Crystallization equipment convenient to clean

By designing a crystallization device including an evaporative crystallization device and a cleaning device, the problems of reduced heat transfer efficiency and structural stability caused by the accumulation of crystallization in the inner wall of the crystallizer are solved, and efficient cleaning of crystallization in the inner wall of the crystallizer is achieved, and equipment performance and product quality are improved.

CN119971543AInactive Publication Date: 2025-05-13HUIZHOU HONGHE RENEWABLE RESOURCES CO LTD
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Patent Information

Application Number
CN202411981962.X
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-12-31
Publication Date
2025-05-13
Estimated Expiration
Not applicable · inactive patent

AI Technical Summary

Technical Problem

The accumulation of crystallization on the inner wall of the crystallizer will reduce heat transfer efficiency and structural stability, affect equipment performance and product quality, and need to be cleaned in time.

Method used

A crystallization device including a base, an evaporative crystallization device, a cleaning device and a waste gas recovery device are designed. The cleaning device consists of a connecting rod, a reciprocating screw, an arc-shaped scraper and a roller. The first stirring rod is driven by a motor to rotate, driving the connecting rod, a reciprocating screw and an arc-shaped scraper to realize crystal cleaning of the inner wall of the isolation barrel.

Benefits of technology

It realizes efficient cleaning of crystallization of the inner wall of the crystallizer, improves the heat transfer efficiency and structural stability of the equipment, thereby extending the service life of the equipment and improving product quality.

✦ Generated by Eureka AI based on patent content.

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Abstract

The invention relates to the technical field of chemical engineering, and provides crystallization equipment convenient to clean, which comprises a base, an evaporative crystallization device, a cleaning device, a waste gas recovery device and a controller. The evaporative crystallization device is arranged above the base, is connected with the base and is used for crystallizing the solution. The cleaning device is arranged in the evaporative crystallization device and used for cleaning the interior of the evaporative crystallization device. The waste gas recovery device is arranged on the side of the evaporative crystallization device, is arranged above the base and is used for recycling waste gas in the evaporative crystallization device. The controller is arranged above the base, is fixedly connected with the base and is used for controlling the evaporative crystallization device and the waste gas recovery device.
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Description

Technical Field

[0001] The invention relates to the technical field of chemical industry, in particular to a crystallization device which is easy to clean. Background Art

[0002] Crystallization equipment, as one of the core equipment in the field of chemical engineering and materials science, has a long history of background technology and is constantly innovating. It is based on the principle that solutes in a solution can spontaneously form crystals under specific conditions. Through a series of precisely designed processes and devices, the material transformation process from liquid to solid is realized. This technology is not only widely used in the purification and preparation of chemical products, such as drug crystallization in the pharmaceutical industry, sugar and salt crystallization in the food industry, but also plays an important role in water treatment and heavy metal recovery in the field of environmental protection. The research and development and improvement of crystallization equipment are always accompanied by in-depth research on solution thermodynamics, kinetics and crystal growth mechanism. From the early simple cooling crystallization tank to the modern continuous crystallizer, vacuum crystallizer, and intelligent crystallization system combining efficient heat exchange technology and advanced automatic control system, each technological innovation has greatly improved the crystallization efficiency, reduced energy consumption, and improved the purity and quality of the product. In particular, in recent years, with the introduction of computer simulation technology and artificial intelligence algorithms, the design and optimization of the crystallization process have become more accurate and efficient, enabling crystallization equipment to better adapt to different material properties and production needs. In addition, the enhancement of environmental awareness has also promoted the development of crystallization equipment in a greener and more sustainable direction. For example, by optimizing the crystallization process, reducing the emission of wastewater and waste gas, and developing crystallization technology that can recycle by-products, not only the negative impact on the environment is reduced, but also the efficiency of resource utilization is improved.

[0003] During the crystallization process of the crystallizer, a layer of crystals will gradually appear on its inner wall. The accumulation of these crystals will not only reduce the heat transfer efficiency of the crystallizer, but may also cause physical damage to its structure, thus affecting the overall performance of the crystallizer and the quality of the crystallized product. Therefore, it is necessary to clean and maintain it in time. Summary of the invention

[0004] The invention aims to solve the technical problem of how to clean the crystals on the inner wall of the crystallizer, and proposes a crystallization device that is easy to clean. The technical solution of the invention is as follows: A crystallization device that is easy to clean includes: a base, an evaporation crystallization device, a cleaning device, a waste gas recovery device, and a controller. The evaporation crystallization device is arranged above the base, connected to the base, and used to crystallize the solution. The cleaning device is arranged inside the evaporation crystallization device, and is used to clean the inside of the evaporation crystallization device. The waste gas recovery device is arranged on the side of the evaporation crystallization device, arranged above the base, and is used to recycle the waste gas in the evaporation crystallization device. The controller is arranged above the base, fixedly connected to the base, and electrically connected to the evaporation crystallization device.

[0005] Furthermore, the evaporation crystallization device includes: a reactor, an isolation cylinder, a heat pipe, a hot water tank, a circulating water pump, a feed pipe, and a discharge pipe. The axis of the reactor is vertically arranged, arranged above the base, and fixedly connected to the base. The axis of the isolation cylinder coincides with the axis of the reactor, is arranged inside the reactor, and is fixedly connected to the reactor, dividing the reactor into two spaces. The heat pipe is spirally arranged between the reactor and the isolation cylinder, and both ends of the heat pipe pass through the reactor, and the heat pipe is fixedly connected to the reactor. The hot water tank is arranged above the base and on the side of the reactor. The hot water tank is fixedly connected to the base and communicated with the water outlet of the heat pipe. A heating wire is arranged in the hot water tank, and the heating wire is electrically connected to the controller. A water injection valve is arranged on the top of the hot water tank. The circulating water pump is arranged between the hot water tank and the reactor, and is fixedly connected to the base. The water outlet of the circulating water pump is connected to the water inlet of the heat pipe, and the water inlet is connected to the hot water tank. The feed pipe passes through the upper part of the reactor, and the feed pipe is connected to the inside of the reactor. The discharge pipe passes through the bottom of the reactor and the lower part of the isolation cylinder, and is communicated with the interior of the isolation cylinder. An electric control valve is arranged in the discharge pipe, and the electric control valve is electrically connected to the controller.

[0006] When the circulating water pump is working, the circulating water pump inputs the hot water in the hot water tank into the heat conduction pipe. The hot water passes through the heat conduction pipe and enters the hot water tank, thus completing the circulation. The hot water in the heat conduction pipe heats the solution in the reactor, and the solution evaporates and crystallizes.

[0007] Furthermore, the evaporation crystallization device comprises: a sealing cover which is sleeved on the upper part of the feed pipe and is threadedly connected to the feed pipe.

[0008] The sealing cover is used to ensure the sealing inside the reactor and prevent the gas from leaking out during the evaporation process and polluting the air.

[0009] Furthermore, the evaporation crystallization device includes: a bracket, a motor, a first stirring rod, and a plurality of second stirring rods. The bracket is arranged above the reactor and is fixedly connected to the reactor. The axis of the motor shaft coincides with the axis of the reactor, the motor shaft passes through the upper part of the reactor, the motor is fixedly connected to the bracket, the motor shaft is rotationally connected to the reactor, and its rotation axis coincides with its own axis, and the motor is electrically connected to the controller. The axis of the first stirring rod coincides with the axis of the motor shaft, is arranged inside the isolation tube, is arranged below the motor shaft, the upper end of the stirring rod is fixedly connected to the motor shaft, and the lower end is rotationally connected to the bottom of the reactor, and its rotation axis coincides with its own axis. A plurality of second stirring rods are perpendicular to the first stirring rod, are arranged inside the isolation tube, and one end of the plurality of second stirring rods is fixedly connected to the first stirring rod.

[0010] When the motor is working, the motor rotates to drive the first stirring rod and the first bevel gear to rotate, the first stirring rod rotates to drive the second stirring rod to rotate, and the second stirring rod rotates to stir the solution, thereby increasing the crystallization effect of the solution.

[0011] Furthermore, the cleaning device includes: two connecting rods, a reciprocating screw rod, an arc scraper, and two rollers. The two connecting rods are perpendicular to the first stirring rod, and the two connecting rods are respectively arranged above and below the plurality of second stirring rods, and are arranged on the side of the first stirring rod, and one end of the two connecting rods is fixedly connected to the first stirring rod. The reciprocating screw rod is parallel to the first stirring rod, and is arranged on the side of the two connecting rods away from the first stirring rod, and is arranged on the side of the plurality of second stirring rods away from the first stirring rod. The two ends of the reciprocating screw rod are respectively rotatably connected to one end of the two connecting rods away from the first stirring rod, and the rotation axis thereof coincides with its own axis. The arc scraper is arranged on the side of the reciprocating screw rod close to the isolation cylinder, and the arc scraper is fixedly connected to the slider on the reciprocating screw rod. The curvature of the arc scraper is the same as the curvature of the isolation cylinder, and the arc scraper is in close contact with the inner surface of the isolation cylinder. The two rollers are symmetrically arranged up and down, respectively sleeved on the upper end and the lower end of the reciprocating screw rod, respectively arranged above and below the two connecting rods, and the two rollers are fixedly connected to the reciprocating screw rod and contact the inner surface of the isolation cylinder.

[0012] When the first stirring rod rotates, the first stirring rod drives the connecting rod to rotate, and the connecting rod drives the reciprocating screw to rotate around the axis of the first stirring rod. The rotation of the reciprocating screw drives the arc scraper and the roller to rotate around the axis of the first stirring rod. The arc scraper scrapes off the crystals on the inner wall of the isolation cylinder, thereby cleaning the isolation cylinder.

[0013] Furthermore, the roller is made of glass fiber reinforced plastic.

[0014] Glass fiber reinforced plastic can remain stable within a certain high temperature range and has excellent heat resistance. At the same time, glass fiber reinforced plastic has a large friction coefficient, which prevents the roller from slipping when rotating around its own axis. At the same time, it also has excellent toughness and corrosion resistance, preventing it from being corroded in the solution for a long time.

[0015] Furthermore, the waste gas recovery device includes: a collecting box, a cooling box, a rotating rod, a first bevel gear, a second bevel gear, a plurality of fan blades, a connecting pipe, a connecting cylinder, and a refrigerator. The collecting box is arranged on the side of the reactor and above the base. The collecting box is fixedly connected to the reactor, and a water outlet valve is arranged at the bottom of the collecting box. The cooling box is cylindrical, and the axis of the cooling box is arranged horizontally. The cooling box is arranged above the collecting box, above the reactor, and on the side of the motor. The cooling box is fixedly connected to the reactor. The axis of the rotating rod coincides with the axis of the cooling box, passes through the side of the cooling box close to the motor, and the rotating rod is rotatably connected to the side of the cooling box close to the motor, and its rotation axis coincides with its own axis. The first bevel gear is sleeved on the motor shaft and arranged above the reactor. The first bevel gear is fixedly connected to the motor shaft. The second bevel gear is sleeved on the rotating rod and arranged on the side of the first bevel gear. The second bevel gear is fixedly connected to the rotating rod and meshes with the first bevel gear. A plurality of fan blades are sleeved on a rotating rod and arranged in a cooling cylinder, and the plurality of fan blades are fixedly connected to the rotating rod. A connecting pipe runs through the lower part of the cooling box and the upper part of the reactor, and is arranged on the side of the plurality of fan blades close to the motor. The upper end of the connecting pipe is connected to the cooling box, and the lower end is connected to the reactor. The axis of the connecting cylinder is arranged vertically, and the connecting cylinder runs through the lower part of the cooling box and the upper part of the collecting box, and is arranged on the side of the plurality of fan blades away from the connecting pipe. The upper part of the connecting cylinder is connected to the cooling box, and the lower part is connected to the collecting box. The cooling end of the refrigerator is arranged inside the cooling box, and is arranged directly above the connecting cylinder. The heat dissipation end of the refrigerator is outside the reactor, and the refrigerator is electrically connected to the controller.

[0016] When the motor rotates, the motor drives the first bevel gear to rotate, the first bevel gear drives the second bevel gear to rotate, the second bevel gear drives the rotating rod to rotate, the rotating rod drives the fan blades to rotate, the fan blades drive the scraper to rotate, and when the fan blades rotate, the gas in the reactor is sucked into the cooling box for cooling and liquefaction, and the liquefied liquid will fall into the collection box for collection.

[0017] When the refrigerator is working, it cools the gas in the cooling box to liquefy it. The liquefied liquid enters the collection box through the connecting tube, which is convenient for the staff to recycle it. Other gases will be discharged to the outside through the filter cotton to prevent air pollution.

[0018] Furthermore, the waste gas recovery device includes: filter cotton and a vent. The filter cotton is arranged in the cooling box, arranged on the side of the refrigerator away from the plurality of fan blades, and the filter cotton is fixedly connected to the cooling box. The vent is arranged on the side of the cooling box close to the filter cotton, and the vent is connected to the inside of the cooling box.

[0019] Furthermore, the filter cotton is made of glass fiber.

[0020] Glass fiber is resistant to high temperature and corrosion, and can maintain stable filtering performance in high temperature and harsh environments.

[0021] It has high filtration efficiency and dust holding capacity.

[0022] Furthermore, a heat insulating pad is provided between the collecting box and the reaction kettle.

[0023] The heat insulation pad between the collection box and the reactor prevents the heat from the reactor from affecting the liquid in the collection box, causing the liquid in the collection box to crystallize, making it more difficult for the staff to recover it.

[0024] Beneficial effects of the present invention: 1. The first stirring rod is driven to rotate by the motor, and the first stirring rod drives the connecting rod, the reciprocating screw rod and the arc scraper to rotate around the axis of the first stirring rod, thereby realizing the cleaning of the crystals around the isolation cylinder.

[0025] 2. The reciprocating screw drives the roller to rotate around the axis of the first rotating rod. The roller rotates around its own axis with the cooperation of the isolation tube. The roller drives the reciprocating screw to rotate around its own axis. The rotation of the reciprocating screw drives the arc scraper to move up and down, thereby increasing the cleaning area.

[0026] 3. The motor drives the first bevel gear, the second bevel gear and the rotating rod to rotate. The rotation of the rotating rod drives the fan blades to rotate. The fan blades suck the gas in the reactor into the cooling box, thereby cooling and recovering the exhaust gas. BRIEF DESCRIPTION OF THE DRAWINGS

[0027] The present invention will be further described in detail below in conjunction with the accompanying drawings and specific embodiments.

[0028] Figure 1 It is a front cross-sectional view of the present invention.

[0029] Explanation of the reference numerals: 1. base; 201. reactor; 202. isolation cylinder; 203. heat pipe; 204. hot water tank; 205. circulating water pump; 206. feed pipe; 2061. sealing cover; 207. discharge pipe; 301. bracket; 302. motor; 303. first stirring rod; 304. second stirring rod; 401. connecting rod; 402. reciprocating screw; 403. arc scraper; 404. roller; 501. collecting box; 502. cooling box; 503. rotating rod; 504. first bevel gear; 505. second bevel gear; 506. fan blade; 507. connecting pipe; 508. connecting cylinder; 509. refrigerator; 601. filter cotton; 602. vent. DETAILED DESCRIPTION

[0030] The following will be combined with the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without making creative work are within the scope of protection of the present invention.

[0031] See also Figure 1 The present invention provides a crystallization device that is easy to clean, including: a base 1, an evaporation crystallization device, a cleaning device, a waste gas recovery device, and a controller. The evaporation crystallization device is arranged above the base 1, connected to the base 1, and is used for crystallizing the solution. The cleaning device is arranged inside the evaporation crystallization device, and is used to clean the inside of the evaporation crystallization device. The waste gas recovery device is arranged on the side of the evaporation crystallization device, and is arranged above the base 1, and is used to recycle the waste gas in the evaporation crystallization device. The controller is arranged above the base 1, fixedly connected to the base 1, and electrically connected to the evaporation crystallization device.

[0032] The evaporation crystallization device includes: a reactor 201, an isolation cylinder 202, a heat pipe 203, a hot water tank 204, a circulating water pump 205, a feed pipe 206, and a discharge pipe 207. The axis of the reactor 201 is vertically arranged, arranged above the base 1, and fixedly connected to the base 1. The axis of the isolation cylinder 202 coincides with the axis of the reactor 201, is arranged inside the reactor 201, and is fixedly connected to the reactor 201, dividing the reactor 201 into two spaces. The heat pipe 203 is spirally arranged between the reactor 201 and the isolation cylinder 202, and both ends of the heat pipe 203 pass through the reactor 201, and the heat pipe 203 is fixedly connected to the reactor 201. The hot water tank 204 is arranged above the base 1 and on the side of the reactor 201. The hot water tank 204 is fixedly connected to the base 1 and communicated with the water outlet end of the heat conducting tube 203. A heating wire is arranged in the hot water tank 204, and the heating wire is electrically connected to the controller. A water injection valve is arranged on the top of the hot water tank 204. The circulating water pump 205 is arranged between the hot water tank 204 and the reactor 201 and is fixedly connected to the base 1. The water outlet end of the circulating water pump 205 is communicated with the water inlet end of the heat conducting tube 203, and the water inlet end is communicated with the hot water tank 204. The feed pipe 206 runs through the upper part of the reactor 201, and the feed pipe 206 is communicated with the inside of the reactor 201. The discharge pipe 207 runs through the bottom of the reactor 201 and the lower part of the isolation cylinder 202, and communicates with the inside of the isolation cylinder 202. An electric control valve is arranged in the discharge pipe 207, and the electric control valve is electrically connected to the controller.

[0033] When the circulating water pump 205 is working, the circulating water pump 205 inputs the hot water in the hot water tank 204 into the heat pipe 203. The hot water passes through the heat pipe 203 and enters the hot water tank 204, thereby completing the circulation. The hot water in the heat pipe 203 heats the solution in the reactor 201, and the solution evaporates and crystallizes.

[0034] The evaporation crystallization device includes a sealing cover 2061. The sealing cover 2061 is sleeved on the upper part of the feed pipe 206 and is threadedly connected to the feed pipe 206.

[0035] The sealing cover 2061 is used to ensure the sealing inside the reactor 201 to prevent the gas in the evaporation process from leaking out and polluting the air.

[0036] The evaporation crystallization device includes: a bracket 301, a motor 302, a first stirring rod 303, and a plurality of second stirring rods 304. The bracket 301 is arranged above the reactor 201 and is fixedly connected to the reactor 201. The axis of the motor 302 shaft coincides with the axis of the reactor 201, the motor 302 shaft passes through the upper part of the reactor 201, the motor 302 is fixedly connected to the bracket 301, the motor 302 shaft is rotatably connected to the reactor 201, and its rotation axis coincides with its own axis, and the motor 302 is electrically connected to the controller. The axis of the first stirring rod 303 coincides with the axis of the motor 302 shaft, is arranged inside the isolation cylinder 202, and is arranged below the motor 302 shaft, the upper end of the stirring rod is fixedly connected to the motor 302 shaft, and the lower end is rotatably connected to the bottom of the reactor 201, and its rotation axis coincides with its own axis. The plurality of second stirring rods 304 are perpendicular to the first stirring rods 303 and are disposed inside the isolation cylinder 202 . One end of the plurality of second stirring rods 304 is fixedly connected to the first stirring rod 303 .

[0037] When the motor 302 is working, the motor 302 rotates to drive the first stirring rod 303 and the first bevel gear 504 to rotate, the first stirring rod 303 rotates to drive the second stirring rod 304 to rotate, and the second stirring rod 304 rotates to stir the solution, thereby increasing the crystallization effect of the solution.

[0038] The cleaning device includes: two connecting rods 401, a reciprocating screw rod 402, an arc scraper 403, and two rollers 404. The two connecting rods 401 are perpendicular to the first stirring rod 303, and the two connecting rods 401 are respectively arranged above and below the plurality of second stirring rods 304, and are arranged on the side of the first stirring rod 303, and one end of the two connecting rods 401 is fixedly connected to the first stirring rod 303. The reciprocating screw rod 402 is parallel to the first stirring rod 303, and is arranged on the side of the two connecting rods 401 away from the first stirring rod 303, and is arranged on the side of the plurality of second stirring rods 304 away from the first stirring rod 303, and the two ends of the reciprocating screw rod 402 are respectively rotatably connected to one end of the two connecting rods 401 away from the first stirring rod 303, and its rotation axis coincides with its own axis. The arc scraper 403 is arranged on the side of the reciprocating screw 402 close to the isolating cylinder 202. The arc scraper 403 is fixedly connected to the slider on the reciprocating screw 402. The curvature of the arc scraper 403 is the same as the curvature of the isolating cylinder 202. The arc scraper 403 is in close contact with the inner surface of the isolating cylinder 202. The two rollers 404 are symmetrically arranged up and down, respectively sleeved on the upper and lower ends of the reciprocating screw 402, and respectively arranged above and below the two connecting rods 401. The two rollers 404 are fixedly connected to the reciprocating screw 402 and contact the inner surface of the isolating cylinder 202.

[0039] When the first stirring rod 303 rotates, the first stirring rod 303 drives the connecting rod 401 to rotate, and the connecting rod 401 drives the reciprocating screw rod 402 to rotate around the axis of the first stirring rod 303. The rotation of the reciprocating screw rod 402 drives the arc scraper 403 and the roller 404 to rotate around the axis of the first stirring rod 303. The arc scraper 403 scrapes off the crystals on the inner wall of the isolation cylinder 202, thereby cleaning the isolation cylinder 202.

[0040] The roller 404 is made of glass fiber reinforced plastic.

[0041] Glass fiber reinforced plastic can remain stable within a certain high temperature range and has excellent heat resistance. At the same time, glass fiber reinforced plastic has a large friction coefficient, which prevents the roller 404 from slipping when rotating around its own axis. At the same time, it also has excellent toughness and corrosion resistance, preventing it from being corroded in the solution for a long time.

[0042] The waste gas recovery device includes: a collecting box 501, a cooling box 502, a rotating rod 503, a first bevel gear 504, a second bevel gear 505, a plurality of fan blades 506, a connecting pipe 507, a connecting tube 508, and a refrigerator 509. The collecting box 501 is arranged on the side of the reactor 201 and above the base 1. The collecting box 501 is fixedly connected to the reactor 201, and a water outlet valve is arranged at the bottom of the collecting box 501. The cooling box 502 is cylindrical, and the axis of the cooling box 502 is arranged horizontally. The cooling box 502 is arranged above the collecting box 501, above the reactor 201, and on the side of the motor 302. The cooling box 502 is fixedly connected to the reactor 201. The axis of the rotating rod 503 coincides with the axis of the cooling box 502, and passes through the side of the cooling box 502 close to the motor 302. The rotating rod 503 is rotatably connected to the side of the cooling box 502 close to the motor 302, and its rotation axis coincides with its own axis. The first bevel gear 504 is sleeved on the rotating shaft of the motor 302 and is arranged above the reactor 201. The first bevel gear 504 is fixedly connected to the rotating shaft of the motor 302. The second bevel gear 505 is sleeved on the rotating rod 503 and is arranged on the side of the first bevel gear 504. The second bevel gear 505 is fixedly connected to the rotating rod 503 and meshes with the first bevel gear 504. A plurality of blades 506 are sleeved on the rotating rod 503 and are arranged in the cooling cylinder. The plurality of blades 506 are fixedly connected to the rotating rod 503. The connecting pipe 507 runs through the lower part of the cooling box 502 and the upper part of the reactor 201, and is arranged on the side of the plurality of blades 506 close to the motor 302. The upper end of the connecting pipe 507 is connected to the cooling box 502, and the lower end is connected to the reactor 201. The axis of the connecting tube 508 is vertically arranged, and the connecting tube 508 passes through the lower part of the cooling box 502 and the upper part of the collecting box 501, and is arranged on the side of the plurality of fan blades 506 away from the connecting tube 507. The upper part of the connecting tube 508 is connected to the cooling box, and the lower part is connected to the collecting box 501. The cooling end of the refrigerator 509 is arranged inside the cooling box 502, and is arranged directly above the connecting tube 508. The heat dissipation end of the refrigerator 509 is outside the reactor 201, and the refrigerator 509 is electrically connected to the controller.

[0043] When the motor 302 rotates, the motor 302 drives the first bevel gear 504 to rotate, the first bevel gear 504 drives the second bevel gear 505 to rotate, the second bevel gear 505 drives the rotating rod 503 to rotate, the rotating rod 503 drives the fan blades 506 to rotate, the fan blades 506 drive the scraper 701 to rotate, and when the fan blades 506 rotate, the gas in the reactor 201 is sucked into the cooling box 502 for cooling and liquefaction, and the liquefied liquid will fall into the collecting box 501 for collection.

[0044] When the refrigerator 509 is working, the refrigerator 509 cools the gas in the cooling box 502 to liquefy it. The liquefied liquid enters the collection box 501 through the connecting tube 508, which is convenient for the staff to recycle. Other gases will be discharged to the outside through the filter cotton 601 to prevent air pollution.

[0045] The waste gas recovery device includes: filter cotton 601 and vent 602. The filter cotton 601 is arranged in the cooling box 502, and is arranged on the side of the refrigerator 509 away from the plurality of fan blades 506. The filter cotton 601 is fixedly connected to the cooling box 502. The vent 602 is arranged on the side of the cooling box 502 close to the filter cotton 601, and the vent 602 is connected to the inside of the cooling box 502.

[0046] The filter cotton 601 is made of glass fiber.

[0047] Glass fiber is resistant to high temperature and corrosion, and can maintain stable filtering performance in high temperature and harsh environments.

[0048] It has high filtration efficiency and dust holding capacity.

[0049] A heat insulating pad is provided between the collecting box 501 and the reaction kettle 201 .

[0050] The heat insulating pad between the collection box 501 and the reaction kettle 201 prevents the heat of the reaction kettle 201 from affecting the liquid in the collection box 501, causing the liquid in the collection box 501 to crystallize, making it more difficult for the staff to recover the liquid.

[0051] Working principle: At the beginning of the work, the staff adds the solution into the reactor 201 through the feed pipe 206, and then the staff seals the feed pipe 206 through the sealing cover 2061. After that, the staff turns on the circulating water pump 205, the motor 302 and the refrigerator 509 through the controller.

[0052] When the circulating water pump 205 is working, the circulating water pump 205 inputs the hot water in the hot water tank 204 into the heat pipe 203. The hot water passes through the heat pipe 203 and enters the hot water tank 204, thereby completing the circulation. The hot water in the heat pipe 203 heats the solution in the reactor 201, and the solution evaporates and crystallizes.

[0053] When the motor 302 is working, the motor 302 rotates to drive the first stirring rod 303 and the first bevel gear 504 to rotate, and the first stirring rod 303 rotates to drive the second stirring rod 304 and the connecting rod 401 to rotate, and the second stirring rod 304 rotates to stir the solution, thereby increasing the crystallization effect of the solution.

[0054] When the connecting rod 401 rotates, the connecting rod 401 drives the reciprocating screw rod 402 to rotate around the axis of the first stirring rod 303. The rotation of the reciprocating screw rod 402 drives the arc scraper 403 and the roller 404 to rotate around the axis of the first stirring rod 303. The arc scraper 403 scrapes off the crystals on the inner wall of the isolation cylinder 202, thereby cleaning the isolation cylinder 202.

[0055] When the roller 404 rotates around the axis of the first stirring rod 303, the roller 404 rotates around its own axis with the cooperation of the isolation cylinder 202. When the roller 404 rotates around its own axis, it drives the reciprocating screw rod 402 to rotate around its own axis. The reciprocating screw rod 402 rotates around its own axis and drives the arc scraper 403 to move up and down, thereby increasing the area for cleaning crystals.

[0056] When the first bevel gear 504 rotates, the first bevel gear 504 drives the second bevel gear 505 to rotate, the second bevel gear 505 drives the rotating rod 503 to rotate, the rotating rod 503 drives the fan blade 506 to rotate, the fan blade 506 drives the scraper 701 to rotate, and when the fan blade 506 rotates, the gas in the reactor 201 is sucked into the cooling box 502 for cooling and liquefaction, and the liquefied liquid will fall into the collecting box 501 for collection.

[0057] When the refrigerator 509 is working, the refrigerator 509 cools the gas in the cooling box 502 to liquefy it. The liquefied liquid enters the collection box 501 through the connecting tube 508, which is convenient for the staff to recycle. Other gases will be discharged to the outside through the filter cotton 601 to prevent air pollution.

[0058] The above are only preferred embodiments of the present invention and are not intended to limit the present invention. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the protection scope of the present invention.

Claims

1. A crystallization device that is easy to clean, characterized in that: include: A base (1), an evaporation crystallization device, a cleaning device, a waste gas recovery device, and a controller; the evaporation crystallization device is arranged above the base (1), connected to the base (1), and used for crystallizing a solution; the cleaning device is arranged inside the evaporation crystallization device, and used for cleaning the inside of the evaporation crystallization device; the waste gas recovery device is arranged on the side of the evaporation crystallization device, arranged above the base (1), and used for recycling the waste gas in the evaporation crystallization device; the controller is arranged above the base (1), fixedly connected to the base (1), and electrically connected to the evaporation crystallization device.

2. The crystallization device that is easy to clean according to claim 1, characterized in that: The evaporation and crystallization device comprises: a reaction kettle (201), an isolation cylinder (202), a heat conducting pipe (203), a hot water tank (204), a circulating water pump (205), a feed pipe (206), and a discharge pipe (207); the axis of the reaction kettle (201) is vertically arranged above the base (1) and fixedly connected to the base (1); the axis of the isolation cylinder (202) coincides with the axis of the reaction kettle (201), is arranged inside the reaction kettle (201), and is in contact with the base (1). The reactor (201) is fixedly connected to the reactor (201) to divide the reactor (201) into two spaces; the heat conduction pipe (203) is spirally arranged between the reactor (201) and the isolation cylinder (202), both ends of the heat conduction pipe (203) pass through the reactor (201), and the heat conduction pipe (203) is fixedly connected to the reactor (201); the hot water tank (204) is arranged above the base (1) and on the side of the reactor (201); the hot water tank (204) is arranged above the base (1) and on the side of the reactor (201); The water tank (204) is fixedly connected to the base (1) and communicated with the water outlet of the heat conducting pipe (203). A heating wire is arranged in the hot water tank (204), and the heating wire is electrically connected to the controller. A water injection valve is arranged on the top of the hot water tank (204). The circulating water pump (205) is arranged between the hot water tank (204) and the reactor (201), and is fixedly connected to the base (1). The water outlet of the circulating water pump (205) is connected to the heat conducting pipe (203). 03), and the water inlet end is connected to the hot water tank (204); the feed pipe (206) passes through the upper part of the reactor (201), and the feed pipe (206) is connected to the inside of the reactor (201); the discharge pipe (207) passes through the bottom of the reactor (201) and the lower part of the isolation cylinder (202), and is connected to the inside of the isolation cylinder (202); an electric control valve is arranged in the discharge pipe (207), and the electric control valve is electrically connected to the controller.

3. The crystallization device that is easy to clean according to claim 2, characterized in that: The evaporation crystallization device comprises: a sealing cover (2061); the sealing cover (2061) is sleeved on the upper part of the feed pipe (206) and is threadedly connected to the feed pipe (206).

4. The crystallization device that is easy to clean according to claim 2, characterized in that: The evaporation and crystallization device comprises: a support (301), a motor (302), a first stirring rod (303), and a plurality of second stirring rods (304); the support (301) is arranged above the reaction kettle (201) and is fixedly connected to the reaction kettle (201); the axis of the motor (302) rotation shaft coincides with the axis of the reaction kettle (201), the motor (302) rotation shaft passes through the upper part of the reaction kettle (201), the motor (302) is fixedly connected to the support (301), the motor (302) rotation shaft is rotatably connected to the reaction kettle (201), the rotation axis coincides with its own axis, and the motor ( 302) is electrically connected to the controller; the axis of the first stirring rod (303) coincides with the axis of the motor (302) shaft, and is arranged inside the isolation tube (202) and below the motor (302) shaft. The upper end of the stirring rod is fixedly connected to the motor (302) shaft, and the lower end is rotatably connected to the bottom of the reactor (201), and its rotation axis coincides with its own axis; a plurality of the second stirring rods (304) are perpendicular to the first stirring rod (303), and are arranged inside the isolation tube (202), and one end of a plurality of the second stirring rods (304) is fixedly connected to the first stirring rod (303).

5. The crystallization device that is easy to clean according to claim 4, characterized in that: The cleaning device comprises: two connecting rods (401), a reciprocating screw rod (402), an arc-shaped scraper (403), and two rollers (404); the two connecting rods (401) are perpendicular to the first stirring rod (303), the two connecting rods (401) are respectively arranged above and below a plurality of the second stirring rods (304), and are arranged on the side of the first stirring rod (303), and one end of the two connecting rods (401) is fixedly connected to the first stirring rod (303); the reciprocating screw rod (402) is parallel to the first stirring rod (303), and is arranged on the side of the two connecting rods (401) away from the first stirring rod (303), and is arranged on the side of the plurality of the second stirring rods (304) away from the first stirring rod (303), and the two ends of the reciprocating screw rod (402) are respectively connected to the two connecting rods (401). The connecting rod (401) is rotatably connected to one end away from the first stirring rod (303), and its rotation axis coincides with its own axis; the arc scraper (403) is arranged on the side of the reciprocating screw rod (402) close to the isolation cylinder (202), the arc scraper (403) is fixedly connected to the slider on the reciprocating screw rod (402), the curvature of the arc scraper (403) is the same as the curvature of the isolation cylinder (202), and the arc scraper (403) is in close contact with the inner surface of the isolation cylinder (202); the two rollers (404) are symmetrically arranged up and down, respectively sleeved on the upper and lower ends of the reciprocating screw rod (402), and respectively arranged above and below the two connecting rods (401), and the two rollers (404) are fixedly connected to the reciprocating screw rod (402) and in contact with the inner surface of the isolation cylinder (202).

6. The crystallization device that is easy to clean according to claim 5, characterized in that: The roller (404) is made of glass fiber reinforced plastic.

7. The crystallization device that is easy to clean according to claim 4, characterized in that: The waste gas recovery device comprises: a collecting box (501), a cooling box (502), a rotating rod (503), a first bevel gear (504), a second bevel gear (505), a plurality of fan blades (506), a connecting pipe (507), a connecting cylinder (508), and a refrigerator (509); the collecting box (501) is arranged on the side of the reaction kettle (201) and above the base (1); the collecting box (501) is fixedly connected to the reaction kettle (201); and a water outlet valve is arranged at the bottom of the collecting box (501); the cooling box (502) is cylindrical; the axis of the cooling box (502) is arranged horizontally; and the cooling box (502) is arranged on the collecting box (501). The cooling box (502) is fixedly connected to the cooling box (201); the axis of the rotating rod (503) coincides with the axis of the cooling box (502), and the rotating rod (503) passes through the side of the cooling box (502) close to the motor (302); the rotating rod (503) is rotatably connected to the side of the cooling box (502) close to the motor (302), and the axis of rotation coincides with its own axis; the first bevel gear (504) is sleeved on the rotating shaft of the motor (302), and is arranged above the cooling box (201); the first bevel gear (504) is rotatably connected to the rotating shaft of the motor (302). The second bevel gear (505) is sleeved on the rotating rod (503) and arranged on the side of the first bevel gear (504). The second bevel gear (505) is fixedly connected to the rotating rod (503) and meshes with the first bevel gear (504). A plurality of fan blades (506) are sleeved on the rotating rod (503) and arranged in the cooling cylinder. A plurality of fan blades (506) are fixedly connected to the rotating rod (503). The connecting pipe (507) passes through the lower part of the cooling box (502) and the upper part of the reactor (201). It is arranged on the side of a plurality of fan blades (506) close to the motor (302). The upper end of the connecting pipe (507) The connecting tube (508) is connected to the cooling box (502), and its lower end is connected to the reactor (201); the axis of the connecting tube (508) is vertically arranged, the connecting tube (508) passes through the lower part of the cooling box (502) and the upper part of the collecting box (501), and is arranged on the side of the plurality of fan blades (506) away from the connecting tube (507); the upper part of the connecting tube (508) is connected to the cooling box, and the lower part is connected to the collecting box (501); the cooling end of the refrigerator (509) is arranged inside the cooling box (502), and is arranged directly above the connecting tube (508); the heat dissipation end of the refrigerator (509) is outside the reactor (201), and the refrigerator (509) is electrically connected to the controller.

8. The crystallization device that is easy to clean according to claim 7, characterized in that: The waste gas recovery device comprises: filter cotton (601) and a vent (602); the filter cotton (601) is arranged in the cooling box (502), and is arranged on the side of the refrigerator (509) away from the plurality of fan blades (506), and the filter cotton (601) is fixedly connected to the cooling box (502); the vent (602) is arranged on the side of the cooling box (502) close to the filter cotton (601), and the vent (602) is connected to the inside of the cooling box (502).

9. The crystallization device that is easy to clean according to claim 8, characterized in that: The filter cotton (601) is made of glass fiber.

10. The crystallization device that is easy to clean according to claim 7, characterized in that: A heat insulating pad is provided between the collecting box (501) and the reaction kettle (201).