Composition with anti-wrinkle and firming effects, its preparation method and its application

Abstract

The present invention relates to the technical field of skin care products, and specifically discloses a composition with anti-wrinkle and firming effects, a preparation method thereof, and an application thereof. The composition with anti-wrinkle and firming effects comprises the following components in parts by mass: 96.997-98.499 parts of a solvent; 0.5-1 part of extract of Corydalis bulbocapnoides; 0.001-0.003 part of extract of Papilionanthe anubis; 1-2 parts of extract of Spirulina platensis. The present invention has the advantages of more quickly smoothing wrinkles.

Description

Technical Field

[0001] The present invention relates to the field of skin care products, and particularly to a composition with anti-wrinkle and firming effects, a preparation method thereof, and an application thereof. Background Art

[0002] As people age, elastase in the skin gradually accumulates. Under the action of elastase, elastin in the skin gradually decomposes and is lost, resulting in gradual skin relaxation, and then fine lines and wrinkles are formed. Facial wrinkles seriously affect beauty. Therefore, consumers will use skin care products with anti-wrinkle effects to repair the skin and make the skin smooth again, so as to meet the pursuit of beauty of consumers.

[0003] In existing anti-wrinkle skin care products, ingredients that inhibit the activity of elastase are added to achieve the effects of anti-wrinkle and firming. However, with the pursuit of raw material safety by people, conventional chemical synthetic ingredients are difficult to meet the needs of consumers for green raw materials. Therefore, existing anti-wrinkle skin care products usually achieve the effects of anti-wrinkle and firming by adding natural plant ingredients. However, the existing skin care products adding natural plant ingredients are relatively average in the effect of inhibiting elastase, and it is difficult to well promote the repair of elastin, resulting in a slow anti-wrinkle effect and difficult to meet the needs of consumers for rapid wrinkle removal. Therefore, there is still room for improvement. Summary of the Invention

[0004] In order to smooth wrinkles more quickly, the present application provides a composition with anti-wrinkle and firming effects, a preparation method thereof, and an application thereof.

[0005] In a first aspect, the present application provides a composition with anti-wrinkle and firming effects, adopting the following technical solution:

[0006] A composition with anti-wrinkle and firming effects, comprising the following components in parts by mass:

[0007] Solvent 96.997 - 98.499 parts;

[0008] Extract of Corydalis bulbocapnoides 0.5 - 1 part;

[0009] Extract of Papilionanthe anubis 0.001 - 0.003 part;

[0010] Extract of Spirulina platensis Geitler 1 - 2 parts.

[0011] By adopting the above technical solution, through the special compounding of the extract of Corydalis bulbocapnoides, the extract of Papilionanthe anubis, and the extract of Spirulina platensis Geitler, under the mutual cooperation of each active ingredient, a very significant effect of inhibiting elastase is achieved, and then the repair of skin elastin is better promoted, so that the skin quickly returns to being smooth and elastic, thereby achieving the effect of quickly smoothing wrinkles.

[0012] Preferably, the solvent is water.

[0013] By adopting the above technical solution, by specifically selecting water as the solvent, each active ingredient can be fully dissolved in the solvent, so as to better exert the synergistic effect and achieve a better anti-wrinkle and firming effect.

[0014] Preferably, the extracts of Corydalis bulbocapnoides, Papilionanthe anubis, and Spirulina platensis are all water-soluble extracts.

[0015] By adopting the above technical solution, by specifically selecting that the extracts of Corydalis bulbocapnoides, Papilionanthe anubis, and Spirulina platensis are all water-soluble extracts, the active ingredients are more easily absorbed by the skin, so that the active ingredients can better penetrate deep into the skin, and further the effect of inhibiting elastase activity can be better exerted, achieving the effect of quickly smoothing wrinkles.

[0016] In the second aspect, the present application provides a preparation method of a composition with anti-wrinkle and firming effects, adopting the following technical solution:

[0017] A preparation method of a composition with anti-wrinkle and firming effects as described above, mixing the solvent, the extract of Corydalis bulbocapnoides, the extract of Papilionanthe anubis, and the extract of Spirulina platensis evenly, and then a composition with anti-wrinkle and firming effects can be obtained.

[0018] By adopting the above technical solution, the prepared composition with anti-wrinkle and firming effects can significantly inhibit the activity of elastase, promote the repair of skin elastin, so that the skin restores smoothness and achieves the effect of quickly smoothing wrinkles.

[0019] In the third aspect, the present application provides an application of a composition with anti-wrinkle and firming effects, adopting the following technical solution:

[0020] An application of a composition with anti-wrinkle and firming effects as described above, adding the composition with anti-wrinkle and firming effects to skin care products to prepare skin care products with anti-wrinkle and firming effects.

[0021] By adopting the above technical solution, the skin care products added with the composition with anti-wrinkle and firming effects have significant anti-wrinkle and firming effects, can quickly smooth wrinkles, and well meet the needs of consumers.

[0022] Preferably, the skin care product is skin care lotion.

[0023] By adopting the above technical solution, by specifically selecting skin care lotion, the active ingredients in the skin care lotion are more easily absorbed by the skin, and the anti-wrinkle and firming effect is more significant, and the effect of smoothing wrinkles is faster.

[0024] Preferably, the skin care lotion comprises the following components in parts by mass:

[0025] Water 87.7 - 92.3 parts;

[0026] Glycerol 2 - 4 parts;

[0027] Butanediol 4 - 6 parts;

[0028] Hexylene glycol 0.4 - 0.6 part;

[0029] p - Hydroxyacetophenone 0.4 - 0.6 part;

[0030] Composition with anti - wrinkle and firming effects 0.9 - 1.1 parts.

[0031] By adopting the above - mentioned technical solution, the addition amount of the composition with anti - wrinkle and firming effects in the skin care lotion is just right, which can play a very good anti - wrinkle and firming effect. At the same time, due to the small addition amount, the process difficulty of adding it to the formula is relatively low, and it has high economic value.

[0032] Preferably, the preparation method of the skin care lotion comprises the following steps:

[0033] Step 1), put water, glycerol, butanediol, and p - hydroxyacetophenone into an emulsifying pan, heat up to 85 - 90 °C, and mix evenly to obtain a premix;

[0034] Step 2), cool the premix to 35 - 40 °C, add hexylene glycol and the composition with anti - wrinkle and firming effects while stirring, stir and dissolve evenly, filter and discharge to obtain the skin care lotion.

[0035] By adopting the above - mentioned technical solution, the quality of the prepared skin care lotion is relatively stable, which can play a very good anti - wrinkle and firming effect, thus achieving the effect of quickly smoothing wrinkles very well.

[0036] To sum up, the present application has the following beneficial effects:

[0037] 1. Due to the special compounding of the extracts of Corydalis bulbocapnoides, Phalaenopsis amabilis var. anubis, and Spirulina platensis in the present application, with the cooperation of various active ingredients, it has a very significant effect of inhibiting elastase, and further better promotes the repair of skin elastin, making the skin quickly recover smooth and elastic, thus achieving the effect of quickly smoothing wrinkles.

[0038] 2. Preferably in the present application, the extracts of Corydalis bulbocapnoides, Papilionanthe anubis, and Spirulina platensis are all water-soluble extracts, making the active ingredients more easily absorbed by the skin, so that the active ingredients can better penetrate deep into the skin, and further enabling the effect of inhibiting elastase activity to be better exerted, achieving the effect of more quickly smoothing wrinkles. Detailed implementation manners

[0039] The present application will be further described in detail below in conjunction with the embodiments.

[0040] Example 1

[0041] A composition with anti-wrinkle and firming effects, comprising the following components:

[0042] Solvent, extract of Corydalis bulbocapnoides, extract of Papilionanthe anubis, extract of Spirulina platensis.

[0043] The solvent is deionized water, sourced from the market.

[0044] The extract of Corydalis bulbocapnoides is purchased from Guangzhou Derui Biotechnology Co., Ltd., a water-soluble extract.

[0045] The extract of Papilionanthe anubis is purchased from Guangzhou Derui Biotechnology Co., Ltd., a water-soluble extract.

[0046] The extract of Spirulina platensis is purchased from Guangzhou Derui Biotechnology Co., Ltd., a water-soluble extract.

[0047] The preparation method of the composition with anti-wrinkle and firming effects is as follows:

[0048] Put 98.499 kg of deionized water, 0.5 kg of extract of Corydalis bulbocapnoides, 0.001 kg of extract of Papilionanthe anubis, and 1 kg of extract of Spirulina platensis into a stirring kettle, with a rotation speed of 100 r / min, stir for 20 min, and mix evenly to obtain the composition with anti-wrinkle and firming effects.

[0049] Example 2

[0050] A composition with anti-wrinkle and firming effects, comprising the following components:

[0051] Solvent, extract of Corydalis bulbocapnoides, extract of Papilionanthe anubis, extract of Spirulina platensis.

[0052] The solvent is deionized water, sourced from the market.

[0053] The extract of Corydalis bulbocapnoides is purchased from Guangzhou Derui Biotechnology Co., Ltd., a water-soluble extract.

[0054] The Anubis extract of Phalaenopsis was purchased from Guangzhou Derui Biotechnology Co., Ltd., and it is a water-soluble extract.

[0055] The extract of Spirulina platensis Geitler was purchased from Guangzhou Derui Biotechnology Co., Ltd., and it is a water-soluble extract.

[0056] The preparation method of the composition with anti-wrinkle and firming effects is as follows:

[0057] Put 97.748 kg of deionized water, 0.75 kg of the extract of Corydalis bulbocapnoides, 0.002 kg of the Anubis extract of Phalaenopsis, and 1.5 kg of the extract of Spirulina platensis Geitler into a stirring kettle, with a rotation speed of 100 r / min, stir for 20 min, and mix evenly to obtain the composition with anti-wrinkle and firming effects.

[0058] Example 3

[0059] A composition with anti-wrinkle and firming effects includes the following components:

[0060] Solvent, the extract of Corydalis bulbocapnoides, the Anubis extract of Phalaenopsis, the extract of Spirulina platensis Geitler.

[0061] The solvent is deionized water, which is commercially available.

[0062] The extract of Corydalis bulbocapnoides was purchased from Guangzhou Derui Biotechnology Co., Ltd., and it is a water-soluble extract.

[0063] The Anubis extract of Phalaenopsis was purchased from Guangzhou Derui Biotechnology Co., Ltd., and it is a water-soluble extract.

[0064] The extract of Spirulina platensis Geitler was purchased from Guangzhou Derui Biotechnology Co., Ltd., and it is a water-soluble extract.

[0065] The preparation method of the composition with anti-wrinkle and firming effects is as follows:

[0066] Put 96.997 kg of deionized water, 1 kg of the extract of Corydalis bulbocapnoides, 0.003 kg of the Anubis extract of Phalaenopsis, and 2 kg of the extract of Spirulina platensis Geitler into a stirring kettle, with a rotation speed of 100 r / min, stir for 20 min, and mix evenly to obtain the composition with anti-wrinkle and firming effects.

[0067] Comparative Example 1

[0068] A composition with anti-wrinkle and firming effects, compared with Example 2, the difference is only that:

[0069] The extract of Centella asiatica is used to replace the extract of Corydalis bulbocapnoides in equal amount.

[0070] The extract of Centella asiatica was purchased from Xi'an Pincheng Biotechnology Co., Ltd., and it is a water-soluble extract.

[0071] Comparative Example 2

[0072] A composition with anti-wrinkle and firming effects, compared with Example 2, the only difference is:

[0073] Replace Phalaenopsis Anubis extract with an equal amount of rosehip extract.

[0074] Rosehip extract was purchased from Lanzhou Waterless Biotechnology Co., Ltd., a water-soluble extract.

[0075] Comparative Example 3

[0076] A composition with anti-wrinkle and firming effects, compared with Example 2, the only difference is:

[0077] The ginseng extract was used to replace the Spirulina extract in equal amounts.

[0078] Ginseng extract was purchased from Shaanxi Bolin Biotechnology Co., Ltd., a water-soluble extract.

[0079] Comparative Example 4

[0080] A composition with anti-wrinkle and firming effects, compared with Example 2, the only difference is:

[0081] An equal amount of Centella asiatica extract was used to replace the medicinal Corydalis strobilus extract.

[0082] Replace Phalaenopsis Anubis extract with an equal amount of rosehip extract.

[0083] The ginseng extract was used to replace the Spirulina extract in equal amounts.

[0084] Centella asiatica extract was purchased from Xi'an Pincheng Biotechnology Co., Ltd., a water-soluble extract.

[0085] Rosehip extract was purchased from Lanzhou Waterless Biotechnology Co., Ltd., a water-soluble extract.

[0086] Ginseng extract was purchased from Shaanxi Bolin Biotechnology Co., Ltd., a water-soluble extract.

[0087] Application Example 1

[0088] A skin care water, comprising the following components:

[0089] Water, glycerin, butylene glycol, hexylene glycol, p-hydroxyacetophenone, a composition with anti-wrinkle and firming effects.

[0090] Water is deionized water, which is commercially available.

[0091] Glycerine is purchased in Malay.

[0092] Butanediol was purchased from LOCAL.

[0093] 2-Hexanediol was purchased from Symrise.

[0094] p-Hydroxyacetophenone was purchased from Symrise.

[0095] The composition with anti-wrinkle and firming effects is the composition with anti-wrinkle and firming effects in Example 1.

[0096] The preparation method of the skin care lotion comprises the following steps:

[0097] Step 1), put 92.3 kg of water, 2 kg of glycerol, 4 kg of butanediol, and 0.4 kg of p-hydroxyacetophenone into an emulsifying pan, heat up to 85 °C, homogenize at 2500 r / min for 3 min, stir at 100 r / min for 15 min, and mix evenly to obtain a premix.

[0098] Step 2), cool the premix to 35 °C, stir at a speed of 60 r / min, add 0.4 kg of 2-hexanediol and 0.9 kg of the composition with anti-wrinkle and firming effects while stirring, stir at a speed of 60 r / min for 15 min, dissolve evenly, and filter through a filter cloth to obtain the skin care lotion.

[0099] Application Example 2

[0100] A skin care lotion, comprising the following components:

[0101] Water, glycerol, butanediol, 2-hexanediol, p-hydroxyacetophenone, and a composition with anti-wrinkle and firming effects.

[0102] The water is deionized water and is sourced from the market.

[0103] Glycerol was purchased from Mallinckrodt.

[0104] Butanediol was purchased from LOCAL.

[0105] 2-Hexanediol was purchased from Symrise.

[0106] p-Hydroxyacetophenone was purchased from Symrise.

[0107] The composition with anti-wrinkle and firming effects is the composition with anti-wrinkle and firming effects in Example 1.

[0108] The preparation method of the skin care lotion comprises the following steps:

[0109] Step 1), put 90 kg of water, 3 kg of glycerol, 5 kg of butanediol, and 0.5 kg of p-hydroxyacetophenone into an emulsifying pan, heat up to 88 °C, homogenize at 2500 r / min for 3 min, stir at 100 r / min for 15 min, and mix evenly to obtain a premix.

[0110] Step 2), cool the premix to 38°C, rotate at 60 r / min, add 0.5 kg hexanediol and 1 kg of a composition with anti-wrinkle and firming effects while stirring, rotate at 60 r / min, stir for 15 minutes, dissolve evenly, filter the material through a filter cloth, and obtain a skin care lotion.

[0111] Application Example 3

[0112] A skin care water, comprising the following components:

[0113] Water, glycerin, butylene glycol, hexylene glycol, p-hydroxyacetophenone, a composition with anti-wrinkle and firming effects.

[0114] Water is deionized water, which is commercially available.

[0115] Glycerine is purchased in Malay.

[0116] Butanediol was purchased from LOCAL.

[0117] Hexylene glycol was purchased from Symrise.

[0118] Para-hydroxyacetophenone was purchased from Symrise.

[0119] The composition with anti-wrinkle and firming effects is the composition with anti-wrinkle and firming effects of Example 1.

[0120] The preparation method of skin care water comprises the following steps:

[0121] Step 1), 87.7 kg water, 4 kg glycerol, 6 kg butylene glycol, and 0.6 kg p-hydroxyacetophenone are put into an emulsifying pot, heated to 90°C, 2500 r / min, homogenized for 3 min, 100 r / min, stirred for 15 min, and mixed evenly to obtain a premix.

[0122] Step 2), cool the premix to 40°C, rotate at 60 r / min, add 0.6 kg hexanediol and 1.1 kg of a composition with anti-wrinkle and firming effects while stirring, rotate at 60 r / min, stir for 15 minutes, dissolve evenly, filter the material through a filter cloth, and obtain a skin care lotion.

[0123] Experiment 1

[0124] The elastase activity inhibition rate of the test samples prepared from the compositions with anti-wrinkle and firming effects of the embodiments and comparative examples was detected.

[0125] Test method:

[0126] 1. React the test sample with elastase.

[0127] 2. Test the absorbance at 495 nm.

[0128] 3. Calculate the elastase activity inhibition rate.

[0129] Sample to be tested:

[0130] Take 1 g of the composition with anti-wrinkle and firming effects and 99 g of deionized water, mix evenly to obtain the sample to be tested.

[0131] The blank sample uses deionized water.

[0132] The positive control sample uses a 20 μg / mL baicalein solution.

[0133] Elastase activity inhibition rate calculation formula:

[0134] Elastase activity inhibition rate (%) = [1 – (A2 / A1)] × 100%;

[0135] In the formula: A1—the average absorbance of the blank test;

[0136] A2—the average absorbance of the solution with the sample dilution added.

[0137] The specific experimental data of Experiment 1 are shown in Table 1.

[0138] Table 1

[0139]

[0140] According to the data comparison of each example and comparative example in Table 1, the elastase activity inhibition rate (%) of the samples to be tested in each example is significantly higher than that of each comparative example. Although the elastase activity inhibition rate (%) of the samples to be tested in each comparative example is higher than that of the positive control, that is, each comparative example also has a certain effect of inhibiting elastase activity, but compared with each example, the effect of inhibiting elastase activity in each comparative example is relatively general. It can be seen that through the special compounding of the extract of Corydalis bulbocapnoides, the extract of Papilionanthe anubis, and the extract of Spirulina platensis in each example, the effect of inhibiting elastase activity can be significantly improved, thereby better promoting the repair of elastin in the skin, making the skin easier to quickly restore smoothness and achieving the effect of quickly smoothing wrinkles.

[0141] This specific embodiment is only an interpretation of the present application and does not limit the present application. Those skilled in the art can make modifications without creative contributions to this embodiment according to needs after reading this specification, but as long as it is within the scope of the claims of the present application, it is protected by the patent law.

Claims

1. A composition with anti-wrinkle and firming effects, characterized in that: The composition includes the following components in parts by weight: Solvent 96.997-98.499 parts; 0.5-1 part of medicinal Corydalis strobilus extract; Phalaenopsis Anubis extract 0.001-0.003 parts; 1-2 parts of Bonate Spirulina extract; The solvent is water; The medicinal Corydalis strobilus extract, Phalaenopsis Anubis extract and Spirulina Bonat extract are all water-soluble extracts.

2. A method for preparing the composition with anti-wrinkle and firming effects according to claim 1, characterized in that: The solvent, the medicinal Corydalis strobilus extract, the Phalaenopsis Anubis extract and the Spirulina Bonat extract are uniformly mixed to obtain a composition with anti-wrinkle and firming effects.

3. An application of the composition with anti-wrinkle and firming effects according to claim 1, characterized in that: The composition with anti-wrinkle and firming effects is added into skin care products to prepare skin care products with anti-wrinkle and firming effects.

4. The use of a composition with anti-wrinkle and firming effects according to claim 3, characterized in that: The skin care product is skin care water.

5. The use of a composition with anti-wrinkle and firming effects according to claim 4, characterized in that: The skin care water comprises the following components in parts by weight: Water 87.7-92.3 parts; 2-4 parts of glycerin; 4-6 parts of butanediol; Hexanediol 0.4-0.6 part; 0.4-0.6 parts of p-hydroxyacetophenone; 0.9-1.1 parts of the composition with anti-wrinkle and firming effects.

6. The use of a composition with anti-wrinkle and firming effects according to claim 5, characterized in that: The preparation method of the skin care water comprises the following steps: Step 1), put water, glycerin, butylene glycol and p-hydroxyacetophenone into an emulsifying pot, heat to 85-90°C, and mix well to obtain a premix; Step 2), cool the premix to 35-40°C, add hexylene glycol and the composition with anti-wrinkle and firming effects while stirring, stir to dissolve evenly, filter the material to obtain skin care water.

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