Liquid glue with ultralow viscosity and high solid content and preparation method thereof

Abstract

The invention relates to the technical field of glue chemical industry, in particular to liquid glue with ultralow viscosity and high solid content and a preparation method thereof.The preparation method comprises the steps that a first part of vinyl silicone oil and a first auxiliary are stirred to obtain base micelles, and rubber mixing operation is conducted on the base micelles to obtain rubber compound; carrying out self-adaptive dilution on the rubber compound by using a second part of vinyl silicone oil by utilizing a self-adaptive dilution model to obtain base rubber; a first part of base glue and a second part of base glue are obtained from the base glue, and the mass of the first part of base glue is the same as that of the second part of base glue; stirring the first part of base glue, the first part of simethicone and the second auxiliary agent according to a preset stirring strategy to obtain glue A; stirring the second part of base glue, the second part of dimethyl silicone oil and a third auxiliary agent according to a stirring strategy to obtain glue B; and carrying out isometric isolation filling on the glue A and the glue B to obtain a liquid glue product. The viscosity of the high-solid-content liquid glue can be reduced, and the stirring efficiency of the high-solid-content liquid glue is improved.

Description

Technical Field

[0001] This invention relates to the field of adhesive chemical technology, and in particular to a liquid adhesive with ultra-low viscosity and high solid content and its preparation method. Background Technology

[0002] As digital products become smaller and more precise, the requirements for structural stability and electrical safety of their internal components (such as chips, bearings, connectors, etc.) have increased significantly.

[0003] Liquid adhesives, as key auxiliary materials, are expected to meet the requirements of low viscosity and insulation in this field. "Low viscosity" means that the low-viscosity liquid adhesive can penetrate into the gaps between tightly bonded metal or electronic components through a pressure-fitting process, forming a strong bond after curing in an airless environment, effectively preventing loosening or leakage of components due to impact or vibration. "Insulation" means that digital product components (such as motherboard chips and solder joints) must avoid short circuits or signal interference. Insulating liquid adhesives fill the gaps between components, forming a physical isolation layer that can shield against electromagnetic interference and prevent electrical faults caused by moisture and dust intrusion.

[0004] Nowadays, liquid adhesives on the market generally pursue high solid content. However, high solid content adhesives have the problem of difficult stirring due to the high consistency of the system during the production process. This will cause the temperature to rise and the distribution of various media in the adhesive to be uneven, which will affect the product's strength and other properties. Improper stirring process will greatly reduce the success rate of adhesive preparation. Summary of the Invention

[0005] This invention provides a method for preparing a liquid adhesive with ultra-low viscosity and high solid content. Its main purpose is to reduce the viscosity of high solid content liquid adhesives and improve the stirring efficiency of high solid content liquid adhesives.

[0006] To achieve the above objectives, the present invention provides a method for preparing a liquid adhesive with ultra-low viscosity and high solid content, comprising: The first pre-constructed vinyl silicone oil and the first pre-constructed additive are stirred to obtain a base micelle, and the base micelle is subjected to a rubber mixing operation to obtain a compound. Using a pre-trained adaptive dilution model, a pre-constructed second part of vinyl silicone oil was used to adaptively dilute the compound to obtain the base rubber. A first portion and a second portion of the base adhesive are obtained from the base adhesive, wherein the first portion and the second portion of the base adhesive have the same mass. According to the preset stirring strategy, the first part of base glue, the pre-constructed first part of dimethyl silicone oil and the pre-constructed second additive are stirred to obtain glue A; According to the stirring strategy, the second base adhesive, the pre-constructed second dimethyl silicone oil, and the pre-constructed third additive are stirred to obtain adhesive B; The A glue and B glue are filled into liquid glue products by separating them into equal volumes.

[0007] Optionally, the step of stirring the pre-constructed first portion of vinyl silicone oil and the pre-constructed first additive to obtain the base micelle includes: The first adjuvant is grouped to obtain a sub-first adjuvant set; Extract one portion of the first auxiliary agent from the first auxiliary agent set in sequence, and add the extracted first auxiliary agent to the first portion of vinyl silicone oil and stir. Using a pre-constructed viscosity sensor, the viscosity change sequence of the first vinyl silicone oil is obtained, and the rate of change of the viscosity change sequence is identified to obtain the viscosity change rate; When the viscosity change rate is less than the preset stirring viscosity interference threshold, it is determined that the first auxiliary agent has been incorporated into the first part of vinyl silicone oil; When the first auxiliary agent is incorporated into the first part of vinyl silicone oil, the steps described above for sequentially extracting one part of the first auxiliary agent from the set of first auxiliary agents are returned until the set of first auxiliary agents is incorporated into the first part of vinyl silicone oil to obtain the base micelle.

[0008] Optionally, the step of mixing the base micelles to obtain the compound rubber includes: The base micelles are subjected to mechanical shearing and mixing operations to obtain a uniform adhesive; The homogeneous rubber is subjected to a vacuum operation to obtain a vacuum environment. The homogeneous rubber under vacuum environment is then heated to 170°C and kept at 170°C for 2 hours to obtain the compound rubber.

[0009] Optionally, the step of stirring the first portion of base adhesive, the pre-constructed first portion of dimethyl silicone oil, and the pre-constructed second additive according to a preset stirring strategy to obtain adhesive A includes: To the first base adhesive, a pre-constructed first part of dimethyl silicone oil and a pre-constructed second additive are added to obtain adhesive A raw material; The A-type adhesive raw material is stirred at a speed of 10-15 Hz for 5 minutes to obtain the first A-type adhesive stirring intermediate. The first A-gel mixing intermediate was stirred at 40 Hz for 30 minutes to obtain the second A-gel mixing intermediate. The A glue preparation container is vacuumed. The second A-glue intermediate, which is in a vacuum environment, is stirred at a speed of 40 Hz for 20 minutes to obtain A-glue.

[0010] Optionally, the step of filling the A and B adhesives with equal volumes to obtain a liquid adhesive product includes: According to the preset filling flow rate, obtain a rated amount of glue A, and according to the filling flow rate, obtain a rated amount of glue B; The rated amount of glue A is sieved to obtain glue A to be packaged, and the rated amount of glue B is sieved to obtain glue B to be packaged. The two adhesives, A and B, to be packaged are isolated and sealed to obtain a liquid adhesive product.

[0011] Optionally, before obtaining the first and second portions of base adhesive from the base adhesive, the method further includes: Obtain the viscosity of the base adhesive; Determine whether the viscosity is within a preset acceptable range; When the viscosity is not within the acceptable range, the base adhesive is determined to be unqualified, and unqualified base adhesive is obtained. The unqualified base adhesive is then transported to a pre-constructed raw material processing device for separation to obtain a raw material set.

[0012] Optionally, the step of transporting the substandard base adhesive to a pre-constructed raw material processing device for separation to obtain a raw material set includes: Using the pre-constructed solid-liquid separation device in the raw material processing equipment, the unqualified base adhesive is centrifuged to obtain fumed silica and the remaining mixed liquid; According to a preset set of boiling points, the remaining mixed liquid is subjected to a temperature gradient distillation operation to obtain hexamethylsilazane, dimethyldiethoxysilane and vinyl silicone oil; The fumed silica, hexamethylsilazane, dimethyldiethoxysilane and vinyl silicone oil are used as raw materials.

[0013] To achieve the above objectives, the present invention also provides a liquid adhesive with ultra-low viscosity and high solids content, produced by the method for preparing the liquid adhesive with ultra-low viscosity and high solids content. When the liquid adhesive is confirmed for use, adhesive A and adhesive B are mixed in a 1:1 ratio according to the pre-constructed usage volume to obtain the liquid adhesive. If it is confirmed that the liquid adhesive will not be used, adhesive A and adhesive B are stored based on a pre-constructed storage state, wherein adhesive A and adhesive B are stored independently, and both adhesive A and adhesive B contain a base adhesive. The base adhesive is composed of the first part of vinyl silicone oil, the first additive, and the second part of vinyl silicone oil; The first additive includes fumed silica, hexamethylsilazane, dimethyldiethoxysilane, and water; The A adhesive is composed of the first part of base adhesive, the first part of dimethyl silicone oil and the second additive, and the B adhesive is composed of the second part of base adhesive, the second part of dimethyl silicone oil and the third additive; The second additive includes a platinum catalyst; The third auxiliary agent includes hydrogen-containing silicone oil and ethynylcyclohexanol.

[0014] To address the above problems, the present invention also provides an electronic device, the electronic device comprising: Memory, storing at least one instruction; The processor executes the instructions stored in the memory to implement the above-described method for preparing a liquid adhesive with ultra-low viscosity and high solid content.

[0015] To address the aforementioned problems, the present invention also provides a computer-readable storage medium storing at least one instruction, which is executed by a processor in an electronic device to implement the above-described method for preparing a liquid adhesive with ultra-low viscosity and high solids content.

[0016] To address the problems described in the background art, this invention first constructs a compound using vinyl silicone oil, then dilutes the compound with more vinyl silicone oil to reduce water addition, resulting in a base adhesive with high insulation and high solids content. Next, this invention produces adhesive A and adhesive B based on this base adhesive. Both adhesive A and adhesive B contain dimethyl silicone oil, which effectively reduces their viscosity, allowing the adhesives to penetrate deeper into crevices and increasing the contact area. Furthermore, when the platinum catalyst added to adhesive A and the hydrogen-containing silicone oil added to adhesive B interact, they rapidly catalyze a cross-linking and curing reaction, quickly completing the bonding process. Therefore, this invention reduces the viscosity of high-solids-content liquid adhesives and improves their mixing efficiency. Attached Figure Description

[0017] Figure 1 This is a schematic flowchart of a method for preparing a liquid adhesive with ultra-low viscosity and high solid content according to an embodiment of the present invention. Figure 2 This is a schematic diagram of an electronic device that implements the liquid adhesive preparation method with ultra-low viscosity and high solid content according to an embodiment of the present invention.

[0018] Explanation of reference numerals in the attached figures: 10. Electronic device; 11. Processor; 12. Memory; 13. Bus.

[0019] The realization of the objective, functional features and advantages of the present invention will be further explained in conjunction with the embodiments and with reference to the accompanying drawings. Detailed Implementation

[0020] It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.

[0021] This application provides a method for preparing a liquid adhesive with ultra-low viscosity and high solids content. The execution entity of this method includes, but is not limited to, at least one of the following electronic devices that can be configured to execute the method provided in this application: a server, a terminal, etc. In other words, the method for preparing the liquid adhesive with ultra-low viscosity and high solids content can be executed by software or hardware installed on a terminal device or a server device, and the software can be a blockchain platform. The server includes, but is not limited to, a single server, a server cluster, a cloud server, or a cloud server cluster.

[0022] Reference Figure 1 The diagram shown is a schematic flow chart of a method for preparing a liquid adhesive with ultra-low viscosity and high solids content according to an embodiment of the present invention. In this embodiment, the method for preparing the liquid adhesive with ultra-low viscosity and high solids content includes: S1. Stir the pre-constructed first part of vinyl silicone oil and the pre-constructed first additive to obtain a base micelle, and perform a rubber mixing operation on the base micelle to obtain a compound.

[0023] The preparation command refers to the electrical signal used to control the equipment to start preparing the liquid adhesive.

[0024] The material supply pipeline is a switchable device used to transport various raw materials.

[0025] The first part of vinyl silicone oil is 10541.3 parts by mass of 1000 viscosity vinyl silicone oil, wherein 1000 viscosity vinyl silicone oil refers to a polydimethylsiloxane fluid containing vinyl functional groups with a kinematic viscosity of 1000 cSt (centistokes, at 25°C).

[0026] The first additive is an additive used to modify the properties of the first portion of vinyl silicone oil. The term "additive" generally refers to a small amount of auxiliary chemical substances added during adhesive production to optimize the adhesive's performance, processing, or storage stability.

[0027] The rubber mixing machine refers to a device that can stir, chop, combine, and heat the adhesive raw materials (the first part of vinyl silicone oil and the first additive) to make the various components of the adhesive more evenly distributed.

[0028] Specifically, in this embodiment of the invention, according to the preparation instructions, a preset program is automatically executed to open the material supply pipeline, thereby sending the first batch of vinyl silicone oil and the first auxiliary agent to the pre-constructed rubber mixing machine.

[0029] Specifically, in this embodiment of the invention, the first additive includes fumed silica, hexamethylsilazane, dimethyldiethoxysilane, and water. Fumed silica refers to an inorganic nanomaterial prepared by a gas-phase synthesis process, with amorphous silica (SiO2) as its core component. Hexamethylsilazane (HMDS) is used to improve hydrophobicity and weather resistance, and enhance processing performance. Dimethyldiethoxysilane is used to improve its dispersibility in the adhesive system and reduce agglomeration. Water is used to adjust viscosity and dilute the adhesive medium.

[0030] Specifically, in this embodiment of the invention, the first auxiliary agent is configured as follows: 8316 parts by mass of fumed silica, 2079 parts by mass of hexamethylsilazane, 77 parts by mass of dimethyldiethoxysilane, and 462 parts by mass of water.

[0031] The stirring refers to the process of stirring the rubber mixing machine. The base colloid refers to the result of stirring the first portion of vinyl silicone oil and the first auxiliary agent.

[0032] The term "rubber mixing" refers to the process of chopping, recombining, and heating in a rubber mixing machine. The term "mixed rubber" refers to the final product of mixing the base rubber molecules.

[0033] The adhesive preparation tank refers to the production area of ​​the base adhesive in this solution, which includes functions for controlling temperature, vacuum level, and stirring speed.

[0034] In detail, in this embodiment of the invention, the step of stirring the first portion of vinyl silicone oil and the first additive to obtain the base micelle includes: The first adjuvant is grouped to obtain a sub-first adjuvant set; Extract one portion of the first auxiliary agent from the first auxiliary agent set in sequence, and add the extracted first auxiliary agent to the first portion of vinyl silicone oil and stir. Using a pre-constructed viscosity sensor, the viscosity change sequence of the first vinyl silicone oil is obtained, and the rate of change of the viscosity change sequence is identified to obtain the viscosity change rate; When the viscosity change rate is less than the preset stirring viscosity interference threshold, it is determined that the first auxiliary agent has been incorporated into the first part of vinyl silicone oil; When the first auxiliary agent is incorporated into the first part of vinyl silicone oil, the steps described above for sequentially extracting one part of the first auxiliary agent from the set of first auxiliary agents are returned until the set of first auxiliary agents is incorporated into the first part of vinyl silicone oil to obtain the base micelle.

[0035] The grouping operation refers to the operation of dispensing the first adjuvant into 10 portions. The sub-first adjuvant set refers to the first adjuvant divided into 10 portions. The sub-first adjuvant refers to one-tenth of the first adjuvant.

[0036] The viscosity sensor refers to a sensor that measures the viscosity of vinyl silicone oil and can be placed on the inner wall of the adhesive preparation container. The viscosity change sequence refers to the data recorded by the viscosity sensor during the time period when a portion of the first additive is added to the first portion of vinyl silicone oil and stirred.

[0037] The viscosity change rate refers to the change in viscosity at the current time point compared to the viscosity at the previous time point in the viscosity change sequence.

[0038] The stirring viscosity interference threshold refers to the viscosity change rate of the first batch of vinyl silicone oil as its viscosity naturally increases during machine stirring.

[0039] The term "fusion state" refers to the state where the first additive is not adhered to the stirrer wall, but is completely kneaded into the first portion of vinyl silicone oil and evenly distributed. Each time point corresponds to a viscosity change rate, and these viscosity change rates are compared to a preset stirring viscosity interference threshold. When the viscosity change rate corresponding to a certain time point is less than the stirring viscosity interference threshold, it indicates that the first additive has been fused into the first portion of vinyl silicone oil.

[0040] Specifically, in this embodiment of the invention, the first additive is first divided into 10 parts to obtain a sub-first additive set. Then, one part of the sub-first additive is extracted from the sub-first additive set and added to the 1000 viscosity vinyl silicone oil, and stirred. Each time a sub-first additive is incorporated into the first part of vinyl silicone oil, the next part of the sub-first additive can be added, until all the sub-first additives in the sub-first additive set are incorporated into the first part of vinyl silicone oil, resulting in a base micelle. In this embodiment of the invention, the stirring progress is controlled by the ratio of the viscosity change rate to the stirring viscosity interference threshold. When the viscosity change rate is greater than the stirring viscosity interference threshold, it indicates that the added sub-first additive is changing the viscosity of the first part of vinyl silicone oil. When the viscosity change rate is less than the stirring viscosity interference threshold, it indicates that the sub-first additive is completely incorporated into the first part of vinyl silicone oil, and at this time, another part of the sub-first additive can be added.

[0041] In detail, in this embodiment of the invention, the step of mixing the base micelles to obtain the compound rubber includes: The base micelles are subjected to mechanical shearing and mixing operations to obtain a uniform adhesive; The homogeneous rubber is subjected to a vacuum operation to obtain a vacuum environment. The homogeneous rubber under vacuum environment is then heated to 170°C and kept at 170°C for 2 hours to obtain the compound rubber.

[0042] The mechanical shearing and mixing operation refers to the process by which the rubber compounding machine breaks down the base rubber balls and then re-extrudes them together. The homogeneous rubber refers to the base rubber balls after the mechanical shearing and mixing operation.

[0043] The vacuuming operation refers to placing the homogeneous adhesive under a vacuum. The heating operation refers to raising the ambient temperature of the homogeneous adhesive. The compound refers to the homogeneous adhesive obtained after vacuuming and heating to 170°C for 2 hours.

[0044] Specifically, in this embodiment of the invention, mechanical shearing and mixing operations are first performed at room temperature, such as 30°C, to obtain a uniform rubber. Then, a vacuum operation is performed using a vacuum machine to maintain the vacuum environment of the uniform rubber. Then, the ambient temperature of the uniform rubber is stabilized at 170°C by electromagnetic heating and maintained for 2 hours. Finally, thermal stress is used to make the various substances in the uniform rubber more evenly distributed, resulting in a compound rubber.

[0045] Specifically, in this embodiment of the invention, the prepared compound can be transported through a pipeline to a glue preparation tank, awaiting the next step.

[0046] S2. Using a pre-trained adaptive dilution model, the pre-constructed second part of vinyl silicone oil is used to adaptively dilute the compound to obtain the base rubber.

[0047] The adaptive dilution model is a regression prediction network model used to automatically control the material supply pipeline, obtain an appropriate amount of the second part of vinyl silicone oil, and configure the corresponding stirring time to adaptively dilute the compound, ensuring that each stirring can make the various media in the glue evenly distributed.

[0048] The second part of the vinyl silicone oil is 8523.9 parts by weight of 1000 viscosity vinyl silicone oil.

[0049] The adaptive dilution operation refers to using an adaptive dilution model to generate the stirring time for each mass portion of vinyl silicone oil, and then controlling the internal stirring of the adhesive preparation tank according to the stirring time.

[0050] The base rubber refers to the final result of diluting the compound rubber with the second part of vinyl silicone oil.

[0051] In detail, in this embodiment of the invention, the pre-trained adaptive dilution model is used to control the material supply pipeline to deliver the pre-constructed second portion of vinyl silicone oil to the adhesive preparation tank in batches, thereby adaptively diluting the compound to obtain the base adhesive, comprising: Using the temperature control device pre-built in the glue preparation tank, the compound is cooled to a preset 30 degrees Celsius to obtain the first compound. Using a pre-trained adaptive dilution model, the material supply pipeline is controlled to obtain a preset initial experimental value of vinyl silicone oil from the second portion of vinyl silicone oil, thus obtaining an experimental amount of silicone oil, and the experimental amount of silicone oil is then delivered to the adhesive preparation tank. In the glue preparation tank, the first compound was vacuum stirred for 5 minutes using the experimental amount of silicone oil to obtain a compound intermediate. During the vacuum stirring of the first compound for 5 minutes, the dilution viscosity change curve of the first compound was obtained. According to the preset dilution adjustment rules in the adaptive dilution model, the initial experimental value is updated to obtain the updated experimental value. The material supply pipeline is controlled to obtain the vinyl silicone oil with the updated experimental value from the second part of vinyl silicone oil to obtain the updated amount of silicone oil, and the updated amount of silicone oil is transported to the glue preparation tank. Using the adaptive dilution model, the effective stirring time of the updated silicone oil is predicted based on the dilution viscosity change curve; In the glue preparation tank, the compound intermediate is subjected to vacuum stirring based on the effective stirring time using the updated amount of silicone oil to obtain an updated compound intermediate, and the updated compound intermediate is used to replace the original compound intermediate. Determine whether the second portion of vinyl silicone oil has been used in its entirety; If the second portion of vinyl silicone oil is not completely used, return to the steps described above for adjusting the dilution amount according to the preset dilution rules in the adaptive dilution model; If the second portion of vinyl silicone oil is used entirely, the updated compound intermediate will be recognized as the base rubber.

[0052] The temperature control device refers to a device that can change the internal temperature of the glue preparation tank.

[0053] The initial experimental value is set to 5%. The experimental amount of silicone oil refers to 5% by mass of the second portion of 1000 viscosity vinyl silicone oil, specifically 8523.9 × 5% by mass of 1000 viscosity vinyl silicone oil. Subsequent portions of 10%, 20%, 30%, and the remainder are calculated similarly.

[0054] The vacuum stirring refers to the process of stirring at a pre-configured uniform speed in a vacuum environment.

[0055] The intermediate compound refers to the intermediate product of the compound after one dilution.

[0056] The dilution viscosity change curve refers to the viscosity change data of the compound during the dilution process.

[0057] The dilution adjustment rule refers to a strategy of adjusting the updated experimental value by using 5%, 10%, 20%, 30%, and 35% according to the logic of adding viscous materials from difficult to easy.

[0058] The step of updating the initial experimental value according to the preset dilution adjustment rules refers to gradually increasing the updated experimental value during the dilution process according to the dilution adjustment rules of 5%, 10%, 20%, 30%, and 35%. For example, the first dilution uses 5% by mass, and the second dilution requires 10% by mass. The updated experimental value refers to the adjusted initial experimental value. The updated amount of silicone oil refers to the amount of vinyl silicone oil with a viscosity of 1000 corresponding to the updated experimental value.

[0059] The effective stirring time refers to the stirring time required to complete the dilution process of the compound intermediate using a renewed amount of silicone oil. The renewed compound intermediate refers to a compound intermediate that has been diluted again, such as subsequent second or third intermediates.

[0060] The phrase "using the updated compound intermediate to replace the compound intermediate" means that in subsequent processes, the compound intermediate will be diluted again based on the updated compound intermediate, rather than being diluted based on the compound intermediate itself.

[0061] Preferably, in this embodiment of the invention, the following batch dilution process configured according to the adaptive dilution model can yield a base adhesive with a relatively uniform dilution effect: Using 5% by mass of 1000 viscosity vinyl silicone oil from the second part of vinyl silicone oil, the compound was vacuum stirred for 10 minutes to obtain the first intermediate. Using 10% by mass of 1000 viscosity vinyl silicone oil from the second part of vinyl silicone oil, the first intermediate was vacuum stirred for 10 minutes to obtain the second intermediate; Using 20% ​​by mass of 1000 viscosity vinyl silicone oil from the second part of vinyl silicone oil and a release agent, the second intermediate was vacuum stirred for 10 minutes to obtain the third intermediate; Using 30% by mass of 1000 viscosity vinyl silicone oil from the second portion of vinyl silicone oil, the third intermediate was vacuum stirred for 10 minutes to obtain the fourth intermediate; Using the remaining 1000 viscosity vinyl silicone oil in the second portion, the fourth intermediate was vacuum-stirred for 30 minutes to obtain the base gel.

[0062] The first intermediate refers to the rubber compound after the first vacuum mixing (dilution). Similarly, the second, third, and fourth intermediates are the rubber compounds after the second, third, and fourth dilutions, respectively.

[0063] In this embodiment of the invention, heating is first turned off, and the compound is cooled to a preset temperature of 30 degrees Celsius using a temperature control device. Then, 5% by mass of 1000 viscosity vinyl silicone oil is vacuum-stirred for 10 minutes to obtain a first intermediate. Next, 10% by mass of 1000 viscosity vinyl silicone oil is vacuum-stirred for another 10 minutes. Then, 20% by mass of 1000 viscosity vinyl silicone oil is vacuum-stirred for 10 minutes. Considering that the mixer and the compound may stick together at this point, a release agent is added at this stage; the specific amount is not limited. This yields a third intermediate. Then, 30% by mass of 1000 viscosity vinyl silicone oil is vacuum-stirred again for 10 minutes to obtain a fourth intermediate. Finally, the remaining 1000 viscosity vinyl silicone oil is vacuum-stirred for 30 minutes to obtain the base compound.

[0064] Therefore, by following the above steps, a base adhesive with low water content and relatively uniform medium distribution can be obtained.

[0065] In detail, in this embodiment of the invention, the step of using the adaptive dilution model to predict the effective stirring time of the updated silicone oil based on the dilution viscosity change curve includes: Using the adaptive dilution model, compound features are identified in the rubber compound to obtain a set of diluted compound features, and compound features are identified in the second vinyl silicone oil to obtain a set of dilution solvent features. The initial experimental values ​​are quantified to obtain the initial dilution vector, and the 5 minutes are quantified to obtain the initial stirring time vector. Based on the initial dilution vector, the initial stirring time vector, the characteristic set of the diluted compound, and the characteristic set of the dilution solvent, the dilution viscosity change of the experimental amount of silicone oil on the first compound is predicted, and a dilution viscosity prediction curve is obtained. The dilution viscosity prediction curve is subjected to curve feature extraction to obtain a predicted dilution feature set, and the dilution viscosity change curve is subjected to curve feature extraction to obtain a true dilution feature set. The distinguishing features between the predicted dilution feature set and the true dilution feature set are identified to obtain a distinguishing feature set. Compound feature identification is performed on the rubber compound intermediate to obtain an updated set of diluted compound features. The updated experimental values ​​are then quantified to obtain an updated dilution vector. Based on the updated set of features of diluted compounds, the set of features of diluents, the updated dilution amount vector and the distinguishing feature set, the dilution viscosity change curve of the updated amount of silicone oil on the compound intermediate is predicted, and the predicted viscosity change curve of the second dilution is obtained. The effective stirring time is obtained by extracting the effective stirring time from the predicted viscosity change curve of the re-dilution.

[0066] The compound feature identification refers to the process of identifying the chemical and physical characteristics of each compound in a compound, as well as the chemical and physical characteristics of the interactions between the compounds.

[0067] The diluted compound feature set refers to the compound feature identification results of the compounded rubber. The diluted solvent feature set refers to the compound feature identification results of the second vinyl silicone oil.

[0068] The quantization operation refers to quantizing data into a format that a computer can recognize, such as converting it into binary.

[0069] The initial dilution vector is the result of the quantification operation of the initial experimental values. The initial stirring time vector refers to the result of the 5-minute quantification operation.

[0070] The process of "predicting the change in dilution viscosity of the first compound by the experimental amount of silicone oil based on the initial dilution vector, the initial stirring time vector, the characteristic set of the diluted compound, and the characteristic set of the dilution solvent, and obtaining the dilution viscosity prediction curve" refers to the first execution process of the adaptive dilution model. Since the initial dilution vector is a percentage value, the calculation result of the dilution viscosity prediction curve is not very accurate and needs to be adjusted according to the actual measured dilution viscosity change curve to improve the accuracy of subsequent dilution viscosity prediction.

[0071] The dilution viscosity prediction curve refers to the viscosity prediction result of the adaptive dilution model for the dilution parameters of "updated experimental value of 5%" and "initial stirring time vector of 5 minutes".

[0072] The curve feature extraction operation refers to the mathematical extraction of the numerical and temporal patterns of a curve.

[0073] The predicted dilution feature set refers to the result of curve feature extraction from the dilution viscosity prediction curve. The true dilution feature set refers to the result of curve feature extraction from the dilution viscosity change curve.

[0074] The operation of identifying the distinguishing features between the predicted dilution feature set and the actual dilution feature set refers to the operation of extracting the distinguishing values ​​and trend changes between the dilution viscosity change curve and the predicted dilution viscosity curve. The distinguishing feature set refers to the set of distinguishing features in both the predicted dilution feature set and the actual dilution feature set.

[0075] The "updated diluted compound feature set" refers to the compound feature identification results of the compound intermediate. The "updated dilution vector" refers to the quantification operation results of the updated experimental values.

[0076] The phrase "predicting the viscosity change curve of the updated amount of silicone oil on the compound intermediate based on the updated feature set of diluted compounds, the feature set of diluted solvents, the updated dilution amount vector, and the distinguishing feature set, and obtaining the predicted viscosity change curve of the second dilution" refers to the second execution process of the adaptive dilution model. This time, it has a distinguishing feature set, which can improve the accuracy of dilution viscosity prediction.

[0077] The predicted viscosity change curve for further dilution refers to the viscosity change curve during the process of diluting the intermediate compound with a new amount of silicone oil.

[0078] The operation of extracting the effective stirring time refers to taking the time point corresponding to the lowest viscosity point in the predicted viscosity change curve after further dilution as the effective stirring time.

[0079] Specifically, in this embodiment of the invention, an adaptive dilution model is used to identify the compound features of the rubber compound and the second portion of vinyl silicone oil, respectively obtaining the feature set of the diluted compound and the feature set of the dilution solvent. Then, the adaptive dilution model is used to quantify the initial experimental value and the 5-minute stirring time to obtain dilution parameters of the initial dilution amount vector and the initial stirring time vector. Then, the dilution viscosity change during the dilution of the first rubber compound using the experimental amount of silicone oil under these dilution parameters is predicted to obtain a dilution viscosity prediction curve.

[0080] Previously, this invention had actually measured the real dilution viscosity change curve using a viscosity sensor. Therefore, based on the trend between the dilution viscosity prediction curve and the dilution viscosity change curve, the adaptive dilution model can be modified for different application scenarios to improve the accuracy of subsequent prediction processes.

[0081] Specifically, the present invention sequentially performs curve feature extraction operations on the dilution viscosity prediction curve and the dilution viscosity change curve to obtain the predicted dilution feature set and the true dilution feature set, respectively. Then, a neural network is used to perform distinguishable feature recognition to obtain the distinguishable feature set.

[0082] Specifically, the present invention will next dilute the rubber compound intermediate. Therefore, the present invention will perform compound feature identification on the rubber compound intermediate to obtain an updated set of diluted compound features. Furthermore, due to the dilution adjustment rules, the amount of diluent in this dilution process also changes. Therefore, the updated experimental value is quantified to obtain an updated dilution vector.

[0083] Specifically, after obtaining the above data, the present invention can predict the dilution viscosity change curve of the updated amount of silicone oil on the compound intermediate based on the updated diluted compound feature set, dilution solvent feature set, updated dilution amount vector and distinguishing feature set, and obtain the re-dilution predicted viscosity change curve. At this time, the re-dilution predicted viscosity change curve can accurately represent the viscosity change law with time during this dilution stirring process. Therefore, the effective stirring time can be extracted from the re-dilution predicted viscosity change curve to obtain the effective stirring time.

[0084] S3. Obtain a first portion of base adhesive and a second portion of base adhesive from the base adhesive, wherein the first portion of base adhesive and the second portion of base adhesive have the same mass.

[0085] The adhesive transport pipeline refers to the switchable pipeline connecting the adhesive preparation tank to adhesive preparation tanks A and B. Adhesive preparation tanks A and B are identical mixing tanks, possessing functions for temperature control, vacuum adjustment, and mixing.

[0086] The first and second portions of the base adhesive are each prepared in quantities of 9000 parts by weight.

[0087] Specifically, in this embodiment of the invention, since the amount of base adhesive in the formulations of adhesive A and adhesive B is the same, the base adhesive is supplied to the preparation tanks of adhesive A and adhesive B of equal mass using the adhesive transport pipeline.

[0088] In detail, in this embodiment of the invention, before obtaining the first and second portions of base adhesive from the base adhesive in the adhesive preparation tank using the pre-constructed adhesive transport pipeline, the method further includes: Obtain the viscosity of the base adhesive; Determine whether the viscosity is within a preset acceptable range; When the viscosity is not within the acceptable range, the base adhesive is determined to be unqualified, and the pre-constructed waste outlet in the adhesive preparation tank is opened to obtain unqualified base adhesive. The unqualified base adhesive is then transported to the pre-constructed raw material processing equipment for separation to obtain a raw material set.

[0089] The viscosity mentioned here refers to the physical property that measures the resistance of a fluid or semi-fluid substance (liquid adhesive) to flow, and is measured in centipoise. This invention can utilize the dynamic viscosity method for measurement, which will not be elaborated upon here.

[0090] The qualified range is configured as 1000~8000 centipoise.

[0091] The waste outlet refers to the bottom notch of the glue preparation container, which is used to discharge substandard base glue.

[0092] The raw material processing equipment refers to the equipment that separates substandard base adhesives into individual raw materials.

[0093] The separation refers to the operation of separating the various media based on their physical properties. The raw material set refers to the separation result of the substandard base adhesive.

[0094] Specifically, in this embodiment of the invention, if the viscosity of the base adhesive is not within the range of 1000~8000 centipoise, it indicates that the base adhesive does not meet the national standard and is therefore deemed unqualified. The unqualified base adhesive is then collected using the waste outlet in the adhesive preparation tank. Finally, the unqualified base adhesive is transported to a raw material processing device for separation to obtain a raw material aggregate.

[0095] In detail, in this embodiment of the invention, the step of transporting the substandard base adhesive to a pre-constructed raw material processing device for separation to obtain a raw material set includes: Using the pre-constructed solid-liquid separation device in the raw material processing equipment, the unqualified base adhesive is centrifuged to obtain fumed silica and the remaining mixed liquid; According to a preset set of boiling points, the remaining mixed liquid is subjected to a temperature gradient distillation operation to obtain hexamethylsilazane, dimethyldiethoxysilane and vinyl silicone oil; The fumed silica, hexamethylsilazane, dimethyldiethoxysilane and vinyl silicone oil are used as raw materials.

[0096] The solid-liquid separation device refers to a centrifuge for separating solids and liquids. The fumed silica is a solid particle that can be directly filtered. The remaining mixed liquid refers to the substandard base adhesive after removing the fumed silica.

[0097] The boiling point set is 126 degrees Celsius, 165 degrees Celsius, and 200 degrees Celsius.

[0098] Specifically, in this embodiment of the invention, the substandard base adhesive is a mixture of fumed silica, hexamethylsilazane, dimethyldiethoxysilane, and vinyl silicone oil. The fumed silica is solid, while the rest are liquid. Therefore, the fumed silica is directly filtered using a solid-liquid separation device to obtain the remaining mixed liquid. Then, considering that the hexamethylsilazane, dimethyldiethoxysilane, and vinyl silicone oil in the remaining mixed liquid have different boiling points, the hexamethylsilazane is extracted by distillation at 126 degrees Celsius, the dimethyldiethoxysilane is extracted by distillation at 165 degrees Celsius, and the high-boiling-point vinyl silicone oil is extracted by distillation at 200 degrees Celsius to obtain the raw material set.

[0099] In this embodiment of the invention, the raw material set can be distributed to various raw material bins to reduce waste during the colloid generation process.

[0100] S4. The first portion of base adhesive, the pre-constructed first portion of dimethyl silicone oil, and the pre-constructed second additive are stirred according to a preset stirring strategy to obtain adhesive A.

[0101] The A-adhesive stirring paddle refers to the device in the A-adhesive preparation tank responsible for stirring the A-adhesive. Similarly, the B-adhesive stirring paddle is the device in the A-adhesive preparation tank responsible for stirring the B-adhesive.

[0102] The stirring strategy refers to stirring in stages at different speeds, followed by stirring under vacuum. Adhesive A is a component of the liquid adhesive product of this invention, and the same applies to adhesive B.

[0103] In detail, in this embodiment of the invention, the A-adhesive is prepared by using a pre-constructed A-adhesive stirring paddle in the A-adhesive preparation tank to stir the first part of the base adhesive, the first part of the dimethyl silicone oil, and the second additive according to a preset stirring strategy to obtain A-adhesive, comprising: Add the first part of dimethyl silicone oil and the second additive to the first part of the base glue in the A glue preparation tank to obtain the A glue raw material; Using the pre-constructed A-glue stirring paddle in the A-glue preparation tank, the A-glue raw material is stirred at a speed of 10~15Hz for 5 minutes to obtain the first A-glue stirring intermediate; Using the A-type glue stirring paddle, the first A-type glue stirring intermediate is stirred at a speed of 40 Hz for 30 minutes to obtain the second A-type glue stirring intermediate. The A glue preparation container is evacuated using a pre-built vacuum device. Using the A-glue stirring paddle, the second A-glue stirring intermediate under vacuum is stirred at a speed of 40 Hz for 20 minutes to obtain A-glue solution.

[0104] The first part of dimethyl silicone oil is prepared in the form of 2250 parts by weight.

[0105] The second additive is a platinum catalyst, prepared in a quantity of 63 parts by mass.

[0106] Wherein, the raw material A refers to a mixture of the first base adhesive, the first dimethyl silicone oil, and the second additive.

[0107] The first A-grade mixing intermediate refers to the result of mixing the A-grade raw material at a speed of 10-15 Hz for 5 minutes.

[0108] The second A-gel mixing intermediate refers to the result of the first A-gel mixing intermediate being stirred at a speed of 40Hz for 30 minutes.

[0109] The vacuuming operation refers to the process of completely removing the air from the A glue preparation container by suction.

[0110] Specifically, in this embodiment of the invention, each part of adhesive A requires 9000 parts by weight of the first base adhesive. Then, 2250 parts by weight of the first dimethyl silicone oil are prepared, followed by 63 parts by weight of platinum catalyst as the second additive.

[0111] The main function of the platinum catalyst is to catalyze the crosslinking reaction. As the core component for curing liquid adhesive, it can efficiently promote the hydrosilylation reaction between polymers containing vinyl groups (such as 1000 viscosity vinyl silicone oil) and compounds containing hydrogen groups (such as hydrogen silicone oil), thereby realizing the transformation of the adhesive from liquid to solid state.

[0112] S5. The second base adhesive, the pre-constructed second dimethyl silicone oil, and the pre-constructed third additive are stirred according to the stirring strategy to obtain adhesive B.

[0113] Specifically, in this embodiment of the invention, the second part of dimethyl silicone oil required for producing adhesive B is prepared in the form of 1908 parts by weight. Then, the third auxiliary agent is prepared in the form of 360 parts by weight of hydrogen-containing silicone oil and 4.5 parts by weight of ethynylcyclohexanol.

[0114] The hydrogen-containing silicone oil reacts with the aforementioned platinum catalyst, causing the liquid adhesive to cure rapidly. The ethynylcyclohexanol acts as an inhibitor, ensuring that the hydrogen-containing silicone oil in adhesive B does not spontaneously react with the second base adhesive.

[0115] Specifically, in this embodiment of the invention, the staged stirring process of glue B is the same as that of glue A, and will not be described in detail here.

[0116] According to the above process, the present invention can obtain glue B.

[0117] S6. The A glue and B glue are filled into liquid glue products by separating them into equal volumes.

[0118] The flow controller refers to a device that controls the flow rate of a fluid.

[0119] The term "equal volume separation filling" refers to filling A glue and B glue separately during the filling process, ensuring that the volume-to-mass ratio of A glue to B glue is 1:1.

[0120] The liquid adhesive product refers to the combination of adhesive product A and adhesive product B.

[0121] In detail, in this embodiment of the invention, the step of using a pre-constructed flow controller to perform equal-volume isolation filling of adhesive A and adhesive B to obtain a liquid adhesive product includes: Using a pre-built flow controller, a rated amount of glue A is obtained from the glue A preparation tank according to a preset filling flow rate, and a rated amount of glue B is obtained from the glue B preparation tank according to the filling flow rate. The rated quantity of glue A is sieved using the first filter screen in the flow controller to obtain glue A to be packaged, and the rated quantity of glue B is sieved using the second filter screen in the flow controller to obtain glue B to be packaged. Both the first filter screen and the second filter screen are 300 mesh filters. Using a pre-built packaging machine, the A glue and B glue to be packaged are isolated and sealed to obtain a liquid glue product.

[0122] The filling flow rate is related to the size of the packaging can and can be adjusted according to the production speed required in the actual scenario.

[0123] The rated quantity of glue A refers to the amount of glue A produced per unit time at the specified filling flow rate. The rated quantity of glue B is similar and will not be elaborated further.

[0124] Both the first and subsequent second filters are 300-mesh filters, but they serve different purposes. The first filter filters adhesive A, and the second filter filters adhesive A to prevent impurities from appearing in the product. A 300-mesh filter refers to a filter with 300 openings per inch.

[0125] The packaging machine refers to equipment that seals products.

[0126] Specifically, in the embodiments of the present invention, during the production process of liquid adhesive, the output speed of adhesive A and adhesive B is controlled by a flow controller, and adhesive A and adhesive B are filtered by a first filter and a second filter respectively to ensure product quality. Finally, the adhesive A and adhesive B to be packaged are sealed into pre-produced packaging cans by a packaging machine to obtain the liquid adhesive product.

[0127] To address the problems described in the background art, this invention first constructs a compound using vinyl silicone oil, then dilutes the compound with more vinyl silicone oil to reduce water addition, resulting in a base adhesive with high insulation and high solids content. Next, this invention produces adhesive A and adhesive B based on this base adhesive. Both adhesive A and adhesive B contain dimethyl silicone oil, which effectively reduces their viscosity, allowing the adhesives to penetrate deeper into crevices and increasing the contact area. Furthermore, when the platinum catalyst added to adhesive A and the hydrogen-containing silicone oil added to adhesive B interact, they rapidly catalyze a cross-linking and curing reaction, quickly completing the bonding process. Therefore, this invention reduces the viscosity of high-solids-content liquid adhesives and improves their mixing efficiency.

[0128] An embodiment of the present invention provides a liquid adhesive prepared from a liquid adhesive with ultra-low viscosity and high solid content. When the liquid adhesive is confirmed for use, adhesive A and adhesive B are mixed in a 1:1 ratio according to the pre-constructed usage volume to obtain the liquid adhesive. If it is confirmed that the liquid adhesive will not be used, adhesive A and adhesive B are stored based on a pre-constructed storage state, wherein adhesive A and adhesive B are stored independently, and both adhesive A and adhesive B contain a base adhesive. The base adhesive is composed of the first part of vinyl silicone oil, the first additive, and the second part of vinyl silicone oil; The first additive includes fumed silica, hexamethylsilazane, dimethyldiethoxysilane, and water; The A adhesive is composed of the first part of base adhesive, the first part of dimethyl silicone oil and the second additive, and the B adhesive is composed of the second part of base adhesive, the second part of dimethyl silicone oil and the third additive; The second additive includes a platinum catalyst; The third auxiliary agent includes hydrogen-containing silicone oil and ethynylcyclohexanol.

[0129] Specifically, in this embodiment of the invention, 1000 viscosity vinyl silicone oil is used as the base adhesive, and then a second 1000 viscosity vinyl silicone oil is used as a diluent, which greatly reduces the conductivity of the base adhesive and increases its solid content. Then, dimethyl silicone oil is added to adhesives A and B respectively to reduce their respective viscosity. Subsequently, a platinum catalyst is added to adhesive A, and hydrogen-containing silicone oil and ethynylcyclohexanol are added to adhesive B.

[0130] In this embodiment of the invention, when only A-type adhesive is used, the curing reaction cannot occur without hydrogen-containing silicone oil. When only B-type adhesive is used, the lack of platinum catalyst allows ethynylcyclohexanol to effectively inhibit the curing reaction of B-type adhesive, resulting in both A-type and B-type adhesives having good stability and being able to cure quickly when A-type and B-type adhesives are used simultaneously.

[0131] like Figure 2 The diagram shown is a schematic representation of an electronic device that implements a method for preparing liquid adhesive with ultra-low viscosity and high solid content, according to an embodiment of the present invention.

[0132] The electronic device 1 may include a processor 10, a memory 11 and a bus 12, and may also include a computer program stored in the memory 11 and executable on the processor 10, such as a method program for preparing a liquid adhesive with ultra-low viscosity and high solid content.

[0133] The memory 11 includes at least one type of readable storage medium, including flash memory, portable hard drive, multimedia card, card-type memory (e.g., SD or DX memory), magnetic memory, disk, optical disk, etc. In some embodiments, the memory 11 can be an internal storage unit of the electronic device 1, such as the portable hard drive of the electronic device 1. In other embodiments, the memory 11 can also be an external storage device of the electronic device 1, such as a plug-in portable hard drive, smart media card (SMC), secure digital card (SD), flash card, etc., equipped on the electronic device 1. Furthermore, the memory 11 includes both internal storage units and external storage devices of the electronic device 1. The memory 11 can be used not only to store application software and various types of data installed on the electronic device 1, such as code for a liquid adhesive preparation method with ultra-low viscosity and high solid content, but also to temporarily store data that has been output or will be output.

[0134] In some embodiments, the processor 10 may be composed of integrated circuits, such as a single packaged integrated circuit or multiple integrated circuits with the same or different functions, including combinations of one or more central processing units (CPUs), microprocessors, digital processing chips, graphics processors, and various control chips. The processor 10 is the control unit of the electronic device, connecting various components of the entire electronic device via various interfaces and lines. It executes programs or modules stored in the memory 11 (e.g., a method for preparing liquid adhesives with ultra-low viscosity and high solids content) and calls data stored in the memory 11 to perform various functions of the electronic device 1 and process data.

[0135] The bus 12 can be a peripheral component interconnect (PCI) bus or an extended industry standard architecture (EISA) bus, etc. The bus 12 can be divided into an address bus, a data bus, a control bus, etc. The bus 12 is configured to realize the connection and communication between the memory 11 and at least one processor 10, etc.

[0136] Figure 2 Only electronic devices with components are shown; it will be understood by those skilled in the art that... Figure 2 The structure shown does not constitute a limitation on the electronic device 1, and may include fewer or more components than shown, or combine certain components, or have different component arrangements.

[0137] For example, although not shown, the electronic device 1 may also include a power supply (such as a battery) to power the various components. Preferably, the power supply can be logically connected to the at least one processor 10 through a power management device, thereby enabling functions such as charging management, discharging management, and power consumption management. The power supply may also include one or more DC or AC power supplies, recharging devices, power fault detection circuits, power converters or inverters, power status indicators, and other arbitrary components. The electronic device 1 may also include various sensors, Bluetooth modules, Wi-Fi modules, etc., which will not be described in detail here.

[0138] Furthermore, the electronic device 1 may also include a network interface. Optionally, the network interface may include a wired interface and / or a wireless interface (such as a Wi-Fi interface, a Bluetooth interface, etc.), which is typically used to establish communication connections between the electronic device 1 and other electronic devices.

[0139] Optionally, the electronic device 1 may further include a user interface, which may be a display, an input unit (such as a keyboard), or a standard wired or wireless interface. Optionally, in some embodiments, the display may be an LED display, a liquid crystal display, a touch-sensitive liquid crystal display, or an OLED (Organic Light-Emitting Diode) touchscreen, etc. The display may also be appropriately referred to as a screen or display unit, used to display information processed in the electronic device 1 and to display a visual user interface.

[0140] The program for preparing a liquid adhesive with ultra-low viscosity and high solid content, stored in the memory 11 of the electronic device 1, is a combination of multiple instructions. When run in the processor 10, it can achieve the following: The first pre-constructed vinyl silicone oil and the first pre-constructed additive are stirred to obtain a base micelle, and the base micelle is subjected to a rubber mixing operation to obtain a compound. Using a pre-trained adaptive dilution model, a pre-constructed second part of vinyl silicone oil was used to adaptively dilute the compound to obtain the base rubber. A first portion and a second portion of the base adhesive are obtained from the base adhesive, wherein the first portion and the second portion of the base adhesive have the same mass. According to the preset stirring strategy, the first part of base glue, the pre-constructed first part of dimethyl silicone oil and the pre-constructed second additive are stirred to obtain glue A; According to the stirring strategy, the second base adhesive, the pre-constructed second dimethyl silicone oil, and the pre-constructed third additive are stirred to obtain adhesive B; The A glue and B glue are filled into liquid glue products by separating them into equal volumes.

[0141] Specifically, the processor 10's implementation method for the above instructions can be found in [reference needed]. Figures 1 to 2 The descriptions of the relevant steps in the corresponding embodiments are not repeated here.

[0142] Furthermore, if the modules / units integrated in the electronic device 1 are implemented as software functional units and sold or used as independent products, they can be stored in a computer-readable storage medium. The computer-readable storage medium can be volatile or non-volatile. For example, the computer-readable medium may include: any entity or device capable of carrying the computer program code, a recording medium, a USB flash drive, a portable hard drive, a magnetic disk, an optical disk, a computer memory, or a read-only memory (ROM).

[0143] The present invention also provides a computer-readable storage medium storing a computer program, which, when executed by a processor of an electronic device, can perform the following: The first pre-constructed vinyl silicone oil and the first pre-constructed additive are stirred to obtain a base micelle, and the base micelle is subjected to a rubber mixing operation to obtain a compound. Using a pre-trained adaptive dilution model, a pre-constructed second part of vinyl silicone oil was used to adaptively dilute the compound to obtain the base rubber. A first portion and a second portion of the base adhesive are obtained from the base adhesive, wherein the first portion and the second portion of the base adhesive have the same mass. According to the preset stirring strategy, the first part of base glue, the pre-constructed first part of dimethyl silicone oil and the pre-constructed second additive are stirred to obtain glue A; According to the stirring strategy, the second base adhesive, the pre-constructed second dimethyl silicone oil, and the pre-constructed third additive are stirred to obtain adhesive B; The A glue and B glue are filled into liquid glue products by separating them into equal volumes.

[0144] In the embodiments provided by this invention, it should be understood that the disclosed devices, systems, and methods can be implemented in other ways. For example, the system embodiments described above are merely illustrative, and actual implementations may have other classification methods.

[0145] The modules described as separate components may or may not be physically separate. The components shown as modules may or may not be physical units; that is, they may be located in one place or distributed across multiple network units. Some or all of the modules can be selected to achieve the purpose of this embodiment according to actual needs.

[0146] Furthermore, the functional modules in the various embodiments of the present invention can be integrated into one processing unit, or each unit can exist physically separately, or two or more units can be integrated into one unit. The integrated unit can be implemented in hardware or in the form of hardware plus software functional modules.

[0147] It will be apparent to those skilled in the art that the present invention is not limited to the details of the exemplary embodiments described above, and that the present invention can be implemented in other specific forms without departing from the spirit or essential characteristics of the present invention.

[0148] Finally, it should be noted that the above embodiments are only used to illustrate the technical solutions of the present invention and are not intended to limit it. Although the present invention has been described in detail with reference to preferred embodiments, those skilled in the art should understand that modifications or equivalent substitutions can be made to the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.

Claims

1. A method for preparing a liquid adhesive with ultra-low viscosity and high solid content, characterized in that, The method includes: The first pre-constructed vinyl silicone oil and the first pre-constructed additive are stirred to obtain a base micelle, and the base micelle is subjected to a rubber mixing operation to obtain a compound. Using a pre-trained adaptive dilution model, a pre-constructed second part of vinyl silicone oil was used to adaptively dilute the compound to obtain the base rubber. A first portion and a second portion of the base adhesive are obtained from the base adhesive, wherein the first portion and the second portion of the base adhesive have the same mass. According to the preset stirring strategy, the first part of base glue, the pre-constructed first part of dimethyl silicone oil and the pre-constructed second additive are stirred to obtain glue A; According to the stirring strategy, the second base adhesive, the pre-constructed second dimethyl silicone oil, and the pre-constructed third additive are stirred to obtain adhesive B; The A glue and B glue are filled into liquid glue products by separating them into equal volumes.

2. The method for preparing a liquid adhesive with ultra-low viscosity and high solid content as described in claim 1, characterized in that, The process of stirring the pre-constructed first portion of vinyl silicone oil and the pre-constructed first additive to obtain a base micelle includes: The first adjuvant is grouped to obtain a sub-first adjuvant set; Extract one portion of the first auxiliary agent from the first auxiliary agent set in sequence, and add the extracted first auxiliary agent to the first portion of vinyl silicone oil and stir. Using a pre-constructed viscosity sensor, the viscosity change sequence of the first vinyl silicone oil is obtained, and the rate of change of the viscosity change sequence is identified to obtain the viscosity change rate; When the viscosity change rate is less than the preset stirring viscosity interference threshold, it is determined that the first auxiliary agent has been incorporated into the first part of vinyl silicone oil; When the first auxiliary agent is incorporated into the first part of vinyl silicone oil, the steps described above for sequentially extracting one part of the first auxiliary agent from the set of first auxiliary agents are returned until the set of first auxiliary agents is incorporated into the first part of vinyl silicone oil to obtain the base micelle.

3. The method for preparing a liquid adhesive with ultra-low viscosity and high solid content as described in claim 2, characterized in that, The process of compounding the base micelles to obtain the mixed rubber includes: The base micelles are subjected to mechanical shearing and mixing operations to obtain a uniform adhesive; The homogeneous rubber is subjected to a vacuum operation to obtain a vacuum environment. The homogeneous rubber under vacuum environment is then heated to 170°C and kept at 170°C for 2 hours to obtain the compound rubber.

4. The method for preparing a liquid adhesive with ultra-low viscosity and high solid content as described in claim 3, characterized in that, The first portion of base adhesive, the pre-constructed first portion of dimethyl silicone oil, and the pre-constructed second additive are stirred according to a preset stirring strategy to obtain adhesive A, comprising: To the first base adhesive, a pre-constructed first part of dimethyl silicone oil and a pre-constructed second additive are added to obtain adhesive A raw material; The A-type adhesive raw material is stirred at a speed of 10-15 Hz for 5 minutes to obtain the first A-type adhesive stirring intermediate. The first A-gel mixing intermediate was stirred at 40 Hz for 30 minutes to obtain the second A-gel mixing intermediate. The A glue preparation container is vacuumed. The second A-glue intermediate, which is in a vacuum environment, is stirred at a speed of 40 Hz for 20 minutes to obtain A-glue.

5. The method for preparing a liquid adhesive with ultra-low viscosity and high solid content as described in claim 4, characterized in that, The process of filling A and B adhesives into a liquid adhesive product by separating and dispensing them into equal volumes includes: According to the preset filling flow rate, obtain a rated amount of glue A, and according to the filling flow rate, obtain a rated amount of glue B; The rated amount of glue A is sieved to obtain glue A to be packaged, and the rated amount of glue B is sieved to obtain glue B to be packaged. The two adhesives, A and B, to be packaged are isolated and sealed to obtain a liquid adhesive product.

6. The method for preparing a liquid adhesive with ultra-low viscosity and high solid content as described in claim 5, characterized in that, Before obtaining the first and second portions of base adhesive from the base adhesive, the method further includes: Obtain the viscosity of the base adhesive; Determine whether the viscosity is within a preset acceptable range; When the viscosity is not within the acceptable range, the base adhesive is determined to be unqualified, and unqualified base adhesive is obtained. The unqualified base adhesive is then transported to a pre-constructed raw material processing device for separation to obtain a raw material set.

7. The method for preparing a liquid adhesive with ultra-low viscosity and high solid content as described in claim 6, characterized in that, The process of transporting the substandard base adhesive to a pre-constructed raw material processing device for separation to obtain a raw material set includes: Using the pre-constructed solid-liquid separation device in the raw material processing equipment, the unqualified base adhesive is centrifuged to obtain fumed silica and the remaining mixed liquid; According to a preset set of boiling points, the remaining mixed liquid is subjected to a temperature gradient distillation operation to obtain hexamethylsilazane, dimethyldiethoxysilane and vinyl silicone oil; The fumed silica, hexamethylsilazane, dimethyldiethoxysilane and vinyl silicone oil are used as raw materials.

8. A liquid adhesive with ultra-low viscosity and high solids content, produced by the preparation method of the liquid adhesive with ultra-low viscosity and high solids content according to claim 1, wherein when the liquid adhesive is confirmed for use, adhesive A and adhesive B are mixed in a 1:1 ratio according to the pre-constructed usage volume to obtain the liquid adhesive; if it is confirmed that the liquid adhesive will not be used, adhesive A and adhesive B are stored according to the pre-constructed storage state, wherein... The storage state is that glue A and glue B are stored independently, characterized in that both glue A and glue B contain a base adhesive; The base adhesive is composed of the first part of vinyl silicone oil, the first additive, and the second part of vinyl silicone oil; The first additive includes fumed silica, hexamethylsilazane, dimethyldiethoxysilane, and water; The A adhesive is composed of the first part of base adhesive, the first part of dimethyl silicone oil and the second additive, and the B adhesive is composed of the second part of base adhesive, the second part of dimethyl silicone oil and the third additive; The second additive includes a platinum catalyst; The third auxiliary agent includes hydrogen-containing silicone oil and ethynylcyclohexanol.

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