Trichosanthes kirilowii maxim waste treatment method and application thereof in preparation of trichosanthes kirilowii maxim wine
The hydroelectric effect treatment is carried out through the hydraulic and electrical reaction tank, and the complex treatment process of Trichosanthes kirilowii waste is solved, the process is simplified and the production efficiency is improved, and high-quality Trichosanthes waste secondary utilization materials suitable for the brewing of Trichosanthes kirilowii wine are obtained.
Patent Information
- Application Number
- CN202510033759.8
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-01-09
- Publication Date
- 2025-03-25
- Estimated Expiration
- 2045-01-09
AI Technical Summary
The existing Trichosanthes waste treatment process is complicated and the equipment is different, which seriously restricts the improvement of production efficiency.
The hydroelectric reaction tank is used for hydroelectric effect treatment, so as to realize the crushing, disinfection, pickling and alkali washing of Trichosanthes waste, and simplify the process flow.
Through the liquid-electric effect treatment, the treatment process of Trichosanthes kirilowii waste is simplified and the production efficiency is improved. The secondary utilization material of Trichosanthes waste obtained has high porosity and large specific surface area, which is suitable for the brewing of Trichosanthes wine.
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Figure CN119680990A_ABST
Abstract
Description
Technical Field
[0001] The invention belongs to the technical field of solid waste treatment, and particularly relates to a method for treating trichosanthes waste and application of the method in preparing trichosanthes wine. Background Art
[0002] Trichosanthes kirilowii is also called medicinal melon, and its scientific name is Trichosanthes kirilowii. Its whole body is a treasure. The melon shell can be used as medicine, and the mature Trichosanthes kirilowii seeds can be used as health and leisure food after being dried, and the roots of Trichosanthes kirilowii can be made into Radix Trichosanthis, which has great utilization value and high economic benefits.
[0003] In the treatment of Trichosanthes, whether it is for medicinal or food use, a large amount of solid waste will be generated, such as Trichosanthes roots, pulp, skin and Trichosanthes kernel meal and other scraps and by-products, which are usually treated as waste. If these Trichosanthes wastes are not comprehensively utilized, it will cause great waste.
[0004] In the secondary processing of the waste of Trichosanthes, it can be fermented into industrial alcohol or Trichosanthes wine. When studying the fermentation of Trichosanthes waste as raw material, it is necessary to perform preliminary treatment on the Trichosanthes waste, such as crushing, disinfection, pickling, alkali washing and other processes (refer to the "A Process for Reusing and Treating Chinese Medicine Waste" disclosed in Publication No. CN115090646A). In particular, although the Trichosanthes root has a high starch content, it also carries more pathogens. The use of pickling or alkali washing can ensure more thorough sterilization, and can also loosen the root fiber, which is conducive to subsequent fermentation.
[0005] However, the above-mentioned processes of crushing, disinfection, pickling, alkali washing, etc. are complicated and the equipment used is also different, which seriously restricts the improvement of production efficiency.
[0006] Therefore, it is necessary to invent a new method or equipment that can simultaneously carry out processes such as crushing, disinfection, pickling, alkali washing, etc. on Trichosanthes waste, which is conducive to improving production efficiency. Summary of the invention
[0007] The object of the present invention is to provide a method for treating Trichosanthes waste and application of the method in preparing Trichosanthes wine, so as to solve the above-mentioned problems.
[0008] On the one hand, a method for treating Trichosanthes waste comprises the following steps:
[0009] Step 1, removing impurities and cleaning the Trichosanthes waste to obtain Trichosanthes waste material;
[0010] Step 2, pouring the Trichosanthes waste material, the ellipsoidal conductive stirring bar and the first solvent into the liquid-electric reaction tank, and sealing the liquid-electric reaction tank;
[0011] When the first electrode and the second electrode arranged in the liquid-electric reaction tank are connected to pulse electricity, a liquid-electric effect is generated, and the waste material of Trichosanthes kirilowii is broken into granular material in the first solvent;
[0012] Step 3: Use a submersible sewage pump to discharge the granular material and water in the liquid-electric reaction tank from the liquid-electric reaction tank, drain them, and obtain the secondary utilization material of the Trichosanthes waste.
[0013] A further improvement is that the liquid-electric reaction tank includes an insulating tank body, a high-voltage pulse power supply, and an air pump. A spherical first reaction zone and a cylindrical second reaction zone are arranged in sequence from top to bottom inside the insulating tank body, and the first reaction zone and the second reaction zone are connected; the high-voltage pulse power supply is respectively connected to a first electrode and a second electrode, the first electrode includes a first conductor embedded in the side wall of the second reaction zone and a second conductor embedded in the bottom of the second reaction zone, and the second electrode includes a third conductor embedded in the side wall of the first reaction zone; the volume of the first reaction zone is smaller than the volume of the second reaction zone.
[0014] As a further improvement, the liquid-electric reaction tank also includes an air pump, a gate valve is installed below the insulating tank body, a discharge port is provided at the bottom of the second reaction zone, the discharge port includes an inverted cone-shaped upper hole section and a cylindrical lower hole section, the upper hole section is connected to the lower hole section, and the lower hole section is connected to the input end of the gate valve; a filter plate that completely covers the upper hole section is also provided at the bottom of the second reaction zone; a circular injection pipe is also provided inside the upper hole section, the injection pipe is located below the filter plate, and the injection pipe is connected to the air pump.
[0015] As a further improvement, the second conductor is sheet-shaped and is provided in multiple pieces, the first conductor is a cylindrical helical spring-shaped structure; the third conductor is a circular ring-shaped structure and is provided in multiple pieces, and the third conductors are arranged at equal intervals in the first reaction zone.
[0016] As a further improvement, a cover for closing the first reaction zone is provided on the top of the insulating tank body, one end of the cover is hinged to the top of the insulating tank body, and a fastener is provided between the other end of the cover and the top of the insulating tank body.
[0017] As a further improvement, the ratio of the volume of the second reaction zone to the volume of the first reaction zone is x, 2.7≤x≤3.1.
[0018] Further improvement, the mass of the waste material of Trichosanthes kirilowii in the insulating tank is m 2 , the mass of the conductive stirrer is m 1 , y=m 1 / m 2 ; 1.5≤y≤2;
[0019] The high-voltage pulse power supply has an output voltage of 10-15 kV, a duration of each current group of 5 s, and a pulse duty cycle of 33.3%.
[0020] In a further improvement, the conductive stirring bar is composed of a cast iron ellipsoid with micropores on the surface, a lead ellipsoid and a chrome-plated iron ellipsoid in a mass ratio of 2:2:1, and the specific surface area of the cast iron ellipsoid with micropores on the surface is greater than 10m 2 / g; the ratio of the major axis to the minor axis of the conductive stirring bar is 3.2:1.
[0021] In a further improvement, the first solvent is one or more of water and an organic solvent.
[0022] On the other hand, the method for treating the waste of Trichosanthes kirilowii is used in the preparation of Trichosanthes kirilowii wine. For example, the Trichosanthes kirilowii waste secondary utilization material prepared by the method for treating the waste of Trichosanthes kirilowii has a particle size of no more than 3 mm (about the size of a mung bean), and the Trichosanthes kirilowii waste secondary utilization material can be graded as needed, so as to be used as raw materials such as Daqu and Xiaoqu for brewing wine, and can also be used to replace some auxiliary materials or fillers (such as bran, grain husks, sugarcane bagasse, etc.) for brewing wine.
[0023] Compared with the prior art, the present invention has the following beneficial effects:
[0024] 1. The present invention can perform similar "crushing", "disinfection", "pickling" and "alkali washing" operations on Trichosanthes waste through the liquid-electric effect carried out in the liquid-electric reaction tank. The operation method is simple, the production process is greatly simplified, and the production efficiency is high.
[0025] 2. The particle size of the recycled material of Trichosanthes waste obtained by the electrohydraulic effect does not exceed 3mm, the porosity can reach 89.3%, and the specific surface area can reach 705m² / g; the Trichosanthes waste has no carbonization phenomenon, and a large amount of foam will not appear in the reaction process. There is no oily substance in the product, and the content of aldehydes in the solution of the product is less than 90mg / 100ml. The solution of the product does not contain ethanol and methanol and is neutral; the recycled material of Trichosanthes waste has a high porosity and a large specific surface area, and the by-products will not affect the subsequent winemaking. Whether the recycled material of Trichosanthes waste is used to make koji or directly replace a part of the winemaking raw materials, it can be used in the brewing of Trichosanthes wine. BRIEF DESCRIPTION OF THE DRAWINGS
[0026] Figure 1 This is a schematic diagram of the structure of the liquid-electric reaction tank of the present invention;
[0027] Figure 2 It is a schematic diagram of the bottom of the insulating tank;
[0028] In the accompanying drawings, the components represented by the reference numerals are listed as follows:
[0029] 10. Insulated tank; 11. Second reaction zone; 12. First reaction zone; 13. Discharge port; 131. Upper hole section; 132. Lower hole section; 14. Gate valve; 15. Cover; 16. Fastener; 17. Filter plate;
[0030] 21. third conductor; 22. first conductor; 23. second conductor;
[0031] 30. Jet pipe. DETAILED DESCRIPTION
[0032] The present invention is further described in detail below through specific embodiments in conjunction with the accompanying drawings.
[0033] In the description of the present invention, it should be noted that, unless otherwise specified, "multiple" means two or more than two; the directions or positional relationships indicated by the terms "upper", "lower", "left", "right", "inner", "outer", "front end", "rear end", "head", "tail", etc. are based on the directions or positional relationships shown in the accompanying drawings, and are only for the convenience of describing the present invention and simplifying the description, and do not indicate or imply that the device or element referred to must have a specific direction, be constructed and operated in a specific direction, and therefore cannot be understood as limiting the present invention. In addition, the terms "first", "second", "third", etc. are only used for descriptive purposes and cannot be understood as indicating or implying relative importance.
[0034] In the description of the present invention, it should be noted that, unless otherwise clearly specified and limited, the terms "installed", "connected", and "connected" should be understood in a broad sense, for example, it can be a fixed connection, a detachable connection, or an integral connection; it can be a mechanical connection or an electrical connection; it can be a direct connection, or it can be indirectly connected through an intermediate medium, or it can be the internal communication of two components. For ordinary technicians in this field, the specific meanings of the above terms in the present invention can be understood according to specific circumstances.
[0035] Example 1
[0036] A method for treating Trichosanthes waste comprises the following steps:
[0037] Step 1, removing impurities and cleaning the Trichosanthes waste to obtain Trichosanthes waste material;
[0038] Step 2, pouring the Trichosanthes waste material, the ellipsoidal conductive stirring bar and the first solvent into the liquid-electric reaction tank, and sealing the liquid-electric reaction tank;
[0039] When the first electrode and the second electrode arranged in the liquid-electric reaction tank are connected to pulse electricity, a liquid-electric effect is generated, and the waste material of Trichosanthes kirilowii is broken into granular material in the first solvent;
[0040] Step 3: Use a submersible sewage pump to discharge the granular material and water in the liquid-electric reaction tank from the liquid-electric reaction tank, drain them, and obtain the secondary utilization material of the Trichosanthes waste.
[0041] In the present invention, the hydroelectric effect refers to:
[0042] When a pulsed high voltage is applied to a pair of electrodes placed in a liquid, the gap between the electrodes is instantly broken down, generating a strong arc spark discharge, accompanied by a series of significant physical, chemical, biological, and mechanical effects. This process is called the liquid-electric effect.
[0043] Liquid phase discharge is an instantaneous energy conversion process. High-density electrical energy can be converted into high-intensity light energy, sound energy, electromagnetic energy, mechanical energy and chemical energy in a very short time with the help of the formation of high-temperature strong plasma in the discharge channel in the liquid, causing drastic changes in the sound, light, electromagnetic, mechanical and chemical states in the environment, and producing mechanical effects, chemical effects, electromagnetic radiation effects, supercritical liquid effects, biological effects, etc.
[0044] The mechanical effect, also known as the mechanical effect, is a shock wave that propagates rapidly (supersonic) through the liquid phase and will exhibit an ultra-high-power mechanical effect to the outside world, that is, it will produce a mechanical effect that can cut and crush solid materials.
[0045] Chemical effect: When liquid phase discharge occurs, the combined effects of sound, light, heat, shock waves and other factors will cause significant changes in the chemical composition of the liquid phase, changing the original chemical properties of the liquid phase and making the liquid extremely chemically active.
[0046] Supercritical liquid effect. The high temperature and high pressure generated by liquid phase discharge puts the local liquid in the liquid phase into a supercritical state, resulting in a huge change in the properties of the liquid.
[0047] Biological effects generally refer to sterilization, inactivation of microorganisms, etc.
[0048] Therefore, in the present invention, similar "crushing", "disinfection", "pickling" and "alkaline washing" operations can be performed on the Trichosanthes waste through the liquid-electric effect in the liquid-electric reaction tank. The operation method is particularly simple, which greatly simplifies the production process and significantly improves the production efficiency.
[0049] Example 2
[0050] like Figure 1~2As shown, the liquid-electric reaction tank includes an insulating tank body 10, a high-voltage pulse power supply, and an air pump. The insulating tank body 10 is preferably made of concrete. The insulating tank body 10 is provided with a spherical first reaction zone 12 and a cylindrical second reaction zone 11 from top to bottom, and the first reaction zone 12 is connected to the second reaction zone 11; the high-voltage pulse power supply is connected to a first electrode and a second electrode respectively, the first electrode includes a first conductor 22 embedded in the side wall of the second reaction zone 11 and a second conductor 23 embedded in the bottom of the second reaction zone 11, and the second electrode includes a third conductor 21 embedded in the side wall of the first reaction zone 12; the volume of the first reaction zone 12 is smaller than the volume of the second reaction zone 11.
[0051] The second conductor 23 is sheet-shaped and is provided in multiple pieces, the first conductor 22 is a cylindrical helical spring-shaped structure; the third conductor 21 is a circular ring-shaped structure and is provided in multiple pieces, and the third conductor 21 is arranged at equal intervals in the first reaction zone 12.
[0052] The ratio of the volume of the second reaction zone 11 to the volume of the first reaction zone 12 is x, 2.7≤x≤3.1.
[0053] The mass of the waste Trichosanthes kirilowii in the insulating tank 10 is m 2 , the mass of the conductive stirrer is m 1 , y=m 1 / m 2 ; 1.5≤y≤2;
[0054] The high-voltage pulse power supply has an output voltage of 10-15 kV, a duration of each current group of 5 s, and a pulse duty cycle of 33.3%.
[0055] The conductive stirring bar is composed of a cast iron ellipsoid with micropores on the surface, a lead ellipsoid and a chrome-plated iron ellipsoid in a mass ratio of 2:2:1, and the specific surface area of the cast iron ellipsoid with micropores on the surface is greater than 10m 2 / g; the ratio of the major axis to the minor axis of the conductive stirring bar is 3.2: 1. The cast iron ellipsoid with micropores on the surface can be made by acid corrosion.
[0056] In this embodiment, the first solvent is preferably water.
[0057] In the present invention, the function of the conductive stirrer is to form a series of conductive channels between the first electrode and the second electrode, so as to better promote the occurrence of the hydroelectric effect, so that the Trichosanthes waste can be better and more evenly crushed.
[0058] It is well known in the field that in the field of winemaking, the raw materials must have a certain porosity, especially for koji making, such as the manual koji stepping process, which is conducive to microbial fermentation. Manual koji stepping can better control the tightness of the koji block, thereby affecting the aeration and fermentation effect. Manual koji stepping can step out a "turtle back shaped" koji block, that is, the four sides are tight and the middle is loose. This shape is conducive to microbial fermentation, increases the fermentation space, and also helps to retain water in the koji block.
[0059] It can be seen that if the brewing raw material can have a sufficiently large porosity / specific surface area, it is beneficial to fermentation whether it is used for koji making or directly replaces part of the brewing raw material. Therefore, the core of the present invention, on the one hand, needs to ensure that the Trichosanthes waste is crushed to a specified particle size in a short time, and on the other hand, it is also necessary to ensure that the Trichosanthes waste secondary utilization material obtained after crushing has sufficient porosity / specific surface area.
[0060] In this embodiment, the fermentation process of trichosanthes wine is in accordance with the fermentation process of the existing GB / T 19328-2007 geographical indication product-Kouzijiao wine, and the brewing raw materials mainly include sorghum, wheat, barley, peas, rice and glutinous rice. In the present invention, in order to ensure the taste, the secondary utilization of trichosanthes waste materials is used to replace 20% of the brewing raw materials. If it is fermented industrial alcohol, the brewing raw materials are all the secondary utilization of trichosanthes waste materials.
[0061] In this embodiment, the volume of the second reaction zone 11 is 18 L, the volume of the first reaction zone 12 is 6 L, and x = 3. 5 kg of Trichosanthes waste material, 8 kg of conductive stirring bar, and y = 1.6; the first solvent fills the first reaction zone 12.
[0062] After reacting in the liquid-electric reactor for 6 minutes, the final secondary utilization material of the waste Trichosanthes kirilowii is obtained, the particle size of which does not exceed 3 mm, the porosity can reach 89.3%, and the specific surface area can reach 705 m² / g; the waste Trichosanthes kirilowii has no carbonization phenomenon, a large amount of foam will not appear during the reaction process, there is no oily substance in the product, the content of aldehydes in the solution of the product is less than 90 mg / 100 ml, and the solution of the product does not contain ethanol and methanol and is neutral.
[0063] Because the first conductor 22 is a cylindrical helical spring structure, the arc trend around it is spirally ascending. Combined with the second reaction zone 11 being cylindrical and the shape and position of the second conductor 23, the ultimate goal is to generate an upward shock wave in the second reaction zone 11, thereby better breaking up the Trichosanthes waste.
[0064] If the volume of the first reaction zone 12 is larger than the volume of the second reaction zone 11, uneven crushing will result. After 10 minutes of reaction in the liquid-electric reactor, there will still be some residual materials with a particle size greater than 5 mm, and the mass of the residual materials accounts for about 12% of the Trichosanthes waste.
[0065] If the first reaction zone 12 and the second reaction zone 11 are both cylindrical structures with the same diameter, or the first reaction zone 12 is a single-leaf hyperbolic structure, these are not conducive to increasing the residence time in the first reaction zone 12; moreover, if the first reaction zone 12 is a single-leaf hyperbolic structure, it will also cause the local arc to be too strong, thereby causing the content of miscellaneous alcohols in the product in the liquid-electric reactor to be too high, exceeding 1770 mg / 100 ml.
[0066] The conductive stirrer must be a combination of three conductive materials of different materials, and the difference in conductivity between the three materials cannot be too large. This is conducive to forming a certain potential difference between the three conductive stirrers of different materials, which is beneficial to the crushing and decomposition of Trichosanthes waste.
[0067] If the conductive stirring bar is a polyhedral structure (such as a cylinder, a cube, an octahedron, etc.), it will cause a portion of the Trichosanthes waste to be carbonized. These carbonized Trichosanthes wastes are difficult to separate and are not conducive to subsequent winemaking.
[0068] If the conductive stirring bar is spherical, its stirring efficiency is not as good as that of the ellipsoidal conductive stirring bar, and it needs to react in the liquid-electric reaction tank for at least 17 minutes, and the particle size of the obtained Trichosanthes waste secondary utilization material does not exceed 3 mm.
[0069] The effects of different compositions of conductive stirrers on the products in the liquid-electric reactor were tested and the results are shown in Table 1: Table 1
[0070]
[0071] As shown in Table 1, the conductive stirrer is made of different materials and has different conductive properties, which will eventually affect the porosity, specific surface area and whether other impurities will appear in the product. The presence of oily substances and a large amount of aldehydes in the product will pollute the recycled material of Trichosanthes waste and affect the subsequent brewing of Trichosanthes wine.
[0072] In addition, the study found that the ratio of the major axis to the minor axis of the conductive stirrer also significantly affects the product. The specific results are shown in Table 2:
[0073] Table 2 The ratio of the major axis to the minor axis of the conductive stirring bar Impact on products 1.5:1 The reaction is carried out in the liquid-electric reactor for at least 13 minutes, and the particle size of the secondary recycling material of the Trichosanthes waste obtained does not exceed 3mm. 2:1 After 15 minutes of reaction in the liquid-electric reactor, the product solution contained ethanol, with a mass fraction of ethanol exceeding 3.3%. 3:1 After 2 minutes of reaction in the liquid-electric reactor, a large amount of foam appeared and the product solution was acidic. 3.2:1 No foam, no carbonization, the product solution does not contain ethanol or methanol; the product solution is neutral 3.5:1 The product solution contains a large amount of methanol, the content exceeds 2550mg / 100ml 5:1 Some of the waste from Trichosanthes kirilowii appeared carbonized
[0074] Therefore, for brewing Trichosanthes wine, the ratio of the major axis to the minor axis of the conductive stirring bar is preferably 3.2:1.
[0075] Example 3
[0076] In Example 2, to facilitate discharging, the liquid-electric reactor also includes an air pump, a gate valve 14 is installed below the insulating tank body 10, and a discharge port 13 is provided at the bottom of the second reaction zone 11. The discharge port 13 includes an inverted cone-shaped upper hole section 131 and a cylindrical lower hole section 132. The upper hole section 131 is connected to the lower hole section 132, and the lower hole section 132 is connected to the input end of the gate valve 14; a filter plate 17 that completely covers the upper hole section 131 is also provided at the bottom of the second reaction zone 11; a circular injection pipe 30 is also provided inside the upper hole section 131, and the injection pipe 30 is located below the filter plate 17, and the injection pipe 30 is connected to the air pump.
[0077] Compressed air is intermittently introduced into the jet pipe 30 through an air pump, thereby applying a pulsed impact force to the area near the discharge port 13 to assist in discharge. The filter plate 17 is used to block the conductive stirring bar, and water and particulate materials can pass through the filter holes on the surface of the filter plate 17 and then be discharged through the discharge port 13. Among them, the structure of the upper hole section 131, in conjunction with the compressed air ejected from the jet pipe 30, can discharge materials more effectively and effectively prevent blockage.
[0078] Example 4
[0079] In Example 2, in order to facilitate the sealing of the insulating tank body 10, a cover 15 for closing the first reaction zone 12 is provided on the top of the insulating tank body 10, one end of the cover 15 is hinged to the top of the insulating tank body 10, and a fastener 16 is provided between the other end of the cover 15 and the top of the insulating tank body 10.
[0080] There are many types of fasteners 16, as long as they can fasten the cover 15. The structure can be as follows:
[0081] The fastener 16 includes a convex plate and an L-shaped pin embedded in the top of the insulating tank 10. The end of the cover 15 is provided with a through hole for the convex plate to enter and exit, and the convex plate is provided with a socket matching the L-shaped pin.
[0082] When the cover 15 is covered, the convex plate emerges from the through hole, and then the L-shaped latch is inserted into the jack. As for sealing, it can be considered to use a sealing ring to seal.
[0083] The above are only preferred embodiments of the present invention and are not intended to limit the present invention. For those skilled in the art, the present invention may have various modifications and variations. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention shall be included in the protection scope of the present invention.
Claims
1. A method for treating Trichosanthes waste, characterized in that: The following steps are involved: Step 1, removing impurities and cleaning the Trichosanthes waste to obtain Trichosanthes waste material; Step 2, pouring the Trichosanthes waste material, the ellipsoidal conductive stirring bar and the first solvent into the liquid-electric reaction tank, and sealing the liquid-electric reaction tank; When the first electrode and the second electrode arranged in the liquid-electric reaction tank are connected to pulse electricity, a liquid-electric effect is generated, and the waste material of Trichosanthes kirilowii is broken into granular material in the first solvent; Step 3: Use a submersible sewage pump to discharge the granular material and water in the liquid-electric reaction tank from the liquid-electric reaction tank, drain them, and obtain the secondary utilization material of the Trichosanthes waste.
2. A method for treating Trichosanthes waste according to claim 1, characterized in that: The liquid-electric reaction tank includes an insulating tank body, a high-voltage pulse power supply, and an air pump. A spherical first reaction zone and a cylindrical second reaction zone are arranged in sequence from top to bottom inside the insulating tank body, and the first reaction zone and the second reaction zone are connected; the high-voltage pulse power supply is respectively connected to a first electrode and a second electrode, the first electrode includes a first conductor embedded in the side wall of the second reaction zone and a second conductor embedded in the bottom of the second reaction zone, and the second electrode includes a third conductor embedded in the side wall of the first reaction zone; the volume of the first reaction zone is smaller than that of the second reaction zone.
3. A method for treating Trichosanthes waste according to claim 2, characterized in that: The liquid-electric reaction tank also includes an air pump, a gate valve is installed below the insulating tank body, a discharge port is arranged at the bottom of the second reaction zone, the discharge port includes an inverted cone-shaped upper hole section and a cylindrical lower hole section, the upper hole section is connected with the lower hole section, and the lower hole section is connected with the input end of the gate valve; a filter plate that completely covers the upper hole section is also arranged at the bottom of the second reaction zone; a circular injection pipe is also arranged inside the upper hole section, the injection pipe is located below the filter plate, and the injection pipe is connected to the air pump.
4. A method for treating Trichosanthes waste according to claim 2, characterized in that: The second conductor is in sheet form and is provided in multiple pieces, the first conductor is in a cylindrical helical spring structure; the third conductor is in a circular ring structure and is provided in multiple pieces, and the third conductor is arranged at equal intervals in the first reaction zone.
5. A method for treating Trichosanthes waste according to claim 2, characterized in that: A cover for sealing the first reaction zone is arranged on the top of the insulating tank body, one end of the cover is hinged to the top of the insulating tank body, and a fastener is arranged between the other end of the cover and the top of the insulating tank body.
6. A method for treating Trichosanthes waste according to claim 4, characterized in that: The ratio of the volume of the second reaction zone to the volume of the first reaction zone is x, 2.7≤x≤3.
1.
7. A method for treating Trichosanthes waste according to claim 6, characterized in that: The mass of the waste Trichosanthes kirilowii in the insulating tank is m2, the mass of the conductive stirring bar is m1, y=m1 / m2; 1.5≤y≤2; The high-voltage pulse power supply has an output voltage of 10-15 kV, a duration of each current group of 5 s, and a pulse duty cycle of 33.3%.
8. A method for treating Trichosanthes waste according to claim 7, characterized in that: The conductive stirring bar is composed of a cast iron ellipsoid with micropores on the surface, a lead ellipsoid and a chrome-plated iron ellipsoid in a mass ratio of 2:2:1, and the specific surface area of the cast iron ellipsoid with micropores on the surface is greater than 10m 2 / g; the ratio of the major axis to the minor axis of the conductive stirring bar is 3.2:
1.
9. A method for treating Trichosanthes waste according to claim 1, characterized in that: The first solvent is one or more of water and an organic solvent.
10. Use of a method for treating Trichosanthes waste according to any one of claims 1 to 9 in preparing Trichosanthes wine.
Citation Information
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