Treatment equipment and method for high-purity silicon carbide synthetic powder

Abstract

The invention discloses treatment equipment and method for high-purity silicon carbide synthetic powder, and relates to the technical field of silicon carbide production.The treatment equipment comprises an acid pickling tank, a liquid discharging pipe is connected to the lower portion of one side of the acid pickling tank in a penetrating mode, a control valve is arranged in the liquid discharging pipe, a water permeable frame is arranged in the acid pickling tank, and meanwhile a discharging pipe is connected to the bottom of the water permeable frame in a penetrating mode; the stand columns are symmetrically installed at the top of the permeable frame, a fixing rod is fixedly installed between every two stand columns in each set, hanging rings are fixedly installed at the tops of the two sets of stand columns, and a fixing frame is fixedly installed between the two fixing rods; the acid liquor can be added more uniformly, too high local concentration caused by non-uniform addition of the acid liquor is avoided, violent reaction is avoided, operation of a user is facilitated, the adding efficiency of the acid liquor is improved, the influence on the pickling quality is avoided, and the practicability is improved.

Description

Technical Field

[0001] The invention relates to the technical field of silicon carbide production, and in particular to a processing device and method for high-purity silicon carbide synthetic powder. Background Art

[0002] Silicon carbide powder refers to micron-sized silicon carbide powder that is ultra-finely crushed and graded by equipment. Due to the incomplete reaction of raw materials in the production process of silicon carbide, as well as the influence of processing equipment and the external environment, impurities such as free carbon will be generated. When a tube furnace is used to remove carbon from silicon carbide powder, air is introduced, so a small amount of silicon dioxide will be generated during the decarbonization. This is because during the synthesis, excess silicon will combine with oxygen in the air to form silicon dioxide. The presence of silicon dioxide is not conducive to the growth of silicon carbide crystals, so people use acid washing to dissolve the silicon dioxide impurities in silicon carbide powder.

[0003] For example, a pickling device for silicon carbide powder production with announcement number CN212669221U, the coordinated use of an overdilution box, an acid-resistant pump, an acid inlet pipe, a water suction pump, a liquid outlet pipe, a water tank, a submersible pump, a water outlet pipe, a first water supply pipe and a second water supply pipe can effectively collect and treat the solution after pickling, effectively avoid the pollution caused by the direct discharge of the acidic solution into the environment, and greatly improve the cleanliness of the device. However, in actual use, as the pickling of silicon carbide powder proceeds, the acid solution reacts continuously with impurities, and the concentration of the acid solution decreases, and it is necessary to add acid solution. If the acid solution is added directly during the process of adding the acid solution, the addition is not uniform, and violent reactions are likely to occur locally, and it is easy to cause acid splashing. The operation has certain risks. If the acid solution cannot be added evenly, the local concentration of the pickling solution is too high, resulting in poor cleaning effect, and over-pickling is prone to occur, affecting the quality of pickling, and there are certain usage defects.

[0004] Therefore, we propose a processing device and method for high-purity silicon carbide synthetic powder in order to solve the above-mentioned problems. Summary of the invention

[0005] The object of the present invention is to provide a processing device and method for high-purity silicon carbide synthetic powder, so as to solve the problem proposed in the above-mentioned background technology that if the acid solution is added directly during the process of adding the acid solution, the addition is not uniform, violent reactions are likely to occur locally, and acid splashes are likely to occur, the operation has certain risks, and if the acid solution cannot be added uniformly, the local concentration of the pickling solution is too high, resulting in poor cleaning effect, and over-pickling is likely to occur, affecting the quality of the pickling.

[0006] To achieve the above object, the present invention provides the following technical solution: a high-purity silicon carbide synthetic powder processing equipment, comprising a pickling tank, a drainage pipe is connected through one side of the pickling tank, and a control valve is arranged inside the drainage pipe, and a water permeable frame is arranged inside the pickling tank, and a discharge pipe is connected through the bottom of the water permeable frame, and a discharge valve is arranged inside the discharge pipe;

[0007] Also includes:

[0008] The columns are symmetrically installed on the top of the water-permeable frame, a fixing rod is fixedly installed between each group of two columns, and a lifting ring is fixedly installed on the top of the two groups of columns, and a fixing frame is fixedly installed between the two fixing rods;

[0009] A rotating assembly is arranged inside and above the water-permeable frame, and the rotating assembly includes a fixing plate;

[0010] Positioning components are symmetrically arranged on both sides of the water-permeable frame;

[0011] A fixed plate is arranged above the inner part of the water-permeable frame, a support frame is symmetrically installed at the bottom of the fixed plate, and one end of the two support frames away from the fixed plate is fixedly connected to the water-permeable frame, and a rotating shaft is rotatably connected to the inner center of the fixed plate, and a driving motor is fixedly installed on one side of the top of the fixed plate, and a first pulley is fixedly installed on the output end of the driving motor, and a second pulley is fixedly installed on the outer upper part of the rotating shaft, and the second pulley is rotatably connected to the first pulley through a belt;

[0012] The stirring blade is symmetrically installed at the lower part of the outside of the rotating shaft, a spiral blade is fixedly installed at the bottom end of the rotating shaft, and a rotating frame is fixedly installed on the outside of the rotating shaft above the second pulley, and an adding pipe is fixedly installed on one side of the inside of the rotating frame, and the adding pipe is rotatably connected to the fixed frame, and the top end of the adding pipe is connected to the adding bucket through a rotating structure, and a U-shaped frame is fixedly installed on the outside of the adding bucket, and the U-shaped frame is fixedly connected to the fixed frame.

[0013] Preferably, a mounting frame is fixedly installed on one side of the outside of the adding tube, and a positioning plate is symmetrically installed on one side of the bottom of the mounting frame, and a rotating gear is rotatably connected between the two positioning plates. At the same time, a plurality of teeth are fixedly installed on the outer side of the top of the fixed plate, and the rotating gear is meshingly connected with the plurality of teeth.

[0014] By adopting the above technical solution, the circular rotation of the mounting frame can drive the rotating gear to rotate.

[0015] Preferably, an annular groove is provided on the top of the fixing plate on one side of the plurality of teeth, and an arc block is slidably connected to one side of the inner part of the annular groove, and the arc block is fixedly connected to the mounting frame.

[0016] By adopting the above technical solution, the rotation of the mounting frame can be supported and limited.

[0017] Preferably, the bottom end of the adding pipe is connected through a first telescopic hose, the bottom end of the first telescopic hose is connected through a mounting pipe, and the bottom end of the mounting pipe is connected through a second telescopic hose.

[0018] By adopting the above technical solution, the acid liquid is added through the second telescopic hose.

[0019] Preferably, one side of the rotating gear passes through a positioning plate on one side through a rotating shaft and is fixedly installed with a rotating shaft, and a rotating rod is fixedly installed at one end of the rotating shaft, and a column block is fixedly installed on one side of the rotating rod, and at the same time, the outside of the column block is slidably connected to a movable frame, and guide rods are symmetrically installed on the top of the movable frame, and the two guide rods are slidably connected to the mounting frame.

[0020] By adopting the above technical solution, the rotation of the rotating shaft can drive the movable frame to move back and forth.

[0021] Preferably, a connecting frame is fixedly installed on the bottom of the movable frame, and a mounting plate is fixedly installed on the other side of the bottom of the mounting frame, and a rotating rod is rotatably connected to the inside of the mounting plate, and the rotating rod is fixedly connected to the mounting tube, and a driven gear is fixedly installed on the outer side of the rotating rod, and a movable plate is fixedly installed on one end of the connecting frame away from the movable frame, and a toothed plate is fixedly installed on the side of the movable plate close to the driven gear, and the toothed plate is meshingly connected to the driven gear.

[0022] By adopting the above technical solution, the reciprocating movement of the mounting plate can drive the rotating rod to reciprocate.

[0023] Preferably, an L-shaped rod is slidably connected to one side of the mounting plate inside the rotating rod, and one end of the L-shaped rod is fixedly connected to the second telescopic hose, and a telescopic spring is sleeved on one side of the outside of the L-shaped rod, and one end of the telescopic spring is fixedly connected to the rotating rod, and a fixing block is fixedly installed on the other end of the telescopic spring, and the fixing block is fixedly connected to the L-shaped rod, and a ball is hinged on the top of the L-shaped rod, and a V-shaped plate is fixedly installed on one side of the mounting plate above the L-shaped rod, and the ball is against the V-shaped plate.

[0024] By adopting the above technical solution, the second telescopic hose can be continuously extended and contracted by reciprocating the rotating rod, which can further increase the adding range of the acid liquid.

[0025] Preferably, the positioning assembly includes inclined blocks symmetrically installed on the upper sides of the water-permeable frame, and two groups of centering blocks are symmetrically installed on the upper inside of the pickling tank, and a V-shaped block is fixedly installed on one side of the inclined block, and a V-shaped groove is provided on one side of the centering block, and the V-shaped block is adaptably connected to the V-shaped groove, and mounting holes are provided through the upper middle part of both sides of the pickling tank, and positioning pins are adaptably connected to the inside of the mounting holes, and positioning holes are provided on the upper middle part of both sides of the water-permeable frame, and the positioning pins are adaptably connected to the positioning holes.

[0026] By adopting the above technical solution, the water-permeable frame can be centered to avoid deviation of the water-permeable frame when it is hoisted into the pickling tank.

[0027] Preferably, the ends of the two positioning pins that are away from each other are fixedly installed with mounting blocks, and column rods are rotatably connected to the two mounting blocks on both sides of the pickling tank, and a rotating plate is slidably connected to the outer side of the column rod, and a return spring is sleeved on the outer side of the column rod at one side of the rotating plate, and the two ends of the return spring are respectively fixedly connected to the rotating plate and the column rod, and the rotating plate is slidably connected to the column rod, and a positioning block is fixedly installed on the upper side of one side of the rotating plate, and a positioning groove is opened on the lower side of one side of the mounting block, and the positioning block is engaged with the positioning groove.

[0028] By adopting the above technical solution, the positioning pin can be positioned, and the water-permeable frame can be positioned by the positioning pin to avoid accidental movement of the water-permeable frame during the subsequent pickling process.

[0029] Compared with the prior art, the beneficial effects of the present invention are as follows: the processing equipment and method of high-purity silicon carbide synthetic powder enable the acid solution to be added more evenly, avoiding uneven addition of the acid solution causing excessive local concentration and causing violent reactions, facilitating operation by users, improving the efficiency of acid solution addition, avoiding affecting the quality of pickling, and improving practicality;

[0030] 1. When pickling silicon carbide powder, add the silicon carbide powder into a water-permeable frame, then hoist the water-permeable frame into the pickling tank through a hoisting device, add a certain amount of acid solution into the pickling tank, and a pH meter is provided in the pickling tank, then the drive motor can be started to drive the first pulley to rotate, then the second pulley is driven to rotate through the belt, so that the rotating shaft is rotated and connected, and the rotating shaft can drive the stirring blade to rotate after the rotating shaft rotates, so that the powder can be stirred, so that the impurities in the powder can react evenly with the acid solution, and the pH value of the acid solution is monitored by the pH meter, and then when it is necessary to add acid solution, the acid solution can be added to the adding bucket, the acid solution can enter the adding pipe, and the acid solution can leak out through the second telescopic hose, and the rotating shaft can drive the adding pipe to rotate through the rotating frame during the rotation process, and the arc block can be driven in the circular process of the rotating frame. The cam is engaged with the gear train and the gear train is engaged with the gear train, and the cam is engaged with the gear train so that the gear train can move in a controlled manner and the cam train can move in a controlled manner, thereby making the cam train more operable.

[0031] 2. When adding acid, the rotating rod rotates back and forth, so that the L-shaped rod can be driven to swing back and forth, so that the second telescopic hose can swing together with the mounting tube. During the reciprocating swing of the L-shaped rod, the ball slides on the V-shaped plate, so that when the L-shaped rod is no longer vertical, the L-shaped rod slides on the rotating rod under the guidance of the V-shaped plate, and the telescopic spring can be stretched. After the L-shaped rod moves, the second telescopic hose can be stretched, so that the second telescopic hose can be lengthened. Then, the reciprocating rotation of the rotating rod can make the second telescopic hose continuously extend and contract, which can further increase the range of acid addition, avoid uneven acid addition, facilitate rapid mixing of the acid, and improve practicality.

[0032] 3. When hoisting the water-permeable frame, lift the water-permeable frame and move it to the top of the pickling tank, control the water-permeable frame to move downward, so that the inclined block fits with the centering block, so that the left and right positions of the water-permeable frame can be centered, and the downward movement of the inclined block can allow the V-shaped block to be inserted into the V-shaped groove, so that the water-permeable frame can be centered front to back, so that it can play a calibration role when hoisting the water-permeable frame to avoid the water-permeable frame from being offset, and then the locating pins can be passed through the mounting holes and the locating holes to position the water-permeable frame, and then the rotating plate can be pushed and rotated to make the rotating plate slide on the column rod and compress the reset spring, and then the locating block on the rotating plate is aligned with the locating groove on the mounting block, and then the rotating plate can be released. Under the action of the reset spring, the locating block is engaged with the locating groove, and then the locating pin can be positioned. The water-permeable frame can be positioned by the locating pin to avoid accidental movement of the water-permeable frame during subsequent pickling, thereby improving the stability of the pickling work. BRIEF DESCRIPTION OF THE DRAWINGS

[0033] Figure 1 It is a schematic diagram of the overall structure of the present invention;

[0034] Figure 2 It is a schematic diagram of the cross-sectional structure of the present invention;

[0035] Figure 3 For the present invention Figure 2 A schematic diagram of the enlarged structure of the middle A area;

[0036] Figure 4 It is a schematic diagram of the cross-sectional structure of the fixing plate of the present invention;

[0037] Figure 5 This is a schematic diagram of the structure of the added tube of the present invention;

[0038] Figure 6 It is a schematic diagram of the local structure of the rotating assembly of the present invention;

[0039] Figure 7 For the present invention Figure 6 Schematic diagram of the enlarged structure of the middle B area;

[0040] Figure 8 It is a schematic diagram of the local structure of the positioning component of the present invention;

[0041] Fig. 9 For the present invention Figure 2 Schematic diagram of the enlarged structure of the middle C area.

[0042] In the figure: 1, pickling tank; 101, drain pipe; 102, permeable frame; 103, discharge pipe; 104, column; 105, fixed rod; 106, fixed frame; 2, rotating assembly; 201, fixed plate; 202, support frame; 203, rotating shaft; 204, driving motor; 205, first pulley; 206, second pulley; 207, stirring blade; 208, spiral blade; 209, rotating frame; 210, adding pipe; 211, U-shaped frame; 212, adding bucket; 213, mounting frame; 214, positioning plate; 215, rotating gear; 216, teeth; 217, annular groove; 218, arc block; 219, first telescopic hose; 220, mounting pipe; 221, the first 2. Telescopic hose; 222. Rotating shaft; 223. Rotating rod; 224. Column block; 225. Movable frame; 226. Guide rod; 227. Connecting frame; 228. Mounting plate; 229. Rotating rod; 230. Driven gear; 231. Movable plate; 232. Tooth plate; 233. L-shaped rod; 234. Telescopic spring; 235. Fixed block; 236. V-shaped plate; 3. Positioning assembly; 301. Oblique block; 302. Centering block; 303. V-shaped block; 304. V-shaped groove; 305. Mounting hole; 306. Positioning pin; 307. Positioning hole; 308. Mounting block; 309. Column rod; 310. Rotating plate; 311. Return spring; 312. Positioning block; 313. Positioning groove. DETAILED DESCRIPTION

[0043] The following will be combined with the drawings in the embodiments of the present invention to clearly and completely describe the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.

[0044] See also Figure 1-Figure 9 The present invention provides a technical solution: a high-purity silicon carbide synthetic powder processing equipment, comprising a pickling tank 1, a drainage pipe 101 is connected through one side of the pickling tank 1, and a control valve is arranged inside the drainage pipe 101, and a water-permeable frame 102 is arranged inside the pickling tank 1, and a discharge pipe 103 is connected through the bottom of the water-permeable frame 102, and a discharge valve is arranged inside the discharge pipe 103;

[0045] Also includes:

[0046] The columns 104 are symmetrically mounted on the top of the water-permeable frame 102, a fixing rod 105 is fixedly mounted between each group of two columns 104, and a lifting ring is fixedly mounted on the top of the two groups of columns 104, and a fixing frame 106 is fixedly mounted between the two fixing rods 105;

[0047] The rotating assembly 2 is arranged inside and above the water-permeable frame 102, and the rotating assembly 2 includes a fixing plate 201;

[0048] A fixed plate 201 is arranged above the inner part of the water-permeable frame 102, a support frame 202 is symmetrically installed at the bottom of the fixed plate 201, and one end of the two support frames 202 away from the fixed plate 201 is fixedly connected to the water-permeable frame 102, and a rotating shaft 203 is rotatably connected to the inner center of the fixed plate 201, and a driving motor 204 is fixedly installed on one side of the top of the fixed plate 201, and a first pulley 205 is fixedly installed on the output end of the driving motor 204, and a second pulley 206 is fixedly installed on the outer upper part of the rotating shaft 203, and the second pulley 206 is rotatably connected to the first pulley 205 through a belt;

[0049] The stirring blade 207 is symmetrically mounted on the lower part of the outer part of the rotating shaft 203, and a spiral blade 208 is fixedly mounted on the bottom end of the rotating shaft 203. A rotating frame 209 is fixedly mounted on the outer part of the rotating shaft 203 above the second pulley 206, and an adding pipe 210 is fixedly mounted on one side of the inner part of the rotating frame 209. The adding pipe 210 is rotatably connected to the fixed frame 106, and an adding bucket 212 is penetrated and connected to the top end of the adding pipe 210 through a rotating structure, and a U-shaped frame 211 is fixedly mounted on the outer part of the adding bucket 212, and the U-shaped frame 211 is fixedly connected to the fixed frame 106;

[0050] A mounting frame 213 is fixedly installed on one side of the outside of the adding pipe 210, and a positioning plate 214 is symmetrically installed on one side of the bottom of the mounting frame 213, and a rotating gear 215 is rotatably connected between the two positioning plates 214, and a plurality of teeth 216 are fixedly installed on the outer side of the top of the fixing plate 201, and the rotating gear 215 is meshed and connected with the plurality of teeth 216;

[0051] An annular groove 217 is formed on the top of the fixing plate 201 on one side of the plurality of teeth 216, and an arc block 218 is slidably connected to one side of the inner side of the annular groove 217, and the arc block 218 is fixedly connected to the mounting frame 213;

[0052] The bottom end of the adding pipe 210 is connected with a first telescopic hose 219, and the bottom end of the first telescopic hose 219 is connected with a mounting pipe 220, and the bottom end of the mounting pipe 220 is connected with a second telescopic hose 221;

[0053] One side of the rotating gear 215 passes through a positioning plate 214 on one side through a rotating shaft and is fixedly installed with a rotating shaft 222, and one end of the rotating shaft 222 is fixedly installed with a rotating rod 223, and one side of the rotating rod 223 is fixedly installed with a column block 224, and at the same time, the outer part of the column block 224 is slidably connected with a movable frame 225, and the top of the movable frame 225 is symmetrically installed with guide rods 226, and the two guide rods 226 are both slidably connected with the mounting frame 213;

[0054] A connecting frame 227 is fixedly installed at the bottom of the movable frame 225, and a mounting plate 228 is fixedly installed on the other side of the bottom of the mounting frame 213, and the mounting plate 228 is internally rotatably connected to a rotating rod 229, and the rotating rod 229 is fixedly connected to the mounting tube 220, and a driven gear 230 is fixedly installed on the outer side of the rotating rod 229, and a movable plate 231 is fixedly installed at one end of the connecting frame 227 away from the movable frame 225, and a tooth plate 232 is fixedly installed on the side of the movable plate 231 close to the driven gear 230, and the tooth plate 232 is meshingly connected to the driven gear 230.

[0055] Embodiment 1: Figure 1-Figure 7As shown, when the silicon carbide powder is pickled, the silicon carbide powder is added to the water-permeable frame 102, and then the water-permeable frame 102 is hoisted into the pickling tank 1 by a hoisting device, a certain amount of acid is added to the pickling tank 1, and a pH meter is provided in the pickling tank 1, and then the driving motor 204 can be started to drive the first pulley 205 to rotate, and then the second pulley 206 is driven to rotate by the belt, so that the rotating shaft 203 is rotated and connected, and after the rotating shaft 203 rotates, the stirring blade 207 can be driven to rotate, and the powder can be stirred, so that the impurities in the powder can react evenly with the acid, and the pH value of the acid is monitored by the pH meter, and then when it is necessary to add acid, the acid can be added to the adding bucket 212, and the acid can enter the adding pipe 210, and the acid can leak out through the second telescopic hose 221, and the rotating shaft 203 can drive the adding pipe 210 to rotate through the rotating frame 209 during the rotation process, and the rotating frame 209 can drive the arc block 218 in the annular groove 21 during the circumferential rotation. 7 internal sliding to support the limit, and the rotating frame 209 can drive the rotating gear 215 to rotate in a circle. After the rotating gear 215 rotates, it can drive the rotating shaft 222 to rotate, so that the column block 224 on the rotating rod 223 rotates in a circle. After the column block 224 rotates in a circle, it can drive the movable frame 225 to move up and down reciprocatingly through the sliding connection with the movable frame 225. After the movement, the movable frame 225 can drive the movable plate 231 to move back and forth through the connecting frame 227, and then drive the rotating rod 229 to rotate back and forth through the engagement of the tooth plate 232 and the driven gear 230, so that the installation pipe 220 and the second telescopic hose 221 can swing back and forth, so that the adding pipe 210 rotates in a circle and the second telescopic hose 221 can swing back and forth, so that the acid solution can be added more evenly, avoiding uneven addition of the acid solution causing excessive local concentration and avoiding causing violent reactions, which is convenient for users to operate, improves the efficiency of adding the acid solution, avoids affecting the quality of pickling, and improves practicality.

[0056] An L-shaped rod 233 is slidably connected to one side of the mounting plate 228 inside the rotating rod 229, and one end of the L-shaped rod 233 is fixedly connected to the second telescopic hose 221, and a telescopic spring 234 is sleeved on one side of the outside of the L-shaped rod 233, and one end of the telescopic spring 234 is fixedly connected to the rotating rod 229, and a fixing block 235 is fixedly installed on the other end of the telescopic spring 234, and the fixing block 235 is fixedly connected to the L-shaped rod 233, and a ball is hinged on the top of the L-shaped rod 233, and a V-shaped plate 236 is fixedly installed on one side of the mounting plate 228 above the L-shaped rod 233, and the ball is abutted against the V-shaped plate 236.

[0057] Embodiment 2: Figure 5-Figure 7As shown, when adding acid, the rotating rod 229 rotates back and forth, so that the L-shaped rod 233 can be driven to swing back and forth, so that the second telescopic hose 221 swings together with the mounting tube 220. During the reciprocating swing of the L-shaped rod 233, the ball slides on the V-shaped plate 236, so that when the L-shaped rod 233 swings and is no longer vertical, the L-shaped rod 233 slides on the rotating rod 229 under the guidance of the V-shaped plate 236, and the telescopic spring 234 can be stretched. After moving, the L-shaped rod 233 can stretch the second telescopic hose 221, so that the second telescopic hose 221 can be lengthened, and then the reciprocating rotation of the rotating rod 229 can make the second telescopic hose 221 continuously expand and contract, which can further increase the adding range of the acid, avoid uneven adding of the acid, facilitate rapid mixing of the acid, and improve practicality.

[0058] Positioning components 3, symmetrically arranged on both sides of the water-permeable frame 102;

[0059] The positioning assembly 3 includes inclined blocks 301 symmetrically installed on both sides of the water-permeable frame 102, and two sets of centering blocks 302 are symmetrically installed on the inside of the pickling tank 1, and a V-shaped block 303 is fixedly installed on one side of the inclined block 301, and a V-shaped groove 304 is provided on one side of the centering block 302, and the V-shaped block 303 is adapted to be connected with the V-shaped groove 304, and mounting holes 305 are provided through the middle of both sides of the pickling tank 1, and the inside of the mounting holes 305 is adapted to be connected with positioning pins 306, and positioning holes 307 are provided on the middle of both sides of the water-permeable frame 102, and the positioning pins 306 are adapted to be connected with the positioning holes 307;

[0060] The ends of the two locating pins 306 that are away from each other are fixedly installed with mounting blocks 308, and both sides of the pickling tank 1 are rotatably connected with column rods 309 located below the two mounting blocks 308, and the outer side of the column rod 309 is slidably connected with a rotating plate 310, and at the same time, a return spring 311 is sleeved on the outer side of the column rod 309 located on one side of the rotating plate 310, and the two ends of the return spring 311 are respectively fixedly connected to the rotating plate 310 and the column rod 309, and the rotating plate 310 is slidably connected to the column rod 309, and a positioning block 312 is fixedly installed on the upper side of one side of the rotating plate 310, and a positioning groove 313 is opened at the lower side of one side of the mounting block 308, and the positioning block 312 is engaged with the positioning groove 313.

[0061] Embodiment 3: Figure 1 and Figure 8-Figure 9As shown, when the water-permeable frame 102 is hoisted, the water-permeable frame 102 is lifted and moved to the top of the pickling tank 1, and the water-permeable frame 102 is controlled to move downward so that the inclined block 301 fits with the centering block 302, so that the left and right positions of the water-permeable frame 102 can be centered, and the downward movement of the inclined block 301 can make the V-shaped block 303 insert into the V-shaped groove 304, so that the water-permeable frame 102 can be centered front and back, so that it can play a calibration role when hoisting the water-permeable frame 102 to avoid the water-permeable frame 102 from being offset, and then the positioning pin 306 can be passed through the mounting hole 305 and aligned with the positioning hole 307. After the water frame 102 is positioned, the rotating plate 310 can be pushed and rotated, so that the rotating plate 310 slides on the column rod 309 and compresses the reset spring 311, and then the positioning block 312 on the rotating plate 310 is aligned with the positioning groove 313 on the mounting block 308. After that, the rotating plate 310 can be released and the positioning block 312 is engaged with the positioning groove 313 under the action of the reset spring 311, so that the positioning pin 306 can be positioned, and the water-permeable frame 102 can be positioned by the positioning pin 306 to avoid accidental movement of the water-permeable frame 102 during the subsequent pickling process, thereby improving the stability of the pickling work.

[0062] Working principle: When using the high-purity silicon carbide synthetic powder processing equipment, first, according to Figure 1-Figure 9As shown, when the silicon carbide powder is pickled, the silicon carbide powder is added to the water-permeable frame 102, and then the water-permeable frame 102 is hoisted into the pickling tank 1 by a hoisting device, a certain amount of acid is added to the pickling tank 1, and a pH meter is provided in the pickling tank 1, and then the driving motor 204 can be started to drive the first pulley 205 to rotate, and then the second pulley 206 is driven to rotate by the belt, so that the rotating shaft 203 is rotated and connected, and after the rotating shaft 203 rotates, the stirring blade 207 can be driven to rotate, and the powder can be stirred so that the impurities in the powder can react evenly with the acid, and the pH value of the acid is monitored by the pH meter, and then when it is necessary to add acid, the acid can be added to the adding bucket 212, and the acid can enter the adding pipe 210, and the acid can leak out through the second telescopic hose 221, and the rotating shaft 203 can be driven by the rotating frame 209 during the rotation process. The adding pipe 210 rotates, and the rotating frame 209 can drive the arc block 218 to slide inside the annular groove 217 to support and limit the position during the circular rotation. The rotating frame 209 can drive the rotating gear 215 to rotate in a circular manner. After the rotating gear 215 rotates, it can drive the rotating shaft 222 to rotate, so that the column block 224 on the rotating rod 223 rotates in a circular manner. After the column block 224 rotates in a circular manner, it can drive the movable frame 225 to reciprocate up and down through the sliding connection with the movable frame 225. After the movable frame 225 moves, it can drive the movable plate 231 to reciprocate through the connecting frame 227, and then drive the rotating rod 229 to reciprocate through the meshing of the tooth plate 232 and the driven gear 230, so that the installation pipe 220 and the second telescopic hose 221 can swing back and forth, so that the second telescopic hose 221 can swing back and forth while the adding pipe 210 rotates in a circular manner;

[0063] When adding acid solution, the rotating rod 229 rotates back and forth, so that the L-shaped rod 233 can be driven to swing back and forth, so that the second telescopic hose 221 can swing together with the mounting tube 220. During the reciprocating swing of the L-shaped rod 233, the ball slides on the V-shaped plate 236. When the L-shaped rod 233 swings and is no longer vertical, the L-shaped rod 233 slides on the rotating rod 229 under the guidance of the V-shaped plate 236, and the telescopic spring 234 can be stretched. After the movement, the L-shaped rod 233 can stretch the second telescopic hose 221, so that the second telescopic hose 221 can be elongated, and then the reciprocating rotation of the rotating rod 229 can make the second telescopic hose 221 continuously extend and contract. When the water-permeable frame 102 is hoisted, the water-permeable frame 102 is lifted and moved to the top of the pickling tank 1, and the water-permeable frame 102 is controlled to move downward, so that the inclined block 301 and the centering block 302 are fitted together, so that the left and right positions of the water-permeable frame 102 can be adjusted. The locating pin 306 can be passed through the mounting hole 305 and the locating hole 307 to position the water permeable frame 102. The rotating plate 310 can be pushed and rotated so that the rotating plate 310 slides on the column rod 309 and compresses the return spring 311. The locating block 312 on the rotating plate 310 is aligned with the locating groove 313 on the mounting block 308. The rotating plate 310 can be released and the locating block 312 is engaged with the locating groove 313 under the action of the return spring 311. The locating pin 306 can be positioned. The water permeable frame 102 can be positioned by the locating pin 306 to avoid accidental movement of the water permeable frame 102 during the subsequent pickling process, thereby improving the stability of the pickling work.

[0064] The contents not described in detail in this specification belong to the prior art known to professional and technical personnel in this field.

[0065] Although the present invention has been described in detail with reference to the aforementioned embodiments, it is still possible for those skilled in the art to modify the technical solutions described in the aforementioned embodiments, or to make equivalent substitutions for some of the technical features therein. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the protection scope of the present invention.

Claims

1. A processing device for high-purity silicon carbide synthetic powder, comprising a pickling tank (1), a drain pipe (101) is connected through one side of the pickling tank (1), and a control valve is arranged inside the drain pipe (101), and a water permeable frame (102) is arranged inside the pickling tank (1), and a discharge pipe (103) is connected through the bottom of the water permeable frame (102), and a discharge valve is arranged inside the discharge pipe (103); It is characterized in that Also includes: The columns (104) are symmetrically mounted on the top of the water-permeable frame (102); a fixing rod (105) is fixedly mounted between each group of two columns (104); a lifting ring is fixedly mounted on the top of the two groups of columns (104); and a fixing frame (106) is fixedly mounted between the two fixing rods (105); A rotating assembly (2) is arranged inside and above the water-permeable frame (102), wherein the rotating assembly (2) comprises a fixing plate (201); Positioning components (3) are symmetrically arranged on both sides of the water-permeable frame (102); A fixed plate (201) is arranged above the inside of the water-permeable frame (102); a support frame (202) is symmetrically installed at the bottom of the fixed plate (201); and one end of the two support frames (202) away from the fixed plate (201) is fixedly connected to the water-permeable frame (102); and a rotating shaft (203) is rotatably connected to the inner center of the fixed plate (201); and a driving motor (204) is fixedly installed on one side of the top of the fixed plate (201); and a first pulley (205) is fixedly installed at the output end of the driving motor (204); and a second pulley (206) is fixedly installed on the outside of the rotating shaft (203); and the second pulley (206) is rotatably connected to the first pulley (205) via a belt; The stirring blade (207) is symmetrically mounted on the outside and below of the rotating shaft (203); a spiral blade (208) is fixedly mounted on the bottom end of the rotating shaft (203); a rotating frame (209) is fixedly mounted on the outside of the rotating shaft (203) above the second pulley (206); an adding pipe (210) is fixedly mounted on one side of the inside of the rotating frame (209); the adding pipe (210) is rotatably connected to the fixed frame (106); an adding bucket (212) is penetrated and connected to the top end of the adding pipe (210) through a rotating structure; a U-shaped frame (211) is fixedly mounted on the outside of the adding bucket (212); and the U-shaped frame (211) is fixedly connected to the fixed frame (106).

2. The processing equipment for high-purity silicon carbide synthetic powder according to claim 1 is characterized in that: A mounting frame (213) is fixedly mounted on one side of the outside of the adding pipe (210), and a positioning plate (214) is symmetrically mounted on one side of the bottom of the mounting frame (213), and a rotating gear (215) is rotatably connected between the two positioning plates (214), and a plurality of teeth (216) are fixedly mounted on the outer side of the top of the fixing plate (201), and the rotating gear (215) is meshingly connected with the plurality of teeth (216).

3. The processing equipment for high-purity silicon carbide synthetic powder according to claim 2 is characterized in that: An annular groove (217) is provided on the top of the fixing plate (201) and one side of the plurality of teeth (216), and an arc block (218) is slidably connected to the inner side of the annular groove (217), and the arc block (218) is fixedly connected to the mounting frame (213).

4. The processing equipment for high-purity silicon carbide synthetic powder according to claim 3 is characterized in that: The bottom end of the adding pipe (210) is connected through a first telescopic hose (219), the bottom end of the telescopic first telescopic hose (219) is connected through a mounting pipe (220), and the bottom end of the mounting pipe (220) is connected through a second telescopic hose (221).

5. The processing equipment for high-purity silicon carbide synthetic powder according to claim 4 is characterized in that: One side of the rotating gear (215) passes through a positioning plate (214) on one side through a rotating shaft and is fixedly installed with a rotating shaft (222), and one end of the rotating shaft (222) is fixedly installed with a rotating rod (223), and one side of the rotating rod (223) is fixedly installed with a column block (224), and at the same time, the outside of the column block (224) is slidably connected to a movable frame (225), and the top of the movable frame (225) is symmetrically installed with guide rods (226), and the two guide rods (226) are both slidably connected to the mounting frame (213).

6. The processing equipment for high-purity silicon carbide synthetic powder according to claim 5, characterized in that: A connecting frame (227) is fixedly installed at the bottom of the movable frame (225), and a mounting plate (228) is fixedly installed on the other side of the bottom of the mounting frame (213), and a rotating rod (229) is rotatably connected inside the mounting plate (228), and the rotating rod (229) is fixedly connected to the mounting tube (220), and a driven gear (230) is fixedly installed on the outer side of the rotating rod (229), and a movable plate (231) is fixedly installed at one end of the connecting frame (227) away from the movable frame (225), and a tooth plate (232) is fixedly installed on the side of the movable plate (231) close to the driven gear (230), and the tooth plate (232) is meshedly connected with the driven gear (230).

7. The processing equipment for high-purity silicon carbide synthetic powder according to claim 6 is characterized in that: An L-shaped rod (233) is slidably connected to one side of the mounting plate (228) inside the rotating rod (229), and one end of the L-shaped rod (233) is fixedly connected to the second telescopic hose (221), and a telescopic spring (234) is sleeved on one side of the outside of the L-shaped rod (233), and one end of the telescopic spring (234) is fixedly connected to the rotating rod (229), and a fixing block (235) is fixedly installed on the other end of the telescopic spring (234), and the fixing block (235) is fixedly connected to the L-shaped rod (233), and a ball bearing is hinged on the top of the L-shaped rod (233), and a V-shaped plate (236) is fixedly installed on one side of the mounting plate (228) above the L-shaped rod (233), and the ball bearing abuts against the V-shaped plate (236).

8. The processing equipment for high-purity silicon carbide synthetic powder according to claim 1, characterized in that: The positioning assembly (3) comprises inclined blocks (301) symmetrically mounted on both sides of the water-permeable frame (102), and two groups of centering blocks (302) are symmetrically mounted on the inside of the pickling tank (1), and a V-shaped block (303) is fixedly mounted on one side of the inclined block (301), and a V-shaped groove (304) is provided on one side of the centering block (302), and the V-shaped block (303) is adaptively connected to the V-shaped groove (304), and mounting holes (305) are provided through the middle of both sides of the pickling tank (1), and positioning pins (306) are adaptively connected inside the mounting holes (305), and positioning holes (307) are provided on the middle of both sides of the water-permeable frame (102), and the positioning pins (306) are adaptively connected to the positioning holes (307).

9. The processing equipment for high-purity silicon carbide synthetic powder according to claim 8, characterized in that: The ends of the two positioning pins (306) that are away from each other are fixedly installed with mounting blocks (308), and column rods (309) are rotatably connected to the two mounting blocks (308) on both sides of the pickling tank (1), and a rotating plate (310) is slidably connected to the outer side of the column rod (309), and a return spring (311) is sleeved on the outer side of the column rod (309) located on one side of the rotating plate (310), and the two ends of the return spring (311) are respectively fixedly connected to the rotating plate (310) and the column rod (309), and the rotating plate (310) is slidably connected to the column rod (309), and a positioning block (312) is fixedly installed on the upper side of one side of the rotating plate (310), and a positioning groove (313) is opened on the lower side of one side of the mounting block (308), and the positioning block (312) is snap-fitted with the positioning groove (313).

10. A method for processing high-purity silicon carbide synthetic powder, using a processing device for high-purity silicon carbide synthetic powder as claimed in any one of claims 1 to 8, characterized in that: The specific processing methods are as follows: Step 1: When the silicon carbide powder is pickled, the silicon carbide powder is added to a water permeable frame (102), and then the water permeable frame (102) is hoisted into a pickling tank (1) by a hoisting device. A certain amount of acid is added to the pickling tank (1), and a pH meter is provided in the pickling tank (1). Then, a driving motor (204) can be started to drive the first pulley (205) to rotate, and then the second pulley (206) is driven to rotate by a belt, so that the rotating shaft (203) is connected to rotate. After the rotating shaft (203) rotates, the stirring blade (207) can be driven to rotate, and the stirring blade (207) can be driven to rotate. The powder is stirred so that the impurities in the powder can react evenly with the acid solution. The pH value of the acid solution is monitored by a pH meter. When the acid solution needs to be added, the acid solution can be added to the adding bucket (212). The acid solution can enter the adding pipe (210). The acid solution can leak out through the second telescopic hose (221). The rotating shaft (203) can drive the adding pipe (210) to rotate through the rotating frame (209) during the rotation process. The rotating frame (209) can drive the arc block (218) in the annular groove (217) during the circular rotation process. The internal sliding is used for supporting and limiting, and the rotating frame (209) can drive the rotating gear (215) to rotate in a circle. After the rotating gear (215) rotates, it can drive the rotating shaft (222) to rotate, so that the column block (224) on the rotating rod (223) rotates in a circle. After the column block (224) rotates in a circle, it can drive the movable frame (225) to move up and down through the sliding connection with the movable frame (225). After the movable frame (225) moves, it can drive the movable plate (231) to move back and forth through the connecting frame (227), thereby The engagement of the toothed plate (232) and the driven gear (230) drives the rotating rod (229) to rotate back and forth, so that the installation tube (220) and the second telescopic hose (221) can swing back and forth, thereby making the adding tube (210) rotate in a circle while the second telescopic hose (221) can swing back and forth, so that the acid solution can be added more evenly, avoiding uneven addition of the acid solution causing excessive local concentration and violent reaction, facilitating the operation of the user, improving the efficiency of adding the acid solution, avoiding affecting the quality of pickling, and improving the practicality; Step 2: When adding acid, the rotating rod (229) rotates back and forth, so that the L-shaped rod (233) can be driven to swing back and forth, so that the second telescopic hose (221) swings together with the mounting tube (220). During the reciprocating swing of the L-shaped rod (233), the ball slides on the V-shaped plate (236), so that when the L-shaped rod (233) swings and is no longer vertical, the L-shaped rod (233) slides on the rotating rod (229) under the guidance of the V-shaped plate (236), and the telescopic spring (234) can be stretched. After the L-shaped rod (233) moves, it can stretch the second telescopic hose (221), so that the second telescopic hose (221) can be elongated. Then, the reciprocating rotation of the rotating rod (229) can cause the second telescopic hose (221) to continuously stretch and contract, which can further increase the range of acid addition, avoid uneven acid addition, facilitate rapid mixing of the acid, and improve practicality. Step 3: When the water permeable frame (102) is hoisted, the water permeable frame (102) is lifted and moved to the top of the pickling tank (1), and the water permeable frame (102) is controlled to move downward so that the inclined block (301) and the centering block (302) are fitted together, so that the left and right positions of the water permeable frame (102) can be centered, and the downward movement of the inclined block (301) can allow the V-shaped block (303) to be inserted into the V-shaped groove (304), so that the water permeable frame (102) can be centered front and back, thereby achieving a calibration effect when the water permeable frame (102) is hoisted to prevent the water permeable frame (102) from being offset, and then the positioning pin (306) can be passed through the mounting hole (305) and the positioning hole (307) to align the water permeable frame (102) is positioned, and then the rotating plate (310) can be pushed and rotated, so that the rotating plate (310) slides on the column rod (309) and compresses the reset spring (311), and then the positioning block (312) on the rotating plate (310) is aligned with the positioning groove (313) on the mounting block (308), and then the rotating plate (310) can be released and the positioning block (312) and the positioning groove (313) can be engaged under the action of the reset spring (311), so that the positioning pin (306) can be positioned, and the water-permeable frame (102) can be positioned by the positioning pin (306), so as to avoid accidental movement of the water-permeable frame (102) during the subsequent pickling process, thereby improving the stability of the pickling work.

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