A detergent fragrance containing lavender extract and use thereof

By combining lavender extract with specific essential oils and designing a double-capsule structure, the problems of short-lasting fragrance and poor antibacterial effect in detergent fragrances have been solved, thus improving fragrance stability and antibacterial effect.

CN120272280BActive Publication Date: 2025-11-04GUANGZHOU LIYUE FLAVORS & FRAGRANCES CO LTD +1
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Patent Information

Application Number
CN202510426399.8
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2025-04-07
Publication Date
2025-11-04
Estimated Expiration
2045-04-07

AI Technical Summary

Technical Problem

Existing detergent fragrances have poor aroma and antibacterial effects, and the fragrance lasts for a short time.

Method used

A double-walled detergent fragrance was prepared by combining lavender extract with juniper fruit oil, sage essential oil, magnolia oil, etc., and using a complex of hydroxypropyl-β-cyclodextrin and sodium alginate as the inner wall material and gum arabic as the outer wall material, thereby increasing the fragrance stability and antibacterial effect.

Benefits of technology

The resulting detergent fragrance has a pleasant and rich aroma, which has a balancing and calming effect on the mind and body. The fragrance is also released slowly and for a long time, which significantly improves the antibacterial effect.

✦ Generated by Eureka AI based on patent content.

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Patent Text Reader

Abstract

The present application relates to a kind of lavender extract-containing detergent essence and its application, belong to essence technical field, the preparation method of the detergent essence includes the following steps: S1, part of raw material is pretreated;S2, preparation inner capsule;S3, preparation outer capsule, finished product.The four of added juniper berry oil, sage oil, white orchid oil and lavender oil can respectively start from inhibiting sympathetic nerve activity, relaxing parasympathetic nerve, calming central nervous system and relieving fatigue, synergistically make the detergent essence prepared has excellent balancing body and mind effect;And juniper berry oil, sweet cicely oil and perilla seed oil can jointly play bacteriostatic effect, make the detergent essence prepared has outstanding bacteriostatic effect.In addition, the present application prepares a kind of double capsule wall detergent essence, better protection is carried out to essential oil, can make the essence product prepared has long and slow release effect.
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Description

Technical Field

[0001] This invention belongs to the field of fragrance technology, specifically relating to a detergent fragrance containing lavender extract and its application. Background Technology

[0002] Fragrance is an artificially formulated mixture containing two or more, even dozens, of fragrance ingredients, possessing a specific aroma. The main raw material used in fragrance formulation is aromatic essential oil, which has functions such as pain relief, anxiety reduction, and hypnosis, and is widely used in detergents, cosmetics, textiles, food, and pharmaceuticals. However, fragrance molecules are unstable, highly volatile, and easily oxidized, greatly limiting their applications. If used directly on textiles, the fragrance's duration is very short. Furthermore, most detergent fragrances currently on the market suffer from poor aroma and antibacterial effects. Therefore, providing a fragrance that solves these problems is of great practical significance. Summary of the Invention

[0003] The purpose of this invention is to provide a detergent fragrance containing lavender extract and its application, which solves the problems of poor aroma, antibacterial and slow-release effects of detergent fragrances in the prior art.

[0004] The objective of this invention can be achieved through the following technical solutions:

[0005] A detergent fragrance containing lavender extract, the preparation method of which specifically includes the following steps:

[0006] S1. Pretreatment of some raw materials: Mix component A, component B and ethanol solution evenly and stir to obtain mixture A. Add emulsifier to mixture A and stir evenly in a temperature-controlled water bath to obtain emulsion for later use. Stir gum arabic and deionized water in a temperature-controlled water bath until completely dissolved to obtain gum arabic solution.

[0007] S2. Preparation of inner capsule: Hydroxypropyl-β-cyclodextrin, sodium alginate and deionized water are stirred in a temperature-controlled water bath until completely dissolved to obtain mixture B. Montmorillonite and deionized water are mixed evenly, sonicated, and then stirred at a controlled temperature to obtain mixture C. Mix mixture B and mixture C and stir evenly at a controlled temperature. After stirring, cool to room temperature to obtain mixture D.

[0008] S3. Preparation of outer capsule and finished product: Add emulsion to mixture D, homogenize at controlled speed to obtain mixed emulsion, add gum arabic solution to mixed emulsion while stirring, sonicate, then oscillate at constant temperature, centrifuge, filter, wash, filter by suction, and dry to obtain detergent fragrance finished product.

[0009] As a preferred embodiment of the present invention, the mass ratio of component A, component B and ethanol solution in step S1 is 1.2-1.4:1-1.2:2.5-3; the mass ratio of mixture A and emulsifier is 1:0.1-0.12; and the mass ratio of gum arabic and deionized water is 1:0.1-0.15.

[0010] As a preferred embodiment of the present invention, component A in step S1 includes juniper fruit oil, sage essential oil, magnolia oil, and lavender essential oil; component B includes juniper fruit oil, spikenard essential oil, and perilla seed oil; and the emulsifier includes any one of Tween40, Tween60, and Span20.

[0011] As a preferred embodiment of the present invention, the mass ratio of juniper fruit oil, sage essential oil, magnolia oil and lavender essential oil in component A is 2-4:1-2:0.5-0.8:1-1.2; the mass ratio of juniper fruit oil, nard essential oil and perilla seed oil in component B is 1-2:0.1-0.2:0.2-0.3.

[0012] Furthermore, the juniper fruit oil and sage essential oil used in this invention were purchased from Shanghai Zixin Biotechnology Co., Ltd.; the spikenard essential oil was purchased from Wuhan Huaxiang Kejie Biotechnology Co., Ltd.; and the magnolia oil, lavender essential oil and perilla seed oil were all purchased from Jiangxi Wanlv Natural Fragrance Co., Ltd.

[0013] As a preferred embodiment of the present invention, the mass concentration of the ethanol solution in step S1 is 10%.

[0014] As a preferred embodiment of the present invention, the stirring time for mixing and stirring in step S1 is 15-30 min; the temperature for stirring evenly in the temperature-controlled water bath is 35-40℃; and the temperature for stirring in the temperature-controlled water bath until complete dissolution is 55-60℃.

[0015] As a preferred embodiment of the present invention, the mass ratio of hydroxypropyl-β-cyclodextrin, sodium alginate and deionized water in step S2 is 4-4.4:1-1.2:60-70; the mass ratio of montmorillonite and deionized water is 1:1.2-1.3; and the mass ratio of mixture B and mixture C is 1:0.05-0.06.

[0016] As a preferred embodiment of the present invention, the temperature at which the temperature-controlled water bath is stirred until complete dissolution in step S2 is 40-45℃; the time for ultrasonication is 10-15 min; the temperature for temperature-controlled stirring is 75-80℃ and the time is 1.5-2 h; and the temperature at which temperature-controlled stirring is uniform is 45-50℃.

[0017] As a preferred embodiment of the present invention, the mass ratio of the mixture D and the emulsion in step S3 is 1.8-2:1; the mass ratio of the mixed emulsion and the gum arabic is 1.2-1.5:1.

[0018] As a preferred embodiment of the present invention, the speed of the controlled homogenization in step S3 is 6500-7000 r / min, and the time is 5 min; the speed of adding gum arabic is 0.3-0.5 g / min; the time of ultrasonication is 5 min; and the time of constant temperature oscillation is 30 min.

[0019] An application of a detergent fragrance containing lavender extract, wherein the detergent fragrance is added to the detergent at a weight percentage of 1-3%.

[0020] The beneficial effects of this invention are:

[0021] Component A of this invention is a blend of juniper fruit oil, sage essential oil, magnolia oil, and lavender essential oil, which enhances the fragrance of the detergent, making it pleasant and rich in aroma, while also having the effects of balancing the mind and body, calming the nerves, and soothing the nerves. Specifically, the main components of juniper fruit oil are limonene, α-pinene, and β-myrcene, which can suppress anxiety by inhibiting sympathetic nerve activity and enhancing parasympathetic nerve activity, thereby reducing respiratory rate and heart rate to some extent. In addition, sage essential oil, with its strong and refreshing aroma and rich in α-pinene and α-thujone, assists juniper fruit oil in soothing the parasympathetic nervous system and preventing fatigue caused by excessive parasympathetic nerve activity. Furthermore, this application also adds magnolia oil, which is rich in methyl methylbutyrate, linalool, and cis-linalool oxide, with linalool exhibiting a significant central nervous system sedative effect. Lavender essential oil, with its long-lasting and gentle aroma, relieves fatigue and soothes, thereby harmonizing the body's balance and promoting relaxation. Therefore, the four essential oils added in this invention—juniper fruit oil, sage essential oil, magnolia oil, and lavender essential oil—can work synergistically to give the resulting detergent fragrance excellent effects of balancing the mind and body by inhibiting sympathetic nerve activity, soothing the parasympathetic nervous system, calming the central nervous system, and relieving fatigue.

[0022] (2) The juniper fruit oil added in this invention has a strong inhibitory effect on Bacillus subtilis, Staphylococcus epidermidis and Staphylococcus aureus; the added spikenard essential oil mainly contains spikenardone, terpinene, aristolochnine and spikenard alcohol, which have a strong bactericidal effect on Escherichia coli and Staphylococcus aureus; the added perilla seed oil is rich in L-perillaldehyde, and also contains isoperillone, trans-limonene and perillone, which have a broad-spectrum antibacterial effect and also have the functions of preservation and fragrance enhancement. Therefore, it can assist the juniper fruit oil and spikenard essential oil to jointly enhance the antibacterial effect of component B, and at the same time promote the release of a rich aroma of component A, further making the obtained detergent fragrance have an outstanding antibacterial effect.

[0023] (3) This invention uses a complex of hydroxypropyl-β-cyclodextrin and sodium alginate as the inner wall material and gum arabic as the outer wall material. Montmorillonite is added to the inner wall material to increase its density, which hinders the release of essential oils encapsulated by the wall material and reduces their release rate. The resulting double-encapsulated detergent fragrance provides better protection for the essential oils and solves the problem of easy volatilization and short fragrance retention time after the essential oils are simply mixed with other detergent components. At the same time, it also makes the finished fragrance product have a long-lasting and slow-release effect, effectively improving the stability of the detergent fragrance. Detailed Implementation

[0024] The technical solutions of the present invention will be clearly and completely described below with reference to the embodiments of the present invention. Obviously, the described embodiments are only some embodiments of the present invention, and not all embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the scope of protection of the present invention.

[0025] The juniper fruit oil and sage essential oil used in the embodiments of this invention were purchased from Shanghai Zixin Biotechnology Co., Ltd.; the spikenard essential oil was purchased from Wuhan Huaxiang Kejie Biotechnology Co., Ltd.; the magnolia oil, lavender essential oil and perilla seed oil were all purchased from Jiangxi Wanlv Natural Fragrance Co., Ltd.; to avoid redundancy, they will not be described in detail below.

[0026] Example 1

[0027] A detergent fragrance containing lavender extract, the preparation method of which specifically includes the following steps:

[0028] S1. Pretreatment of some raw materials: Mix component A, component B and 10% ethanol solution evenly and stir for 15 minutes to obtain mixture A. Add emulsifier to mixture A and stir evenly in a water bath at 35°C to obtain emulsion for later use. Stir gum arabic and deionized water in a water bath at 60°C until completely dissolved to obtain gum arabic solution.

[0029] The mass ratio of component A, component B, and ethanol solution is 1.2:1.2:2.5; the mass ratio of mixture A and emulsifier is 1:0.11; and the mass ratio of gum arabic and deionized water is 1:0.13.

[0030] Component A comprises juniper fruit oil, sage essential oil, magnolia oil, and lavender essential oil in a mass ratio of 3:1.5:0.5:1; Component B comprises juniper fruit oil, nard essential oil, and perilla seed oil in a mass ratio of 2:0.15:0.2; and the emulsifier is Span20.

[0031] S2. Preparation of inner capsule: Hydroxypropyl-β-cyclodextrin, sodium alginate and deionized water are stirred in a water bath at 40°C until completely dissolved to obtain mixture B. Montmorillonite and deionized water are mixed evenly, sonicated for 15 min, and then stirred at 75°C for 1.5 h to obtain mixture C. Mix mixture B and mixture C and stir evenly at 50°C. After stirring, cool to room temperature to obtain mixture D.

[0032] The mass ratio of hydroxypropyl-β-cyclodextrin, sodium alginate, and deionized water is 4:1.1:60; the mass ratio of montmorillonite and deionized water is 1:1.2; and the mass ratio of mixture B and mixture C is 1:0.05.

[0033] S3. Preparation of outer capsule and finished product: Add emulsion to mixture D, homogenize at 6500 r / min for 5 min to obtain mixed emulsion, add gum arabic solution to mixed emulsion at a rate of 0.5 g / min while stirring, sonicate for 5 min, then oscillate at constant temperature for 30 min, centrifuge, filter, wash, filter by suction, and dry to obtain detergent fragrance finished product.

[0034] The mass ratio of the mixture D to the emulsion is 1.8:1; the mass ratio of the mixed emulsion to the gum arabic is 1.2:1.

[0035] In this embodiment, the detergent fragrance is added to the detergent at 1% of the total mass of the detergent product to obtain the detergent product, which is laundry liquid.

[0036] Example 2

[0037] A detergent fragrance containing lavender extract, the preparation method of which specifically includes the following steps:

[0038] S1. Pretreatment of some raw materials: Mix component A, component B and 10% ethanol solution evenly and stir for 30 minutes to obtain mixture A. Add emulsifier to mixture A and stir evenly in a water bath at 38°C to obtain emulsion for later use. Stir gum arabic and deionized water in a water bath at 55°C until completely dissolved to obtain gum arabic solution.

[0039] The mass ratio of component A, component B, and ethanol solution is 1.3:1:2.7; the mass ratio of mixture A and emulsifier is 1:0.12; and the mass ratio of gum arabic and deionized water is 1:0.15.

[0040] Component A comprises juniper fruit oil, sage essential oil, magnolia oil, and lavender essential oil in a mass ratio of 2:2:0.7:1.1; Component B comprises juniper fruit oil, nard essential oil, and perilla seed oil in a mass ratio of 1:0.2:0.3; and the emulsifier is Tween 40.

[0041] S2. Preparation of inner capsule: Hydroxypropyl-β-cyclodextrin, sodium alginate and deionized water are stirred in a water bath at 43°C until completely dissolved to obtain mixture B. Montmorillonite and deionized water are mixed evenly, sonicated for 10 min, and then stirred at 78°C for 2 h to obtain mixture C. Mix mixture B and mixture C and stir evenly at 45°C. After stirring, cool to room temperature to obtain mixture D.

[0042] The mass ratio of hydroxypropyl-β-cyclodextrin, sodium alginate, and deionized water is 4.4:1.2:65; the mass ratio of montmorillonite and deionized water is 1:1.3; and the mass ratio of mixture B and mixture C is 1:0.06.

[0043] S3. Preparation of outer capsule and finished product: Add emulsion to mixture D, homogenize at 6750 r / min for 5 min to obtain mixed emulsion, add gum arabic solution to mixed emulsion at a rate of 0.3 g / min while stirring, sonicate for 5 min, then oscillate at constant temperature for 30 min, centrifuge, filter, wash, filter by suction, and dry to obtain detergent fragrance finished product.

[0044] The mass ratio of the mixture D to the emulsion is 1.9:1; the mass ratio of the mixed emulsion to the gum arabic is 1.5:1.

[0045] In this embodiment, the detergent fragrance is added to the detergent at 3% of the total mass of the detergent product to obtain the detergent product, which is dishwashing liquid.

[0046] Example 3

[0047] A detergent fragrance containing lavender extract, the preparation method of which specifically includes the following steps:

[0048] S1. Pretreatment of some raw materials: Mix component A, component B and 10% ethanol solution evenly and stir for 23 minutes to obtain mixture A. Add emulsifier to mixture A and stir evenly in a water bath at 40°C to obtain emulsion for later use. Stir gum arabic and deionized water in a water bath at 57°C until completely dissolved to obtain gum arabic solution.

[0049] The mass ratio of component A, component B, and ethanol solution is 1.4:1.1:3; the mass ratio of mixture A and emulsifier is 1:0.1; the mass ratio of gum arabic and deionized water is 1:0.1.

[0050] Component A comprises juniper fruit oil, sage essential oil, magnolia oil, and lavender essential oil in a mass ratio of 4:1.8:0.8:1.2; component B comprises juniper fruit oil, nard essential oil, and perilla seed oil in a mass ratio of 1.5:0.1:0.25; the emulsifier is Tween 60.

[0051] S2. Preparation of inner capsule: Hydroxypropyl-β-cyclodextrin, sodium alginate and deionized water were stirred in a water bath at 45°C until completely dissolved to obtain mixture B. Montmorillonite and deionized water were mixed evenly, sonicated for 13 min, and then stirred at 80°C for 2 h to obtain mixture C. Mixture B and mixture C were mixed and stirred evenly at 48°C. After stirring, the mixture was cooled to room temperature to obtain mixture D.

[0052] The mass ratio of hydroxypropyl-β-cyclodextrin, sodium alginate, and deionized water is 4.2:1:70; the mass ratio of montmorillonite and deionized water is 1:1.25; and the mass ratio of mixture B and mixture C is 1:0.06.

[0053] S3. Preparation of outer capsule and finished product: Add emulsion to mixture D, homogenize at 7000 r / min for 5 min to obtain mixed emulsion, add gum arabic solution to mixed emulsion at a rate of 0.4 g / min while stirring, sonicate for 5 min, then oscillate at constant temperature for 30 min, centrifuge, filter, wash, filter by suction, and dry to obtain detergent fragrance finished product.

[0054] The mass ratio of the mixture D to the emulsion is 2:1; the mass ratio of the mixed emulsion to the gum arabic is 1.3:1.

[0055] In this embodiment, the detergent fragrance is added to the detergent at 2% of the total mass of the detergent product to obtain the detergent product, which is laundry liquid.

[0056] Comparative Example 1

[0057] Compared with Example 3, the difference is that juniper fruit oil is not added to component A in step S1 of Comparative Example 1. That is, component A consists of sage essential oil, magnolia oil and lavender essential oil in a mass ratio of 3.13:2.14:2.53; the other operation steps and parameters remain unchanged.

[0058] Comparative Example 2

[0059] Compared with Example 3, the difference is that sage essential oil is not added to component A in step S1 of Comparative Example 2. That is, component A consists of juniper fruit oil, magnolia oil and lavender essential oil in a mass ratio of 4.6:1.4:1.8; the other operation steps and parameters remain unchanged.

[0060] Comparative Example 3

[0061] Compared with Example 3, the difference is that no magnolia oil is added to component A in step S1 of Comparative Example 3. That is, component A consists of juniper fruit oil, sage essential oil and lavender essential oil in a mass ratio of 4.26:2.06:1.48; the other operation steps and parameters remain unchanged.

[0062] Comparative Example 4

[0063] Compared with Example 3, the difference is that lavender essential oil is not added to component A in step S1 of Comparative Example 4. That is, component A consists of juniper fruit oil, sage essential oil and magnolia oil in a mass ratio of 4.4:2.2:1.2; the other operation steps and parameters remain unchanged.

[0064] Comparative Example 5

[0065] Compared with Example 3, the difference is that juniper fruit oil is not added to component B in step S1 of Comparative Example 5. That is, component B consists of spikenard oil and perilla seed oil in a mass ratio of 0.85:1; the other operation steps and parameters remain unchanged.

[0066] Comparative Example 6

[0067] Compared with Example 3, the difference is that no spikenard oil is added to component B in step S1 of Comparative Example 6. That is, component B consists of juniper fruit oil and perilla seed oil in a mass ratio of 1.55:0.3; the other operation steps and parameters remain unchanged.

[0068] Comparative Example 7

[0069] Compared with Example 3, the difference is that perilla seed oil is not added to component B in step S1 of Comparative Example 7. That is, component B consists of juniper fruit oil and spikenard essential oil in a mass ratio of 1.63:0.22; the remaining operation steps and parameters remain unchanged.

[0070] Comparative Example 8

[0071] Compared with Example 3, the difference is that hydroxypropyl-β-cyclodextrin was not added in step S2 of Comparative Example 8. Specifically, sodium alginate and deionized water were stirred in a water bath at 45°C until completely dissolved to obtain mixture B. Montmorillonite and deionized water were mixed evenly, sonicated for 13 minutes, and then stirred at 80°C for 2 hours to obtain mixture C. Mixture B and mixture C were mixed and stirred evenly at 48°C. After stirring, the mixture was cooled to room temperature to obtain mixture D.

[0072] The mass ratio of sodium alginate to deionized water is 5.2:70; the mass ratio of montmorillonite to deionized water is 1:1.25; and the mass ratio of mixture B to mixture C is 1:0.06.

[0073] All other operating steps and parameters remain unchanged.

[0074] Comparative Example 9

[0075] Compared with Example 3, the difference is that sodium alginate is not added in step S2 of Comparative Example 9. Specifically, hydroxypropyl-β-cyclodextrin and deionized water are stirred in a water bath at 45°C until completely dissolved to obtain mixture B. Montmorillonite and deionized water are mixed evenly, sonicated for 13 min, and then stirred at 80°C for 2 h to obtain mixture C. Mixture B and mixture C are mixed and stirred evenly at 48°C. After stirring, the mixture is cooled to room temperature to obtain mixture D.

[0076] The mass ratio of hydroxypropyl-β-cyclodextrin to deionized water is 5.2:70; the mass ratio of montmorillonite to deionized water is 1:1.25; and the mass ratio of mixture B to mixture C is 1:0.06.

[0077] All other operating steps and parameters remain unchanged.

[0078] Comparative Example 10

[0079] Compared with Example 3, the difference is that montmorillonite is not added in step S2 of Comparative Example 10. Specifically, hydroxypropyl-β-cyclodextrin, sodium alginate and deionized water are stirred in a water bath at 45°C until completely dissolved to obtain mixture B. Mixture B is then cooled to room temperature to obtain mixture D.

[0080] The mass ratio of hydroxypropyl-β-cyclodextrin, sodium alginate, and deionized water is 4.2:1:70.

[0081] All other operating steps and parameters remain unchanged.

[0082] Test Example 1

[0083] (1) Fragrance richness and comfort test: Cotton cloth (specification 20cm*20cm) was ultrasonically cleaned for 10min each with distilled water, anhydrous ethanol and distilled water, and then dried in a ventilated place to remove the impurities remaining in the cotton fibers. Then, the cotton cloth after removing the impurities was immersed in the detergent products prepared in Examples 1-3, Comparative Examples 1-4 and Comparative Examples 8-10 respectively in a constant temperature water bath at 30℃ for 1h, and then dried at room temperature.

[0084] A sensory evaluation panel composed of 12 professional sensory evaluators immediately conducted sensory evaluations on the soaked cotton fabric to test its aroma and calming effects. The sensory evaluation used a 5-point scale; a higher score indicated better overall aroma comfort and calming effects after the cotton fabric was soaked. The average score from the sensory evaluation panel was taken as the final score. Descriptions of each characteristic and scoring criteria are shown in Table 1, and the final results are shown in Table 2.

[0085] (2) Slow-release performance test: After the cotton fabric tested in (1) above was placed for 14 days and 28 days, a sensory evaluation group composed of 12 professional sensory evaluators who evaluated the cotton fabric tested in (1) above was invited to evaluate the cotton fabric again using the same standards in Table 1. The average value of the sensory evaluation group was taken as the final score value. The final results are shown in Table 3, which reflects the slow-release performance of the product. The higher the final score value, the more durable the product is and the better the slow-release performance.

[0086] Table 1

[0087]

[0088]

[0089] Table 2

[0090]

[0091] As can be seen from the rating values ​​in Table 2 after 0 days, the detergent fragrance prepared by this invention has a comfortable and rich aroma, and also has the effects of balancing the mind and body, and calming the nerves. Specifically, this is because the four essential oils added to this invention—juniper fruit oil, sage essential oil, magnolia oil, and lavender essential oil—can respectively inhibit sympathetic nerve activity, soothe the parasympathetic nervous system, calm the central nervous system, and relieve fatigue, thus synergistically giving the prepared detergent fragrance an excellent effect of balancing the mind and body.

[0092] As can be seen from the rating values ​​in Table 2 after 14 days and 28 days, the detergent fragrance prepared by this invention has a long-lasting and slow-release effect.

[0093] Test Example 2

[0094] According to QB / T 2738-2012, the antibacterial properties of the detergents prepared in Examples 1-3 and 5-7 were tested, and the results are shown in Table 3.

[0095] Table 3

[0096]

[0097] As can be seen from Table 3, the detergent fragrance prepared by this invention has outstanding antibacterial effect.

[0098] In the description of this specification, the references to terms such as "an embodiment," "example," "specific example," etc., indicate that a specific feature, structure, material, or characteristic described in connection with that embodiment or example is included in at least one embodiment or example of the present invention. In this specification, the illustrative expressions of the above terms do not necessarily refer to the same embodiment or example. Furthermore, the specific features, structures, materials, or characteristics described may be combined in any suitable manner in one or more embodiments or examples.

[0099] The above description is merely an example and illustration of the present invention. Those skilled in the art can make various modifications or additions to the specific embodiments described or use similar methods to replace them, as long as they do not deviate from the invention or exceed the scope defined in the claims, they should all fall within the protection scope of the present invention.

Claims

1. A detergent fragrance containing lavender extract, characterized in that, The preparation method of the detergent fragrance is as follows: S1. Pretreatment of some raw materials: Mix component A, component B and ethanol solution evenly and stir to obtain mixture A. Add emulsifier to mixture A and stir evenly in a temperature-controlled water bath to obtain emulsion for later use. Stir gum arabic and deionized water in a temperature-controlled water bath until completely dissolved to obtain gum arabic solution. S2. Preparation of inner capsule: Hydroxypropyl-β-cyclodextrin, sodium alginate and deionized water are stirred in a temperature-controlled water bath until completely dissolved to obtain mixture B. Montmorillonite and deionized water are mixed evenly, sonicated, and then stirred at a controlled temperature to obtain mixture C. Mix mixture B and mixture C and stir evenly at a controlled temperature. After stirring, cool to room temperature to obtain mixture D. S3. Preparation of outer capsule and finished product: Add emulsion to mixture D, homogenize at controlled speed to obtain mixed emulsion, add gum arabic solution to mixed emulsion while stirring, sonicate, then oscillate at constant temperature, centrifuge, filter, wash, filter by suction, and dry to obtain detergent fragrance finished product. In step S1, component A is composed of juniper fruit oil, sage essential oil, magnolia oil, and lavender essential oil in a mass ratio of 2-4:1-2:0.5-0.8:1-1.2; component B is composed of juniper fruit oil, nard essential oil, and perilla seed oil in a mass ratio of 1-2:0.1-0.2:0.2-0.

3.

2. The detergent fragrance containing lavender extract according to claim 1, characterized in that, In step S1, the mass ratio of component A, component B, and ethanol solution is 1.2-1.4:1-1.2:2.5-3; the mass ratio of mixture A and emulsifier is 1:0.1-0.12; and the mass ratio of gum arabic and deionized water is 1:0.1-0.

15.

3. The detergent fragrance containing lavender extract according to claim 1, characterized in that, The emulsifier includes any one of Tween40, Tween60, and Span20.

4. The detergent fragrance containing lavender extract according to claim 1, characterized in that, The stirring time for mixing and stirring in step S1 is 15-30 min; the temperature for stirring evenly in the temperature-controlled water bath to obtain the emulsion is 35-40℃; and the temperature for stirring until completely dissolved in the temperature-controlled water bath to obtain the gum arabic liquid is 55-60℃.

5. The detergent fragrance containing lavender extract according to claim 1, characterized in that, In step S2, the mass ratio of hydroxypropyl-β-cyclodextrin, sodium alginate, and deionized water is 4-4.4:1-1.2:60-70; the mass ratio of montmorillonite and deionized water is 1:1.2-1.3; and the mass ratio of mixture B and mixture C is 1:0.05-0.

06.

6. The detergent fragrance containing lavender extract according to claim 1, characterized in that, In step S2, the temperature at which the mixture B is stirred until completely dissolved in a temperature-controlled water bath is 40-45℃; the time for sonication is 10-15 min; the temperature at which the mixture C is stirred is 75-80℃ for 1.5-2 h; and the temperature at which the mixture D is stirred until uniform is obtained is 45-50℃.

7. The detergent fragrance containing lavender extract according to claim 1, characterized in that, In step S3, the mass ratio of the mixture D to the emulsion is 1.8-2:1; the mass ratio of the mixed emulsion to the gum arabic is 1.2-1.5:

1.

8. The detergent fragrance containing lavender extract according to claim 1, characterized in that, In step S3, the speed of the controlled homogenization is 6500-7000 r / min, and the time is 5 min; the speed of adding gum arabic is 0.3-0.5 g / min; the time of ultrasonication is 5 min; and the time of constant temperature oscillation is 30 min.

9. The use of a detergent fragrance containing lavender extract as described in any one of claims 3-8 in a detergent, characterized in that, The detergent fragrance is added to the detergent at a mass percentage of 1-3%.

Citation Information

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