACADAMIATERNIFOLIA seed oil, PRUNUS AMYGDALUS DULCIS oil, jojoba seed oil, and tocopherol acetate, stir evenly until the mixture is evenly mixed and discharged.

[0207] The raw materials for preparing the fermented oil for hair use include: sweet almonds, macadamia seeds, rhizomes of Anemarrhena asphodeloides and citron fruits, with a mass ratio of 1:1:1:1.

[0208] The preparation method of the fermented oil for hair is as follows:

[0209] (1) The freshly harvested raw materials are stored at 0-5°C for 72 hours, taken out, mixed and chopped, placed in a culture solution, and inoculated with strain A for culture; the fermentation temperature is 30°C and the time is 72 hours.

[0210] (2) After the fermentation in step (1) is completed, a new strain B is inoculated and the fermentation is continued; centrifugation is performed, and the supernatant is removed to obtain the fermented oil.

[0211] Wherein, in step (1), the components of the culture solution are: casein peptone (trypsin digestion) 10.0g, beef extract powder 10.0g, yeast extract powder 10.0g, glucose 25.0g, Tween 80 1.0g, sodium acetate 5.0g, ammonium citrate tribasic 2.0g, K2HPO4 2.0g, MgSO4·7H2O 0.2g, MnSO4·H2O 0.05g, agar 15.0g, and distilled water 1000.0mL.

[0212] The strain A is: Bacillus glucanolyticus (China Industrial Microbiological Culture Collection Administration Center, CICC 23909) and Pediococcus pentosaceus (China Industrial Microbiological Culture Collection Administration Center, CICC 22228), with an inoculation amount of 5 vol% and an inoculation ratio of 3:2.

[0213] The strain B is: Issaffron orientalis (China Industrial Microbiological Culture Collection Center, CICC 32866), the inoculation amount is 5 vol%, the fermentation temperature is 37° C., and the fermentation time is 48 h.

[0214] Example 7

[0215] This embodiment provides a hair conditioner, and the raw materials for its preparation include, by weight:

[0216] Isoalkanes 53

[0217] Polydimethylsiloxane, polydimethylsiloxane alcohol (mass ratio is 1:1) 42

[0218] Isohexadecane 4

[0219] Fragrance 0.9

[0220] Caprylic / capric triglyceride 0.7

[0221] Fermented oil for hair1

[0222] MAURITIA FLEXUOSA FRUIT OIL 0.3

[0223] Macadamia ternifolia seed oil 0.2

[0224] Sweet almond (PRUNUS AMYGDALUSDULCIS) oil 0.5

[0225] Jojoba (SIMMONDSIA CHINENSIS) seed oil 0.5

[0226] Tocopheryl acetate 0.05.

[0227] A method for preparing the hair conditioner comprises the following steps:

[0228] (1) Add cyclopentasiloxane, polydimethylsiloxane and polydimethylsiloxane alcohol into a stirring emulsifier, start stirring, and stir until the mixture is uniform and transparent;

[0229] (2) Add isohexadecane, flavor, caprylic / capric triglyceride into an emulsifier and keep stirring;

[0230] (3) Add fermented oil, MAURITIA FLEXUOSA fruit oil, MACADAMIATERNIFOLIA seed oil, PRUNUS AMYGDALUS DULCIS oil, jojoba seed oil, and tocopherol acetate, stir evenly until the mixture is evenly mixed and discharged.

[0231] The raw materials for preparing the fermented oil for hair use include: sweet almonds, macadamia seeds, rhizomes of Anemarrhena asphodeloides and citron fruits, with a mass ratio of 1:1:1:1.

[0232] The preparation method of the fermented oil for hair is as follows:

[0233] (1) The freshly harvested raw materials are stored at 0-5°C for 72 hours, taken out, mixed and chopped, placed in a culture solution, and inoculated with strain A for culture; the fermentation temperature is 30°C and the time is 72 hours.

[0234] (2) After the fermentation in step (1) is completed, a new strain B is inoculated and the fermentation is continued; centrifugation is performed, and the supernatant is removed and an equal volume of methyl tert-butyl ether is added;

[0235] (3) After operating at a temperature of 30° C. and a rotation speed of 300 r / min for 40 min, the solvent phase is separated by centrifugation at 10,000 r / min for 3 min at room temperature, and then an equal volume of 0.1 wt % NaCl solution is added to wash the solvent phase, and the methyl tert-butyl ether is removed by rotary evaporation after drying over anhydrous sodium sulfate, and then the oil is dried to obtain the oil.

[0236] Wherein, in step (1), the components of the culture solution are: casein peptone (trypsin digestion) 10.0g, beef extract powder 10.0g, yeast extract powder 10.0g, glucose 25.0g, Tween 80 1.0g, sodium acetate 5.0g, ammonium citrate tribasic 2.0g, K2HPO4 2.0g, MgSO4·7H2O 0.2g, MnSO4·H2O 0.05g, agar 15.0g, and distilled water 1000.0mL.

[0237] The strain A is: Bacillus glucanolyticus (China Industrial Microbiological Culture Collection Administration Center, CICC 23909) and Pediococcus pentosaceus (China Industrial Microbiological Culture Collection Administration Center, CICC 22228), with an inoculation amount of 5 vol% and an inoculation ratio of 3:2.

[0238] The strain B is: Issaffron orientalis (China Industrial Microbiological Culture Collection Center, CICC 32866), the inoculation amount is 5 vol%, the fermentation temperature is 37° C., and the fermentation time is 48 h.

[0239] Example 8

[0240] This embodiment provides a hair conditioner, and the raw materials for its preparation include, by weight:

[0241] Cyclopentasiloxane 53

[0242] Polydimethylsiloxane, polydimethylsiloxane alcohol (mass ratio is 1:1) 42

[0243] Isohexadecane 4

[0244] Fragrance 0.9

[0245] Caprylic / capric triglyceride 0.7

[0246] Fermented oil for hair 2.5

[0247] Tocopheryl acetate 0.05.

[0248] A method for preparing the hair conditioner comprises the following steps:

[0249] (1) Add cyclopentasiloxane, polydimethylsiloxane and polydimethylsiloxane alcohol into a stirring emulsifier, start stirring, and stir until the mixture is uniform and transparent;

[0250] (2) Add isohexadecane, flavor, caprylic / capric triglyceride into an emulsifier and keep stirring;

[0251] (3) Add fermented oil, MAURITIA FLEXUOSA fruit oil, MACADAMIATERNIFOLIA seed oil, PRUNUS AMYGDALUS DULCIS oil, jojoba seed oil, and tocopherol acetate, stir evenly until the mixture is evenly mixed and discharged.

[0252] The raw materials for preparing the fermented oil for hair use include: sweet almonds, macadamia seeds, rhizomes of Anemarrhena asphodeloides and citron fruits, with a mass ratio of 1:1:1:1.

[0253] The preparation method of the fermented oil for hair is as follows:

[0254] (1) The freshly harvested raw materials are stored at 0-5°C for 72 hours, taken out, mixed and chopped, placed in a culture solution, and inoculated with strain A for culture; the fermentation temperature is 30°C and the time is 72 hours.

[0255] (2) After the fermentation in step (1) is completed, a new strain B is inoculated and the fermentation is continued; centrifugation is performed, and the supernatant is removed and an equal volume of methyl tert-butyl ether is added;

[0256] (3) After operating at a temperature of 30° C. and a rotation speed of 300 r / min for 40 min, the solvent phase is separated by centrifugation at 10,000 r / min for 3 min at room temperature, and then an equal volume of 0.1 wt % NaCl solution is added to wash the solvent phase, and the methyl tert-butyl ether is removed by rotary evaporation after drying over anhydrous sodium sulfate, and then the oil is dried to obtain the oil.

[0257] Wherein, in step (1), the components of the culture solution are: casein peptone (trypsin digestion) 10.0g, beef extract powder 10.0g, yeast extract powder 10.0g, glucose 25.0g, Tween 80 1.0g, sodium acetate 5.0g, ammonium citrate tribasic 2.0g, K2HPO4 2.0g, MgSO4·7H2O 0.2g, MnSO4·H2O 0.05g, agar 15.0g, and distilled water 1000.0mL.

[0258] The strain A is: Bacillus glucanolyticus (China Industrial Microbiological Culture Collection Administration Center, CICC 23909) and Pediococcus pentosaceus (China Industrial Microbiological Culture Collection Administration Center, CICC 22228), with an inoculation amount of 5 vol% and an inoculation ratio of 3:2.

[0259] The strain B is: Issaffron orientalis (China Industrial Microbiological Culture Collection Center, CICC 32866), the inoculation amount is 5 vol%, the fermentation temperature is 37° C., and the fermentation time is 48 h.

[0260] Performance Testing

[0261] Test 1: This method uses equipment to measure the improvement in glossiness and combing properties of hair pieces before and after using the sample to reflect the product's ability to nourish the hair.

[0262] Reagents and consumables: cleaning solution; in vitro human hair bundle (length ≥10cm, net weight ≥6g).

[0263] Test substance: Sample group: Examples 1-6.

[0264] Test method:

[0265] (1) Baseline dry hair test: The hair bundle to be tested is fully moistened with running constant temperature clean water, treated with cleaning solution, and placed in a constant temperature and humidity chamber (20-25°C, 40%-60%) for more than 4 hours. The hair bundle is then taken out and fixed in the test position for combing cycle test and gloss test.

[0266] (2) Dry hair sample test: The hair to be tested is fully moistened with running constant temperature clean water, and the sample is evenly applied on the surface of the hair at a rate of 0.2 g per gram of hair for about 30 seconds. After being left to stand for about 3-5 minutes, it is placed in a constant temperature and humidity chamber (20-25°C, 40%-60%) to stabilize for more than 4 hours. The hair is then taken out and fixed in the test position for combing cycle test and gloss test.

[0267] (3) Record the combing work value and glossiness value of the test hair bundle before and after using the sample and perform data processing.

[0268] Combing power change rate = (A s -A0) / A0*100%.

[0269] Where: A0--combing work of baseline test;

[0270] A S --Combing work of the post-sampling treatment test.

[0271] Glossiness change rate = (C s -C0) / C0*100%.

[0272] Where: C0--gloss of baseline test;

[0273] C S --Glossiness of the sample after treatment test.

[0274] Table 1 Test results

[0275] Combing power change rate / % Gloss test results % Example 1 -28.313 15.235 Example 2 -18.215 8.352 Example 3 -17.021 7.683 Example 4 -19.821 9.783 Example 5 -26.711 13.721 Example 6 -15.211 6.723 Example 7 -21.031 11.283 Example 8 -22.821 12.031

[0276] Performance test 2: Anti-hair breakage efficacy test

[0277] The strength of hair is determined by its tensile properties. Hair that is difficult to stretch or break is relatively strong. It is usually expressed in terms of parameters such as tensile force (load), stress, elongation, and total work done at the breaking point, yield point, or specified point. This method is to uniformly stretch a single hair of equal length on a CTX texture analyzer until the hair breaks, and calculate the tensile strength and work done at break based on the curve. Since ambient temperature and humidity affect the tensile properties of hair, temperature and humidity control measures are required during the test to ensure that the temperature and humidity of the test environment are stable during and during the test.

[0278] Reagents and consumables: cleaning solution (sodium dodecyl sulfate solution); in vitro human hair bundle (length ≥15cm, net weight ≥6g).

[0279] Sample group: Test Examples 1 to 8.

[0280] Test method:

[0281] (1) Test before using the sample: The hair strand to be tested is fully moistened with running constant temperature clean water, and after being treated with the cleaning solution, it is placed in a constant temperature and humidity chamber [(26±2)℃, (60±10)%RH] to dry naturally for 24 hours, and a single-strand tensile test is performed, and the test data of each time is recorded.

[0282] (2) Test after using the sample: Rinse the hair bundle to be tested with running constant temperature clean water or do not rinse according to the sample usage instructions. Apply 0.2g of sample per gram of hair bundle or the amount in accordance with the sample usage instructions evenly on the surface of the hair. After leaving it for a period of time, place the isolated hair in a constant temperature and humidity chamber [(26±2)℃, (60±10)%RH] to dry naturally for 24 hours, perform a single-strand tensile test, and record the test data for each time.

[0283] Tensile strength change rate = (C s -C0) / C0*100%.

[0284] In the formula: C0---tensile strength of the sample before use;

[0285] C s ---Tensile strength of the sample after use.

[0286] Table 2 Tensile strength test results

[0287] Tensile strength change rate / % Example 1 23.812 Example 2 18.213 Example 3 17.125 Example 4 20.014 Example 5 22.124 Example 6 15.241 Example 7 21.153 Example 8 21.673

[0288] Performance test 3: color protection performance test

[0289] The hair is semi-permanently dyed by dyeing agents, which stabilizes the pigment of the hair in the form of care. A precise color difference sensor is used to test the color difference of the hair sample group and the control group, so as to reduce the significant degree of hair color difference to measure the effect of the sample on improving hair color protection. The color difference calculation formula is as follows:

[0290]

[0291] In the formula, ΔE represents the color difference before and after, L t represents the L value of the hair color after the calibration time t, L0 represents the L value of the hair color at the initial time, a t represents the a value of the hair color after the calibration time t, a0 represents the a value of the hair color at the initial time, b t represents the b value of the hair color after calibration time t, and b0 represents the b value of the hair color at the initial time.

[0292] Materials: Light yellow, bleached flat hair, 15cm, 3.0g.

[0293] Environmental requirements: Temperature: 21.0℃±1.0℃; Humidity: 50%±10%.

[0294] Hair Color Care Test Program

[0295] Twenty-seven identical flat hair bundles (3.0 g, 15 cm, bleached hair bundles) were randomly selected and divided into nine groups. The hair bundles were placed in a constant temperature and humidity environment [(21±1)℃, (50±10)%RH] for 24 hours.

[0296] The 9 groups of hair bundles were dyed with the same amount of dye, and after dyeing, they were placed in a constant temperature and humidity environment [(21±1)℃, (50±10)%RH] for 24 hours;

[0297] The color values ​​of 9 groups of hair bundles were tested using colorimeter CL400 (Before);

[0298] 9 groups of hair bundles were treated with the products of Examples 1 to 8 or clean water (control group) respectively: after washing the hair bundles, wipe off the excess water, take a sample of 0.1 g / g from each hair bundle and apply it to the hair, after 1 minute of sampling, place the isolated hair in a constant temperature and humidity environment [(21±1)°C, (50±10)%RH] to dry naturally for 24 hours, and repeat this operation 50 times in total; the color value (After) of the 9 groups of hair bundles was tested by colorimeter CL400.

[0299] At the same time, test the anti-hair breakage situation of each group of hair bundles according to the method of Test 2.

[0300] Table 3 Test results

[0301]

[0302] Performance Test 4: Stability Test

[0303] The products prepared in Examples 1 to 8 were placed at 0°C and 45°C for 90 days to check their properties, and then placed alternately at 0°C and 45°C for 12 hours. This was repeated 6 times to check the properties of the products.

[0304] Table 4 Test results

[0305]

[0306]

[0307] Performance Test 5: Hair Scale Test Solution

[0308] Randomly select 2 flat hair bundles (3.0g, 15cm, damaged hair bundles) and equilibrate them in a constant temperature and humidity environment [(21±1)℃, (50+±10)%RH] for 24 hours; after washing the hair bundles, wipe off the excess moisture, and sample 0.1g of the product of Example 1 from each hair bundle of the sample group and evenly apply it to the hair, and accept the sample for 1 minute, a total of 1 operation, and the control group is treated with the blank control group according to the above steps. The ex vivo hair was placed in a constant temperature and humidity environment [(21±1)℃(50±10)%RH] to dry naturally for 24 hours; after 24 hours, 3 hair bundles were randomly selected from each group for electron microscopy comparison. See the specific results for details. Figure 1 and Figure 2 .in, Figure 1 is the sample group, Figure 2 It is the control group.

[0309] Traditional fermented oil uses yeast to decompose oil into small molecular oils to promote absorption; first, the strains of oil decomposition have certain production capacity limitations, and are finally mixed with macromolecular oils, so the effect is not ideal. The present invention uses two types of strains for fermentation, starting with the plant raw materials themselves, and using yeast to decompose the plant oil obtained by the strains, which can controllably adjust the oil to a certain extent.

[0310] However, the inventors found that the above method has low yield and high cost. Therefore, they simulated the ecological protection mechanism, stored the freshly picked plants at low temperature, and then carried out enzymatic hydrolysis and double fermentation. This not only can achieve higher yield, but also better hair care effect. At the same time, when matching hair care products, more macromolecules and siloxanes of the same type are selected for compounding, so that skin care products with higher product stability can be obtained.

[0311] Finally, it should be noted that the above embodiments are only used to illustrate the technical solutions of the present invention, rather than to limit it. Although the present invention has been described in detail with reference to the aforementioned embodiments, those skilled in the art should understand that they can still modify the technical solutions described in the aforementioned embodiments, or replace some or all of the technical features therein with equivalents. However, these modifications or replacements do not cause the essence of the corresponding technical solutions to deviate from the scope of the technical solutions of the embodiments of the present invention.

Claims

1. A fermented oil for hair, characterized in that: The raw materials for its preparation include: sweet almond, macadamia nut seeds, rhizome of Anemarrhena asphodeloides and citron fruit.

2. A fermented oil for hair use according to claim 1, characterized in that: The mass ratio of the sweet almond, macadamia nut seeds, rhizome of Anemarrhena asphodeloides and citron fruit is 1:1:1:

1.

3. A hair conditioner, characterized in that: The invention comprises a fermented oil for hair use as claimed in claim 1 or 2.

4. A hair conditioner according to claim 3, characterized in that: The preparation raw materials include: hair conditioning agent, moisturizing agent, fragrance, hair care agent, moisturizing agent and antioxidant.

5. A hair conditioner according to claim 3, characterized in that: According to the mass fraction, the raw materials for its preparation include: Cyclopentasiloxane 50-60 Dimethicone, Dimethiconol 35-45 Isohexadecane 4-5 Fragrance 0.8-1 Caprylic / capric triglyceride 0.1-1 Fermented oil for hair 0.1-1 MAURITIA FLEXUOSA FRUIT OIL 0.1-1 Macadamia ternifolia seed oil 0.1-1 Sweet almond (PRUNUS AMYGDALUSDULCIS) oil 0.1-1 Jojoba (SIMMONDSIA CHINENSIS) seed oil 0.1-1 Tocopheryl acetate 0.02-0.

06.

6. A hair conditioner according to claim 3, characterized in that: According to the mass fraction, the raw materials for its preparation include: Cyclopentasiloxane 53 Dimethicone, Dimethiconol 42 Isohexadecane 4 Fragrance 0.9 Caprylic / capric triglyceride 0.7 Fermented oil for hair1 MAURITIA FLEXUOSA FRUIT OIL 0.3 Macadamia ternifolia seed oil 0.2 Sweet almond (PRUNUS AMYGDALUSDULCIS) oil 0.5 Jojoba (SIMMONDSIA CHINENSIS) seed oil 0.5 Tocopheryl acetate 0.

05.

7. A method for preparing a hair conditioner according to any one of claims 3 to 6, characterized in that: Here are the steps: (1) Add cyclopentasiloxane, polydimethylsiloxane and polydimethylsiloxane alcohol into a stirring emulsifier, start stirring, and stir until the mixture is uniform and transparent; (2) Add isohexadecane, flavor, caprylic / capric triglyceride into an emulsifier and keep stirring; (3) Add fermented oil, MAURITIA FLEXUOSA fruit oil, MACADAMIATERNIFOLIA seed oil, PRUNUS AMYGDALUS DULCIS oil, jojoba seed oil, and tocopherol acetate, stir evenly until the mixture is evenly mixed and discharged.

8. The hair conditioner according to any one of claims 3 to 6 is used in the field of daily chemicals.

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