Powerful moisturizing cream and preparation method thereof

Abstract

The invention discloses a powerful moisturizing cream. The invention discloses a moisturizing hand cream, which is prepared from the following raw materials in percentage by weight: 0.2 to 0.4 percent of carbomer, 9 to 10 percent of humectant, 0.1 to 0.2 percent of chlorphenesin, 0.8 to 1 percent of silicon dioxide, 1.5 to 2 percent of sorbitan olivate, 2 to 2.5 percent of cetostearyl alcohol olivate, 0.8 to 1.2 percent of cetostearyl alcohol, 0.4 to 0.6 percent of potassium cetyl phosphate, 16 to 18 percent of grease, 0.4 to 0.6 percent of tocopheryl acetate, 0.3 to 0.5 percent of arginine, 0.01 to 0.03 percent of lactobionic acid, 0.6 to 0.8 percent of additive-free concept preservative and the balance of water. 2-2.5% of a moisturizing additive, 0.05-0.1% of a synergistic additive, and the balance of water. According to the present invention, the excellent use feeling such as good moisturizing degree, no greasiness and no oily gloss can be achieved.

Description

Technical Field

[0001] The present invention belongs to the field of skin care products, and particularly relates to a powerful moisturizing cream and a preparation method thereof. Background Art

[0002] At present, the moisturizing effect of products on the market is not persistent. For products with slightly better moisturizing effect, they have a sticky feeling in use, a strong oily feeling on the face, and the situation of oiliness appears, resulting in a poor experience. Summary of the Invention

[0003] The purpose of the present invention is to provide a toner that can clean facial skin and moisturize facial skin.

[0004] To achieve the above purpose, the present invention adopts the following technical solutions: A powerful moisturizing cream, which comprises the following raw materials in weight percentages: Carbomer 0.2 - 0.4%, humectant 9 - 10%, Chlorphenesin 0.1 - 0.2%, silica 0.8 - 1%, Sorbitan Oleate 1.5 - 2%, Cetearyl Olivate 2 - 2.5%, Cetearyl Alcohol 0.8 - 1.2%, Potassium Cetyl Phosphate 0.4 - 0.6%, oil 16 - 18%, Tocopheryl Acetate 0.4 - 0.6%, Arginine 0.3 - 0.5%, Lactobionic Acid 0.01 - 0.03%, additive-free concept preservative 0.6 - 0.8%, moisturizing additive 2 - 2.5%, synergistic additive 0.05 - 0.1%, and the balance is water.

[0005] The oil is composed of a mixture of olive oil, squalane, Caprylic / Capric Triglyceride, shea butter, and jojoba oil in a weight ratio of 1 - 3:4 - 6:4 - 6:5 - 7:1 - 2.

[0006] The humectant is composed of a mixture of glycerin, propylene glycol, and sodium hyaluronate in a weight ratio of 5 - 7:2 - 4:0.1 - 0.2.

[0007] The additive-free concept preservative is composed of the following raw materials in weight percentages: Octanoyl Hydroxamic Acid 7%, 1,2 - Hexanediol 5%, Propylene Glycol 83%, and Ethylhexylglycerin 5%.

[0008] The moisturizing additive is composed of a mixture of Tremella fuciformis Berk. fruit body extract and soluble proteoglycan in a weight ratio of 0.1:2 - 3.

[0009] The synergistic additive is Pseudopimpinella anisum extract.

[0010] The preparation method of the eryngium foetidum extract is as follows: Take the whole herb of eryngium foetidum, wash it and dry it in the sun, add acetic acid aqueous solution with a concentration of 0.5-1 mol / L, grind it, add it to the enzymatic hydrolysis solution, carry out enzymatic hydrolysis fermentation at 35-40 °C for 9-10 hours, sterilize and inactivate enzymes at high temperature, filter with a microporous filter membrane, concentrate the filtrate, dry it, and pulverize it to obtain the product.

[0011] The dosage of the acetic acid aqueous solution is 5-10% of the weight of the whole herb of eryngium foetidum.

[0012] The enzyme in the enzymatic hydrolysis solution is a mixture of cellulase and β-glucanase with a weight ratio of 10:0.8-1.

[0013] A preparation method of a powerful moisturizing cream includes the following steps: (1) Mix water, carbomer, moisturizer, chlorphenesin, and silica, add them to an emulsifying pot, stir and heat to 80-90 °C, and keep warm for 25-40 minutes; (2) Add sorbitan oleate, cetearyl olivate, cetearyl alcohol, potassium cetyl phosphate, oil, and tocopheryl acetate to an oil phase pot, stir and heat to 85-90 °C, and keep warm for 16-20 minutes.

[0014] (3) Under the stirring state of the emulsifying pot, pump the mixture in the oil phase pot into the emulsifying pot, turn on the homogenizer for homogenization for 4-5 minutes, and then keep warm and stir at 80-90 °C for 20-30 minutes; (4) Cool down to 60-65 °C, add arginine, and stir for 4-7 minutes.

[0015] (5) Cool down to 40-45 °C, add synergistic additives, lactic acid, additive-free concept preservative, and moisturizing additives, and stir for 10-20 minutes; (6) Cool down to 36-38 °C, discharge the material, fill and package it after passing the inspection, and store the finished product in the warehouse.

[0016] Eryngium foetidum, a perennial herb with a special aroma, grows on fertile and moist land such as the edge of forests, roadsides, slopes, and open fields. It is distributed in Guangdong, Guangxi, Hainan, Yunnan and other places. According to the records in the "Manual of Commonly Used Chinese Herbal Medicines" of the Guangzhou Military Region, it has the effects of dispelling wind and removing heat, and promoting digestion with its fragrance. It is widely sourced in the Guangzhou area. After experiments, adding its enzymatically hydrolyzed product to skin care products can achieve a moisturizing effect; The present invention enhances the moisturizing effect on the skin by selecting plant oils that are moisturizing and skin-friendly, as well as strong moisturizing ingredients such as glycerin, sodium hyaluronate, soluble proteoglycan, and Tremella fuciformis extract. Moreover, the skin-friendly plant oils can reduce the floating of oil on the skin surface, thereby avoiding a shiny face. By compounding squalane and caprylic / capric triglyceride with a refreshing skin feel, the experience of the cream is enhanced. The addition of silica can also effectively reduce the oiliness of the skin, enabling the product to achieve an excellent use feeling with good humidity retention, no greasiness, and no oil shine.

[0017] Figures 1-3 It is the record of the moisturizing efficacy test of the product in Example 1 of the present invention; Figures 4-6 It is the record of the basic performance test of the product in Example 1 of the present invention. Detailed implementation method

[0018] Example 1 A powerful moisturizing cream, which comprises the following raw materials in percentage by weight: Carbomer 0.2%, moisturizer 9%, chlorphenesin 0.1%, silica 0.8%, sorbitan oleate 1.5%, cetearyl olivate 2%, cetearyl alcohol 0.8%, potassium cetyl phosphate 0.4%, oil 16%, tocopheryl acetate 0.4%, arginine 0.3%, lactic acid 0.01%, additive-free concept preservative 0.6%, moisturizing additive 2%, synergistic additive 0.05%, and the balance is water.

[0019] The oil is composed of a mixture of olive oil, squalane, caprylic / capric triglyceride, shea butter, and jojoba oil in a weight ratio of 1:4:4:5:1.

[0020] The moisturizer is composed of a mixture of glycerin, propylene glycol, and sodium hyaluronate in a weight ratio of 5:2:0.1.

[0021] The additive-free concept preservative is composed of the following raw materials in percentage by weight: octanoyl hydroxamic acid 7%, 1,2-hexanediol 5%, propylene glycol 83%, and ethylhexylglycerin 5%.

[0022] The moisturizing additive is composed of a mixture of Tremella fuciformis fruiting body extract and soluble proteoglycan in a weight ratio of 0.1:2.

[0023] The synergistic additive is Eryngium foetidum extract.

[0024] The preparation method of the Eryngium foetidum extract is as follows: Take the whole herb of Eryngium foetidum, wash and dry it in the sun, add 0.5 mol / l acetic acid aqueous solution, grind it, add it to the enzymatic hydrolysis solution, carry out enzymatic hydrolysis fermentation at 35 °C for 9 hours, sterilize and inactivate the enzyme at high temperature, filter with a microporous membrane, concentrate the filtrate, dry it, and pulverize it to obtain the extract.

[0025] The dosage of the aqueous acetic acid solution is 5% of the weight of the whole plant of *Eryngium foetidum*.

[0026] The enzyme in the enzymolysis solution is a mixture of cellulase and β-glucanase with a weight ratio of 10:0.8.

[0027] A method for preparing a powerful moisturizing cream, comprising the following steps: (1) Mix water, carbomer, moisturizer, chlorphenesin, and silica, add them to an emulsifying pot, stir and heat to 80 °C, and keep warm for 25 minutes; (2) Add sorbitan oleate, cetearyl olivate, cetearyl alcohol, potassium cetyl phosphate, oil, and tocopheryl acetate to an oil phase pot, stir and heat to 85 °C, and keep warm for 16 minutes.

[0028] (3) Under the stirring state of the emulsifying pot, pump the mixture in the oil phase pot into the emulsifying pot, turn on the homogenizer for homogenization for 4 minutes, and then keep stirring at 80 °C for 20 minutes; (4) Cool down to 60 °C, add arginine, and stir for 4 minutes; (5) Cool down to 40 °C, add synergistic additive, lactic acid, additive-free concept preservative, and moisturizing additive, and stir for 10 minutes; (6) Cool down to 36 °C, discharge the material, fill and package it after passing the inspection, and store the finished product in the warehouse. Example

[0029] A powerful moisturizing cream, which comprises the following raw materials in the following weight percentages: Carbomer 0.4%, moisturizer 10%, chlorphenesin 0.2%, silica 1%, sorbitan oleate 2%, cetearyl olivate 2.5%, cetearyl alcohol 1.2%, potassium cetyl phosphate 0.6%, oil 18%, tocopheryl acetate 0.6%, arginine 0.5%, lactic acid 0.03%, additive-free concept preservative 0.8%, moisturizing additive 2.5%, synergistic additive 0.1%, and the balance is water.

[0030] The oil is composed of a mixture of olive oil, squalane, caprylic / capric triglyceride, shea butter, and jojoba oil with a weight ratio of 3:6:6:7:2.

[0031] The moisturizer is composed of a mixture of glycerol, propylene glycol, and sodium hyaluronate with a weight ratio of 7:4:0.2.

[0032] The additive-free concept preservative is composed of the following raw materials in weight percentages: octanoyl hydroxamic acid 7%, 1,2-hexanediol 5%, propylene glycol 83%, and ethylhexylglycerin 5%.

[0033] The moisturizing additive is composed of tremella fruiting body extract and soluble proteoglycan in a weight ratio of 0.1:3.

[0034] The synergistic additive is false coriander extract.

[0035] The preparation method of the false coriander extract solution is as follows: Take the whole herb of false coriander, wash it, dry it in the sun, add 1 mol / l acetic acid aqueous solution, grind it, add it to the enzymatic hydrolysis solution, carry out enzymatic hydrolysis fermentation at 40 °C for 10 hours, sterilize and inactivate enzymes at high temperature, filter with a microporous membrane, concentrate the filtrate, dry it, and pulverize it to obtain.

[0036] The dosage of the acetic acid aqueous solution is 10% of the weight of the whole herb of false coriander.

[0037] The enzyme in the enzymatic hydrolysis solution is a mixture of cellulase and β-glucanase in a weight ratio of 10:1.

[0038] A preparation method of a powerful moisturizing cream includes the following steps: (1) Mix water, carbomer, moisturizer, chlorphenesin, and silica, add them to an emulsifying pot, stir and heat to 90 °C, and keep warm for 40 minutes; (2) Add sorbitan oleate, cetearyl olivate, cetearyl alcohol, potassium cetyl phosphate, oil, and tocopheryl acetate to an oil phase pot, stir and heat to 90 °C, and keep warm for 20 minutes.

[0039] (3) Under the stirring state of the emulsifying pot, pump the mixture in the oil phase pot into the emulsifying pot, turn on the homogenizer for homogenization for 5 minutes, and then keep warm and stir at 90 °C for 30 minutes; (4) Cool down to 65 °C, add arginine, and stir for 7 minutes; (5) Cool down to 45 °C, add the synergistic additive, lactic acid, no-additive concept preservative, and moisturizing additive, and stir for 20 minutes; (6) Cool down to 38 °C, discharge the material, fill and package it after passing the inspection, and store the finished product in the warehouse. Example

[0040] A powerful moisturizing cream, which includes the following raw materials in the following weight percentages: Carbomer 0.3%, moisturizer 9%, chlorphenesin 0.15%, silica 0.9%, sorbitan oleate 1.7%, cetearyl olivate 2%, cetearyl alcohol 1%, potassium cetyl phosphate 0.5%, oil 17%, tocopheryl acetate 0.5%, arginine 0.4%, lactic acid 0.02%, no-additive concept preservative 0.7%, moisturizing additive 2%, synergistic additive 0.06%, and the rest is water.

[0041] The oil and fat is composed of a mixture of olive oil, squalane, caprylic / capric triglyceride, shea butter, and jojoba oil with a weight ratio of 2:5:5:6:1.

[0042] The moisturizer is composed of a mixture of glycerol, propylene glycol, and sodium hyaluronate with a weight ratio of 6:3:0.15.

[0043] The additive-free concept preservative is composed of the following raw materials by weight percentage: 7% of octanoyl hydroxamic acid, 5% of 1,2-hexanediol, 83% of propylene glycol, and 5% of ethylhexylglycerin.

[0044] The moisturizing additive is composed of a mixture of tremella fruiting body extract and soluble proteoglycan with a weight ratio of 0.1:2.5.

[0045] The synergistic additive is the extract of eryngium foetidum.

[0046] The preparation method of the eryngium foetidum extract is as follows: Take the whole herb of eryngium foetidum, wash it, dry it in the sun, add 0.6 mol / l acetic acid aqueous solution, grind it, add it to the enzymatic hydrolysis solution, carry out enzymatic hydrolysis fermentation at 35 °C for 9 hours, sterilize and inactivate the enzyme at high temperature, filter it with a microporous filter membrane, concentrate the filtrate, dry it, and pulverize it to obtain the product.

[0047] The dosage of the acetic acid aqueous solution is 8% of the weight of the whole herb of eryngium foetidum.

[0048] The enzyme in the enzymatic hydrolysis solution is a mixture of cellulase and β-glucanase with a weight ratio of 10:0.9.

[0049] A preparation method of a powerful moisturizing cream includes the following steps: (1) Mix water, carbomer, moisturizer, chlorphenesin, and silica, add them to an emulsifying pot, stir and heat to 85 °C, and keep warm for 30 minutes; (2) Add sorbitan oleate, cetearyl olivate, cetearyl alcohol, potassium cetyl phosphate, oil and fat, and tocopheryl acetate to an oil phase pot, stir and heat to 85 °C, and keep warm for 16 minutes.

[0050] (3) Under the stirring state of the emulsifying pot, pump the mixture in the oil phase pot into the emulsifying pot, turn on the homogenizer for homogenization for 4 minutes, and then keep stirring and warming at 85 °C for 25 minutes; (4) Cool down to 60 °C, add arginine, and stir for 4 - 7 minutes.

[0051] (5) Cool down to 40 °C, add the synergistic additive, lactic acid, additive-free concept preservative, and moisturizing additive, and stir for 15 minutes; (6) Cool down to 37 °C, discharge the material, fill and package it after passing the inspection, and store the finished product in the warehouse.

[0052] Comparative Example 1: A strong moisturizing cream (without synergistic additives), which comprises the following raw materials in weight percentages: Carbomer 0.3%, humectant 9%, chlorphenesin 0.15%, silica 0.9%, sorbitan oleate 1.7%, cetyl stearyl olivate 2%, cetyl stearyl alcohol 1%, potassium cetyl phosphate 0.5%, oil 17%, tocopheryl acetate 0.5%, arginine 0.4%, lactic acid 0.02%, additive-free concept preservative 0.7%, moisturizing additive 2%, and the balance is water. The preparation method is the same as that of Example 3, without adding synergistic additives.

[0053] Performance Test 1: Detection basis: QTC-C-LAB-TOP-042 "In Vitro Test Method for Moisturizing Efficacy of Cosmetics (Weighing Method)", Method 1 Breathable Tape Method; Detection method: Weigh the sample of Example 3 of the present invention on a glass plate covered with medical breathable tape (accurate to 0.1 mg), apply it evenly, use the product of Comparative Example 1 as a control sample, place the two samples in an environment with a temperature of (22 ± 2) °C and a humidity of (50 ± 10)%, weigh and record the data at regular intervals, and calculate the moisturizing rate;

[0054] As can be seen from the attached Figures 1-3 It can be seen that the product of the present invention has a good moisturizing effect compared with traditional moisturizing products. At the same time, it can be seen from Performance Test 1 that adding synergistic additives will have a better moisturizing effect.

Claims

1. A powerful moisturizing cream, characterized in that, It comprises the following raw materials in the following weight percentages: Carbomer 0.2 - 0.4%, humectant 9 - 10%, chlorphenesin 0.1 - 0.2%, silica 0.8 - 1%, sorbitan oleate 1.5 - 2%, cetearyl olivate 2 - 2.5%, cetearyl alcohol 0.8 - 1.2%, potassium cetyl phosphate 0.4 - 0.6%, oil 16 - 18%, tocopheryl acetate 0.4 - 0.6%, arginine 0.3 - 0.5%, lactic acid 0.01 - 0.03%, additive - free concept preservative 0.6 - 0.8%, moisturizing additive 2 - 2.5%, synergistic additive 0.05 - 0.1%, and the balance is water.

2. The super moisturizing cream according to claim 1, characterized in that The oil is composed of a mixture of olive oil, squalane, caprylic / capric triglyceride, shea butter, and jojoba oil with a weight ratio of 1 - 3:4 - 6:4 - 6:5 - 7:1 - 2.

3. The super moisturizing cream according to claim 1, characterized in that, The humectant is composed of a mixture of glycerol, propylene glycol, and sodium hyaluronate with a weight ratio of 5 - 7:2 - 4:0.1 - 0.

2.

4. A powerful moisturizing cream according to claim 1, characterized in that, The additive - free concept preservative is composed of the following raw materials in weight percentages: octanoyl hydroxamic acid 7%, 1,2 - hexanediol 5%, propylene glycol 83%, and ethylhexylglycerin 5%.

5. A strong moisturizing cream according to claim 1, characterized in that, The moisturizing additive is composed of a mixture of tremella fruiting body extract and soluble proteoglycan with a weight ratio of 0.1:2 - 3.

6. A powerful moisturizing cream according to claim 1, characterized in that, The synergistic additive is Pseudopimpinella anisum extract.

7. The super moisturizing cream according to claim 6, characterized in that, The preparation method of the Pseudopimpinella anisum extract solution is as follows: Take the whole herb of Pseudopimpinella anisum, wash it and dry it in the sun, add 0.5 - 1 mol / l acetic acid aqueous solution, grind it, add it to the enzymatic hydrolysis solution, carry out enzymatic hydrolysis fermentation at 35 - 40 °C for 9 - 10 hours, perform high - temperature sterilization and inactivation of enzymes, filter with a microporous membrane, concentrate the filtrate, dry it, and pulverize it to obtain the product.

8. A powerful moisturizing cream according to claim 7, characterized in that, The dosage of the acetic acid aqueous solution is 5 - 10% of the weight of the whole herb of Pseudopimpinella anisum.

9. A powerful moisturizing cream according to claim 7, characterized in that, The enzyme in the enzymatic hydrolysis solution is a mixture of cellulase and β - glucanase with a weight ratio of 10: 0.8 - 1.

10. A method for preparing the powerful moisturizing cream according to claim 1, characterized in that, It includes the following steps: (1) Mix water, carbomer, humectant, chlorphenesin, and silica, add them to an emulsifying pot, stir and heat to 80 - 90 °C, and keep warm for 25 - 40 minutes; (2) Add sorbitan oleate, cetearyl olivate, cetearyl alcohol, potassium cetyl phosphate, oil, and tocopheryl acetate to an oil - phase pot, stir and heat to 85 - 90 °C, and keep warm for 16 - 20 minutes.

11. (3) Under the stirring state of the emulsifying pot, pump the mixture in the oil - phase pot into the emulsifying pot, turn on the homogenizer for homogenization for 4 - 5 minutes, and then keep warm and stir at 80 - 90 °C for 20 - 30 minutes; (4) Cool down to 60 - 65 °C, add arginine, and stir for 4 - 7 minutes; (5) Cool down to 40 - 45 °C, add the synergistic additive, lactic acid, additive - free concept preservative, and moisturizing additive, and stir for 10 - 20 minutes; (6) Cool down to 36 - 38 °C, discharge the material, fill and package it after passing the inspection, and store the finished product in the warehouse.

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