Cell factor activity protection type supercritical carbon dioxide drying equipment

Abstract

The invention discloses cell factor activity protection type supercritical carbon dioxide drying equipment, and particularly relates to the technical field of drying equipment.The structure comprises an equipment box, a first gas storage bottle is placed on one side in the equipment box, and a booster pump is placed on the side, away from the first gas storage bottle, of a second gas storage bottle; a booster pump is installed above the equipment box, a heating mechanism is installed above the booster pump, a drying chamber is installed above the equipment box, a hydraulic telescopic rod is hoisted at the top in the drying chamber, a drying mechanism is installed at the bottom in the drying chamber, and an adsorption cover is installed on the side wall of the drying chamber. Firstly, cells can be rapidly dried, water in the cells can be rapidly driven to rapidly dry the cells through the arrangement of the spraying mechanism, and meanwhile, the activity of the cells cannot be affected by long-time drying.

Description

Technical Field

[0001] This application relates to the technical field of drying equipment. More specifically, this application relates to a supercritical carbon dioxide drying equipment for protecting cytokine activity. Background Art

[0002] Supercritical carbon dioxide drying is a technology that uses the special properties of CO2 in the supercritical state (temperature higher than 31.1°C, pressure higher than 7.38 MPa, at this time CO2 has both the low viscosity of a gas and the high diffusivity of a liquid) for drying. Its core principle is to utilize the high permeability and solubility of SC-CO2 to efficiently remove moisture or solvents in the material, while avoiding problems such as thermal damage, structural damage, or solvent residues that may be caused by traditional drying (such as hot air drying, vacuum drying); However, when the existing critical carbon dioxide drying device dries cells, the long drying time will cause the activity of the cells to decrease, and the short drying time will affect the drying effect; Therefore, a supercritical carbon dioxide drying equipment for protecting cytokine activity is proposed to solve the above problems. Summary of the Invention

[0003] In order to overcome the above-mentioned defects of the prior art, this application provides a supercritical carbon dioxide drying equipment for protecting cytokine activity to solve the problems raised in the above background art.

[0004] To achieve the above object, this application provides the following technical solution: A supercritical carbon dioxide drying equipment for protecting cytokine activity, including an equipment box. On one side inside the equipment box, a first gas storage cylinder is placed, and on one side of the first gas storage cylinder, a second gas storage cylinder is placed. On the side of the second gas storage cylinder away from the first gas storage cylinder, a booster pump is placed, and above the booster pump, a heating mechanism is installed. Above the equipment box, a drying chamber is installed, and a hydraulic telescopic rod is suspended from the top of the drying chamber. One end of the hydraulic telescopic rod is installed with a sealing cover, and inside the sealing cover, a spraying mechanism is installed. At the bottom of the drying chamber, a drying mechanism is installed, and an adsorption cover is installed on the side wall of the drying chamber.

[0005] Preferably, air vent valves are installed at the bottle mouths of the first gas storage cylinder and the second gas storage cylinder, and first ventilation pipes are installed on the air vent valves. The first gas storage cylinder and the second gas storage cylinder are both connected to the booster pump through the first ventilation pipes, and a first electromagnetic valve is installed between the booster pump and the heating mechanism.

[0006] Preferably, the heating mechanism includes a heating box, heating coils, a heating pipe, a first intake joint, a first outlet joint, and a first temperature sensor. Among them, a plurality of heating coils for heating the heating pipe are installed inside the heating box, and the heating pipe passes through the inside of the plurality of heating coils to form an "S" shaped structure. One end of the heating pipe is installed with a first intake joint, and the other end of the heating pipe is installed with a first outlet joint. At the same time, first temperature sensors are installed inside both the first intake joint and the first outlet joint.

[0007] Preferably, a tee pipe is installed above the first outlet joint, and a first branch pipe and a second branch pipe are installed on the tee pipe. One end of the first branch pipe and one end of the second branch pipe are both connected with a second intake joint.

[0008] Preferably, the sealing cover forms a liftable structure with the top of the drying chamber through a hydraulic telescopic rod, and springs are installed at the bottom edge of the sealing cover. At the same time, bellows are wrapped around the springs, and a wire winding wheel is installed on one side of the sealing cover.

[0009] Preferably, the spraying mechanism includes an elbow pipe, a second solenoid valve, a second temperature sensor, a spray head, and a pressure sensor. Among them, the elbow pipe is installed inside the sealing cover, and a plurality of second solenoid valves are installed on the inner side of the elbow pipe. The spray head is installed at the bottom of the second solenoid valve. A second temperature sensor is installed on one side wall of the sealing cover, and a pressure sensor is installed on the other side wall of the sealing cover.

[0010] Preferably, one end of the first branch pipe bypasses the wire winding wheel and communicates with the inside of the elbow pipe, and the elbow pipe communicates with the spray head through the second solenoid valve.

[0011] Preferably, the drying mechanism includes a workbench, a drying plate, an air storage chamber, a third solenoid valve, and an air jet valve. Among them, the drying plate is installed on the surface of the workbench, and a cavity is provided inside the workbench. An air storage chamber is provided at the bottom of the cavity. The third solenoid valve is installed above the air storage chamber, and the air jet valve is installed on the third solenoid valve.

[0012] Preferably, the drying plate is a honeycomb-shaped air-permeable structure, and the air storage chamber communicates with the air jet valve through the third solenoid valve.

[0013] Preferably, a recovery bottle is installed on one side of the bottom of the equipment box. A fourth solenoid valve is installed on one side of the adsorption cover, and an air pump is installed on one side of the fourth solenoid valve. A second ventilation pipe is installed between the air pump and the recovery bottle.

[0014] The technical effects and advantages of this application: Compared with the prior art, this cytokine activity-protected supercritical carbon dioxide drying equipment can first quickly dry cells, and through the setting of the spraying mechanism, it can quickly drive the moisture inside the cells to dry the cells more rapidly, and at the same time, it will not affect the activity of the cells due to long-term drying.

[0015] Compared with the prior art, in this cytokine activity-protected supercritical carbon dioxide drying equipment, the sealing cover moves up and down as the hydraulic telescopic rod extends and retracts. When drying, the sealing cover moves down to cover the drying mechanism, and the setting of the spring plays a role in shock absorption. The setting of the sealing cover makes the cells form a relatively sealed space on the drying plate. Carbon dioxide gas enters the spray head through the second solenoid valve and sprays the supercritical carbon dioxide onto the surface of the cells to dry the surface of the cells. At the same time, the supercritical carbon dioxide passes through the gas storage chamber and the third solenoid valve and is sprayed from the bottom of the jet valve onto the drying plate, so that the supercritical carbon dioxide dries the cells from the bottom. After drying, the carbon dioxide is recovered into the interior of the recovery bottle through the second air pipe from the adsorption cover. At this time, the air pump provides power for the adsorption cover. BRIEF DESCRIPTION OF THE DRAWINGS

[0016] Figure 1 is a schematic diagram of the overall structure of this application; Figure 2 is a top view structural schematic diagram of the heating mechanism of this application; Figure 3 is a structural schematic diagram of the sealing cover and the spraying mechanism of this application; Figure 4 is a structural schematic diagram of the drying mechanism of this application; Figure 5 is this application Figure 1 The enlarged structural schematic diagram at position A in.

[0017] The reference numerals are: 1, equipment box; 2, first gas storage cylinder; 201, ventilation valve; 202, first ventilation pipe; 3, second gas storage cylinder; 4, booster pump; 401, first solenoid valve; 5, heating mechanism; 501, heating box; 502, heating coil; 503, heating pipe; 504, first air inlet joint; 505, first air outlet joint; 506, first temperature sensor; 507, tee; 508, first gas distribution pipe; 509, second gas distribution pipe; 510, second air inlet joint; 6, drying chamber; 7, hydraulic telescopic rod; 8, sealing cover; 801, wire winding wheel; 802, spring; 803, bellows; 9, spraying mechanism; 901, elbow pipe; 902, second solenoid valve; 903, second temperature sensor; 904, spray head; 905, pressure sensor; 10, drying mechanism; 1001, workbench; 1002, drying plate; 1003, gas storage chamber; 1004, third solenoid valve; 1005, air jet valve; 11, adsorption hood; 12, recovery bottle; 13, fourth solenoid valve; 14, air pump; 15, second ventilation pipe. Detailed implementation manners

[0018] Next, the technical solutions in the embodiments of the present application will be clearly and completely described in conjunction with the accompanying drawings in the embodiments of the present application. Obviously, the described embodiments are only a part of the embodiments of the present application, rather than all the embodiments. Based on the embodiments in the present application, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present application. Embodiment

[0019] As Figures 1 to 5 shown, a cytokine activity protection type supercritical carbon dioxide drying device includes an equipment box 1. A first gas storage cylinder 2 is placed on one side inside the equipment box 1, and a second gas storage cylinder 3 is placed on one side of the first gas storage cylinder 2. A booster pump 4 is placed on the side of the second gas storage cylinder 3 away from the first gas storage cylinder 2, and a heating mechanism 5 is installed above the booster pump 4. A drying chamber 6 is installed above the equipment box 1, and a hydraulic telescopic rod 7 is suspended from the top of the interior of the drying chamber 6. One end of the hydraulic telescopic rod 7 is installed with a sealing cover 8, and a spraying mechanism 9 is installed inside the sealing cover 8. A drying mechanism 10 is installed at the bottom of the interior of the drying chamber 6, and an adsorption hood 11 is installed on the side wall of the drying chamber 6.

[0020] At the mouths of the first gas storage cylinder 2 and the second gas storage cylinder 3, ventilation valves 201 are installed, and first ventilation pipes 202 are installed on the ventilation valves 201. The first gas storage cylinder 2 and the second gas storage cylinder 3 are both connected to a booster pump 4 through the first ventilation pipes 202. A first solenoid valve 401 is installed between the booster pump 4 and the heating mechanism 5. The carbon dioxide gas inside the first gas storage cylinder 2 and the second gas storage cylinder 3 enters the booster pump 4 through the first ventilation pipes 202 for pressurization, and then the first solenoid valve 401 is opened, and the carbon dioxide enters the heating mechanism 5 for heating.

[0021] The heating mechanism 5 includes a heating box 501, heating coils 502, a heating pipe 503, a first air inlet joint 504, a first air outlet joint 505, and a first temperature sensor 506. Among them, a plurality of heating coils 502 for heating the heating pipe 503 are installed inside the heating box 501, and the heating pipe 503 passes through the inside of the plurality of heating coils 502 to form an "S" shaped structure. One end of the heating pipe 503 is installed with a first air inlet joint 504, and the other end of the heating pipe 503 is installed with a first air outlet joint 505. At the same time, first temperature sensors 506 are installed inside the first air inlet joint 504 and the first air outlet joint 505.

[0022] Above the first air outlet joint 505, a three-way pipe 507 is installed, and a first branch pipe 508 and a second branch pipe 509 are installed on the three-way pipe 507. One end of the first branch pipe 508 and one end of the second branch pipe 509 are both connected with a second air inlet joint 510. The carbon dioxide gas enters the inside of the three-way pipe 507 through the first air outlet joint 505. A part of the carbon dioxide gas enters the spraying mechanism 9 through the first branch pipe 508, and another part of the carbon dioxide gas enters the inside of the drying mechanism 10 through the second branch pipe 509 and the second air inlet joint 510.

[0023] The sealing cover 8 and the top of the drying chamber 6 form a liftable structure through a hydraulic telescopic rod 7. A spring 802 is installed at the bottom edge of the sealing cover 8. At the same time, a corrugated pipe 803 is wrapped around the spring 802. A wire winding wheel 801 is installed on one side of the sealing cover 8.

[0024] The spraying mechanism 9 includes an elbow pipe 901, a second solenoid valve 902, a second temperature sensor 903, a spray head 904, and a pressure sensor 905. Among them, the elbow pipe 901 is installed inside the sealing cover 8, and a plurality of second solenoid valves 902 are installed on the inner side of the elbow pipe 901. The spray head 904 is installed at the bottom of the second solenoid valve 902. A second temperature sensor 903 is installed on one side wall of the sealing cover 8, and a pressure sensor 905 is installed on the other side wall of the sealing cover 8.

[0025] One end of the first sub-air pipe 508 bypasses the wire winding wheel 801 and is internally connected to the elbow 901, and the elbow 901 is connected to the spray head 904 through the second solenoid valve 902.

[0026] The drying mechanism 10 includes a workbench 1001, a drying plate 1002, an air storage chamber 1003, a third solenoid valve 1004, and an air jet valve 1005. Among them, the drying plate 1002 is mounted on the surface of the workbench 1001, and a cavity is provided inside the workbench 1001. The bottom of the cavity is provided with an air storage chamber 1003. The third solenoid valve 1004 is mounted above the air storage chamber 1003, and the air jet valve 1005 is mounted on the third solenoid valve 1004. The drying plate 1002 is a honeycomb-shaped air-permeable structure, and the air storage chamber 1003 is connected to the air jet valve 1005 through the third solenoid valve 1004. During drying, the sealing cover 8 moves downward to cover the drying mechanism 10, and the spring 802 plays a role in shock absorption. The sealing cover 8 makes the cells form a relatively sealed space on the drying plate 1003. Carbon dioxide gas enters the spray head 904 through the second solenoid valve 902, and the carbon dioxide in the critical state is sprayed onto the surface of the cells to dry the surface of the cells. At the same time, the carbon dioxide in the critical state passes through the air storage chamber 1003 and the third solenoid valve 1004 and is sprayed from the air jet valve 1005 onto the drying plate 1002 from the bottom, so that the carbon dioxide in the critical state performs a drying operation on the bottom of the cells.

[0027] A recovery bottle 12 is mounted on one side of the bottom of the equipment box 1. A fourth solenoid valve 13 is mounted on one side of the adsorption cover 11, and an air pump 14 is mounted on one side of the fourth solenoid valve 13. A second air pipe 15 is mounted between the air pump 14 and the recovery bottle 12.

[0028] The working process of this application is as follows: First, place the cells to be dried on the surface of the drying plate 1002. Both the first gas cylinder 2 and the second gas cylinder 3 store carbon dioxide. Open the ventilation valve 201, and the carbon dioxide gas inside the first gas cylinder 2 and the second gas cylinder 3 enters the booster pump 4 through the first air pipe 202 for pressurization. Then open the first solenoid valve 401, and the carbon dioxide enters the heating mechanism 5 for heating; When the carbon dioxide is heated in the heating mechanism 5, first, the carbon dioxide enters the inside of the heating pipe 503 through the first air inlet joint 504, and then the heating coil 502 is powered on, and the carbon dioxide gas is heated by electromagnetic heating. During the heating process, the first temperature sensor 506 senses the temperature of the carbon dioxide gas inside the heating pipe 503 in real time. After the heating is completed, the carbon dioxide gas is discharged from the first air outlet joint 505; Carbon dioxide gas enters the interior of the tee 507 through the first air outlet joint 505. A part of the carbon dioxide gas enters the spraying mechanism 9 through the first branch air pipe 508, and another part of the carbon dioxide gas enters the interior of the drying mechanism 10 through the second branch air pipe 509 and the second air inlet joint 510; First, the drying chamber 6 is a sealed space relative to the outside world to avoid the influence of external air on the drying effect. During drying, the sealing cover 8 moves up and down with the telescopic movement of the hydraulic telescopic rod 7. When drying, the sealing cover 8 moves down to cover the drying mechanism 10, and the spring 802 plays a role in shock absorption. The setting of the sealing cover 8 enables the cells to form a relatively sealed space on the drying plate 1003. Carbon dioxide gas enters the spray head 904 through the second solenoid valve 902, and the carbon dioxide in the critical state is sprayed onto the surface of the cells to dry the surface of the cells. At the same time, the carbon dioxide in the critical state passes through the gas storage chamber 1003 and the third solenoid valve 1004 and is sprayed from the bottom of the drying plate 1002 through the air jet valve 1005, so that the carbon dioxide in the critical state performs drying operations from the bottom of the cells. After drying, the carbon dioxide is recovered into the interior of the recovery bottle 12 through the second ventilation pipe 15 from the adsorption cover 11. At this time, the air pump 14 provides power for the adsorption cover 11. The above is the working principle of this cell factor activity protection type supercritical carbon dioxide drying equipment.

Claims

1. A cytokine activity-protected supercritical carbon dioxide drying device, comprising an equipment box (1). Inside one side of the equipment box (1), a first gas storage cylinder (2) is placed, and a second gas storage cylinder (3) is placed on one side of the first gas storage cylinder (2), characterized in that: On the side of the second gas storage cylinder (3) away from the first gas storage cylinder (2), a booster pump (4) is placed, and a heating mechanism (5) is installed above the booster pump (4). Above the equipment box (1), a drying chamber (6) is installed. Inside the drying chamber (6), a hydraulic telescopic rod (7) is suspended from the top of the chamber. One end of the hydraulic telescopic rod (7) is equipped with a sealing cover (8), and inside the sealing cover (8), a spraying mechanism (9) is installed. At the bottom of the drying chamber (6), a drying mechanism (10) is installed, and an adsorption hood (11) is installed on the side wall of the drying chamber (6).

2. The supercritical carbon dioxide drying equipment with cytokine activity protection according to claim 1, characterized in that: At the bottle mouths of the first gas storage cylinder (2) and the second gas storage cylinder (3), air vent valves (201) are installed, and first ventilation pipes (202) are installed on the air vent valves (201). Both the first gas storage cylinder (2) and the second gas storage cylinder (3) are connected to the booster pump (4) through the first ventilation pipes (202). A first solenoid valve (401) is installed between the booster pump (4) and the heating mechanism (5).

3. A cytokine activity-protecting supercritical carbon dioxide drying device according to claim 1, characterized in that: The heating mechanism (5) includes a heating box (501), heating coils (502), a heating pipe (503), a first air inlet joint (504), a first air outlet joint (505), and a first temperature sensor (506). Among them, inside the heating box (501), multiple heating coils (502) for heating the heating pipe (503) are installed, and the heating pipe (503) passes through the inside of the multiple heating coils (502) to form an "S" - shaped structure. One end of the heating pipe (503) is equipped with a first air inlet joint (504), and the other end of the heating pipe (503) is equipped with a first air outlet joint (505). At the same time, first temperature sensors (506) are installed inside both the first air inlet joint (504) and the first air outlet joint (505).

4. A cytokine activity protection type supercritical carbon dioxide drying device according to claim 3, characterized in that: Above the first air outlet joint (505), a three - way pipe (507) is installed, and a first branch pipe (508) and a second branch pipe (509) are installed on the three - way pipe (507). One end of the first branch pipe (508) and one end of the second branch pipe (509) are both connected to a second air inlet joint (510).

5. A cytokine activity-protecting supercritical carbon dioxide drying device according to claim 4, characterized in that: The sealing cover (8) forms a liftable structure with the top of the drying chamber (6) through the hydraulic telescopic rod (7). At the bottom edge of the sealing cover (8), a spring (802) is installed, and a corrugated pipe (803) is wrapped around the spring (802). A wire winding wheel (801) is installed on one side of the sealing cover (8).

6. The supercritical carbon dioxide drying device with cytokine activity protection according to claim 5, characterized in that: The spraying mechanism (9) includes an elbow pipe (901), a second solenoid valve (902), a second temperature sensor (903), a spray head (904), and a pressure sensor (905). Among them, the elbow pipe (901) is installed inside the sealing cover (8), and multiple second solenoid valves (902) are installed on the inner side of the elbow pipe (901). The bottom of the second solenoid valve (902) is equipped with a spray head (904). A second temperature sensor (903) is installed on one side wall of the sealing cover (8), and a pressure sensor (905) is installed on the other side wall of the sealing cover (8).

7. A cytokine activity protection type supercritical carbon dioxide drying device according to claim 6, characterized in that: One end of the first sub-air pipe (508) bypasses the wire winding wheel (801) and is communicated with the inside of the elbow pipe (901), and the elbow pipe (901) is communicated with the spray head (904) through the second electromagnetic valve (902).

8. A cytokine activity-protecting supercritical carbon dioxide drying device according to claim 1, characterized in that: The drying mechanism (10) includes a workbench (1001), a drying plate (1002), an air storage chamber (1003), a third electromagnetic valve (1004) and an air jet valve (1005). Among them, the drying plate (1002) is installed on the surface of the workbench (1001), and a cavity is provided inside the workbench (1001), and the air storage chamber (1003) is provided at the bottom of the cavity. The third electromagnetic valve (1004) is installed above the air storage chamber (1003), and the air jet valve (1005) is installed on the third electromagnetic valve (1004).

9. The supercritical carbon dioxide drying device for protecting cytokine activity according to claim 8, characterized in that: The drying plate (1002) is a honeycomb-shaped air-permeable structure, and the air storage chamber (1003) is communicated with the air jet valve (1005) through the third electromagnetic valve (1004).

10. A cytokine activity-protecting supercritical carbon dioxide drying device according to claim 8, characterized in that: A recovery bottle (12) is installed on one side of the bottom of the equipment box (1). A fourth electromagnetic valve (13) is installed on one side of the adsorption hood (11), and an air pump (14) is installed on one side of the fourth electromagnetic valve (13). A second air pipe (15) is installed between the air pump (14) and the recovery bottle (12).

Images