Preparation method of sulfur-containing silane coupling agent

Abstract

The invention is applicable to the technical field of preparation of silane coupling agents, and particularly relates to a preparation method of a sulfur-containing silane coupling agent, which comprises the following steps: acquiring solution concentration information of a to-be-reacted substance; detecting that the triggering device executes the first triggering operation; detecting the temperature and pressure conditions of the current reaction system; and based on the solution concentration information, the first trigger operation and the temperature and pressure conditions, performing a synthesis activity of the sulfur-containing silane coupling agent to generate the sulfur-containing silane coupling agent. According to the preparation method of the sulfur-containing silane coupling agent provided by the invention, the problem that the quality of the prepared sulfur-containing silane coupling agent is low as the possibility of personal errors is increased due to dependence on experience and judgment of operators in the traditional preparation process of the sulfur-containing silane coupling agent can be solved.

Description

Technical Field

[0001] The present application belongs to the technical field of silane coupling agent preparation, and in particular relates to a method for preparing a sulfur-containing silane coupling agent. Background Art

[0002] Silane coupling agents refer to a class of compounds containing silicon atoms and organic groups, which are usually used to improve the interfacial adhesion between inorganic materials (such as glass, ceramics, metals) and organic materials (such as plastics, resins). They enhance the interaction between two different materials by forming chemical bonds on the surface of the materials. Sulfur-containing silane coupling agents are compounds that introduce sulfur-containing groups (such as thiols, disulfides, etc.) based on silane coupling agents.

[0003] The traditional preparation process of sulfur-containing silane coupling agents relies on the experience and judgment of the operators, which increases the possibility of human error (for example, due to differences in experience, judgment and skills, the operating steps, time or conditions are different, thus affecting the quality of the final prepared product), resulting in a low amount of prepared sulfur-containing silane coupling agents. Summary of the invention

[0004] The embodiment of the present application provides a method for preparing a sulfur-containing silane coupling agent, which can solve the problem that in the traditional preparation process of sulfur-containing silane coupling agents, the possibility of human error is increased, resulting in low quality of the prepared sulfur-containing silane coupling agent.

[0005] In a first aspect, an embodiment of the present application provides a method for preparing a sulfur-containing silane coupling agent, comprising:

[0006] Obtaining solution concentration information of a substance to be reacted;

[0007] Detecting that the trigger device performs a first trigger operation; wherein the trigger device is used to start a synthesis reaction of a sulfur-containing silane coupling agent;

[0008] Detecting the temperature and pressure conditions of the current reaction system; wherein the temperature and pressure conditions are used to indicate whether the reaction is within the required reaction condition range;

[0009] Based on the solution concentration information, the first trigger operation and the temperature and pressure conditions, a synthesis activity of the sulfur-containing silane coupling agent is performed to generate the sulfur-containing silane coupling agent.

[0010] The above technical solutions in the embodiments of the present application have at least the following technical effects:

[0011] The method for preparing a sulfur-containing silane coupling agent provided by the present application first obtains the solution concentration information of the reactant, which can reduce the difference in manual operation (for example, manually judging whether the solution concentration of the current reactant reaches the required concentration), thereby helping to reduce the influence of the operator's experience and judgment on the quality of the subsequently prepared sulfur-containing silane coupling agent. Secondly, the detection trigger device is executed by the first trigger operation, which can automatically start the synthesis reaction of the sulfur-containing silane coupling agent, thereby greatly reducing manual participation, reducing human errors, and improving the consistency and repeatability of the operation, thereby helping to improve the quality of the subsequently prepared sulfur-containing silane coupling agent. Thirdly, by detecting the temperature and pressure conditions of the current reaction system, it can be confirmed whether the reaction is under the required reaction conditions, thereby helping to prevent the reactant from reacting under inappropriate conditions, thereby helping to improve the quality of the subsequently prepared sulfur-containing silane coupling agent. Then, based on the solution concentration information, the first trigger operation and the temperature and pressure conditions, the synthesis activity of the sulfur-containing silane coupling agent is performed to generate the sulfur-containing silane coupling agent. The solution concentration, the trigger operation and the temperature and pressure conditions can be comprehensively considered to precisely control the various parameters of the reaction so that the results of the reaction are within the expected quality standards, thereby helping to improve the quality of the prepared sulfur-containing silane coupling agent.

[0012] In a possible implementation of the first aspect, based on the solution concentration information, the first trigger operation and the temperature and pressure conditions, performing a synthesis activity of the sulfur-containing silane coupling agent to generate the sulfur-containing silane coupling agent includes:

[0013] When the solution concentration information of the reactant reflects that the current solution concentration reaches the preset concentration and it is detected that the trigger device has executed the first trigger operation, the temperature and pressure conditions of the current reaction system are detected. If the temperature and pressure conditions reflect that the current conditions meet the required conditions, the synthesis activity of the sulfur-containing silane coupling agent is performed to generate the sulfur-containing silane coupling agent.

[0014] In a possible implementation of the first aspect, the sulfur-containing silane coupling agent preparation equipment includes a sulfur-containing silane coupling agent preparation device, and a control device communicatively connected to the sulfur-containing silane coupling agent preparation device, and the method further includes:

[0015] The control device monitors the preparation signal sent by the sulfur-containing silane coupling agent preparation device; wherein the preparation signal carries the mark and preparation data corresponding to the sulfur-containing silane coupling agent preparation device;

[0016] Based on the mark corresponding to the sulfur-containing silane coupling agent preparation device, the sulfur-containing silane coupling agent preparation device is determined to be a marking device, and based on the preparation data, the sulfur-containing silane coupling agent preparation device is determined to be in a preparation state; wherein the marking device is used to indicate a device that has created a preparation business with the control device in the past period; and the preparation state is used to indicate that the preheating time of the sulfur-containing silane coupling agent preparation device after startup does not exceed a preset time;

[0017] The control device determines to change the setting data of the preparation service.

[0018] In a possible implementation of the first aspect, after determining that the sulfur-containing silane coupling agent preparation device is a marking device based on a mark corresponding to the sulfur-containing silane coupling agent preparation device, and determining that the sulfur-containing silane coupling agent preparation device is in a preparation state based on the preparation data, the method further includes:

[0019] The preparation information acquisition method in the setting data of the preparation business is changed to the first acquisition method; or, the current business importance in the setting data of the preparation business is changed to the first importance; wherein the first importance is greater than the current business importance.

[0020] In a possible implementation manner of the first aspect, after the control device monitors the preparation signal sent by the sulfur-containing silane coupling agent preparation device, the method further includes:

[0021] When the control device monitors the preparation signal sent by the sulfur-containing silane coupling agent preparation device, the current tag is set to the first tag; wherein the first tag is used to indicate that the setting data of the preparation service can be changed.

[0022] In a possible implementation manner of the first aspect, after the control device determines to change the setting data of the preparation service, the method further includes:

[0023] In the case where the preparation instruction sent by the sulfur-containing silane coupling agent preparation device is obtained within the first time period, or in the case where the preparation instruction sent by the sulfur-containing silane coupling agent preparation device is not obtained within the first time period, the setting data of the current preparation business is changed to the previous setting data, and the current label is set to the second label; wherein the second label is used to indicate that the setting data of the preparation business cannot be changed.

[0024] In a possible implementation manner of the first aspect, the method further includes:

[0025] Sending preparation process data of the sulfur-containing silane coupling agent to be prepared to the sulfur-containing silane coupling agent preparation device according to the preparation event;

[0026] In the case where the preparation state of the preparation event is obtained to be an artificially terminated preparation state, the mark corresponding to the preparation event is adjusted to the target mark, and a preset signal corresponding to the preparation event is generated; if a signal for continuing the reaction is obtained within a preset time, the preset signal is discarded, and the preparation process data is continued to be sent to the sulfur-containing silane coupling agent preparation according to the preparation event; wherein the target mark is the mark corresponding to the event when the sulfur-containing silane coupling agent preparation device is preparing; the preset signal is used to indicate that at the end of the preset time, the mark corresponding to the preparation event is adjusted to the preset mark, the preset mark is the mark corresponding to the event when the sulfur-containing silane coupling agent preparation device is ready to prepare but has not yet prepared, and the sulfur-containing silane coupling agent preparation device clears all events except the mark with the target mark;

[0027] In the case where the preparation state of the preparation event is obtained to be a non-artificially terminated preparation state, the mark corresponding to the preparation event is adjusted to the target mark, and a target signal corresponding to the preparation event is generated; if a signal of a recovery reaction is obtained within a target time length, the target signal is discarded, and the preparation process data continues to be sent to the sulfur-containing silane coupling agent preparation according to the preparation event; wherein the target signal is used to indicate that the mark corresponding to the preparation event is adjusted to a preset mark at the end of the target time length.

[0028] In a possible implementation of the first aspect, the artificial suspension of preparation status is used to indicate that the operator actively triggers the suspension of preparation operation, maintains the preparation connection with the sulfur-containing silane coupling agent preparation device, and does not continue to send the preparation process data to the sulfur-containing silane coupling agent preparation device.

[0029] In a possible implementation manner of the first aspect, the method further includes:

[0030] When an operator's triggering operation to end the reaction is obtained within the preset time, or when no signal to continue the reaction is obtained within the preset time, the mark corresponding to the preparation event is adjusted to the preset mark.

[0031] In a possible implementation of the first aspect, the non-human suspension of preparation status is used to indicate that the operator did not actively trigger the suspension of preparation operation, did not maintain the preparation connection with the sulfur-containing silane coupling agent preparation device, and did not continue to send the preparation process data to the sulfur-containing silane coupling agent preparation device.

[0032] In a possible implementation manner of the first aspect, the method further includes:

[0033] When no signal of a recovery reaction is obtained within the target time period, the mark corresponding to the preparation event is adjusted to the preset mark.

[0034] In a second aspect, an embodiment of the present application provides a sulfur-containing silane coupling agent preparation system, which is used to implement the sulfur-containing silane coupling agent preparation method described in any one of the first aspects above, and the sulfur-containing silane coupling agent preparation system is applied to a sulfur-containing silane coupling agent preparation device, and the sulfur-containing silane coupling agent preparation system includes:

[0035] An acquisition unit, used to acquire solution concentration information of a substance to be reacted;

[0036] A detection unit, used for detecting that a first triggering operation is performed on a triggering device; wherein the triggering device is used for starting a synthesis reaction of a sulfur-containing silane coupling agent;

[0037] A monitoring unit, used to detect the temperature and pressure conditions of the current reaction system; wherein the temperature and pressure conditions are used to indicate whether the reaction is within the required reaction condition range;

[0038] A control unit is used to perform a synthesis activity of the sulfur-containing silane coupling agent based on the solution concentration information, the first trigger operation and the temperature and pressure conditions to generate the sulfur-containing silane coupling agent.

[0039] In a third aspect, an embodiment of the present application provides a sulfur-containing silane coupling agent preparation device, comprising a memory, a processor, and a computer program stored in the memory and executable on the processor, wherein when the processor executes the computer program, the sulfur-containing silane coupling agent preparation method described in any one of the first aspects above is implemented.

[0040] It can be understood that the beneficial effects of the second to third aspects mentioned above can be found in the relevant description of the first aspect mentioned above, and will not be repeated here. BRIEF DESCRIPTION OF THE DRAWINGS

[0041] In order to more clearly illustrate the technical solutions in the embodiments of the present application, the drawings required for use in the embodiments or the description of the prior art will be briefly introduced below. Obviously, the drawings described below are only some embodiments of the present application. For ordinary technicians in this field, other drawings can be obtained based on these drawings without paying any creative work.

[0042] Figure 1 It is a schematic diagram of a process for preparing a sulfur-containing silane coupling agent provided in one embodiment of the present application;

[0043] Figure 2 It is a schematic diagram of the implementation process of changing the setting data of the preparation business in the method for preparing a sulfur-containing silane coupling agent provided in one embodiment of the present application;

[0044] Figure 3 It is a schematic diagram of a process for implementing the adjustment of the symbols corresponding to the preparation events in the method for preparing the sulfur-containing silane coupling agent provided in one embodiment of the present application;

[0045] Figure 4 Schematic diagram of the structure of the system for preparing the sulfur-containing silane coupling agent provided in the embodiment of the present application;

[0046] Figure 5 It is a schematic diagram of the structure of the sulfur-containing silane coupling agent preparation equipment provided in the embodiment of the present application. DETAILED DESCRIPTION

[0047] In the following description, specific details such as specific system structures, technologies, etc. are provided for the purpose of illustration rather than limitation, so as to provide a thorough understanding of the embodiments of the present application. However, it should be clear to those skilled in the art that the present application may also be implemented in other embodiments without these specific details. In other cases, detailed descriptions of well-known systems, devices, circuits, and methods are omitted to prevent unnecessary details from obstructing the description of the present application.

[0048] It should be understood that when used in the present specification and the appended claims, the term "comprising" indicates the presence of described features, wholes, steps, operations, elements and / or components, but does not exclude the presence or addition of one or more other features, wholes, steps, operations, elements, components and / or combinations thereof.

[0049] It should also be understood that the term “and / or” used in the specification and appended claims refers to any and all possible combinations of one or more of the associated listed items, and includes these combinations.

[0050] As used in the specification and appended claims of this application, the term "if" can be interpreted as "when" or "uponce" or "in response to determining" or "in response to detecting" depending on the context. Similarly, the phrase "if it is determined" or "if the described condition or event is detected" can be interpreted as meaning "uponce determined" or "in response to determining" or "uponce the described condition or event is detected" or "in response to detecting the described condition or event" depending on the context.

[0051] In addition, in the description of the present application specification and the appended claims, the terms "first", "second", "third", etc. are only used to distinguish the descriptions and cannot be understood as indicating or implying relative importance.

[0052] References to "one embodiment" or "some embodiments" etc. described in the specification of this application mean that one or more embodiments of the present application include specific features, structures or characteristics described in conjunction with the embodiment. Therefore, the statements "in one embodiment", "in some embodiments", "in some other embodiments", "in some other embodiments", etc. that appear in different places in this specification do not necessarily refer to the same embodiment, but mean "one or more but not all embodiments", unless otherwise specifically emphasized in other ways. The terms "including", "comprising", "having" and their variations all mean "including but not limited to", unless otherwise specifically emphasized in other ways.

[0053] In the related art, silane coupling agents refer to a class of compounds containing silicon atoms and organic groups, which are usually used to improve the interfacial adhesion between inorganic materials (such as glass, ceramics, metals) and organic materials (such as plastics, resins). They enhance the interaction between two different materials by forming chemical bonds on the surface of the materials. Sulfur-containing silane coupling agents are compounds that introduce sulfur-containing groups (such as thiols, disulfides, etc.) on the basis of silane coupling agents.

[0054] The traditional preparation process of sulfur-containing silane coupling agents relies on the experience and judgment of the operators, which increases the possibility of human error (for example, due to differences in experience, judgment and skills, the operating steps, time or conditions are different, thus affecting the quality of the final prepared product), resulting in a low amount of prepared sulfur-containing silane coupling agents.

[0055] In order to solve the above problems, the embodiments of the present application provide a method for preparing a sulfur-containing silane coupling agent.

[0056] In the method, the solution concentration information of the reactant is first obtained, which can reduce the difference in manual operation (for example, manually judging whether the solution concentration of the current reactant reaches the required concentration), thereby helping to reduce the influence of the operator's experience and judgment on the quality of the subsequently prepared sulfur-containing silane coupling agent. Secondly, the detection trigger device is executed by the first trigger operation, which can automatically start the synthesis reaction of the sulfur-containing silane coupling agent, thereby greatly reducing manual participation, reducing human errors, and improving the consistency and repeatability of the operation, thereby helping to improve the quality of the subsequently prepared sulfur-containing silane coupling agent. Thirdly, the temperature and pressure conditions of the current reaction system are detected to confirm whether the reaction is under the required reaction conditions, thereby helping to prevent the reactant from reacting under inappropriate conditions, thereby helping to improve the quality of the subsequently prepared sulfur-containing silane coupling agent. Then, based on the solution concentration information, the first trigger operation and the temperature and pressure conditions, the synthesis activity of the sulfur-containing silane coupling agent is performed to generate the sulfur-containing silane coupling agent. The solution concentration, the trigger operation and the temperature and pressure conditions can be comprehensively considered to precisely control the various parameters of the reaction so that the results of the reaction are within the expected quality standards, thereby helping to improve the quality of the prepared sulfur-containing silane coupling agent.

[0057] The method for preparing a sulfur-containing silane coupling agent provided in the embodiment of the present application can be applied to a sulfur-containing silane coupling agent preparation device. In this case, the sulfur-containing silane coupling agent preparation device is the executor of the method for preparing a sulfur-containing silane coupling agent provided in the embodiment of the present application. The embodiment of the present application does not impose any restrictions on the specific type of the sulfur-containing silane coupling agent preparation device.

[0058] For example, the sulfur-containing silane coupling agent preparation equipment may include a sulfur-containing silane coupling agent preparation device and a control device that is communicatively connected to the sulfur-containing silane coupling agent preparation device. The sulfur-containing silane coupling agent preparation device may include a reactor (such as a reactor), a heating device (such as a heater), and an extraction device (such as a liquid-liquid extraction device). The reactor is used to accommodate the reactants for chemical reaction. The heating device is used to control the temperature in the reactor to ensure that the reaction can be carried out at a suitable temperature. The extraction device is used to separate the reaction product and the unreacted raw material to obtain a pure sulfur-containing silane coupling agent. The control device can heat the reactor containing the reactants with the heating device to obtain a primary product, and input it into the extraction device. The control device can separate and purify the primary product with the extraction device to obtain a pure sulfur-containing silane coupling agent finished product.

[0059] For example, the control device can be a single chip microcomputer, a mobile phone, a tablet computer, a notebook computer, an ultra-mobile personal computer (UMPC), a netbook, a desktop computer, a computing device or a computer connected to a wireless modem, a laptop computer, a handheld communication device, a handheld computing device, etc.

[0060] In order to better understand the method for preparing the sulfur-containing silane coupling agent provided in the embodiment of the present application, the specific implementation process of the method for preparing the sulfur-containing silane coupling agent provided in the embodiment of the present application is exemplarily introduced below.

[0061] Figure 1 A schematic flow chart of a method for preparing a sulfur-containing silane coupling agent provided in an embodiment of the present application is shown. The method for preparing a sulfur-containing silane coupling agent comprises:

[0062] S100, obtaining solution concentration information of a substance to be reacted.

[0063] It can be understood that the solution concentration information of the reactant may be the solution concentration information containing sulfur groups and silane groups.

[0064] For example, a spectrum analyzer (such as a spectrophotometer) can be used to calculate the concentration based on the absorbance of specific compounds (such as sulfide and silane groups) in the solution to be tested. The ion concentration of the solution of the reactant can also be calculated by measuring the conductivity of the solution, thereby obtaining the solution concentration information of the reactant.

[0065] By setting up in this way, by obtaining the solution concentration information of the reactant, the difference in human operation (for example, manual judgment of whether the current solution concentration of the reactant reaches the required concentration) can be reduced, thereby helping to reduce the impact of the operator's experience and judgment on the quality of the subsequently prepared sulfur-containing silane coupling agent.

[0066] S200, detecting that the trigger device performs a first trigger operation, wherein the trigger device is used to start a synthesis reaction of a sulfur-containing silane coupling agent.

[0067] It is understandable that the first trigger operation may be an operation of clicking or touching a button. The trigger device may be a button or a switch.

[0068] For example, when a button or a switch is used as a trigger device, the state change of the switch can be detected by a proximity sensor. When the button is pressed (the first trigger operation), the sensor can sense the state change of the switch.

[0069] With such arrangement, by detecting that the trigger device has executed the first trigger operation, the synthesis reaction of the sulfur-containing silane coupling agent can be automatically started, thereby greatly reducing manual participation, reducing human errors, and improving the consistency and repeatability of the operation, thereby helping to improve the quality of the subsequently prepared sulfur-containing silane coupling agent.

[0070] S300, detecting the temperature and pressure conditions of the current reaction system, wherein the temperature and pressure conditions are used to indicate whether the reaction is within the required reaction condition range.

[0071] It will be appreciated that the temperature-pressure conditions may include temperature conditions and pressure conditions.

[0072] For example, the temperature condition of the current reaction system can be detected by a temperature sensor or an infrared thermometer.

[0073] For example, the pressure condition of the current reaction system can be detected by a pressure sensor. The pressure condition of the current reaction system can be detected by a gas pressure gauge.

[0074] In this way, by detecting the temperature and pressure conditions of the current reaction system, it can be confirmed whether the reaction is under the desired reaction conditions, thereby helping to prevent the reactants from reacting under inappropriate conditions, thereby helping to improve the quality of the subsequently prepared sulfur-containing silane coupling agent.

[0075] S400 , based on the solution concentration information, the first trigger operation and the temperature and pressure conditions, a synthesis activity of the sulfur-containing silane coupling agent is performed to generate the sulfur-containing silane coupling agent.

[0076] It is understood that the solution concentration information can be analyzed to determine whether to perform a synthesis reaction (for example, the synthesis reaction is not performed when the concentration is lower than a certain concentration, and the synthesis reaction is started when the concentration is higher than a certain concentration). Determine whether the user has a synthesis reaction requirement, for example, when it is detected that the trigger device is triggered by the first trigger operation, it means that the user has a synthesis reaction requirement; otherwise, it means that the user does not have a synthesis reaction requirement. Set temperature and pressure conditions, for example, if the current temperature and pressure meet the requirements, the synthesis activity is allowed to be performed; otherwise, the synthesis activity is not allowed to be performed.

[0077] For example, when the solution concentration information of the reactant reflects that the current solution concentration reaches the preset concentration and it is detected that the trigger device is triggered by the first trigger operation, it means that the current reactant can react and the user has a synthetic reaction requirement, so the temperature and pressure conditions of the current reaction system can be detected. If the temperature and pressure conditions reflect that the current conditions meet the required conditions, the synthesis activity of the sulfur-containing silane coupling agent is performed to generate the sulfur-containing silane coupling agent.

[0078] In this way, based on the solution concentration information, the first trigger operation and the temperature and pressure conditions, the synthesis activity of the sulfur-containing silane coupling agent is performed to generate the sulfur-containing silane coupling agent. The solution concentration, the trigger operation and the temperature and pressure conditions can be comprehensively considered to accurately control the various parameters of the reaction so that the results of the reaction are within the expected quality standards, thereby helping to improve the quality of the prepared sulfur-containing silane coupling agent.

[0079] In a possible implementation, S400, based on the solution concentration information, the first trigger operation and the temperature and pressure conditions, performs a synthesis activity of the sulfur-containing silane coupling agent to generate the sulfur-containing silane coupling agent, including:

[0080] When the solution concentration information of the reactant reflects that the current solution concentration reaches the preset concentration and it is detected that the trigger device is triggered by the first trigger operation, the temperature and pressure conditions of the current reaction system are detected. If the temperature and pressure conditions reflect that the current conditions reach the required conditions, the synthesis activity of the sulfur-containing silane coupling agent is performed to generate the sulfur-containing silane coupling agent.

[0081] For example, when the solution concentration information of the reactant reflects that the current solution concentration reaches the preset concentration and it is detected that the trigger device is triggered by the first trigger operation, it means that the current reactant can react and the user has a synthetic reaction requirement, so the temperature and pressure conditions of the current reaction system can be detected. If the temperature and pressure conditions reflect that the current conditions meet the required conditions, the synthesis activity of the sulfur-containing silane coupling agent is performed to generate the sulfur-containing silane coupling agent.

[0082] For example, when the solution concentration information of the reactant reflects that the current solution concentration reaches the preset concentration, and it is detected that the trigger device is triggered by the first trigger operation, it means that the current reactant can react and the user has a synthetic reaction requirement, so the temperature and pressure conditions of the current reaction system can be detected. If the temperature and pressure conditions reflect that the current conditions do not meet the required conditions, the synthesis activity of the sulfur-containing silane coupling agent is not performed, and S100, S200 and S300 are continued.

[0083] With such a setting, the entire synthesis process can be automatically operated by using multiple data such as concentration information, trigger operation, temperature and pressure conditions as the basis for judgment, thereby eliminating the need for manual intervention by users and reducing human errors, which helps to improve the quality of the prepared sulfur-containing silane coupling agent.

[0084] In a possible implementation, the sulfur-containing silane coupling agent preparation equipment includes a sulfur-containing silane coupling agent preparation device, and a control device communicatively connected to the sulfur-containing silane coupling agent preparation device. The sulfur-containing silane coupling agent preparation method also includes:

[0085] S410, the control device monitors the preparation signal sent by the sulfur-containing silane coupling agent preparation device, wherein the preparation signal carries the mark and preparation data corresponding to the sulfur-containing silane coupling agent preparation device.

[0086] It can be understood that the preparation signal is used to inform the control device that the sulfur-containing silane coupling agent preparation device is in a preparation state. The mark can be the model of the device, the IP of the device, etc. The preparation data is used to indicate the current preparation status of the sulfur-containing silane coupling agent preparation device, for example, start, stop, test, calibration, etc.

[0087] For example, after the sulfur-containing silane coupling agent preparation device is started, a preparation relationship must be established between the reactor and the heating device (for example, a heating relationship between the heating device and the reactor), and the time for establishing the preparation relationship can be 20 seconds, 30 seconds, etc. After the reactor and the heating device establish the preparation relationship, the preparation data is interacted with the control device in the mode capable of controlling the preparation process. During the process of establishing the preparation relationship between the reactor and the heating device, a preparation signal can be sent to the control device.

[0088] Such a setting, through the synchronous operation of the reactor and the heating device, helps to avoid reaction instability caused by uneven heating or failure to meet reaction conditions. At the same time, the real-time transmission of the preparation signal can allow the control device to quickly know the current equipment status and progress, which helps to make timely decisions to adjust the reaction conditions.

[0089] S420, based on the mark corresponding to the sulfur-containing silane coupling agent preparation device, determine that the sulfur-containing silane coupling agent preparation device is a marked device, and based on the preparation data, determine that the sulfur-containing silane coupling agent preparation device is in a preparation state. The marked device is used to indicate a device that has created a preparation business with the control device in the past period. The preparation state is used to indicate that the preheating time of the sulfur-containing silane coupling agent preparation device after startup does not exceed the preset time.

[0090] For example, after obtaining the symbol corresponding to the sulfur-containing silane coupling agent preparation device, the symbol can be matched with the symbol in the preset symbol library. If it matches, it is determined that the sulfur-containing silane coupling agent preparation device is a marked device; otherwise, it is determined that the sulfur-containing silane coupling agent preparation device is not a marked device. The preset symbol library can be created by inputting symbols in advance.

[0091] For example, the preparation data is analyzed to determine whether the sulfur-containing silane coupling agent preparation device is in the preparation state, that is, the preheating time after startup does not exceed the preset time. If it is determined that the sulfur-containing silane coupling agent preparation device is in the preparation state, it means that the sulfur-containing silane coupling agent preparation device is likely to be creating a preparation business with the control device. The preparation business can be a business of preparing sulfur-containing silane coupling agents.

[0092] With such a setting, it is possible to automatically identify which devices have performed preparation work with the control device in the past, thereby allowing for more efficient management of the preparation equipment. Furthermore, with further real-time understanding of the status of the equipment, it is helpful to make subsequent decisions on adjusting the setting data of the preparation work in a timely manner, thereby reducing errors in human operations.

[0093] In a possible implementation, in step S420, after determining that the sulfur-containing silane coupling agent preparation device is a marking device based on the mark corresponding to the sulfur-containing silane coupling agent preparation device, and determining that the sulfur-containing silane coupling agent preparation device is in a preparation state based on the preparation data, the sulfur-containing silane coupling agent preparation method further includes:

[0094] The preparation information acquisition method in the preparation service setting data is changed to the first acquisition method. Alternatively, the current service importance in the preparation service setting data is changed to the first importance. The first importance is greater than the current service importance.

[0095] It can be understood that the preparation information acquisition method in the setting data of the preparation business may include method a (the time for acquiring two adjacent preparation information may be 60s), method b (the time for acquiring two adjacent preparation information may be 10s), etc. Therefore, the preparation information acquisition method in the setting data of the preparation business may be changed to method b, that is, the second acquisition method is changed to the first acquisition method. The business importance level in the setting data of the preparation business may include level x (allowing the action of creating the preparation business to be acquired later), level y (not allowing the action of creating the preparation business to be acquired later), etc. Therefore, the current business importance level in the setting data of the preparation business may be changed to level y, that is, the first importance level.

[0096] Such a setting can effectively reduce unnecessary waiting time in the preparation process, avoid missing the best preparation time, and ensure optimal product quality and output.

[0097] S430: The control device determines to change the setting data of the preparation service.

[0098] It can be understood that the setting data of the preparation service includes the time length for obtaining two adjacent preparation information. The longer the time length for obtaining two adjacent preparation information, the later the action of creating the preparation service is obtained, and the control device can enter the rest mode. The shorter the time length for obtaining two adjacent preparation information, the earlier the action of creating the preparation service is obtained, and the control device cannot enter the rest mode, and the required energy consumption will increase.

[0099] For example, a device that has not created a preparation service with the control device in the past may need to perform testing, calibration and other steps. Therefore, it is allowed to obtain the action of creating the preparation service later. However, a device that has created a preparation service with the control device in the past has completed testing, calibration and other steps. Therefore, if the action of creating the preparation service is obtained later, the best preparation time may be missed. For example, if the preheating time after startup exceeds the preset time before preparation is performed, the best preparation time will be missed. Therefore, the control device can change the duration of obtaining two adjacent preparation information (for example, shorten the duration), that is, change the setting data of the preparation service.

[0100] With such a setting, it can be decided whether to obtain the instruction to create the preparation business earlier according to the actual situation, so as to start the preparation process faster. On the one hand, it helps to avoid missing the best preparation time and ensure the best product quality and output. On the other hand, it helps to avoid obtaining the instruction to create the preparation business too early, which leads to increased energy consumption of the control device.

[0101] In a possible implementation, in step S410, after the control device monitors the preparation signal sent by the sulfur-containing silane coupling agent preparation device, the sulfur-containing silane coupling agent preparation method further includes:

[0102] When the control device monitors the preparation signal sent by the sulfur-containing silane coupling agent preparation device, the current tag is set to the first tag, wherein the first tag is used to indicate that the setting data of the preparation business can be changed.

[0103] It can be understood that the label can be a first label, a second label, etc. Different labels are used to indicate different changes in the setting data of the preparation service. The first label is used to indicate that the setting data of the preparation service can be changed. The second label is used to indicate that the setting data of the preparation service cannot be changed.

[0104] For example, after monitoring the preparation signal sent by the sulfur-containing silane coupling agent preparation device, the current tag can be parsed first, and whether the setting data of the preparation service can be changed can be determined according to the current tag. If it is determined that the setting data of the preparation service can be changed, steps S420 and S430 can be further executed; otherwise, the current process can be directly stopped.

[0105] This setup allows for greater clarity in decision execution, reduces incorrect decisions due to unclear status, and helps ensure optimal product quality and output.

[0106] In a possible implementation, in step S430, before the control device determines to change the setting data of the preparation service, the method for preparing the sulfur-containing silane coupling agent further includes:

[0107] In the case where the preparation instruction sent by the sulfur-containing silane coupling agent preparation device is obtained within the first time period, or in the case where the preparation instruction sent by the sulfur-containing silane coupling agent preparation device is not obtained within the first time period, the setting data of the current preparation business is changed to the previous setting data, and the current label is set to the second label. The second label is used to indicate that the setting data of the preparation business cannot be changed.

[0108] It can be understood that the first duration can be the duration for which the required setting data is allowed to be retained after the setting data of the preparation service is changed to the required setting data (for example, changed from the second acquisition method to the first acquisition method). For example, the first duration can be 10 seconds, 20 seconds, 30 seconds, etc. The preparation instruction can be an instruction requesting preparation.

[0109] For example, when the preparation instruction sent by the sulfur-containing silane coupling agent preparation device is obtained within the first time period, the action of creating the preparation business with the control device can be completed. At this time, in order to avoid the control device being in a non-resting mode all the time, the first acquisition method can be changed to the second acquisition method, that is, the setting data of the current preparation business is changed to the previous setting data.

[0110] For example, when a preparation instruction sent by a sulfur-containing silane coupling agent preparation device is obtained within the first time period, it means that there is currently no need to create a preparation business. At this time, in order to avoid the control device being in a non-resting mode all the time, the first acquisition method can be changed to the second acquisition method, that is, the setting data of the current preparation business is changed to the previous setting data.

[0111] This setting allows the setting data to be flexibly changed according to actual conditions, which helps to maintain the flexibility of the preparation process and thus meet the dynamic changes in production needs.

[0112] In a possible implementation, the method for preparing a sulfur-containing silane coupling agent further includes:

[0113] S500: Sending preparation process data of the sulfur-containing silane coupling agent to be prepared to a sulfur-containing silane coupling agent preparation device according to the preparation event.

[0114] It is understood that when a preparation event is identified or triggered, the preparation process data can be sent to the sulfur-containing silane coupling agent preparation device. The event can be detected by a sensor or manually selected by an operator. The preparation process data can include data such as raw material ratio, reaction temperature, reaction time, pressure, stirring speed, etc.

[0115] With this setup, the preparation process data is sent to the equipment in an automated manner, which reduces operator intervention and the possibility of human error.

[0116] S600, when the preparation state of the preparation event is obtained to be the artificially terminated preparation state, the mark corresponding to the preparation event is adjusted to the target mark, and a preset signal corresponding to the preparation event is generated. If a signal to continue the reaction is obtained within the preset time, the preset signal is discarded, and the preparation process data is continued to be sent to the sulfur-containing silane coupling agent preparation according to the preparation event. Among them, the target mark is the mark corresponding to the event when the sulfur-containing silane coupling agent preparation device is preparing. The preset signal is used to indicate that the mark corresponding to the preparation event is adjusted to the preset mark at the end of the preset time. The preset mark is the mark corresponding to the event when the sulfur-containing silane coupling agent preparation device is ready to prepare but has not yet prepared. The sulfur-containing silane coupling agent preparation device clears all events except the mark with the target mark.

[0117] It is understandable that the preset duration can be 1 minute, 2 minutes, 3 minutes, etc.

[0118] For example, the preparation status of a preparation event may change. For example, during the reaction process, the operator terminates certain operations, but the equipment still maintains monitoring and control, that is, the sign of the preparation event changes from the target sign to the preset sign. For another example, it is impossible to obtain the key parameters (such as temperature, pressure, flow rate, etc.) in the reaction process of the sulfur-containing silane coupling agent preparation device. When this problem is detected, certain operations are terminated, that is, the sign of the preparation event changes from the target sign to the preset sign. In the traditional preparation process, if the sign of the preparation event changes from the target sign to the preset sign, the preparation event may be cleared, but it is actually expected to continue to execute the preparation event, which will cause a delay in the preparation process.

[0119] For example, unknown factors may be encountered during the preparation process (for example, the preparation is stopped to add raw materials, or the preparation is stopped to check the preparation status under the current preparation process). At this time, the operator may stop certain operations (that is, the preparation status of the preparation event is obtained as the artificially stopped preparation status), so the mark of the preparation event changes from the target mark to the preset mark. In order to avoid the preparation event not being cleared, the mark corresponding to the preparation event can be adjusted to the target mark within the preset time, and the mark corresponding to the preparation event can be adjusted to the preset mark after the preset time, that is, the preset signal. If a signal to continue the reaction is obtained within the preset time (for example, a signal to resume the reaction sent by the operator) indicates that the unknown factors have been handled within the preset time, and it is actually expected to continue to execute the preparation event, then the preset signal is discarded. Therefore, even if the mark of the preparation event changes from the target mark to the preset mark, the preparation process data can continue to be sent to the sulfur-containing silane coupling agent preparation according to the preparation event.

[0120] Such a setting can monitor the state changes in the preparation process in real time, and adjust the operation strategy according to different situations to ensure the continuity and stability of the preparation and avoid problems that cause delays in the preparation process.

[0121] S700, when it is obtained that the preparation status of the preparation event is a non-artificially aborted preparation status, the mark corresponding to the preparation event is adjusted to the target mark, and a target signal corresponding to the preparation event is generated. If a signal for resuming the reaction is obtained within the target duration, the target signal is discarded, and the preparation process data is continuously sent to the preparation of the sulfur-containing silane coupling agent according to the preparation event. The target signal is used to indicate that the mark corresponding to the preparation event is adjusted to the preset mark at the end of the target duration.

[0122] It can be understood that during the preparation process, unknown factors may be encountered (for example, the sensor cannot feedback the parameter information during the reaction process to the control device). At this time, in order to avoid blind preparation, the system may automatically abort some operations (that is, it is obtained that the preparation status of the preparation event is a non-artificially aborted preparation status). Therefore, the mark of the preparation event changes from the target mark to the preset mark. In order to avoid the preparation event from being cleared, the mark corresponding to the preparation event can be adjusted to the target mark within the target duration, and the mark corresponding to the preparation event is adjusted to the preset mark, that is, the target signal, at the end of the target duration. If a signal for resuming the reaction is obtained within the target duration, it means that the unknown factors (that is, the sensor cannot feedback the parameter information during the reaction process to the control device) are processed within the preset duration, and it is actually expected to continue to execute the preparation event. Then, the target signal is discarded. Therefore, even when the mark of the preparation event changes from the target mark to the preset mark, the preparation process data can still be continuously sent to the preparation of the sulfur-containing silane coupling agent according to the preparation event.

[0123] With such a setting, it is possible to monitor the state changes during the preparation process in real time, adjust the operation strategy according to different situations, ensure the continuity and stability of the preparation, and avoid the problem of delaying the preparation process.

[0124] In a possible implementation manner, the artificially aborted preparation status is used to indicate that the operator actively triggers the operation of aborting the preparation, maintains the preparation connection with the sulfur-containing silane coupling agent preparation device, and does not continue to send the preparation process data to the sulfur-containing silane coupling agent preparation device.

[0125] It can be understood that maintaining the preparation connection with the sulfur-containing silane coupling agent preparation device may be that the operator aborts some operations during the reaction process, but the system still maintains the monitoring and control relationship of the reaction process.

[0126] For example, when the preparation state of the preparation event is obtained as an artificially terminated preparation state, the mark of the preparation event is changed from the target mark to the preset mark, but the preparation connection with the sulfur-containing silane coupling agent preparation device is still maintained, and the preparation process data is not continuously sent to the sulfur-containing silane coupling agent preparation device. For example, certain operations such as heating and pressurizing are terminated. At this time, the preparation process data related to temperature and pressure may not be sent.

[0127] Such a setting helps to quickly identify the status of events during the preparation process and provide data support for making corresponding decisions later.

[0128] In a possible implementation, the method for preparing a sulfur-containing silane coupling agent further includes:

[0129] When an operator's triggering operation to end the reaction is obtained within the preset time, or when a signal to continue the reaction is not obtained within the preset time, the mark corresponding to the preparation event is adjusted to the preset mark.

[0130] It can be understood that when the operator's triggering operation to end the reaction is obtained within the preset time, or when the signal to continue the reaction is not obtained within the preset time, it means that the operator wants to end the current preparation event (for example, a serious problem occurs during the reaction process), that is, the operator does not actually want to continue to execute the preparation event. Therefore, the mark corresponding to the preparation event is adjusted to the preset mark, and the preparation event will be cleared later.

[0131] This setting can be flexibly adjusted according to actual conditions to make the reaction process clear, that is, when the current preparation event is no longer considered valid, it will not be executed, thereby avoiding subsequent confusion or misunderstanding that may be caused by it, so as to improve the overall preparation efficiency.

[0132] In a possible implementation, the non-human suspension of preparation state is used to indicate that the operator did not actively trigger the suspension of preparation operation, did not maintain the preparation connection with the sulfur-containing silane coupling agent preparation device, and did not continue to send preparation process data to the sulfur-containing silane coupling agent preparation device.

[0133] It can be understood that failure to maintain the preparation connection with the sulfur-containing silane coupling agent preparation device may be due to the operator terminating certain operations during the reaction process, but the system still maintains the relationship of monitoring and controlling the reaction process, for example, parameter information during the reaction process cannot be obtained through sensors.

[0134] For example, when the preparation state of the preparation event is obtained as a non-artificially terminated preparation state, the mark of the preparation event is changed from the target mark to the preset mark, but the preparation connection with the sulfur-containing silane coupling agent preparation device is not maintained, and the preparation process data is not continued to be sent to the sulfur-containing silane coupling agent preparation device. For example, certain operations such as heating and pressurizing are terminated. At this time, since the parameter information in the reaction process cannot be obtained through the sensor, the preparation process data related to temperature and pressure cannot be sent.

[0135] Such a setting helps to quickly identify the status of events during the preparation process and provide data support for making corresponding decisions later.

[0136] In a possible implementation, the method for preparing a sulfur-containing silane coupling agent further includes:

[0137] When no signal of a recovery reaction is obtained within the target duration, the mark corresponding to the preparation event is adjusted to a preset mark.

[0138] It is understandable that if the signal of the recovery reaction is not obtained within the target time, it means that the parameter information of the reaction process cannot be obtained through the sensor. At this time, there is no need to continue the preparation event. Therefore, the mark corresponding to the preparation event can be adjusted to the preset mark. The preparation event will also be cleared later.

[0139] This setting can be flexibly adjusted according to actual conditions to make the reaction process clear, that is, when the current preparation event is no longer considered valid, it will not be executed, thereby avoiding subsequent confusion or misunderstanding that may be caused by it, so as to improve the overall preparation efficiency.

[0140] It should be understood that the size of the serial numbers of the steps in the above embodiments does not mean the order of execution. The execution order of each process should be determined by its function and internal logic, and should not constitute any limitation on the implementation process of the embodiments of the present application.

[0141] Corresponding to the method for preparing the sulfur-containing silane coupling agent described in the above embodiment, the embodiment of the present application further provides a system for preparing the sulfur-containing silane coupling agent, and each unit of the system can implement each step of the method for preparing the sulfur-containing silane coupling agent. Figure 5 The structural block diagram of the sulfur-containing silane coupling agent preparation system provided in the embodiment of the present application is shown. For the convenience of explanation, only the part related to the embodiment of the present application is shown.

[0142] Reference Figure 5 , the sulfur-containing silane coupling agent preparation system includes:

[0143] The acquisition unit is used to acquire the solution concentration information of the reactant.

[0144] The detection unit is used to detect that the trigger device performs a first trigger operation. The trigger device is used to start the synthesis reaction of the sulfur-containing silane coupling agent.

[0145] The monitoring unit is used to detect the temperature and pressure conditions of the current reaction system, wherein the temperature and pressure conditions are used to indicate whether the reaction is within the required reaction condition range.

[0146] The control unit is used to perform a synthesis activity of the sulfur-containing silane coupling agent based on the solution concentration information, the first trigger operation and the temperature and pressure conditions to generate the sulfur-containing silane coupling agent.

[0147] It should be noted that the information interaction, execution process, etc. between the above-mentioned systems / units are based on the same concept as the method embodiment of the present application. Their specific functions and technical effects can be found in the method embodiment part and will not be repeated here.

[0148] Those skilled in the art can clearly understand that, for the convenience and simplicity of description, only the division of the above-mentioned functional units is used as an example for illustration. In practical applications, the above-mentioned functions can be assigned to different functional units as needed, that is, the internal structure of the system can be divided into different functional units to complete all or part of the functions described above. The functional units in the embodiment can be integrated into a processing unit, or each unit can exist physically separately, or two or more units can be integrated into one unit. The above-mentioned integrated unit can be implemented in the form of hardware or in the form of software functional units. In addition, the specific names of the functional units are only for the convenience of distinguishing each other, and are not used to limit the scope of protection of this application. The specific working process of the units in the above-mentioned system can refer to the corresponding process in the aforementioned method embodiment, which will not be repeated here.

[0149] The present application also provides a sulfur-containing silane coupling agent preparation device, Figure 5 This is a schematic diagram of the structure of a sulfur-containing silane coupling agent preparation device provided in one embodiment of the present application. Figure 5 As shown, the sulfur-containing silane coupling agent preparation device 6 of this embodiment includes: at least one processor 60 ( Figure 5 Only one is shown), at least one memory 61 ( Figure 5 Only one is shown in the figure) and a computer program 62 stored in the at least one memory 61 and executable on the at least one processor 60. When the processor 60 executes the computer program 62, the sulfur-containing silane coupling agent preparation device 6 implements the steps in any of the above-mentioned sulfur-containing silane coupling agent preparation method embodiments, or the sulfur-containing silane coupling agent preparation device 6 implements the functions of each unit in the above-mentioned system embodiments.

[0150] Exemplarily, the computer program 62 may be divided into one or more units, which are stored in the memory 61 and executed by the processor 60 to complete the present application. The one or more units may be a series of computer program instruction segments capable of completing specific functions, which are used to describe the execution process of the computer program 62 in the sulfur-containing silane coupling agent preparation device 6.

[0151] The sulfur-containing silane coupling agent preparation equipment 6 may include a sulfur-containing silane coupling agent preparation device and a control device that is communicatively connected to the sulfur-containing silane coupling agent preparation device. The sulfur-containing silane coupling agent preparation device may include a reactor (such as a reactor), a heating device (such as a heater) and an extraction device (such as a liquid-liquid extraction device). The reactor is used to accommodate the reactants for chemical reaction. The heating device is used to control the temperature in the reactor to ensure that the reaction can be carried out at an appropriate temperature. The extraction device is used to separate the reaction products and unreacted raw materials to obtain pure sulfur-containing silane coupling agent. The control device may heat the reactor accommodating the reactants with a heating device to obtain a preliminary product and input it into the extraction device. The control device may separate and purify the preliminary product with an extraction device to obtain a pure sulfur-containing silane coupling agent finished product. The sulfur-containing silane coupling agent preparation equipment 6 may include, but is not limited to, a processor 60 and a memory 61. Those skilled in the art will understand that Figure 5 This is only an example of the sulfur-containing silane coupling agent preparation device 6 and does not constitute a limitation on the sulfur-containing silane coupling agent preparation device 6. It may include more or fewer components than shown in the figure, or a combination of certain components, or different components, for example, it may also include input and output devices, network access devices, buses, etc.

[0152] The processor 60 may be a central processing unit (CPU), or other general-purpose processors, digital signal processors (DSP), application-specific integrated circuits (ASIC), field-programmable gate arrays (FPGA) or other programmable logic devices, discrete gate or transistor logic devices, discrete hardware components, etc. A general-purpose processor may be a microprocessor or any conventional processor, etc.

[0153] In some embodiments, the memory 61 may be an internal storage unit of the sulfur-containing silane coupling agent preparation device 6, such as a hard disk or memory of the sulfur-containing silane coupling agent preparation device 6. In other embodiments, the memory 61 may also be an external storage device of the sulfur-containing silane coupling agent preparation device 6, such as a plug-in hard disk, a smart memory card (Smart Media Card, SMC), a secure digital (Secure Digital, SD) card, a flash card (Flash Card), etc. equipped on the sulfur-containing silane coupling agent preparation device 6. Further, the memory 61 may also include both the internal storage unit of the sulfur-containing silane coupling agent preparation device 6 and an external storage device. The memory 61 is used to store an operating system, an application program, a boot loader (BootLoader), data, and other programs, such as the program code of the computer program, etc. The memory 61 may also be used to temporarily store data that has been output or is to be output.

[0154] An embodiment of the present application further provides a computer-readable storage medium, wherein the computer-readable storage medium stores a computer program, and when the computer program is executed by a processor, the steps in any of the above method embodiments are implemented.

[0155] An embodiment of the present application provides a computer program product. When the computer program product is run on a sulfur-containing silane coupling agent preparation device, the sulfur-containing silane coupling agent preparation device implements the steps in any of the above method embodiments.

[0156] If the integrated unit is implemented in the form of a software functional unit and sold or used as an independent product, it can be stored in a computer-readable storage medium. Based on this understanding, the present application implements all or part of the process in the above-mentioned embodiment method, which can be completed by instructing the relevant hardware through a computer program, and the computer program can be stored in a computer-readable storage medium, and the computer program can implement the steps of the above-mentioned various method embodiments when executed by the processor. Among them, the computer program includes a computer program code, and the computer program code can be in source code form, object code form, executable file or some intermediate form. The computer-readable medium may at least include: any entity or device capable of carrying the computer program code to the sulfur-containing silane coupling agent preparation device, a recording medium, a computer memory, a read-only memory (ROM, Read-Only Memory), a random access memory (RAM, RandomAccess Memory), an electric carrier signal, a telecommunication signal, and a software distribution medium. For example, a USB flash drive, a mobile hard disk, a magnetic disk or an optical disk.

[0157] In the above embodiments, the description of each embodiment has its own emphasis. For parts that are not described or recorded in detail in a certain embodiment, reference can be made to the relevant descriptions of other embodiments.

[0158] Those of ordinary skill in the art will appreciate that the units and algorithm steps of each example described in conjunction with the embodiments disclosed herein can be implemented in electronic hardware, or a combination of computer software and electronic hardware. Whether these functions are performed in hardware or software depends on the specific application and design constraints of the technical solution. Professional and technical personnel can use different methods to implement the described functions for each specific application, but such implementation should not be considered to be beyond the scope of this application.

[0159] In the embodiments provided in the present application, it should be understood that the disclosed sulfur-containing silane coupling agent preparation equipment, sulfur-containing silane coupling agent preparation system and sulfur-containing silane coupling agent preparation method can be implemented in other ways. For example, the above-described sulfur-containing silane coupling agent preparation equipment and sulfur-containing silane coupling agent preparation system embodiments are only schematic. For example, the division of the units is only a logical function division. There may be other division methods in actual implementation, such as multiple units or components can be combined or integrated into another system, or some features can be ignored or not executed. Another point is that the mutual coupling or direct coupling or communication connection shown or discussed can be an indirect coupling or communication connection through some interfaces, devices or units, which can be electrical, mechanical or other forms.

[0160] The units described as separate components may or may not be physically separated, and the components shown as units may or may not be physical units, that is, they may be located in one place or distributed on multiple network units. Some or all of the units may be selected according to actual needs to achieve the purpose of the solution of this embodiment.

[0161] The embodiments described above are only used to illustrate the technical solutions of the present application, rather than to limit them. Although the present application has been described in detail with reference to the aforementioned embodiments, a person skilled in the art should understand that the technical solutions described in the aforementioned embodiments may still be modified, or some of the technical features may be replaced by equivalents. Such modifications or replacements do not deviate the essence of the corresponding technical solutions from the spirit and scope of the technical solutions of the embodiments of the present application, and should all be included in the protection scope of the present application.

Claims

1. A method for preparing a sulfur-containing silane coupling agent, characterized in that: The method comprises: Obtaining solution concentration information of a substance to be reacted; Detecting that the trigger device performs a first trigger operation; wherein the trigger device is used to start a synthesis reaction of a sulfur-containing silane coupling agent; Detecting the temperature and pressure conditions of the current reaction system; wherein the temperature and pressure conditions are used to indicate whether the reaction is within the required reaction condition range; Based on the solution concentration information, the first trigger operation and the temperature and pressure conditions, a synthesis activity of the sulfur-containing silane coupling agent is performed to generate the sulfur-containing silane coupling agent.

2. The method for preparing a sulfur-containing silane coupling agent according to claim 1, wherein: Based on the solution concentration information, the first trigger operation and the temperature and pressure conditions, performing a synthesis activity of the sulfur-containing silane coupling agent to generate the sulfur-containing silane coupling agent includes: When the solution concentration information of the reactant reflects that the current solution concentration reaches the preset concentration and it is detected that the trigger device has executed the first trigger operation, the temperature and pressure conditions of the current reaction system are detected. If the temperature and pressure conditions reflect that the current conditions meet the required conditions, the synthesis activity of the sulfur-containing silane coupling agent is performed to generate the sulfur-containing silane coupling agent.

3. The method for preparing a sulfur-containing silane coupling agent according to claim 1, characterized in that: The sulfur-containing silane coupling agent preparation equipment includes a sulfur-containing silane coupling agent preparation device, and a control device that is communicatively connected to the sulfur-containing silane coupling agent preparation device. The method further includes: The control device monitors the preparation signal sent by the sulfur-containing silane coupling agent preparation device; wherein the preparation signal carries the mark and preparation data corresponding to the sulfur-containing silane coupling agent preparation device; Based on the mark corresponding to the sulfur-containing silane coupling agent preparation device, the sulfur-containing silane coupling agent preparation device is determined to be a marking device, and based on the preparation data, the sulfur-containing silane coupling agent preparation device is determined to be in a preparation state; wherein the marking device is used to indicate a device that has created a preparation business with the control device in the past period; and the preparation state is used to indicate that the preheating time of the sulfur-containing silane coupling agent preparation device after startup does not exceed a preset time; The control device determines to change the setting data of the preparation service.

4. The method for preparing a sulfur-containing silane coupling agent according to claim 3, characterized in that: After determining that the sulfur-containing silane coupling agent preparation device is a marking device based on the mark corresponding to the sulfur-containing silane coupling agent preparation device, and determining that the sulfur-containing silane coupling agent preparation device is in a preparation state based on the preparation data, the method further includes: The preparation information acquisition method in the setting data of the preparation business is changed to the first acquisition method; or, the current business importance in the setting data of the preparation business is changed to the first importance; wherein the first importance is greater than the current business importance.

5. The method for preparing a sulfur-containing silane coupling agent according to claim 3, characterized in that: After the control device monitors the preparation signal sent by the sulfur-containing silane coupling agent preparation device, the method further includes: When the control device monitors the preparation signal sent by the sulfur-containing silane coupling agent preparation device, the current tag is set to the first tag; wherein the first tag is used to indicate that the setting data of the preparation service can be changed.

6. The method for preparing a sulfur-containing silane coupling agent according to claim 3, characterized in that: After the control device determines to change the setting data of the preparation service, the method further includes: In the case where the preparation instruction sent by the sulfur-containing silane coupling agent preparation device is obtained within the first time period, or in the case where the preparation instruction sent by the sulfur-containing silane coupling agent preparation device is not obtained within the first time period, the setting data of the current preparation business is changed to the previous setting data, and the current label is set to the second label; wherein the second label is used to indicate that the setting data of the preparation business cannot be changed.

7. The method for preparing a sulfur-containing silane coupling agent according to claim 1, characterized in that: The method further comprises: Sending preparation process data of the sulfur-containing silane coupling agent to be prepared to the sulfur-containing silane coupling agent preparation device according to the preparation event; In the case where the preparation state of the preparation event is obtained to be an artificially terminated preparation state, the mark corresponding to the preparation event is adjusted to the target mark, and a preset signal corresponding to the preparation event is generated; if a signal for continuing the reaction is obtained within a preset time, the preset signal is discarded, and the preparation process data is continued to be sent to the sulfur-containing silane coupling agent preparation according to the preparation event; wherein the target mark is the mark corresponding to the event when the sulfur-containing silane coupling agent preparation device is preparing; the preset signal is used to indicate that at the end of the preset time, the mark corresponding to the preparation event is adjusted to the preset mark, the preset mark is the mark corresponding to the event when the sulfur-containing silane coupling agent preparation device is ready to prepare but has not yet prepared, and the sulfur-containing silane coupling agent preparation device clears all events except the mark with the target mark; In the case where the preparation state of the preparation event is obtained to be a non-artificially terminated preparation state, the mark corresponding to the preparation event is adjusted to the target mark, and a target signal corresponding to the preparation event is generated; if a signal of a recovery reaction is obtained within a target time length, the target signal is discarded, and the preparation process data continues to be sent to the sulfur-containing silane coupling agent preparation according to the preparation event; wherein the target signal is used to indicate that the mark corresponding to the preparation event is adjusted to a preset mark at the end of the target time length.

8. The method for preparing a sulfur-containing silane coupling agent according to claim 7, characterized in that: The artificial suspension of preparation state is used to indicate that the operator actively triggers the suspension of preparation operation, maintains the preparation connection with the sulfur-containing silane coupling agent preparation device, and does not continue to send the preparation process data to the sulfur-containing silane coupling agent preparation device.

9. The method for preparing a sulfur-containing silane coupling agent according to claim 7, characterized in that: The method further comprises: When an operator's triggering operation to end the reaction is obtained within the preset time, or when no signal to continue the reaction is obtained within the preset time, the mark corresponding to the preparation event is adjusted to the preset mark.

10. The method for preparing a sulfur-containing silane coupling agent according to claim 7, characterized in that: The non-artificial suspension of preparation state is used to indicate that the operator has not actively triggered the suspension of preparation operation, has not maintained the preparation connection with the sulfur-containing silane coupling agent preparation device, and has not continued to send the preparation process data to the sulfur-containing silane coupling agent preparation device; The method further comprises: When no signal of a recovery reaction is obtained within the target time period, the mark corresponding to the preparation event is adjusted to the preset mark.

Images