A device for extracting rubidium-cesium refined salt from low-grade lepidolite

By designing a low-grade lithium mica rubidium cesium refined salt extraction device containing stirring, heating and vibration mechanisms, the problems of uneven material mixing and bottoming in traditional processes are solved, and the extraction efficiency and product quality are significantly improved.

CN119746784APending Publication Date: 2025-04-04JIANGXI JINZHI NEW ENERGY CO LTD
View PDF 0 Cites 1 Cited by

Patent Information

Application Number
CN202510059660.5
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-01-15
Publication Date
2025-04-04

AI Technical Summary

Technical Problem

In the traditional process of extracting rubidium cesium fine salt from low-grade lithium mica, uneven material mixing and bottoming phenomenon lead to low extraction efficiency, poor product quality, and it is difficult for traditional stirring devices to clean up the materials attached to the tank wall.

Method used

A rubidium cesium refined salt extraction device including a stirring mechanism, a heating mechanism and a vibration mechanism is designed. The stirring mechanism realizes the up and downward rush of the material through the lifting plate and the reciprocating screw, while the scraper and spiral plate promote the spiral rise of the material and removes the residue of the tank wall. The heating mechanism increases the temperature through the heating pipe and accelerates the reaction rate, while the vibration mechanism enhances the collision frequency between the substances through slight vibration.

Benefits of technology

It significantly improves the extraction efficiency of rubidium cesium refined salt, ensures uniform mixing of reactants, avoids material sinking, and improves the thoroughness of the reaction and consistency and stability of product quality.

✦ Generated by Eureka AI based on patent content.

Smart Images

  • Figure CN119746784A_ABST
    Figure CN119746784A_ABST
Patent Text Reader

Abstract

The present invention relates to the field of ore extraction, and in particular to a device for extracting rubidium and cesium refined salt from low-grade lepidolite, comprising an extraction tank, a top plate installed on the top of the extraction tank by bolts, a feed hopper arranged on the upper front side of the top plate, a liquid inlet arranged on the rear side of the extraction tank, a motor arranged on the upper side of the top plate, a motor output shaft arranged downward, a stirring frame connected to the motor output shaft, the stirring frame rotatably connected to the extraction tank, a discharge pipe connected to the bottom of the extraction tank, and a solenoid valve arranged on the discharge pipe. The present invention significantly improves the extraction efficiency of rubidium and cesium refined salt from low-grade lepidolite through a stirring mechanism, and the lifting plate cooperates with a reciprocating screw rod to realize the up and down surging of the material, ensures the uniform mixing of the reactants, and avoids the problem of material sinking to the bottom in the traditional method. The design of the scraper and the spiral plate not only promotes the spiral rise of the material, but also effectively removes the residue on the tank wall, improves the thoroughness of the reaction, reduces the possibility of secondary pollution, and provides purer raw materials for subsequent processes.
Need to check novelty before this filing date? Find Prior Art

Description

Technical Field

[0001] The invention relates to the field of ore extraction, in particular to a device for extracting rubidium-cesium refined salt from low-grade lepidolite. Background Art

[0002] In the traditional process of extracting rubidium and cesium refined salt from low-grade lepidolite, uneven material mixing and sedimentation are key issues affecting the extraction efficiency. Due to the complex composition of lepidolite ore, traditional stirring equipment is difficult to ensure that all materials are evenly dispersed in the reaction solution, resulting in some materials failing to fully participate in the chemical reaction. Especially when the material density is large, it is easy to settle to the bottom of the extraction tank to form a sediment layer, further hindering the reaction. This incomplete reaction not only reduces the extraction rate of rubidium and cesium refined salt, but may also affect product quality due to the presence of residues. In addition, the traditional stirring device is not effective in cleaning the materials attached to the tank wall, making these materials unable to participate in subsequent reactions, resulting in waste of resources and increasing the workload of cleaning and maintenance.

[0003] Therefore, in view of the above problems, a device for extracting rubidium-cesium refined salt from low-grade lepidolite is now developed. Summary of the invention

[0004] In order to overcome the shortcomings of the existing devices, the present invention provides a device for extracting rubidium-cesium refined salt from low-grade lepidolite.

[0005] The technical implementation scheme of the present invention is: a rubidium-cesium refined salt extraction device for low-grade lithium mica, comprising an extraction tank, a top plate is installed on the top of the extraction tank by bolts, a feed hopper is arranged on the upper front side of the top plate, a liquid inlet is arranged on the rear of the extraction tank, a motor is arranged on the upper side of the top plate, the motor output shaft is arranged downward, a stirring frame is connected to the motor output shaft, the stirring frame is rotatably connected to the extraction tank, a discharge pipe is connected to the bottom of the extraction tank, a solenoid valve is arranged on the discharge pipe, a stirring mechanism is arranged inside the extraction tank, the stirring mechanism is used to stir the material in the extraction tank so that the material is always in motion to prevent the material from sinking to the bottom, and a heating mechanism is arranged on the extraction tank, the heating mechanism is used to increase the temperature and increase the reaction rate.

[0006] In a preferred embodiment of the present invention, the stirring mechanism includes a lifting plate, four limit rods are connected in the extraction tank, the lifting plate is slidably connected between the limit rods, a reciprocating screw is arranged at the bottom of the stirring frame, a connecting piece is connected to the inner side of the lifting plate, the connecting piece is slidably connected to the reciprocating screw, a scraper is connected to the stirring frame, the scraper is thin at the bottom and thick at the top, a spiral plate is arranged on the scraper, the spiral plate is used to drive the material to spirally tumble, a limit plate is arranged on the lifting plate, and the limit plate is located on the inner side of the scraper.

[0007] In a preferred embodiment of the present invention, the heating mechanism includes a mounting plate, four mounting plates are slidably connected to the extraction tank, the mounting plates are inserted into the partition of the extraction tank, the inner sides of the mounting plates are connected to heating tubes, and the upper parts of the mounting plates are connected to sealing blocks.

[0008] In a preferred embodiment of the present invention, a vibration mechanism is further included, and the vibration mechanism includes an installation box. The installation box is arranged on the right side of the extraction tank, and a vibration component is installed in the installation box. The extraction tank is placed on a mounting base, and a shock-absorbing component is arranged on the mounting base. The shock-absorbing component acts on the extraction tank.

[0009] In a preferred embodiment of the present invention, a limiting mechanism is further included, and the limiting mechanism includes a mounting part. Four groups of the mounting parts are connected to the extraction tank, and the mounting parts are rotatably connected to the limiting parts. The limiting parts are used to lock and limit the mounting plate, and a torsion spring is connected between the limiting parts and the adjacent mounting parts.

[0010] In a preferred embodiment of the present invention, a pressure relief mechanism is further included, and the pressure relief mechanism includes a wide-mouth structure and a narrow-mouth structure. A pressure relief pipe is arranged on the lifting plate, and the wide-mouth structure and the narrow-mouth structure are arranged inside the pressure relief pipe. The wide-mouth structure and the narrow-mouth structure cooperate to make the internal air pressure of the extraction tank match the external air pressure to prevent pressure difference.

[0011] In a preferred embodiment of the present invention, a reinforcement mechanism is further included, wherein the reinforcement mechanism includes a reinforcement plate, three groups of the reinforcement plates are connected to the bottom of the spiral plate, through holes are opened on the reinforcement plates, and the reinforcement plates are used to improve the material guiding ability of the spiral plate.

[0012] In a preferred embodiment of the present invention, an end cover is rotatably provided on the top of the feed hopper.

[0013] In a preferred embodiment of the present invention, the top of each mounting plate is provided with a handle.

[0014] By adopting the above technical solution, compared with the prior art, the present invention has the following advantages: 1. The present invention significantly improves the extraction efficiency of rubidium cesium refined salt from low-grade lepidolite through the stirring mechanism. The lifting plate cooperates with the reciprocating screw rod to realize the up and down surging of the material, ensuring the uniform mixing of the reactants and avoiding the problem of material sinking to the bottom in the traditional method. The design of the scraper and spiral plate not only promotes the spiral rise of the material, but also effectively removes the residue on the tank wall, improves the thoroughness of the reaction, reduces the possibility of secondary pollution, and provides purer raw materials for subsequent processes.

[0015] 2. The present invention greatly accelerates the chemical reaction rate and improves the reaction conditions by combining the heating mechanism with the vibration mechanism. The heating tube directly heats the material in the extraction tank, shortening the reaction time, and the slight vibration generated by the vibration mechanism further breaks the contact barrier between the materials and enhances the collision frequency between the substances. This synergistic effect not only increases the output of rubidium cesium refined salt, but also ensures the consistency and stability of product quality. BRIEF DESCRIPTION OF THE DRAWINGS

[0016] Figure 1 It is a schematic diagram of the three-dimensional structure of the present invention.

[0017] Figure 2 It is a partial cross-sectional three-dimensional structural schematic diagram of the present invention.

[0018] Figure 3 It is a schematic diagram of a first partial cross-sectional three-dimensional structure of the stirring mechanism of the present invention.

[0019] Figure 4 It is a schematic diagram of a second partial cross-sectional three-dimensional structure of the stirring mechanism of the present invention.

[0020] Figure 5 It is a partial cross-sectional three-dimensional structural schematic diagram of the heating mechanism of the present invention.

[0021] Figure 6 It is a schematic diagram of the three-dimensional structure of the heating mechanism of the present invention.

[0022] Figure 7 It is a partial cross-sectional three-dimensional structural schematic diagram of the vibration mechanism of the present invention.

[0023] Figure 8 It is a partial cross-sectional three-dimensional structural schematic diagram of the limiting mechanism of the present invention.

[0024] Fig. 9 It is a partial cross-sectional three-dimensional structural schematic diagram of the pressure relief mechanism of the present invention.

[0025] Fig.10 It is a schematic diagram of the three-dimensional structure of the reinforcement mechanism of the present invention.

[0026] Among them, the above-mentioned drawings include the following figure marks: 1. extraction tank, 2. top plate, 3. feed hopper, 4. liquid inlet, 5. motor, 6. stirring frame, 7. discharge pipe, 8. solenoid valve, 9. stirring mechanism, 91. lifting plate, 92. limit rod, 93. reciprocating screw rod, 94. connecting piece, 95. scraper, 96. spiral plate, 97. limit plate, 10. heating mechanism, 101. mounting plate, 102. heating tube, 103. sealing block, 11. vibration mechanism, 111. mounting box, 112. vibration assembly, 113. mounting base, 114. shock-absorbing assembly, 12. limit mechanism, 121. mounting piece, 122. limit piece, 123. torsion spring, 13. pressure relief mechanism, 131. wide-mouth structure, 132. narrow-mouth structure, 14. reinforcement mechanism, 141. reinforcement plate, 142. through hole. DETAILED DESCRIPTION

[0027] First of all, it should be pointed out that in the different described embodiments, the same parts are provided with the same reference numerals or the same component names, wherein the disclosure contained in the entire description can be transferred to the same parts with the same reference numerals or the same component names. Selected positional descriptions in the description, such as top, bottom, lateral, etc., also refer to the directly described and shown figures and are transferred to the new positions in the case of a change in position.

[0028] Example 1

[0029] A device for extracting rubidium-cesium refined salt from low-grade lepidolite, such as Figure 1-Figure 10 As shown, it includes an extraction tank 1, a top plate 2 is installed on the top of the extraction tank 1 by bolts, a feed hopper 3 is arranged on the upper front side of the top plate 2, and an end cover is rotatably arranged on the top of the feed hopper 3, a liquid inlet 4 is arranged at the rear of the extraction tank 1, a motor 5 is arranged on the upper side of the top plate 2, the output shaft of the motor 5 is arranged downward, a stirring frame 6 is connected to the output shaft of the motor 5, and the stirring frame 6 is rotatably connected to the extraction tank 1, a discharge pipe 7 is connected to the bottom of the extraction tank 1, and a solenoid valve 8 is arranged on the discharge pipe 7, a stirring mechanism 9 is arranged inside the extraction tank 1, and the stirring mechanism 9 is used to stir the material in the extraction tank 1 so that the material is always in motion to prevent the material from sinking to the bottom, and a heating mechanism 10 is arranged on the extraction tank 1, and the heating mechanism 10 is used to increase the temperature and increase the reaction rate.

[0030] It should be noted that when extracting rubidium and cesium salt from lithium mica, the device can be used for auxiliary operation. First, the material is added to the extraction tank 1 through the feed hopper 3, and then the reaction solution is fed into the extraction tank 1 through the liquid inlet 4. After that, the motor 5 is started. The output shaft of the motor 5 will drive the stirring frame 6 to rotate, so as to mix the material and the reaction solution. In this process, the stirring mechanism 9 and the heating mechanism 10 are started synchronously. The stirring mechanism 9 can directly act on the bottom of the extraction tank 1, so that the material at the bottom can surge upward. At the same time, the heating mechanism can make the material quickly react with the reaction to improve the extraction efficiency. After the extraction is completed, the motor 5 is turned off. At this time, the extracted solution will flow outward through the discharge pipe 7, and the collection of the extracted material can be completed by controlling the solenoid valve 8.

[0031] The stirring mechanism 9 includes a lifting plate 91, four limiting rods 92 are connected in the extraction tank 1, the lifting plate 91 is slidably connected between the limiting rods 92, a reciprocating screw rod 93 is arranged at the bottom of the stirring frame 6, a connecting piece 94 is connected to the inner side of the lifting plate 91, the connecting piece 94 is slidably connected to the reciprocating screw rod 93, a scraper 95 is connected to the stirring frame 6, the scraper 95 is thin at the bottom and thick at the top, a spiral plate 96 is arranged on the scraper 95, the spiral plate 96 is used to drive the material to spirally surge, a limiting plate 97 is arranged on the lifting plate 91, and the limiting plate 97 is located on the inner side of the scraper 95.

[0032] It should be noted that as the stirring frame 6 starts to rotate, the stirring frame 6 will drive the reciprocating screw 93 to move. Under the action of the reciprocating screw 93, the connecting piece 94 will drive the lifting plate 91 to reciprocate up and down. During the up and down reciprocating movement, the lifting plate 91 will push the material at the bottom, causing the material to surge upward. At the same time, the stirring frame 6 will drive the scraper 95 and the spiral plate 96 to move synchronously during the movement, so that the material surging upward will spiral up and scrape off the material attached to the inner wall of the extraction tank 1 to avoid material residue on the inner wall of the extraction tank 1.

[0033] The heating mechanism 10 includes a mounting plate 101, and four mounting plates 101 are slidably connected to the extraction tank 1. The mounting plates 101 are inserted into the compartment of the extraction tank 1. The tops of the mounting plates 101 are provided with handles. The inner sides of the mounting plates 101 are connected to heating tubes 102, and the upper parts of the mounting plates 101 are connected to sealing blocks 103.

[0034] It should be noted that during the extraction process, the heating tube 102 is started synchronously. The heat generated by the heating tube 102 will increase the temperature in the extraction tank 1, thereby allowing the material and the reaction solution to react and fuse faster. When no maintenance or replacement is required, the handle can be pulled upwards so that the mounting plate 101 drives the heating plate out of the extraction tank 1, thereby completing the removal.

[0035] Example 2

[0036] It also includes a vibration mechanism 11, which includes an installation box 111. The installation box 111 is arranged on the right side of the extraction tank 1, and a vibration component 112 is installed in the installation box 111. The extraction tank 1 is placed on a mounting base 113, and a shock absorbing component 114 is arranged on the mounting base 113. The shock absorbing component 114 acts on the extraction tank 1.

[0037] It should be noted that during the operation of the device, as the stirring frame 6 starts to rotate, the vibration component 112 is started synchronously, and the vibration component 112 begins to generate vibration force, causing the extraction tank 1 to begin to vibrate slightly. At the same time, under the action of the shock-absorbing component 114, the extraction tank 1 can maintain a small amplitude of shaking, thereby assisting the material in the extraction tank 1 to accelerate the reaction.

[0038] It also includes a limiting mechanism 12, which includes a mounting member 121. Four groups of mounting members 121 are connected to the extraction tank 1. The mounting members 121 are all rotatably connected to limiting members 122. The limiting members 122 are used to lock and limit the mounting plate 101. A torsion spring 123 is connected between the limiting member 122 and the adjacent mounting member 121.

[0039] It should be noted that in order to improve the stability of the mounting plate 101, the mounting plate 101 is limited and blocked by the limiting member 122. When the mounting plate 101 needs to be taken out, the limiting member 122 needs to be flipped outward first so that the torsion spring 123 is deformed under the force. At this time, the limiting member 122 no longer blocks the mounting plate 101, and the mounting plate 101 can be directly taken out.

[0040] It also includes a pressure relief mechanism 13, which includes a wide-mouth structure 131 and a narrow-mouth structure 132. A pressure relief pipe is arranged on the lifting plate 91, and the wide-mouth structure 131 and the narrow-mouth structure 132 are arranged inside the pressure relief pipe. The wide-mouth structure 131 and the narrow-mouth structure 132 cooperate to make the internal air pressure of the extraction tank 1 match the external air pressure to prevent pressure difference.

[0041] It also includes a reinforcement mechanism 14 , which includes a reinforcement plate 141 . Three groups of reinforcement plates 141 are connected to the bottom of the spiral plate 96 . Through holes 142 are opened on the reinforcement plates 141 . The reinforcement plates 141 are used to improve the material guiding ability of the spiral plate 96 .

[0042] It should be understood that the above description is only for exemplary purposes and is not meant to limit the present invention. Those skilled in the art will appreciate that variations of the present invention will be included within the scope of the claims herein.

Claims

1. A device for extracting rubidium-cesium refined salt from low-grade lepidolite, characterized in that: The invention comprises an extraction tank (1), wherein a top plate (2) is installed on the top of the extraction tank (1) by bolts, a feed hopper (3) is arranged on the upper front side of the top plate (2), a liquid inlet (4) is arranged on the rear side of the extraction tank (1), a motor (5) is arranged on the upper side of the top plate (2), the output shaft of the motor (5) is arranged downward, a stirring frame (6) is connected to the output shaft of the motor (5), the stirring frame (6) is rotatably connected to the extraction tank (1), a discharge pipe (7) is connected to the bottom of the extraction tank (1), a solenoid valve (8) is arranged on the discharge pipe (7), a stirring mechanism (9) is arranged inside the extraction tank (1), the stirring mechanism (9) is used to stir the material in the extraction tank (1), so that the material is always in a moving state to prevent the material from sinking to the bottom, and a heating mechanism (10) is arranged on the extraction tank (1), the heating mechanism (10) is used to increase the temperature and increase the reaction rate.

2. The device for extracting rubidium-cesium refined salt from low-grade lepidolite according to claim 1, characterized in that: The stirring mechanism (9) comprises a lifting plate (91). Four limiting rods (92) are connected inside the extraction tank (1). The lifting plate (91) is slidably connected between the limiting rods (92). A reciprocating screw rod (93) is arranged at the bottom of the stirring frame (6). A connecting piece (94) is connected inside the lifting plate (91). The connecting piece (94) is slidably connected to the reciprocating screw rod (93). A scraper (95) is connected to the stirring frame (6). The scraper (95) is thin at the bottom and thick at the top. A spiral plate (96) is arranged on the scraper (95). The spiral plate (96) is used to drive the material to spirally surge. A limiting plate (97) is arranged on the lifting plate (91). The limiting plate (97) is located inside the scraper (95).

3. The device for extracting rubidium-cesium refined salt from low-grade lepidolite according to claim 2, characterized in that: The heating mechanism (10) comprises a mounting plate (101), four mounting plates (101) are slidably connected to the extraction tank (1), the mounting plates (101) are inserted into the interlayer of the extraction tank (1), the inner sides of the mounting plates (101) are connected to heating tubes (102), and the upper parts of the mounting plates (101) are connected to sealing blocks (103).

4. The device for extracting rubidium-cesium refined salt from low-grade lepidolite according to claim 3, characterized in that: The invention also comprises a vibration mechanism (11), wherein the vibration mechanism (11) comprises an installation box (111), the installation box (111) is arranged on the right side of the extraction tank (1), a vibration component (112) is installed in the installation box (111), the extraction tank (1) is placed on a installation base (113), a shock absorbing component (114) is arranged on the installation base (113), and the shock absorbing component (114) acts on the extraction tank (1).

5. The device for extracting rubidium-cesium refined salt from low-grade lepidolite according to claim 4, characterized in that: The invention also comprises a limiting mechanism (12), wherein the limiting mechanism (12) comprises a mounting member (121), four groups of the mounting members (121) are connected to the extraction tank (1), and the mounting members (121) are all rotatably connected to limiting members (122), the limiting members (122) are used to lock and limit the mounting plate (101), and a torsion spring (123) is connected between the limiting member (122) and the adjacent mounting member (121).

6. The device for extracting rubidium-cesium refined salt from low-grade lepidolite according to claim 5, characterized in that: The invention also includes a pressure relief mechanism (13), wherein the pressure relief mechanism (13) includes a wide-mouth structure (131) and a narrow-mouth structure (132); a pressure relief pipe is arranged on the lifting plate (91); the wide-mouth structure (131) and the narrow-mouth structure (132) are arranged inside the pressure relief pipe; the wide-mouth structure (131) and the narrow-mouth structure (132) cooperate to make the internal air pressure of the extraction tank (1) match the external air pressure, thereby preventing a pressure difference.

7. The device for extracting rubidium-cesium refined salt from low-grade lepidolite according to claim 6, characterized in that: It also includes a reinforcement mechanism (14), the reinforcement mechanism (14) including a reinforcement plate (141), three groups of the reinforcement plates (141) are connected to the bottom of the spiral plate (96), the reinforcement plates (141) are all provided with through holes (142), and the reinforcement plates (141) are all used to improve the material guiding capability of the spiral plate (96).

8. The device for extracting rubidium-cesium refined salt from low-grade lepidolite according to claim 1, characterized in that: The top of the feed hopper (3) is rotatably provided with an end cover.

9. The device for extracting rubidium-cesium refined salt from low-grade lepidolite according to claim 3, characterized in that: The top of the mounting plate (101) is provided with a handle.

Citation Information

Cited By

  • Method and device for separating alum compounds from lepidolite pickle liquor at low temperature and preparing high-purity rubidium carbonate and cesium carbonate

    CN121718720A